CN109387342A - Low leakage sealed service check method - Google Patents

Low leakage sealed service check method Download PDF

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Publication number
CN109387342A
CN109387342A CN201710677441.9A CN201710677441A CN109387342A CN 109387342 A CN109387342 A CN 109387342A CN 201710677441 A CN201710677441 A CN 201710677441A CN 109387342 A CN109387342 A CN 109387342A
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CN
China
Prior art keywords
valve
low leakage
service check
test
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710677441.9A
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Chinese (zh)
Inventor
肖安山
邹兵
邱平
马志刚
王春鹏
毛华平
王志强
韩嘉兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Bao Hua Sealing Polytron Technologies Inc
China Petroleum and Chemical Corp
Sinopec Engineering Inc
Sinopec Qingdao Safety Engineering Institute
Original Assignee
Suzhou Bao Hua Sealing Polytron Technologies Inc
China Petroleum and Chemical Corp
Sinopec Engineering Inc
Sinopec Qingdao Safety Engineering Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Bao Hua Sealing Polytron Technologies Inc, China Petroleum and Chemical Corp, Sinopec Engineering Inc, Sinopec Qingdao Safety Engineering Institute filed Critical Suzhou Bao Hua Sealing Polytron Technologies Inc
Priority to CN201710677441.9A priority Critical patent/CN109387342A/en
Publication of CN109387342A publication Critical patent/CN109387342A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • G01M3/28Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for pipes, cables or tubes; for pipe joints or seals; for valves ; for welds
    • G01M3/2876Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for pipes, cables or tubes; for pipe joints or seals; for valves ; for welds for valves
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Examining Or Testing Airtightness (AREA)

Abstract

The present invention relates to a kind of low leakage sealed service check methods, mainly solve the problems, such as that service check can not be sealed to Leak seals parts under working condition in the prior art.The present invention is by using the method for carrying out low Leak seals parts service check under the conditions of Work condition analogue, service check is sealed using low leakage sealed performance inspection device, the low leakage sealed performance inspection device includes that the technical solution for simulating working condition system, seal assembly test station and leak detection system preferably solves the above problem, be can be used in low leakage sealed service check.

