CN109387077A - A kind of vacuum hotpressing stove temperature control system - Google Patents

A kind of vacuum hotpressing stove temperature control system Download PDF

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Publication number
CN109387077A
CN109387077A CN201710693474.2A CN201710693474A CN109387077A CN 109387077 A CN109387077 A CN 109387077A CN 201710693474 A CN201710693474 A CN 201710693474A CN 109387077 A CN109387077 A CN 109387077A
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CN
China
Prior art keywords
temperature
mold
electromagnetic heater
supply unit
power supply
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Pending
Application number
CN201710693474.2A
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Chinese (zh)
Inventor
肖震
韩珩
解伟
钟炳文
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Longyan Cercis Innovation Research Institute
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Longyan Cercis Innovation Research Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN201710693474.2A priority Critical patent/CN109387077A/en
Publication of CN109387077A publication Critical patent/CN109387077A/en
Pending legal-status Critical Current

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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/04Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated adapted for treating the charge in vacuum or special atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • F27B5/14Arrangements of heating devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • F27B5/18Arrangement of controlling, monitoring, alarm or like devices

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Moulds For Moulding Plastics Or The Like (AREA)

Abstract

The present invention provides a kind of vacuum hotpressing stove temperature control system, the system comprises: power supply unit, control device, electromagnetic heater, mold, temperature-detecting device, muff;The control device is arranged between the power supply unit and electromagnetic heater, control device is used to control the size of the power supply unit and electromagnetic heater energization and power-off or control power supply unit to electromagnetic heater output electric current, and then control electromagnetic heater is to the heating temperature of mold.Vacuum hotpressing stove temperature control system of the invention has preferable temperature incubation function, so that magnetic powder is hot pressed into green compact at a relative constant temperature always, magnet obtained will have preferable magnetic property.

