CN109387528A - A kind of liquid-scattering absorption coaxial joint test shearing equipment of electric field - Google Patents
A kind of liquid-scattering absorption coaxial joint test shearing equipment of electric field Download PDFInfo
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- CN109387528A CN109387528A CN201811445041.6A CN201811445041A CN109387528A CN 109387528 A CN109387528 A CN 109387528A CN 201811445041 A CN201811445041 A CN 201811445041A CN 109387528 A CN109387528 A CN 109387528A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/02—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
- G01N23/06—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and measuring the absorption
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
- G01N23/201—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials by measuring small-angle scattering
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
- G01N23/207—Diffractometry using detectors, e.g. using a probe in a central position and one or more displaceable detectors in circumferential positions
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- Crystallography & Structural Chemistry (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
Abstract
The invention discloses a kind of liquid-scatterings to absorb the coaxial joint test shearing equipment of electric field, including synchrotron radiation light source, hollow motor, interior conductive window, outer conductive window, stator, rotor and sealing ring, there is cylindrical hollow structure among hollow motor, stator is to extend cylindrical body boss on plate body, cylindrical body boss, which runs through, offers light hole, upper and lower sides on cylindrical body boss positioned at light hole offer the first liquid injection hole, rotor is that open up the section of through-hole be step-like disc structure at middle part, outer conductive window is fixedly connected on one end of rotor, just through-hole is blocked, the other end of rotor is mounted on one end of hollow motor, the plate body of stator is fixedly connected on the other end of hollow motor, the cylindrical body boss of stator passes through the cylindrical hollow structure of hollow motor, the cylindrical body boss end of stator is fixedly connected with interior conductive window , the present invention have the advantages that can using a kind of equipment carry out kinds of experiments, shearing force and electric field force can be applied simultaneously, experimental efficiency is high.
Description
Technical field
The present invention relates to machinery equipment field, are more particularly to a kind of coaxial joint test shearing of liquid-scattering absorption electric field
Equipment.
Background technique
Synchrotron radiation is that the charged particle of speed close to the light velocity (v ≈ c) is released when arcuately track moves in magnetic field
Electromagnetic radiation, since it is observed on synchrotron, be just otherwise known as " synchrotron radiation " or " synchrotron
Radiation ".For a long time, synchrotron radiation is the thing that do not welcome by high-energy physics scholar, because it consumes the energy of accelerator,
Hinder the raising of particle energy.But people just recognize synchrotron radiation within the scope of from far infrared to X-ray quickly
Continuous spectrum, high intensity, highly collimated, high degree of polarization, characteristic such as accurately control at the light-pulse generator of excellent properties, can be to
Carry out many front line science technical research that other light sources cannot achieve.Then on almost all of high-energy electron accelerator,
The synchrotron radiation light beam line and the various experimental provisions using synchronizable optical of " parasitism operation " are all built.So far, synchrotron radiation fills
The construction set and research, application on it, experienced the development of three generations.
With the variation of extra electric field significant changes occur for the mechanical property of liquid (especially complex fluid), mainly and liquid
The Assembling Behavior of body (or complex fluid) internal particle is related.There are no perfect synchrotron radiation original position is real for existing experimental technique
Equipment is tested, shearing force and electric field force cannot be applied simultaneously, so that the X-ray diffraction under experiment condition in situ, little Jiao cannot be completed
The Collaborative experiments such as scattering, X-ray absorption.For the defect of the synchrotron radiation original position experimental facilities of the prior art, it is necessary to design
A kind of liquid-scattering absorption coaxial joint test shearing equipment of electric field obtains liquid for synchronous under electric field shearing condition in situ
The experiment informations such as diffraction, scattering, the absorption of (complex fluid).
Summary of the invention
Technical problem to be solved by the present invention lies in the synchrotron radiation original position experimental facilities that the prior art is not perfect, no
Electric field force and shearing force can be applied simultaneously, not can be carried out the experiments such as in-situ synchronization X-ray diffraction, small-angle scattering, X-ray absorption
Problem.
