CN109364781A - A kind of device and method preparing PETROLEUM PROCESSING catalyst - Google Patents
A kind of device and method preparing PETROLEUM PROCESSING catalyst Download PDFInfo
- Publication number
- CN109364781A CN109364781A CN201811430731.4A CN201811430731A CN109364781A CN 109364781 A CN109364781 A CN 109364781A CN 201811430731 A CN201811430731 A CN 201811430731A CN 109364781 A CN109364781 A CN 109364781A
- Authority
- CN
- China
- Prior art keywords
- shaft
- rotating shaft
- rotation
- gear
- mixing tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/21—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by their rotating shafts
- B01F27/2122—Hollow shafts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/808—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with stirrers driven from the bottom of the receptacle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/30—Driving arrangements; Transmissions; Couplings; Brakes
- B01F35/32—Driving arrangements
- B01F35/32005—Type of drive
- B01F35/3204—Motor driven, i.e. by means of an electric or IC motor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
Abstract
The invention discloses a kind of device and method for preparing PETROLEUM PROCESSING catalyst, including pedestal, the chassis interior is equipped with motor housing, motor is equipped with inside the motor housing, the base top is equipped with mixing tank, first rotating shaft is equipped with inside the mixing tank, the first rotating shaft surface is equipped with the second shaft, second shaft one end is flexibly connected with first rotating shaft, second shaft one end is equipped with connecting rod, and described connecting rod one end is equipped with gear, is equipped with cavity inside the mixing tank, the gear two sides are equipped with rack gear, and second shaft surface is equipped with stirring sheet.The present invention is by being equipped with first rotating shaft and the second shaft, be conducive to drive first rotating shaft rotation by motor, first rotating shaft drives the rotation of the second shaft, the gear of second shaft one end drives the second shaft rotation, salting liquid is passed through by infusion port, it rotates knob and adjusts hole size, integrally make dipping effect of the invention more preferable.
Description
Technical field
The present invention relates to the preparation fields of nonpetroleum processing catalyst, in particular to a kind of to prepare PETROLEUM PROCESSING catalyst
Device and method.
Background technique
Infusion process and purpose Catalyst is claimed to produce to impregnate the method for manufacturing catalyst for crucial and specific step
In a kind of widely applied method.Infusion process is impregnated on column porous carrier and is permeated in the form of salting liquid based on active component
Column inner surface, and form the principle of effective catalyst.Usually the liquid containing active material is gone to soak all kinds of carriers, when dipping is flat
After weighing apparatus, remove remaining liq, then carries out the post-processing of the processes such as drying identical with the precipitation method, roasting, activation.Through drying, by water
Divide evaporation evolution, the salt of active component can be made to be retained on the inner surface of carrier, the salt of these metals and metal oxide
It is evenly distributed in the pore of carrier, to get the carried catalyst of high degree of dispersion after heated decomposition and activation.And current market
The dipping effect of upper production PETROLEUM PROCESSING catalyst is less desirable.
Therefore, it is necessary to solve the above problems to invent a kind of equipment for preparing PETROLEUM PROCESSING catalyst.
Summary of the invention
The purpose of the present invention is to provide a kind of device and method for preparing PETROLEUM PROCESSING catalyst, by be equipped with motor,
First rotating shaft and the second shaft, are conducive in using the present invention, and carrier is put into mixing tank by feed inlet, open electricity
Machine, motor drive first rotating shaft rotation, and first rotating shaft drives the rotation of the second shaft, and the gear of second shaft one end drives second turn
Axis rotation is passed through salting liquid by infusion port, and rotation knob adjusts hole size, controls salting liquid rate, integrally make this hair
Bright dipping effect is more preferable, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme: a kind of equipment for preparing PETROLEUM PROCESSING catalyst, packet
Pedestal is included, the chassis interior is equipped with motor housing, motor is equipped with inside the motor housing, and the base top is equipped with mixing tank,
It is equipped with first rotating shaft inside the mixing tank, the first rotating shaft surface is equipped with the second shaft, second shaft one end and the
One shaft is flexibly connected, and second shaft one end is equipped with connecting rod, and described connecting rod one end is equipped with gear, sets inside the mixing tank
There is cavity, the gear two sides are equipped with rack gear, and second shaft surface is equipped with stirring sheet, is equipped with inside the first rotating shaft
Control shaft, the control shaft top are equipped with knob, and the top knob portion is equipped with infusion port, the first rotating shaft and control shaft surface
It is all provided with hole, the infusion port side is equipped with feed inlet, and described first rotating shaft one end is fixedly connected with motor output shaft, described
The first rotating shaft other end is flexibly connected with mixing tank.