Description

A kind of vacuum hotpressing stove temperature control system
Technical field
The present invention relates to magnet manufacturing field, in particular to a kind of vacuum hotpressing stove temperature control system.
Background technique
Vacuum hotpressing stove is usually used in preparing anisotropic neodymium iron boron magnetic body.The preparation process of anisotropic neodymium iron boron magnetic body Are as follows: magnetic powder is first packed into mold, is hot pressed into green compact under a certain temperature and pressure, green compact be it is cylindric, then green compact is put into Deformation is depressed in the bigger mold of diameter under a certain temperature and pressure, deformed magnet is disc-shaped, after deformation in magnet Portion's structure changes, and improves magnetic property.During hot pressing and thermal deformation two, temperature is all mostly important factor.
The heating method of vacuum hotpressing stove uses induction heating, and temperature rises fast when the characteristics of induction heating is to heat, Stop temperature after heating declining rapidly, be not easy that temperature is made to maintain preset value in this way, can not also keep the temperature, influence magnet performance and The consistency of product.
Summary of the invention
In order to solve vacuum hotpressing stove can not heated at constant temperature the technical issues of, the present invention is implemented as follows:
A kind of vacuum hotpressing stove temperature control system, the system comprises: power supply unit, control device, electromagnetic heater, mould Tool, temperature-detecting device, muff;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation and electromagnetic heater are powered and power off, and then control electromagnetic heater to the heating of mold or do not heat;
The temperature-detecting device is electrically connected with control device, for detecting the temperature of mould inside;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold, power supply unit and electromagnetic heater power off, electromagnetic heater Mold is not heated;When temperature-detecting device detects that temperature reaches default minimum temperature threshold in mold, power supply unit with Electromagnetic heater is powered, and electromagnetic heater heats mold;
The muff package is partly wrapped on the outside of mold, for keeping the temperature to mold.
Preferably, the muff is made of mullite fiber;Its chemical constituent is the AL of 72%-75%2O3, 17%- 20% SiO2, remaining group is divided into ZrO2And Fe2O3
A kind of vacuum hotpressing stove temperature control system, the system comprises: power supply unit, control device, electromagnetic heater, mould Tool, temperature-detecting device;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation exports the size of electric current to electromagnetic heater, and then controls electromagnetic heater to the heating power of mold;
The temperature-detecting device is electrically connected with control device, for detecting the temperature of mould inside;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold, power supply unit becomes smaller to the electric current that electromagnetic heater exports, Electromagnetic heater is reduced to the heating power of mold;When temperature-detecting device detects that temperature reaches default minimum temperature in mold When threshold value, power supply unit becomes larger to the electric current that electromagnetic heater exports, and increases electromagnetic heater to the heating power of mold.
Preferably, the difference of the maximum temperature threshold value and minimum temperature threshold is not more than 20 DEG C.
Further, the difference of the maximum temperature threshold value and minimum temperature threshold is 5 DEG C.
The beneficial effects of the present invention are:
The present invention maintains the relative constant of temperature in mold using two kinds of mentalities of designing: thinking is first is that in mold outer sheath With the preferable muff of thermal insulation property, cooperation control power supply unit and electromagnetic heater are powered and power off to maintain temperature in mold It is relative constant;Thinking is second is that by changing size of the power supply unit to electromagnetic heater output electric current, so that mold receives Thermal energy and the thermal energy of mold and air exchange reach balance in certain temperature range, for maintaining the opposite of temperature in mold It is constant.
Detailed description of the invention
Fig. 1 is a kind of vacuum hotpressing stove temperature control system structural schematic diagram provided in an embodiment of the present invention.
Specific embodiment
In order to describe the technical content, the structural feature, the achieved object and the effect of this invention in detail, below in conjunction with embodiment And attached drawing is cooperated to be explained in detail.
Embodiment 1
A kind of vacuum hotpressing stove temperature control system (as shown in Figure 1), the system comprises: power supply unit, control device, electromagnetism Heater, mold 1, temperature-detecting device, muff 2;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation and electromagnetic heater are powered and power off, and then control electromagnetic heater to the heating of mold 1 or do not heat;
The temperature-detecting device is electrically connected with control device, for detecting the temperature inside mold 1;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold 1, power supply unit and electromagnetic heater power off, electromagnetic heater Mold 1 is not heated;When temperature-detecting device detects that temperature reaches default minimum temperature threshold in mold 1, power supply unit It is powered with electromagnetic heater, electromagnetic heater heats mold 1;The difference of the maximum temperature threshold value and minimum temperature threshold No more than 20 DEG C;
The muff 2 package is partly wrapped in 1 outside of mold, for being kept the temperature to mold 1, the muff 2 by Mullite fiber is made;Its chemical constituent is the AL of 72% (being weight percentage below)2O3, 20% SiO2, 4% ZrO2With 4% Fe2O3.Mullite fiber maximum operation (service) temperature has significant thermal insulation property up to 1600 degree.