The present invention is solution above-mentioned technical problem by the following technical programs: a kind of liquid-scattering absorbs electric field and coaxially joins
Close test shearing equipment, including synchrotron radiation light source, hollow motor, interior conductive window, outer conductive window, stator, rotor and close
Seal, the interior conductive window are fixedly connected on the stator, and the stator is connected in the hollow motor, described to lead outside
Electric window is fixedly connected on the rotor, and the stator is equipped with the first liquid injection hole, and the interior conductive window is equipped with second
Liquid injection hole, second liquid injection hole are communicated with first liquid injection hole, between the outer conductive window and the interior conductive window
Gap is formed, passes through the first liquid injection hole in the gap and fills fluid sample, be connected with brush on the outer conductive window, it is described
Brush is grounded, and is fixedly connected with high pressure positive electrode on the stator, the interior conductive window and the rotor connected on the stator
High voltage electric field is formed between the outer conductive window of upper connection, the high voltage electric field is applied on the fluid sample, the synchronization
Radiating light source irradiates the fluid sample.
Preferably, the direction of the high voltage electric field on the fluid sample and the side of the synchrotron radiation light source are applied to
It is vertical with the fluid sample shear direction to identical.
Preferably, there is cylindrical hollow structure among the hollow motor, the stator is to extend cylinder on plate body
Body boss, the rotor are that open up the section of through-hole be step-like disc structure at middle part.
Preferably, for the cylindrical body boss through light hole is offered, first liquid injection hole is provided with cylindrical body boss
On the light hole upper and lower sides, the outer conductive window is fixedly connected on one end of the rotor, blocks described turn just
Through-hole on son, the other end of the rotor are mounted on one end of the hollow motor, and the plate body of the stator is fixedly connected
In the other end of hollow motor, the cylindrical body boss of the stator passes through the cylindrical hollow structure of hollow motor, the stator
Cylindrical body boss end be fixedly connected with the interior conductive window, the cylindrical body boss end of the stator and the interior conduction
Window is stuck in the through-hole of the rotor, and high pressure positive electrode is fixedly connected on the plate body of the stator.
Preferably, the internal diameter of the cylindrical hollow structure of the hollow motor, the cylindrical body boss of the stator and interior
The internal diameter of the outer diameter of conductive window and the rotor is equal.
Preferably, the rotor is bolted to connection on the pressing plate of the hollow motor.
Preferably, it is sealed between the rotor and the stator by sealing ring.
Preferably, the stator and the rotor are made of tetrafluoroethene material.
Preferably, the interior conductive window and outer conductive window is conductive and window material is metallic beryllium, polyamides of aluminizing
Imines or pyrolytic graphite.
Preferably, the interior conductive window and the outer conductive window are transparent to x-ray, the synchrotron radiation light source transmitting
X-ray passes through the light hole and interior conductive window is irradiated on fluid sample.
The present invention has the advantage that compared with prior art
(1) outer conductive window is mounted on the rotor, and can be rotated with rotor, and stator does not rotate, the opposite fortune of stator and rotor
It is dynamic that shearing force is generated to fluid sample.
(2) by installing brush on outer conductive window, high pressure positive electrode is installed on stator, it can be in interior conductive window and outer
Apply high voltage electric field between conductive window.
(3) synchrotron radiation original position is thus allowed in fact by applying shearing force and high voltage electric field simultaneously to fluid sample
It tests.
(4) experimental facilities provided by the invention can carry out X-ray diffraction, small since window material is to X-ray transparent
The kinds of experiments such as angle scattering and X-ray absorption.
Detailed description of the invention
In order to illustrate more clearly of technical solution of the present invention, attached drawing needed in invention description will be made below
Simply introduce, it should be apparent that, drawings in the following description are only some embodiments of the invention, common for this field
For technical staff, without creative efforts, it is also possible to obtain other drawings based on these drawings.
A kind of solid of the liquid-scattering absorption coaxial joint test shearing equipment of electric field disclosed in Fig. 1 embodiment of the present invention
Figure；
A kind of main view of the liquid-scattering absorption coaxial joint test shearing equipment of electric field disclosed in Fig. 2 embodiment of the present invention
Figure；
A kind of main view of the liquid-scattering absorption coaxial joint test shearing equipment of electric field disclosed in Fig. 3 embodiment of the present invention
The face the A cross-sectional view of figure；
A kind of side view of the liquid-scattering absorption coaxial joint test shearing equipment of electric field disclosed in Fig. 4 embodiment of the present invention
Figure；
A kind of vertical view of the liquid-scattering absorption coaxial joint test shearing equipment of electric field disclosed in Fig. 5 embodiment of the present invention
Figure.