Description

Low leakage sealed service check method
Technical field
The present invention relates to a kind of low leakage sealed service check methods.
Background technique
In recent years, with the continuous aggravation of domestic air pollution, volatile organic matter (VOCs) emission control becomes environmental protection One of major tasks of improvement.Most materials, medium belong to volatile organic compounds in petrochemical enterprise production process, And the static seals such as numerous valves, flange, pump and dynamic sealing assembly involved in process equipment, meeting can not during production run Generate a large amount of VOCs leakage discharge with avoiding, causes petrochemical industry to become one of the primary discharge source of atmosphere VOCs.For Air pollution is administered, " planning of national environmental protection " 12th Five-Year Plan " " clearly proposes: " reinforcing petrochemical industry production, conveying and storage Process volatile organic contaminant emission control ".Petrochemical enterprise is to reduce environmental pollution, reduce refining losses, also Continue to increase the emission control to VOCs.According to statistics, apparatus assembly leakage (i.e. uncontrollable discharge) Zhan Shihua VOCs is discharged about 70%, it is VOCs primary discharge source, solving apparatus assembly leakage becomes the most important thing of petrochemical industry control VOCs discharge. And in the reason of causing apparatus assembly to leak, remove the originals such as seal assembly maintenance not in place, manual operation or Rig up error Because outer, the failure of equipment sealing material and wherein most important reason are mainly manifested in sealing materials type selecting such as gasket, filler etc. Grade not enough, be not up to expected by performance.Therefore, the performance verification of equipment seal assembly, it is ensured that seal assembly all technical reaches It is to realize that the source of apparatus assembly zero leakage guarantees to related seals class requirement.
It is directed to the inspection of low Leak seals parts both at home and abroad at present, is mainly carried out under normal temperature and pressure or specific temperature conditions It examines, lacks working condition lower seal service check means, cannot really reflect leakproofness of the sealing element under working condition Energy.
Anti- loss seal assembly verifying bench is established, seeks to carry out the equipment seal assembly such as low leakage valve, flange Performance verification guarantees that the design of petrochemical industry water-tight equipment and type selecting meet the requirements, equipment leakage is reduced from source, realizes to VOCs " the source control " of discharge.
Summary of the invention
The technical problem to be solved by the present invention is in the prior art can not under working condition to Leak seals parts into The problem of row sealing performance is examined provides a kind of new low leakage sealed service check method.This method has Work condition analogue, reality Test the advantage that medium is optional, detection method is various.
To solve the above problems, The technical solution adopted by the invention is as follows: a kind of low leakage sealed service check method, is adopted Low leakage sealed service check is carried out with the low leakage sealed performance inspection device with Work condition analogue function, the low leakage is close Sealing property verifying attachment includes simulation working condition system, seal assembly test station and leak detection system, simulation working condition system by Compressor, head tank, surge tank and heating and cooling system composition, it includes a valve and filler or method that seal assembly, which tests station, Blue to test station with gasket, leak detection system includes detector, and leak detection system is connected with the test station, compressor Outlet is connected with heating device entrance, and heating means exit is connected with test station, tests station outlet line after heat exchanger It is connected respectively with surge tank, suction port of compressor, head tank, test medium pipeline is connected on head tank;Control system and operating condition mould Quasi- system is connected;
When carrying out low leakage sealed service check, include the following steps:
(1) test medium enters system to testing pressure by pressure reducing valve after surge tank, and by heater by medium temperature Degree is promoted to test temperature, closes air intake valve, system maintains test pressure by pressure reducing valve, and passes through heater and controlling temp type companion The torrid zone carries out sealing property of sealing component inspection after maintaining test temperature, experiment condition to reach requirement;
(2) after sealing element test ending, air intake valve is opened, and test medium is dropped by pressure reducing valve after valve and cooler Pressure, cooling, are emitted into system;
(3) discharge gas can improve raw material pressure inside the tank after entering system, at this moment close pressure surge tank imported valve, open Gas storage surge tank inlet valve simultaneously opens supercharger by the gas compression of discharge to gas storage surge tank, just to head tank pressure recovery Gas storage surge tank imported valve, close compressor are closed after constant value, and open pressure surge tank inlet valve;
(4) medium is supplemented in head tank after being depressured by counterbalance valve in gas storage surge tank when normal experiment, and system is first By gas storage surge tank, into system, make-up gas illustrates to damage due to leakage if raw material pressure inside the tank is reduced to normal value Helium is insufficient in mistake system, the tonifying Qi into system to system regulating valve of test medium steel cylinder is at this moment automatically opened, when head tank pressure Power closes regulating valve when being restored to normal value.
In above-mentioned technical proposal, it is preferable that described device has the function of Work condition analogue.
In above-mentioned technical proposal, it is preferable that detector is photoionization detector (PID), flame ionization detector (FID) or mass spectrograph.
In above-mentioned technical proposal, it is preferable that test station is valve and filler or flange and gasket.
In above-mentioned technical proposal, it is preferable that test(ing) medium is helium or methane.
In above-mentioned technical proposal, it is preferable that described device can simulate high temperature and pressure and change to operating condition between normal temperature and pressure, By designing the change frequency of different parameters, seal assembly performance parameter under the conditions of specific operation is obtained.
In above-mentioned technical proposal, it is preferable that test station outlet line is connected with heat exchanger tube pass, and heat exchanger shell pass passes through Pipeline is connected with cooler.
The object of the present invention is to provide a kind of valve of Work condition analogue function, flange and the low leakage sealed performances of sealing material The method of inspection.It is able to achieve low leakage (anti-loss) service check to valve and filler, flange and gasket, can to new purchase or The valve of inventory, filler, flange, gasket sealing performance detect and quality control, and the equipment of new device is selected Whether type design rationally carries out simplation verification, and the present invention, which is able to achieve, carries out service check to the equipment seal assembly such as valve, flange, The performance certification system of seal assembly is set up, guarantees that the design of the water-tight equipments such as valve, flange and type selecting meet the requirements, from source Equipment leakage is reduced on head, is realized " the source control " discharged to VOCs, is achieved preferable technical effect.