After magnetic powder is packed into mold 1, different magnetic powders has different hot pressing temperatures, according to the difference of processing magnetic powder, setting Different temperature thresholds.When beginning to warm up, 1 temperature of mold is gradually increasing by room temperature, when reaching default maximum temperature threshold value, is supplied Electric installation and electromagnetic heater power off, and electromagnetic heater does not heat mold 1, kept the temperature by muff 2 to mold 1, because protecting The material of temperature set 2 is special, has preferable heat insulation effect, after a period of time, the temperature of mold 1 can just drop to preset minimum Temperature threshold, power supply unit and electromagnetic heater are powered at this time, and electromagnetic heater heats mold 1, until 1 temperature of mold reaches When default maximum temperature threshold value, power supply unit and electromagnetic heater are powered off, and electromagnetic heater does not heat mold 1.And so on Circulation realizes the opposite heated at constant temperature to magnetic powder.The size of constant temperature depends on the difference of maximum temperature threshold value and minimum temperature threshold Value, generally, the difference is smaller, and the effect of heated at constant temperature is more obvious.
Embodiment 2
A kind of vacuum hotpressing stove temperature control system (as shown in Figure 1), the system comprises: power supply unit, control device, electromagnetism Heater, mold 1, temperature-detecting device, muff 2;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation and electromagnetic heater are powered and power off, and then control electromagnetic heater to the heating of mold 1 or do not heat;
The temperature-detecting device is electrically connected with control device, for detecting the temperature inside mold 1;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold 1, power supply unit and electromagnetic heater power off, electromagnetic heater Mold 1 is not heated;When temperature-detecting device detects that temperature reaches default minimum temperature threshold in mold 1, power supply unit It is powered with electromagnetic heater, electromagnetic heater heats mold 1;The difference of the maximum temperature threshold value and minimum temperature threshold No more than 10 DEG C;
The muff 2 package is partly wrapped in 1 outside of mold, for being kept the temperature to mold 1, the muff 2 by Mullite fiber is made;The AL that its chemical constituent is 75%2O3, 17% SiO2, 3% ZrO2With 5% Fe2O3.Mullite Fiber maximum operation (service) temperature has significant thermal insulation property up to 1600 degree.
After magnetic powder is packed into mold 1, different magnetic powders has different hot pressing temperatures, according to the difference of processing magnetic powder, setting Different temperature thresholds.When beginning to warm up, 1 temperature of mold is gradually increasing by room temperature, when reaching default maximum temperature threshold value, is supplied Electric installation and electromagnetic heater power off, and electromagnetic heater does not heat mold 1, kept the temperature by muff 2 to mold 1, because protecting The material of temperature set 2 is special, has preferable heat insulation effect, after a period of time, the temperature of mold 1 can just drop to preset minimum Temperature threshold, power supply unit and electromagnetic heater are powered at this time, and electromagnetic heater heats mold 1, until 1 temperature of mold reaches When default maximum temperature threshold value, power supply unit and electromagnetic heater are powered off, and electromagnetic heater does not heat mold 1.And so on Circulation realizes the opposite heated at constant temperature to magnetic powder.The size of constant temperature depends on the difference of maximum temperature threshold value and minimum temperature threshold Value, generally, the difference is smaller, and the effect of heated at constant temperature is more obvious.
Embodiment 3
A kind of vacuum hotpressing stove temperature control system (as shown in Figure 1), the system comprises: power supply unit, control device, electromagnetism Heater, mold 1, temperature-detecting device, muff 2;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation and electromagnetic heater are powered and power off, and then control electromagnetic heater to the heating of mold 1 or do not heat;
The temperature-detecting device is electrically connected with control device, for detecting the temperature inside mold 1;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold 1, power supply unit and electromagnetic heater power off, electromagnetic heater Mold 1 is not heated;When temperature-detecting device detects that temperature reaches default minimum temperature threshold in mold 1, power supply unit It is powered with electromagnetic heater, electromagnetic heater heats mold 1;The difference of the maximum temperature threshold value and minimum temperature threshold No more than 5 DEG C;
The muff 2 package is partly wrapped in 1 outside of mold, for being kept the temperature to mold 1, the muff 2 by Mullite fiber is made;The AL that its chemical constituent is 74%2O3, 18% SiO2, 6% ZrO2With 2% Fe2O3.Mullite Fiber maximum operation (service) temperature has significant thermal insulation property up to 1600 degree.
After magnetic powder is packed into mold 1, different magnetic powders has different hot pressing temperatures, according to the difference of processing magnetic powder, setting Different temperature thresholds.When beginning to warm up, 1 temperature of mold is gradually increasing by room temperature, when reaching default maximum temperature threshold value, is supplied Electric installation and electromagnetic heater power off, and electromagnetic heater does not heat mold 1, kept the temperature by muff 2 to mold 1, because protecting The material of temperature set 2 is special, has preferable heat insulation effect, after a period of time, the temperature of mold 1 can just drop to preset minimum Temperature threshold, power supply unit and electromagnetic heater are powered at this time, and electromagnetic heater heats mold 1, until 1 temperature of mold reaches When default maximum temperature threshold value, power supply unit and electromagnetic heater are powered off, and electromagnetic heater does not heat mold 1.And so on Circulation realizes the opposite heated at constant temperature to magnetic powder.The size of constant temperature depends on the difference of maximum temperature threshold value and minimum temperature threshold Value, generally, the difference is smaller, and the effect of heated at constant temperature is more obvious.
Embodiment 4
A kind of vacuum hotpressing stove temperature control system (as shown in Figure 1), the system comprises: power supply unit, control device, electromagnetism Heater, mold 1, temperature-detecting device;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation exports the size of electric current to electromagnetic heater, and then controls electromagnetic heater to the heating power of mold 1;