Preferably, the mixing tank bottom is equipped with appendix, and the appendix cross sectional shape is set as waveform.
Preferably, the wheel and rack matches, and the quantity of the rack gear is two.
Preferably, the quantity of described hole is multiple, and described knob one end is fixedly connected with control shaft.
Preferably, the quantity of second shaft is two, and the quantity of the stirring sheet is eight.
A method of PETROLEUM PROCESSING catalyst being prepared, the equipment including the preparation PETROLEUM PROCESSING catalyst is also wrapped
Include following steps:
S1: carrier is put into mixing tank by feed inlet；
S2: open motor, motor output shaft rotation drive first rotating shaft rotation, first rotating shaft rotation drive the second shaft with
It is rotated centered on first rotating shaft, the second shaft rotation driven gear moves in cavity, simultaneously because the effect of rack gear, gear exist
It is rolled in cavity, spur roller gear drives the second shaft rotation, and the second shaft rotation drives stirring sheet rotation, so that second turn
Axis rotation while can rotation, raw material is sufficiently stirred；
S3: salting liquid is passed through by infusion port；
S4: turning knob, knob drive control shaft rotation, adjust the opposite of control shaft and first rotating shaft surface hole defect
Area controls the rate of salting liquid, salting liquid is enabled to be sufficiently submerged in carrier.
Technical effect and advantage of the invention:
1, by being equipped with motor, first rotating shaft and the second shaft, be conducive in using the present invention, to carry by feed inlet
Body is put into mixing tank, opens motor, and motor drives first rotating shaft rotation, and first rotating shaft drives the second shaft to rotate, and second turn
The gear of axis one end drives the second shaft rotation, is passed through salting liquid by infusion port, rotation knob adjusts hole size, controls salt
Solution speeds integrally make dipping effect of the invention more preferable；
2, wavy by being conducive to that in using the present invention, hot steam is passed through in appendix equipped with appendix
Appendix increases the contact area with mixing tank bottom, to enhance appendix to the heating effect of mixing tank, accelerates leaching
Stain speed.
Detailed description of the invention
Fig. 1 is overall structure diagram of the invention.
Fig. 2 is schematic enlarged-scale view at A in Fig. 1 of the invention.
Fig. 3 is first rotating shaft structure top view of the invention.
In figure: 1 pedestal, 2 motor housings, 3 motors, 4 mixing tanks, 5 first rotating shafts, 6 second shafts, 7 connecting rods, 8 gears, 9 skies
Chamber, 10 rack gears, 11 stirring sheets, 12 control shafts, 13 knobs, 14 infusion ports, 15 holes, 16 feed inlets, 17 appendixs.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
It is described the present invention provides a kind of equipment for preparing PETROLEUM PROCESSING catalyst as shown in Figs. 1-3, including pedestal 1
It is equipped with motor housing 2 inside pedestal 1, motor 3 is equipped with inside the motor housing 2, mixing tank 4 is equipped at the top of the pedestal 1, it is described mixed
First rotating shaft 5 is equipped with inside mould assembling 4,5 surface of first rotating shaft is equipped with the second shaft 6, described second shaft, 6 one end and first
Shaft 5 is flexibly connected, and described second shaft, 6 one end is equipped with connecting rod 7, and described 7 one end of connecting rod is equipped with gear 8, in the mixing tank 4
Portion is equipped with cavity 9, and 8 two sides of gear are equipped with rack gear 10, and 6 surface of the second shaft is equipped with stirring sheet 11, and described first
It is equipped with control shaft 12 inside shaft 5, knob 13 is equipped at the top of the control shaft 12, is equipped with infusion port 14 at the top of the knob 13,
The first rotating shaft 5 and 12 surface of control shaft are all provided with hole 15, and 14 side of infusion port is equipped with feed inlet 16.
