CN109387427A - A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force - Google Patents
A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force Download PDFInfo
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- CN109387427A CN109387427A CN201811509700.8A CN201811509700A CN109387427A CN 109387427 A CN109387427 A CN 109387427A CN 201811509700 A CN201811509700 A CN 201811509700A CN 109387427 A CN109387427 A CN 109387427A
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- anvil
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- polycrystalline diamond
- hard alloy
- high pressure
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/02—Details
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/24—Investigating strength properties of solid materials by application of mechanical stress by applying steady shearing forces
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Abstract
The invention discloses a kind of plycrystalline diamond Buddha's warrior attendant-compound anvils of hard alloy for generating high pressure shearing force, belong to field of high-voltage technology.Its main feature is that the anvil body for being the anvil is cylindrical type, and it is divided into upper layer and lower layer, upper layer is polycrystalline diamond layer, and lower layer is hard alloy layer, has a circle chamfering on the top of the polycrystalline diamond layer of anvil, the angle, θ of chamfering is 5~30 °.The top surface of plycrystalline diamond Buddha's warrior attendant layer after chamfering is the acting surface of anvil, and acting surface is circle.This kind of anvil is compared with the single-crystal diamond anvil applied now, the advantages that tool is easily worked, toughness is high, acting surface size is big, sample cavity diameter can reach Centimeter Level, it can be widely applied to the research for carrying out the variation of high pressure material properties using rotary press, meet in high shear substance system is studied in high-pressure physics field the needs of required sample size is larger, shearing force is higher, can carry out electrical measurement etc..
Description
Technical field
The compound anvil of the polycrystalline diamond-hard alloy that the present invention relates to a kind of for generating high pressure shearing force, tool
It is used in the rotary press device to press anvil for body.
Background technique
It is shown according to reported theoretical and experimental results in recent years, certain materials is applied simultaneously under high pressure and are cut
Shearing stress can significantly accelerated substance distortion of lattice, reduce substance pressure phase transition, or even change its phase transformation path, especially to stratiform
The variation of the structure of matter influences significant.Shear stress thus is applied to material simultaneously under high pressure, some lists can be obtained
Unavailable new construction, new phenomenon and new property under only hyperbaric environment.Under traditional hydrostatic pressing environment, pressure suffered by sample is
Isotropic, phase transformation can just occur after the energy that the external world applies is more than material phase transformation energy barrier, and by applying shearing
Stress, stress can be concentrated in a certain region of sample, and phase transformation occurs first in this region, so as to which phase-change pressure is greatly reduced
Power.
Buddha's warrior attendant is utilized as anvil is made into after raw material polishing processing usually using single-crystal diamond in Static pressure experiment
Stone opposed anvils device pressurizes, and both can produce high pressure can also carry out optics survey for diamond as optical window
Amount.In recent years, some rotary press devices apply high pressure high shear force to laboratory sample using single-crystal diamond as anvil,
The advantage is that can the variation to inner sample directly measured, and higher pressure can be applied to sample, but in reality
Test in actual use discovery single-crystal diamond as anvil on rotary press, there is also some drawbacks.One side monocrystalline
The production and processing of diamond are limited by technology and cost, are difficult to be made into large scale anvil, are led to the sample that can be tested
Product amount very pettiness, is more difficult to apply in actual production, and experiment shows only just to be easier to using large scale anvil
Biggish shear stress is generated, so that material easily be made to be abnormal transformation.On the other hand, though single-crystal diamond extreme hardness,
It is that toughness and wearability are poor, in an experiment, especially easy to damage in rotation process, experimental cost is high.So an urgent demand
It finds other materials and preparation method substitution single-crystal diamond is fabricated to anvil for rotary press.
Summary of the invention
The purpose of the present invention is being directed to, existing single-crystal diamond anvil can not be made into large scale and toughness, wearability are poor
Deficiency, provide it is a kind of for generating the compound anvil of polycrystalline diamond-hard alloy of high pressure shearing force, pass through improvement pressure
The shape and material of anvil so that can accommodate bigger sample size in high pressure high shear experiment, while playing the toughness for improving anvil
And wearability, increase the effect of the service life of anvil.
The purpose of the present invention is realized by following technical measures:
A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force, anvil anvil body are circle
Cylinder is divided into upper layer and lower layer, and upper layer is polycrystalline diamond layer 1, and lower layer is hard alloy layer 2, and polycrystalline diamond layer 1 and hard close
Layer gold 2 is combined in the integral mode of direct sintering；Polycrystalline diamond layer 1 is cylindrical body, and there is a circle chamfering on top, it is described fall
The angle, θ at angle is 5~30 °.
The top surface of polycrystalline diamond layer after chamfering is the acting surface of anvil, and acting surface is circle.The hard alloy 2
Generally use Talide.