The temperature-detecting device is electrically connected with control device, for detecting the temperature inside mold 1;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold 1, power supply unit becomes smaller to the electric current that electromagnetic heater exports, Electromagnetic heater is reduced to the heating power of mold 1;When temperature-detecting device detects that temperature reaches default lowest temperature in mold 1 When spending threshold value, power supply unit becomes larger to the electric current that electromagnetic heater exports, and increases electromagnetic heater to the heating power of mold 1; The difference of the maximum temperature threshold value and minimum temperature threshold is not more than 20 DEG C.
After magnetic powder is packed into mold 1, different magnetic powders has different hot pressing temperatures, according to the difference of processing magnetic powder, setting Different temperature thresholds.When beginning to warm up, 1 temperature of mold is gradually increasing by room temperature, when reaching default maximum temperature threshold value, is supplied Electric installation becomes smaller to electromagnetic heater output electric current, reduces electromagnetic heater to the heating power of mold 1;Mold 1 and sky at this time Heat exchange occurs for gas, and (1) when the heat that mold 1 obtains is equal with the heat that air exchanges therewith, the temperature of mold 1 will Maintain maximum temperature threshold value;(2) when the heat that mold 1 obtains is less than the heat that air exchanges therewith, the temperature of mold 1 Degree, which will be gradually decrease until, reaches minimum temperature threshold, and power supply unit becomes larger to the electric current that electromagnetic heater exports, and increases electromagnetism Heater is to the heating power of mold 1, and the temperature of mold 1 slowly increases, until temperature reaches default maximum temperature threshold in mold 1 When value, power supply unit becomes smaller to the electric current that electromagnetic heater exports, so on circulate;(3) when the heat that mold 1 obtains is greater than When the heat that air exchanges therewith, temperature will be more than maximum temperature threshold value, and power supply unit exports electricity to electromagnetic heater Stream will continue to become smaller until temperature drops to maximum temperature threshold value or less.Control device controls the power supply unit to electromagnetic heater The size for exporting electric current depends on the heat exchange amount of mold 1 and air, increases or reduce the size of electric current, its purpose is to So that thermal energy and mold 1 that mold 1 receives and the thermal energy of air exchange reach balance in certain temperature range, for maintaining Temperature is relative constant in mold 1.
Embodiment 5
A kind of vacuum hotpressing stove temperature control system (as shown in Figure 1), the system comprises: power supply unit, control device, electromagnetism Heater, mold 1, temperature-detecting device;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is for controlling the confession Electric installation exports the size of electric current to electromagnetic heater, and then controls electromagnetic heater to the heating power of mold 1;
The temperature-detecting device is electrically connected with control device, for detecting the temperature inside mold 1;When temperature detection fills It sets when detecting that temperature reaches default maximum temperature threshold value in mold 1, power supply unit becomes smaller to the electric current that electromagnetic heater exports, Electromagnetic heater is reduced to the heating power of mold 1;When temperature-detecting device detects that temperature reaches default lowest temperature in mold 1 When spending threshold value, power supply unit becomes larger to the electric current that electromagnetic heater exports, and increases electromagnetic heater to the heating power of mold 1; The difference of the maximum temperature threshold value and minimum temperature threshold is not more than 5 DEG C.
After magnetic powder is packed into mold 1, different magnetic powders has different hot pressing temperatures, according to the difference of processing magnetic powder, setting Different temperature thresholds.When beginning to warm up, 1 temperature of mold is gradually increasing by room temperature, when reaching default maximum temperature threshold value, is supplied Electric installation becomes smaller to electromagnetic heater output electric current, reduces electromagnetic heater to the heating power of mold 1;Mold 1 and sky at this time Heat exchange occurs for gas, and (1) when the heat that mold 1 obtains is equal with the heat that air exchanges therewith, the temperature of mold 1 will Maintain maximum temperature threshold value;(2) when the heat that mold 1 obtains is less than the heat that air exchanges therewith, the temperature of mold 1 Degree, which will be gradually decrease until, reaches minimum temperature threshold, and power supply unit becomes larger to the electric current that electromagnetic heater exports, and increases electromagnetism Heater is to the heating power of mold 1, and the temperature of mold 1 slowly increases, until temperature reaches default maximum temperature threshold in mold 1 When value, power supply unit becomes smaller to the electric current that electromagnetic heater exports, so on circulate;(3) when the heat that mold 1 obtains is greater than When the heat that air exchanges therewith, temperature will be more than maximum temperature threshold value, and power supply unit exports electricity to electromagnetic heater Stream will continue to become smaller until temperature drops to maximum temperature threshold value or less.Control device controls the power supply unit to electromagnetic heater The size for exporting electric current depends on the heat exchange amount of mold 1 and air, increases or reduce the size of electric current, its purpose is to So that thermal energy and mold 1 that mold 1 receives and the thermal energy of air exchange reach balance in certain temperature range, for maintaining Temperature is relative constant in mold 1.
The above description is only an embodiment of the present invention, is not intended to limit scope of patent protection of the invention, all utilizations Equivalent structure or equivalent flow shift made by description of the invention and accompanying drawing content is applied directly or indirectly in other correlations Technical field, be included within the scope of the present invention.