Further, in the above-mentioned technical solutions, 4 bottom of mixing tank is equipped with appendix 17, and the appendix 17 is cut
Face is shaped to waveform, increases the contact area of appendix 7 and mixing tank 4, improves heating efficiency；
Further, in the above-mentioned technical solutions, the gear 8 matches with rack gear 10, and the quantity of the rack gear 10 is
Two, gear 8 is rolled in cavity 9, to drive 6 rotation of the second shaft；
Further, in the above-mentioned technical solutions, the quantity of described hole 15 is multiple, described 13 one end of knob and control
Axis 12 is fixedly connected, and makes it possible to control the opposite of 12 surface hole defect 15 of first rotating shaft 5 and control shaft by turning knob 13
Area；
Further, in the above-mentioned technical solutions, described 5 one end of first rotating shaft is fixedly connected with 3 output shaft of motor, described
5 other end of first rotating shaft is flexibly connected with mixing tank 4, and first rotating shaft 5 is rotated；
Further, in the above-mentioned technical solutions, the quantity of second shaft 6 is two, the number of the stirring sheet 11
Amount is eight, makes it possible to that carrier and salting liquid is sufficiently stirred, the active component in salting liquid is enabled to immerse load
In body.
Working method of the present invention:
Carrier is put into mixing tank 4 by feed inlet 16 in using the present invention referring to Figure of description 1-3, is opened
Motor 3, the rotation of 3 output shaft of motor drive first rotating shaft 5 to rotate, and the rotation of first rotating shaft 5 drives the second shaft 6 with first rotating shaft 5
Centered on rotate, 6 rotation driven gear 8 of the second shaft moves in cavity 9, simultaneously because the effect of rack gear 10, gear 8 is in sky
It being rolled in chamber 9, gear 8, which rolls, drives 6 rotation of the second shaft, and 6 rotation of the second shaft drives stirring sheet 11 to rotate, so that the
Two shafts 6 while rotation can rotation, raw material is sufficiently stirred, salting liquid is passed through by infusion port 14, rotation rotation
Button 13, the rotation of knob 13 drive control shaft 12 to rotate, adjust the relative area of control shaft 12 and 5 surface hole defect 15 of first rotating shaft,
The rate for controlling salting liquid enables salting liquid to be sufficiently submerged in carrier, whole more preferable using dipping effect of the invention；
Hot steam is passed through in appendix 17 in using the present invention referring to Figure of description 1, wavy gas transmission
Pipe 17 increases the contact area with 4 bottom of mixing tank, to enhance appendix 17 to the heating effect of mixing tank 4, accelerates
Impregnating speed.
Embodiment 2
A method of PETROLEUM PROCESSING catalyst being prepared, the equipment including the preparation PETROLEUM PROCESSING catalyst is also wrapped
Include following steps:
S1: carrier is put into mixing tank 4 by feed inlet 16；
S2: opening motor 3, and the rotation of 3 output shaft of motor drives first rotating shaft 5 to rotate, and the rotation of first rotating shaft 5 drives second turn
Axis 6 is rotated centered on first rotating shaft 5, and 6 rotation driven gear 8 of the second shaft moves in cavity 9, simultaneously because rack gear 10
Effect, gear 8 roll in cavity 9, and gear 8, which rolls, drives 6 rotation of the second shaft, and 6 rotation of the second shaft drives stirring sheet 11
Rotation so that the second shaft 6 rotation while can rotation, raw material is sufficiently stirred；
S3: salting liquid is passed through by infusion port 14；
S4: turning knob 13, the rotation of knob 13 drive control shaft 12 to rotate, adjust control shaft 12 and 5 surface of first rotating shaft
The relative area of hole 15 controls the rate of salting liquid, salting liquid is enabled to be sufficiently submerged in carrier.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (6)
1. a kind of equipment for preparing PETROLEUM PROCESSING catalyst, including pedestal (1), it is characterised in that: be equipped with inside the pedestal (1)
Motor housing (2), the motor housing (2) is internal to be equipped with motor (3), is equipped with mixing tank (4) at the top of the pedestal (1), the mixing
First rotating shaft (5) are equipped with inside case (4), first rotating shaft (5) surface is equipped with the second shaft (6), second shaft (6) one
End is flexibly connected with first rotating shaft (5), and described second shaft (6) one end is equipped with connecting rod (7), and described connecting rod (7) one end is equipped with tooth
It takes turns (8), is equipped with cavity (9) inside the mixing tank (4), gear (8) two sides are equipped with rack gear (10), second shaft
(6) surface is equipped with stirring sheet (11), is equipped with control shaft (12) inside the first rotating shaft (5), sets at the top of the control shaft (12)
Have knob (13), is equipped with infusion port (14) at the top of the knob (13), the first rotating shaft (5) and control shaft (12) surface are all provided with
Hole (15), infusion port (14) side are equipped with feed inlet (16), and described first rotating shaft (5) one end and motor (3) export
Axis is fixedly connected, and first rotating shaft (5) other end is flexibly connected with mixing tank (4).