The whole height of anvil between 5~20cm, the thickness of polycrystalline diamond layer is between 0.5~5cm, anvil radius
R between 1~10cm, the size of acting surface r is between 0~R.
When compressor operation, upper and lower two anvils are placed in rotary press, and for acting surface to together, centre is packed into gasket material
And sample, external motivating force makes to generate pressure between two anvils and shear stress is tested, and can produce 20GPa's or more
Pressure.
The invention has the following advantages that
1. the anvil of larger size can be fabricated to, acting surface diameter can reach 10cm or more, and sample cavity diameter can reach li
More than meter level, larger sample size can be accommodated and tested, the experiment effect being unable to reach supplemented with single-crystal diamond anvil.
Although joined bonding agent 2. the structure of polycrystalline diamond is the different fine-particle diamond sintered body of orientation,
Hardness is lower than single-crystal diamond, makes to test accessible maximum pressure lower than single-crystal diamond anvil, but due to polycrystalline diamond
In there are a large amount of crystal boundaries, interface bond angle can change, and sintered body macro manifestations are isotropism, therefore be not easy along single solution
Manage facial cleft.And contain a small amount of metal in sintered body, so that the anvil in the present invention has good toughness, play increase anvil
Service life effect.
3. polycrystalline diamond is electrically conductive, high pressure electrical measurement is directly carried out using the anvil in the invention.
4. the thermal coefficient of polycrystalline diamond is 700W/mK, it can heat and test in high pressure shearing force as anvil
It is middle to carry out good heat conduction；
5. polycrystalline diamond coefficient of friction is only 0.1~0.3, it is easier to carry out rotation process as anvil；
6. the affinity very little between polycrystalline diamond and non-ferrous metal and nonmetallic materials, so that the anvil after experiment can weigh
It is multiple to use.
7. anvil, which meets material, can contain the conductive material of sufficient amount, to keep anvil conductive, this gives the high pressure electricity of material
Measurement provides a great convenience.
8. saving superhard characteristic by Material cladding, increasing toughness.Compared with monocrystal material anvil, have
More useful mechanical performance is conducive to the various mechanics processing to material.
Detailed description of the invention
Attached drawing 1 is that the present invention is a kind of for generating the compound anvil of polycrystalline diamond-hard alloy of high pressure shearing force
Schematic perspective view；
Attached drawing 2 is two anvils to the structural schematic diagram for carrying out high pressure high shear experiment together.
The components in the drawings are labeled as follows: 1, polycrystalline diamond layer；2, hard alloy layer；3, round anvil acting surface；
4, the anvil in the present invention；5, gasket material and sample.5, sample；6, gasket material.
Specific embodiment
Presently preferred embodiments of the present invention is specifically addressed with reference to the accompanying drawing, it is necessary to which indicated herein is this implementation
Example is further described only for the present invention, should not be understood as limiting the scope of the invention, the technology in the field is ripe
Some nonessential modifications and adaptations can be made according to the content of aforementioned present invention by practicing personnel.
Specific embodiment:
As depicted in figs. 1 and 2,
The compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force, anvil anvil body are cylindrical body,
Cylindrical anvil radius R is 6cm, and anvil is divided into upper layer and lower layer, and upper layer is polycrystalline diamond layer 1, and lower layer is hard alloy layer 2,
In conjunction with the mode integral with direct sintering with hard alloy layer 2 of polycrystalline diamond layer 1；There is a circle on 1 top of polycrystalline diamond layer
Chamfering, the angle, θ of the chamfering are 25 °；The top surface of polycrystalline diamond layer after chamfering is the acting surface of anvil, and acting surface is circle
Shape, radius r are 5cm.
If chamfering is less than 5 ° in the present invention, no dimensional threshold, experimental pressure does not increase；If chamfering is greater than 30 °, edges and corners
Cleavage is easily rupturable, can greatly reduce the service life of anvil.The production of chamfering can lead to machining to realize.
Sample cavity diameter (does not have to gasket material to be installed) between 0~10cm when sample cavity diameter is 10cm, can root
It requires to be adjusted according to specific experiment.Round acting surface directly acts on gasket material and sample and generates high pressure.
The hard alloy generally uses Talide.
Preparation process:
The mixture of diamond dust and its binder powder is placed into pre-molding on cement carbide substrate, is then existed
It is sintered into one under high-temperature and high-pressure conditions, resulting materials are processed into the anvil geometric dimension of requirement.The size of anvil, plycrystalline diamond
Maximum pressure that the thickness of diamond layer, the size of acting surface and sample cavity diameter reach as needed for testing and shear stress
Designed by size and the weight of used belt type press, specific value can have according to the experience of High-Voltage Experimentation, experiment
Body requires and anvil working principle is adjusted.