Claims (5)

1. a kind of vacuum hotpressing stove temperature control system, which is characterized in that the system comprises: power supply unit, control device, electromagnetism add Hot device, mold, temperature-detecting device, muff;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is described for Denso for controlling It sets and is powered and powers off with electromagnetic heater, and then control electromagnetic heater to the heating of mold or do not heat;
The temperature-detecting device is electrically connected with control device, for detecting the temperature of mould inside;When temperature-detecting device is examined When measuring temperature in mold and reaching default maximum temperature threshold value, power supply unit and electromagnetic heater are powered off, and electromagnetic heater is to mould Tool does not heat;When temperature-detecting device detects that temperature reaches default minimum temperature threshold in mold, power supply unit and electromagnetism Heater is powered, and electromagnetic heater heats mold;
The muff package is partly wrapped on the outside of mold, for keeping the temperature to mold.
2. vacuum hotpressing stove temperature control system as described in claim 1, which is characterized in that the muff is by mullite fiber It is made;Its chemical constituent is the AL of 72%-75%2O3, 17%-20% SiO2, remaining group is divided into ZrO2And Fe2O3
3. a kind of vacuum hotpressing stove temperature control system, which is characterized in that the system comprises: power supply unit, control device, electromagnetism add Hot device, mold, temperature-detecting device;
The control device is arranged between the power supply unit and electromagnetic heater, and control device is described for Denso for controlling The size to electromagnetic heater output electric current is set, and then controls electromagnetic heater to the heating power of mold;
The temperature-detecting device is electrically connected with control device, for detecting the temperature of mould inside;When temperature-detecting device is examined When measuring temperature in mold and reaching default maximum temperature threshold value, power supply unit becomes smaller to the electric current that electromagnetic heater exports, and reduces Heating power of the electromagnetic heater to mold;When temperature-detecting device detects that temperature reaches default minimum temperature threshold in mold When, power supply unit becomes larger to the electric current that electromagnetic heater exports, and increases electromagnetic heater to the heating power of mold.
4. the vacuum hotpressing stove temperature control system as described in claims 1 to 3 is any, which is characterized in that the maximum temperature threshold The difference of value and minimum temperature threshold is not more than 20 DEG C.
5. vacuum hotpressing stove temperature control system as claimed in claim 4, which is characterized in that the maximum temperature threshold value with it is minimum The difference of temperature threshold is 5 DEG C.
CN201710693474.2A 2017-08-14 2017-08-14 A kind of vacuum hotpressing stove temperature control system Pending CN109387077A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710693474.2A CN109387077A (en) 2017-08-14 2017-08-14 A kind of vacuum hotpressing stove temperature control system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710693474.2A CN109387077A (en) 2017-08-14 2017-08-14 A kind of vacuum hotpressing stove temperature control system

Publications (1)

Publication Number Publication Date
CN109387077A true CN109387077A (en) 2019-02-26

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Country Status (1)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003017425A (en) * 2001-06-29 2003-01-17 Sony Corp Diffusion furnace type semiconductor manufacturing equipment
CN101462348A (en) * 2008-10-27 2009-06-24 黄旭峰 Electromagnetic heating system of injection mould machine
CN105783501A (en) * 2016-03-16 2016-07-20 中国科学院宁波材料技术与工程研究所 Vacuum hot-pressing sintering furnace
CN105964321A (en) * 2016-06-30 2016-09-28 长安大学 Device and method for heating asphalt in laboratory
CN106800419A (en) * 2017-01-18 2017-06-06 太原科技大学 A kind of preparation method of the enhanced Al-Mg-B ceramic material of SWCN

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003017425A (en) * 2001-06-29 2003-01-17 Sony Corp Diffusion furnace type semiconductor manufacturing equipment
CN101462348A (en) * 2008-10-27 2009-06-24 黄旭峰 Electromagnetic heating system of injection mould machine
CN105783501A (en) * 2016-03-16 2016-07-20 中国科学院宁波材料技术与工程研究所 Vacuum hot-pressing sintering furnace
CN105964321A (en) * 2016-06-30 2016-09-28 长安大学 Device and method for heating asphalt in laboratory
CN106800419A (en) * 2017-01-18 2017-06-06 太原科技大学 A kind of preparation method of the enhanced Al-Mg-B ceramic material of SWCN

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