2. a kind of equipment for preparing PETROLEUM PROCESSING catalyst according to claim 1, it is characterised in that: the mixing tank
(4) bottom is equipped with appendix (17), and appendix (17) cross sectional shape is set as waveform.
3. a kind of equipment for preparing PETROLEUM PROCESSING catalyst according to claim 1, it is characterised in that: the gear (8)
Match with rack gear (10), the quantity of the rack gear (10) is two.
4. a kind of equipment for preparing PETROLEUM PROCESSING catalyst according to claim 1, it is characterised in that: described hole (15)
Quantity be it is multiple, described knob (13) one end is fixedly connected with control shaft (12).
5. a kind of equipment for preparing PETROLEUM PROCESSING catalyst according to claim 1, it is characterised in that: second shaft
(6) quantity is two, and the quantity of the stirring sheet (11) is eight.
6. a kind of method for preparing PETROLEUM PROCESSING catalyst, it is characterised in that: add including preparing petroleum as described in claim 1
The equipment of work catalyst, further comprising the steps of:
S1: carrier is put into mixing tank (4) by feed inlet (16)；
S2: opening motor (3), and the rotation of motor (3) output shaft drives first rotating shaft (5) rotation, and first rotating shaft (5) rotation drives the
Two shafts (6) are rotated centered on first rotating shaft (5), and the second shaft (6) rotation driven gear (8) moves in cavity (9), together
When due to rack gear (10) effect, gear (8) rolls in the cavity (9), and gear (8), which rolls, drives the second shaft (6) rotation, the
(6) rotation of two shafts drive stirring sheet (11) rotation so that the second shaft (6) rotation while can rotation, to original
Material is sufficiently stirred；
S3: salting liquid is passed through by infusion port (14)；
S4: turning knob (13), knob (13) rotation drive control shaft (12) rotation, adjust control shaft (12) and first rotating shaft
(5) relative area of surface hole defect (15), controls the rate of salting liquid, salting liquid is enabled to be sufficiently submerged in carrier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811430731.4A CN109364781A (en) | 2018-11-28 | 2018-11-28 | A kind of device and method preparing PETROLEUM PROCESSING catalyst |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811430731.4A CN109364781A (en) | 2018-11-28 | 2018-11-28 | A kind of device and method preparing PETROLEUM PROCESSING catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109364781A true CN109364781A (en) | 2019-02-22 |
Family
ID=65377246
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811430731.4A Withdrawn CN109364781A (en) | 2018-11-28 | 2018-11-28 | A kind of device and method preparing PETROLEUM PROCESSING catalyst |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109364781A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114505078A (en) * | 2022-03-02 | 2022-05-17 | 马超 | Hydrodesulfurization catalyst and preparation method thereof |
-
2018
- 2018-11-28 CN CN201811430731.4A patent/CN109364781A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114505078A (en) * | 2022-03-02 | 2022-05-17 | 马超 | Hydrodesulfurization catalyst and preparation method thereof |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190222 |