Corresponding component title represented by number in figure:
Outer 1 rotor of conductive window, 2 hollow motor 3
5 sealing ring 6 of conductive window in stator 4
101 through-hole of brush, 201 first order step 202
203 third level step of second level step, 204 pressing plate 301
401 light hole of cylindrical body boss, 402 first liquid injection hole 403
404 plate body of high pressure positive electrode, 405 second liquid injection hole 501
Specific embodiment
It elaborates below to the embodiment of the present invention, the present embodiment carries out under the premise of the technical scheme of the present invention
Implement, the detailed implementation method and specific operation process are given, but protection scope of the present invention is not limited to following implementation
Example.
As Figure 1-Figure 5, a kind of liquid-scattering absorbs the coaxial joint test shearing equipment of electric field, including synchrotron radiation light
Source (not shown), outer conductive window 1, rotor 2, hollow motor 3, stator 4, interior conductive window 5 and sealing ring 6.
The outer conductive window 1 is the structure that circular edge has screw hole, and the outer conductive window 1 is solid by bolt
Surely it is connected to one end of the rotor 2.The outer conductive window 1 is transparent to x-ray.Electricity is connected on the outer conductive window 1
Brush 101, the brush 101 are grounded.
The rotor 2 is that the section that middle part opens up through-hole 201 is step-like disc structure, step-like disc structure by
Grade rises, and is followed successively by first order step 202, second level step 203 and third level step 204,202 center of first order step is logical
Hole 201, second level step 203 are higher than first order step 202, and third level step 204 is higher than second level step 203, described to lead outside
Electric window 1 blocks through-hole 201 just.
The hollow motor 3 is the hollow structure that there is cylindrical body in centre, and one end of the hollow motor 3 inwardly offers recessed
Slot (schemes not mark), the hollow structure concentric co-axial of the groove and the cylindrical body, has pressing plate 301 inside the hollow motor 3,
The pressing plate 301 is stuck in the groove of the hollow motor 3,301 center of pressing plate be equipped with circular hole, the circular hole and it is described in
The hollow structure diameter of the cylindrical body of empty motor 3 is identical, and the thickness of the pressing plate 301 is greater than the depth of groove, the pressing plate
In the groove, a part protrusion, the third level step 204 of the rotor 2 is overlapped on the pressing plate 301 to 301 a part cards
In a part of protrusion.Screw hole is offered on the pressing plate 301, the rotor 2 is mounted on the hollow motor 3 by bolt
On pressing plate 301.
The stator 4 is to extend cylindrical body boss 401 on plate body 405, runs through at 401 center of cylindrical body boss and opens up
There is light hole 402, the upper and lower sides that light hole 402 is located on cylindrical body boss 401 offer the first liquid injection hole 403.The stator 4
Plate body 405 four angles on offer screw hole, the screw hole is screwed in by bolt, stator 4 is fixedly connected on hollow motor
3 other end, the cylindrical body boss 401 of the stator 4 pass through the cylindrical hollow structure of hollow motor 3.The plate of the stator 4
It is fixedly connected with high pressure positive electrode 404 on shape body 405, connects on the interior conductive window 5 and the rotor 2 connected on the stator 4
High voltage electric field is formed between the outer conductive window 1 connect.The high voltage electric field is applied on the fluid sample, the synchrotron radiation
Light source transmitting X-ray passes through the light hole 402 and interior conductive window 5 is irradiated on fluid sample.It is applied to the liquid
The direction of the high voltage electric field on sample is identical as the direction of the synchrotron radiation light source, with the fluid sample shear direction
Vertically.The direction of synchrotron radiation light source refer to synchrotron radiation light source transmitting X-ray direction, shear direction refer to rotor 2 with
The direction for the axial shearing force perpendicular to the stator 4 and the rotor 2 that relative motion generates is formed between stator 4.