The working principle of anvil of the present invention is, when compressor operation, upper and lower two anvils are placed in rotary press, are made
With in face of together, centre loading gasket material and sample, external motivating force make to generate pressure and shearing between two anvils
Stress is tested, and can produce the pressure of 20GPa or more.
Claims (3)
1. a kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force, which is characterized in that anvil
Anvil body is cylindrical body, is divided into upper layer and lower layer, and upper layer is polycrystalline diamond layer (1), and lower layer is hard alloy layer (2), plycrystalline diamond Buddha's warrior attendant
In conjunction with rock layers (1) mode integral with direct sintering with hard alloy layer (2)；Polycrystalline diamond layer (1) is cylindrical body, top
There is a circle chamfering at end, and the angle, θ of the chamfering is 5 °~30 °；The top surface of polycrystalline diamond layer after chamfering is the effect of anvil
Face, acting surface are circle.
2. it is according to claim 1 for generating the compound anvil of polycrystalline diamond-hard alloy of high pressure shearing force,
It is characterized in that, the material of the hard alloy layer (2) uses Talide.
3. it is according to claim 1 for generating the compound anvil of polycrystalline diamond-hard alloy of high pressure shearing force,
It is characterized in that, the whole height of anvil is between 5~20cm, the thickness of polycrystalline diamond layer between 0.5~5cm and/or
Anvil radius R is between 1~10cm.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811509700.8A CN109387427A (en) | 2018-12-11 | 2018-12-11 | A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811509700.8A CN109387427A (en) | 2018-12-11 | 2018-12-11 | A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force |
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| CN109387427A true CN109387427A (en) | 2019-02-26 |
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| CN201811509700.8A Pending CN109387427A (en) | 2018-12-11 | 2018-12-11 | A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112808170A (en) * | 2020-12-30 | 2021-05-18 | 深圳市海明润超硬材料股份有限公司 | Hard alloy composite anvil and preparation method thereof |
| CN114112892A (en) * | 2021-11-05 | 2022-03-01 | 南通爱尔思轻合金精密成型有限公司 | Experimental method for simulating grain boundary migration |
Citations (5)
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|---|---|---|---|---|
| US5780139A (en) * | 1996-09-18 | 1998-07-14 | Rogers Tool Works, Inc. | Multi-layer anvil for ultra high pressure presses |
| CN102527296A (en) * | 2012-01-06 | 2012-07-04 | 吉林大学 | Multi-stage filleted high-pressure anvil |
| CN102671578A (en) * | 2012-05-15 | 2012-09-19 | 四川大学 | Polycrystalline diamond-tungsten carbide rigid alloy composite anvil for generating ultrahigh pressure |
| CN108745204A (en) * | 2018-08-09 | 2018-11-06 | 吉林师范大学 | The polycrystalline diamond anvil and preparation method thereof of optic test can be achieved |
| CN209372549U (en) * | 2018-12-11 | 2019-09-10 | 吉林师范大学 | A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force |
-
2018
- 2018-12-11 CN CN201811509700.8A patent/CN109387427A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5780139A (en) * | 1996-09-18 | 1998-07-14 | Rogers Tool Works, Inc. | Multi-layer anvil for ultra high pressure presses |
| CN102527296A (en) * | 2012-01-06 | 2012-07-04 | 吉林大学 | Multi-stage filleted high-pressure anvil |
| CN102671578A (en) * | 2012-05-15 | 2012-09-19 | 四川大学 | Polycrystalline diamond-tungsten carbide rigid alloy composite anvil for generating ultrahigh pressure |
| CN108745204A (en) * | 2018-08-09 | 2018-11-06 | 吉林师范大学 | The polycrystalline diamond anvil and preparation method thereof of optic test can be achieved |
| CN209372549U (en) * | 2018-12-11 | 2019-09-10 | 吉林师范大学 | A kind of compound anvil of polycrystalline diamond-hard alloy for generating high pressure shearing force |
Non-Patent Citations (1)
| Title |
|---|
| 王海阔;贺端威;许超;刘方明;邓佶睿;何飞;王永坤;寇自力;: "复合型多晶金刚石末级压砧的制备并标定六面顶压机6-8型压腔压力至35GPa", 物理学报, no. 18, pages 1 - 7 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112808170A (en) * | 2020-12-30 | 2021-05-18 | 深圳市海明润超硬材料股份有限公司 | Hard alloy composite anvil and preparation method thereof |
| CN114112892A (en) * | 2021-11-05 | 2022-03-01 | 南通爱尔思轻合金精密成型有限公司 | Experimental method for simulating grain boundary migration |
| CN114112892B (en) * | 2021-11-05 | 2024-05-24 | 南通爱尔思轻合金精密成型有限公司 | Experimental method for simulating grain boundary migration |
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