Detailed description of the invention
Fig. 1 is the flow diagram of the method for the invention.
In Fig. 1,1, head tank;2, gas storage surge tank;3, compressor;4, pressure surge tank;5, heater;6, detector; 7, cooler.
The present invention will be further described below by way of examples, but is not limited only to the present embodiment.
Specific embodiment
[embodiment 1]
A kind of low leakage sealed service check method, as shown in Figure 1, a kind of low leakage sealed performance inspection device is provided, Including simulation working condition system, seal assembly test station and leak detection system, simulation working condition system is by compressor, raw material Tank, surge tank and heating and cooling system composition, it is maximum by automatically controlling pressure, temperature, the flow velocity operating condition of simulation field device Degree simulated field conditions;It is valve and filler experiment station that seal assembly, which tests station,;Leak detection system include detector, Leak detection system is connected with the test station, and compressor outlet is connected with heating device entrance, heating means exit and examination It tests station to be connected, test station outlet line is connected with surge tank, suction port of compressor, head tank respectively after heat exchanger, raw material Test medium pipeline is connected on tank;Control system is connected with Simulated System;.
Test station outlet line is connected with heat exchanger tube pass, and heat exchanger shell pass is connected by pipeline with cooler.
The leak detection system includes PID, FID, mass spectrometer detector.Described device can simulate high temperature and pressure and arrive Operating condition changes between normal temperature and pressure, by designing the change frequency of different parameters, obtains seal assembly under the conditions of specific operation It can parameter
When installation, simulation working condition system, seal assembly are tested into station and leak detection system three parts group as shown in Figure 1 It is fitted together, forms low leakage sealed service check method completely with Work condition analogue function.
When carrying out low leakage sealed service check, include the following steps:
(1) test medium enters system to testing pressure by pressure reducing valve after surge tank, and by heater by medium temperature Degree is promoted to test temperature.Air intake valve is closed, system maintains test pressure by pressure reducing valve, and passes through heater and controlling temp type companion The torrid zone carries out sealing property of sealing component inspection after maintaining test temperature, experiment condition to reach requirement, obtains the slip of sealing element;
(2) after sealing element test ending, air intake valve is opened, and test medium is dropped by pressure reducing valve after valve and cooler Pressure, cooling, are emitted into system;
(3) discharge gas can improve raw material pressure inside the tank after entering system, at this moment close pressure surge tank imported valve, open Gas storage surge tank inlet valve simultaneously opens supercharger by the gas compression of discharge to gas storage surge tank, just to head tank pressure recovery Gas storage surge tank imported valve, close compressor are closed after constant value, and open pressure surge tank inlet valve;
(4) medium is supplemented in head tank after being depressured by counterbalance valve in gas storage surge tank when normal experiment, and system is first By gas storage surge tank into system make-up gas, if explanation is due to leakage loss when raw material pressure inside the tank is reduced to normal value Helium is insufficient in system, the tonifying Qi into system to system regulating valve of test medium steel cylinder is at this moment automatically opened, when raw material pressure tank Regulating valve is closed when being restored to normal value.
[embodiment 2]
According to condition and step described in embodiment, only testing station is flange and gasket test station in fact.
When carrying out low leakage sealed service check, include the following steps:
(1) test medium enters system to testing pressure by pressure reducing valve after surge tank, and by heater by medium temperature Degree is promoted to test temperature.Air intake valve is closed, system maintains test pressure by pressure reducing valve, and passes through heater and controlling temp type companion The torrid zone carries out sealing property of sealing component inspection after maintaining test temperature, experiment condition to reach requirement, obtains the slip of sealing element;
(2) after sealing element test ending, air intake valve is opened, and test medium is dropped by pressure reducing valve after valve and cooler Pressure, cooling, are emitted into system;
(3) discharge gas can improve raw material pressure inside the tank after entering system, at this moment close pressure surge tank imported valve, open Gas storage surge tank inlet valve simultaneously opens supercharger by the gas compression of discharge to gas storage surge tank, just to head tank pressure recovery Gas storage surge tank imported valve, close compressor are closed after constant value, and open pressure surge tank inlet valve;
(4) medium is supplemented in head tank after being depressured by counterbalance valve in gas storage surge tank when normal experiment, and system is first By gas storage surge tank into system make-up gas, if explanation is due to leakage loss when raw material pressure inside the tank is reduced to normal value Helium is insufficient in system, the tonifying Qi into system to system regulating valve of test medium steel cylinder is at this moment automatically opened, when raw material pressure tank Regulating valve is closed when being restored to normal value.
The present invention is able to achieve low leakage (anti-loss) service check to valve and filler, flange and gasket, can be to new Purchase or the valve of inventory, filler, flange, gasket sealing performance detect and quality controls, and new device is set Whether standby Selection and Design rationally carries out simplation verification, and the present invention, which is able to achieve, carries out performance to the equipment seal assembly such as valve, flange It examines, it is established that the performance certification system of seal assembly guarantees that the design of the water-tight equipments such as valve, flange and type selecting conform to It asks, equipment leakage is reduced from source, realize " the source control " discharged to VOCs, achieve preferable technical effect.
Compared with the present invention, the existing low Leak seals parts method of inspection both at home and abroad, mainly in normal temperature and pressure or specific It tests under the conditions of temperature, test(ing) medium cannot be replaced, detection means is single, lack working condition lower seal service check Ability cannot really reflect sealing performance of the sealing element under working condition.