The interior conductive window 5 is transparent to x-ray.The interior conductive window 5 is cylindrical body, on the interior conductive window 5
Equipped with the second liquid injection hole 501, second liquid injection hole 501 is communicated with first liquid injection hole 403.The interior conductive window 5
Edge has screw hole, and 401 end of cylindrical body boss of the stator 4 also offers screw hole, and the interior conductive window 5 is logical
Cross 401 end of cylindrical body boss that bolt is fixedly connected on the stator 4,401 end of cylindrical body boss of the stator 4 and
The interior conductive window 5 is stuck in the through-hole 201 of the rotor 2, positioned at 202 region of first order step of the rotor 2；
Gap is formed between 401 side of cylindrical body boss of the stator 4 and the second level step 203 of the rotor 2, is passed through in gap
Sealing ring 6 is installed to be tightly connected.
Specifically, the cylindrical body boss 401 of the internal diameter of the cylindrical hollow structure of the hollow motor 3, the stator 4 with
And the outer diameter of interior conductive window 5 and the internal diameter of the rotor 2 are equal.
Specifically, form gap between the outer conductive window 1 and the interior conductive window 5, by the in the gap
One liquid injection hole 403 fills fluid sample.
Specifically, the stator 4 and the rotor 2 are made of tetrafluoroethene material.
Specifically, the interior conductive window 5 and the outer conductive window 1 is conductive and window material be metallic beryllium, aluminize it is poly-
Acid imide or pyrolytic graphite.
The course of work of the invention are as follows: the fluid sample needed for test injection in the first liquid injection hole 403 first, fluid sample
At the gap that the first liquid injection hole 403 is then passed through that the second liquid injection hole 501 reaches interior conductive window 5 and outer conductive window 1,
And gap is filled up, the side and 2 contact position of rotor of cylindrical body boss 401 are sealed by sealing ring 6, and fluid sample will not be from
Gap between interior conductive window 5 and outer conductive window 1 flows to other places.Due to the material of interior conductive window 5 and outer conductive window 1
All can be by X-ray, and high voltage electric field can be applied between interior conductive window 5 and outer conductive window 1, while outer conductive window
Mouth 1 forms relative motion between the rotation of rotor 2 and stator 4 on rotor 2, generates shearing force to fluid sample, therefore this sets
Standby to carry out the experiment such as X-ray diffraction, small-angle scattering and X-ray absorption simultaneously, synchrotron radiation light source passes through in experimentation
The light hole 402 and interior conductive window 5 are irradiated on fluid sample, and light is cast out from outer conductive window 1, pass through spy
It surveys device (not shown) to receive, wherein small-angle scattering and X-ray diffraction are carried out in the x-ray bombardment to fluid sample of a wavelength
Experiment, collects scattered signal by detector.X-ray absorption is to select the x-ray bombardment of different-waveband enterprising to fluid sample
Row experiment, sees fluid sample in the absorbing state of different-waveband.
By above technical scheme, a kind of coaxial joint test of liquid-scattering absorption electric field provided by the present invention, which is sheared, to be set
It is standby to have the advantages that kinds of experiments is carried out using a kind of equipment, shearing force and electric field force can be applied simultaneously, experimental efficiency is high.
It can be rotated by the way that outer conductive window 1 to be mounted on rotor 2 with rotor 2, and stator 4 does not rotate, stator 4 and rotor 2 it is opposite
Movement generates shearing force to fluid sample.By installing brush 101 on outer conductive window 2, high pressure positive electricity is installed on stator 4
Pole can apply high voltage electric field between interior conductive window 5 and outer conductive window 1.It, can be with since window material is to X-ray transparent
The experiment such as X-ray diffraction, small-angle scattering and X-ray absorption is carried out simultaneously.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (10)
1. a kind of liquid-scattering absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that including synchrotron radiation light source, in
Empty motor, interior conductive window, outer conductive window, stator, rotor and sealing ring, it is described fixed that the interior conductive window is fixedly connected on
On son, the stator is connected in the hollow motor, and the outer conductive window is fixedly connected on the rotor, the stator
It is equipped with the first liquid injection hole, the interior conductive window is equipped with the second liquid injection hole, second liquid injection hole and first fluid injection
Hole communicates, and forms gap between the outer conductive window and the interior conductive window, is filled out in the gap by the first liquid injection hole
Fluid sample is filled, brush is connected on the outer conductive window, the brush is grounded, and is fixedly connected with high positive pressure on the stator
Electrode forms high voltage electric field between the outer conductive window connected on the interior conductive window and the rotor connected on the stator,
The high voltage electric field is applied on the fluid sample, and the synchrotron radiation light source irradiates the fluid sample.
2. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
The direction for being applied to the high voltage electric field on the fluid sample is identical as the direction of the synchrotron radiation light source, with the liquid
Body sample shear direction is vertical.
3. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
There is cylindrical hollow structure among the hollow motor, the stator is to extend cylindrical body boss, the rotor on plate body
It is step-like disc structure for the section that middle part opens up through-hole.
4. a kind of liquid-scattering according to claim 3 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
For the cylindrical body boss through light hole is offered, first liquid injection hole is provided with the light hole on cylindrical body boss
Upper and lower sides, the outer conductive window are fixedly connected on one end of the rotor, block the through-hole on the rotor just, and described turn
The other end of son is mounted on one end of the hollow motor, and the plate body of the stator is fixedly connected on the another of hollow motor
End, the cylindrical body boss of the stator pass through the cylindrical hollow structure of hollow motor, the cylindrical body boss end of the stator
It is fixedly connected with the interior conductive window, the cylindrical body boss end of the stator and the interior conductive window are stuck in the rotor
Through-hole in, high pressure positive electrode is fixedly connected on the plate body of the stator.
5. a kind of liquid-scattering according to claim 3 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
The outer diameter of the internal diameter of the cylindrical hollow structure of the hollow motor, the cylindrical body boss of the stator and interior conductive window with
And the internal diameter of the rotor is equal.
6. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
The rotor is bolted to connection on the pressing plate of the hollow motor.
7. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
It is sealed between the rotor and the stator by sealing ring.
8. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
The stator and the rotor are made of tetrafluoroethene material.
9. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, which is characterized in that
The interior conductive window and outer conductive window is conductive and window material is metallic beryllium, aluminize polyimides or pyrolytic graphite.
10. a kind of liquid-scattering according to claim 1 absorbs the coaxial joint test shearing equipment of electric field, feature exists
In the interior conductive window and the outer conductive window are transparent to x-ray, and the synchrotron radiation light source transmitting X-ray passes through institute
It states light hole and interior conductive window is irradiated on fluid sample.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201811445041.6A CN109387528B (en) | 2018-11-29 | 2018-11-29 | Coaxial combined test shearing equipment for liquid scattering absorption electric field |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811445041.6A CN109387528B (en) | 2018-11-29 | 2018-11-29 | Coaxial combined test shearing equipment for liquid scattering absorption electric field |
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| CN109387528A true CN109387528A (en) | 2019-02-26 |
| CN109387528B CN109387528B (en) | 2023-10-03 |
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Citations (5)
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-
2018
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|---|---|---|---|---|
| JPH0643562U (en) * | 1992-11-19 | 1994-06-10 | 理学電機株式会社 | X-ray analyzer |
| US20010030295A1 (en) * | 1999-07-02 | 2001-10-18 | Holl Richard A. | Electromagnetic wave assisted chemical processing |
| CN101365942A (en) * | 2005-11-30 | 2009-02-11 | 环境学有限公司 | Method of and equipment for measuring ionic mobility |
| WO2012013668A1 (en) * | 2010-07-27 | 2012-02-02 | Fondazione Bruno Kessler | Improved x-ray diffractometer and method of installing said improved x-ray diffractometer. |
| CN105181724A (en) * | 2015-10-21 | 2015-12-23 | 吉林大学 | In-situ rotary fiber sample platform based on X-ray small-angle scatterometer |
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| Title |
|---|
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| P. PANINE ET AL.: "Combined rheometry and small-angle x-ray scattering", 《REVIEW OF SCIENTIFIC INSTRUMENTS》, vol. 74, no. 4, pages 2451 - 2455, XP012040788, DOI: 10.1063/1.1556943 * |
| SILVIA PABISCH ET AL.: "SAXS and in-situ SAXS to follow the structural evolution in hybrid materials", 《MATER. RES. SOC. SYMP. PROC.》, vol. 1754, pages 3 - 11 * |
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