Claims (7)

1. a kind of low leakage sealed service check method, using the low leakage sealed performance inspection device with Work condition analogue function Low leakage sealed service check is carried out, the low leakage sealed performance inspection device includes simulation working condition system, seal assembly examination Station and leak detection system are tested, simulation working condition system is made of compressor, head tank, surge tank and heating and cooling system, close It includes that a valve and filler or flange and gasket test station that sealing assembly, which tests station, and leak detection system includes detector, Leak detection system is connected with the test station, and compressor outlet is connected with heating device entrance, heating means exit and examination It tests station to be connected, test station outlet line is connected with surge tank, suction port of compressor, head tank respectively after heat exchanger, raw material Test medium pipeline is connected on tank;Control system is connected with Simulated System;
When carrying out low leakage sealed service check, include the following steps:
(1) test medium enters system to testing pressure by pressure reducing valve after surge tank, and is proposed medium temperature by heater Test temperature is risen to, closes air intake valve, system maintains test pressure by pressure reducing valve, and passes through heater and controlling temp type heating tape Sealing property of sealing component inspection is carried out after maintaining test temperature, experiment condition to reach requirement;
(2) after sealing element test ending, air intake valve is opened, and be depressured test medium by pressure reducing valve after valve and cooler, Cooling, is emitted into system;
(3) discharge gas can improve raw material pressure inside the tank after entering system, at this moment close pressure surge tank imported valve, open gas storage Surge tank inlet valve simultaneously opens supercharger by the gas compression of discharge to gas storage surge tank, to head tank pressure recovery normal value Gas storage surge tank imported valve, close compressor are closed afterwards, and open pressure surge tank inlet valve;
(4) medium is supplemented in head tank after being depressured by counterbalance valve in gas storage surge tank when normal experiment, and system relies on first Gas storage surge tank make-up gas into system illustrates if raw material pressure inside the tank is reduced to normal value due to leakage loss system Helium is insufficient in uniting, and the tonifying Qi into system to system regulating valve of test medium steel cylinder is at this moment automatically opened, when raw material pressure tank is extensive Regulating valve is closed when arriving normal value again.
2. low leakage sealed service check method according to claim 1, it is characterised in that described device has Work condition analogue Function.
3. low leakage sealed service check method according to claim 1, it is characterised in that detector is photoionization detection Device, flame ionization detector or mass spectrograph.
4. low leakage sealed service check method according to claim 1, it is characterised in that test station is valve and filler Or flange and gasket.
5. low leakage sealed service check method according to claim 1, it is characterised in that test medium is helium or methane.
6. low leakage sealed service check method according to claim 1, it is characterised in that described device can simulate high temperature High pressure changes to operating condition between normal temperature and pressure, by designing the change frequency of different parameters, seals under the conditions of acquisition specific operation Assembly property parameter.
7. low leakage sealed service check method according to claim 1, it is characterised in that test station outlet line and change Hot device tube side is connected, and heat exchanger shell pass is connected by pipeline with cooler.
CN201710677441.9A 2017-08-09 2017-08-09 Low leakage sealed service check method Pending CN109387342A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6259769B2 (en) * 1980-03-05 1987-12-12 Nippon Oil Co Ltd
CN101118197A (en) * 2007-09-06 2008-02-06 中国核动力研究设计院 High-temperature high pressure helium leak detection method and apparatus for detecting leakage thereof
CN101806662A (en) * 2009-02-12 2010-08-18 方存正 Low temperature test device
CN103454168A (en) * 2013-09-10 2013-12-18 浙江省泵阀产品质量检验中心 Rapid gas decompression (RGD) detection system and method of anti-explosion O-shaped ring for petrochemical valve
CN105118536A (en) * 2015-08-18 2015-12-02 中国人民解放军陆军军官学院 Adjustable charge-discharge type high temperature and high pressure helium gas experimental system and method
CN105181267A (en) * 2015-07-17 2015-12-23 武汉工程大学 Device for testing leakage rate of bolted flange connection system

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6259769B2 (en) * 1980-03-05 1987-12-12 Nippon Oil Co Ltd
CN101118197A (en) * 2007-09-06 2008-02-06 中国核动力研究设计院 High-temperature high pressure helium leak detection method and apparatus for detecting leakage thereof
CN101806662A (en) * 2009-02-12 2010-08-18 方存正 Low temperature test device
CN103454168A (en) * 2013-09-10 2013-12-18 浙江省泵阀产品质量检验中心 Rapid gas decompression (RGD) detection system and method of anti-explosion O-shaped ring for petrochemical valve
CN105181267A (en) * 2015-07-17 2015-12-23 武汉工程大学 Device for testing leakage rate of bolted flange connection system
CN105118536A (en) * 2015-08-18 2015-12-02 中国人民解放军陆军军官学院 Adjustable charge-discharge type high temperature and high pressure helium gas experimental system and method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
国际标准化组织: "《ISO 15848-1》", 31 December 2016 *

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Application publication date: 20190226