CN109363020A - A kind of preparation method of orange beverage - Google Patents

A kind of preparation method of orange beverage Download PDF

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Publication number
CN109363020A
CN109363020A CN201811195138.6A CN201811195138A CN109363020A CN 109363020 A CN109363020 A CN 109363020A CN 201811195138 A CN201811195138 A CN 201811195138A CN 109363020 A CN109363020 A CN 109363020A
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CN
China
Prior art keywords
orange
preparation
juice
added
resin
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Pending
Application number
CN201811195138.6A
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Chinese (zh)
Inventor
林慧霞
肖玉娟
傅奇
郝春莉
陈琳珉
邓杭凤
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Xiamen Huaxia University
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Xiamen Huaxia University
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Application filed by Xiamen Huaxia University filed Critical Xiamen Huaxia University
Priority to CN201811195138.6A priority Critical patent/CN109363020A/en
Publication of CN109363020A publication Critical patent/CN109363020A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • A23L2/06Extraction of juices from citrus fruits
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/72Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/80Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/84Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Zoology (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The present invention discloses a kind of preparation method of orange beverage, belong to field of beverage, it include pretreatment, pericarp processing, mixing, sterilization and etc., and absorption bitter taste, the adsorbent resin preparation method thereof are carried out using absorption resin are as follows: use the calcium chloride solution that mass fraction is 5-10% as water phase, and the oily phase of water phase quality 30-50% is added, stirring is warming up to 80 DEG C or more and keeps the temperature 2 hours, continue to be warming up to 90 DEG C of heat preservations 10 hours, then filtration washing, preparation absorption resin.

Description

A kind of preparation method of orange beverage
Technical field
The present invention relates to a kind of preparation methods of orange beverage, belong to technical field of food beverage.
Background technique
With the raising of industrial automation level and the raising of quality of life, people can enjoy various more and more Beverage is for quenching one's thirst.The beverage sold currently on the market is multifarious, many kinds of, such as soda, fruit drink, cream drink Material, tea beverage etc..Wherein fruit drink is made of the juicing of various fruit, and nutrition is relatively abundanter, contains multivitamin, You Yiwei Raw element C is most, and the minerals such as calcic, phosphorus (inorganic salts).And orange beverage can also be mended other than can be with replenishing vitamins C Potassium, riboflavin increase the content of high-quality cholesterol in vivo, prevent heart disease and headstroke.
Currently on the market usually production orange beverage, be squeeze the juice after removing the peel orange or belt leather squeeze the juice, pulp It separately squeezes the juice with pericarp, then removes pericarp bitter taste, remix the few of production orange juice, be primarily due in orange peel containing more Bitter principle, in the process of production and processing, phenomena such as being easy to produce precipitating and bitter taste, seriously affects the further hair of orange juice processing Exhibition.
In some cases, it is adsorbed using absorption resin, but existing absorption resin adsorption time is long, water absorption rate It is low, at high cost, and existing absorption resin is mostly to mix pericarp and pulp to adsorb together, is caused in absorption bitter taste Meanwhile a part itself for also having adsorbed fruit juice is fragrant and sweet, affects the mouthfeel of beverage.
Summary of the invention
It is an object of the invention to: in view of the above problems, provide it is a kind of it is in good taste, additive is few, utmostly Retain the preparation method of the orange beverage of orange nutrition.
The present invention is achieved through the following technical solutions:
A kind of preparation method of orange beverage, including the following steps:
(1) it pre-processes: after the peeling of fresh orange, obtaining pulp and pericarp, by pulp crushing, juicing obtains new orange Juice, crosses homogenizer under normal temperature conditions, and homogenization pressure 5-8MP obtains homogeneous orange juice;
(2) pericarp is handled: will obtain pericarp slurry after peel crushing, the water that pericarp starches 2-3 times of weight is added, then adds Pectase and cellulase digest 60-80min under the conditions of 40 DEG C, and under the conditions of 80 DEG C after enzyme deactivation, filtering obtains clear liquid, will Clear liquid obtains peel juice by absorption resin;Wherein, the amount for adsorbing resin is 4-5 times of clear liquid weight, adsorption time 10- 20 minutes, adsorption temp was 12 DEG C -15 DEG C, and absorption pH value is 7.5, and above-mentioned adsorption temp and time and pH value can make Absorption resin can effectively absorb the bitter taste in pericarp.
(3) it mixes: peel juice obtained in homogeneous orange juice obtained in step (1) and step (2) is mixed to get mixing Xanthan gum, citric acid, xylitol and stevioside glycosides are added in juice, and after being sufficiently mixed uniformly, homogenizer is crossed under the conditions of 40-45 DEG C, Homogenization pressure is 7-10MP, obtains orange juice;
(4) sterilize: orange juice obtained in step (3) sterilizes 15-20min under the conditions of 80-85 DEG C;Packaging is completed in sterilization After orange beverage can be obtained.
Wherein, the total amount of the pectase and cellulase of addition is the 1-3% that pericarp starches weight;Xanthan gum, lemon is added Acid, xylitol and stevioside glycosides are 1-2%, 0.02-0.04%, 0.03-0.05% and 0.01-0.02% of mixed juice weight.
As an improvement, the invention discloses a kind of preparation method of orange beverage, the weight ratio of pectase and cellulase For 1:1.
As an improvement, the invention discloses a kind of preparation method of orange beverage, the citric acid and sweet tea that are added in step (3) The weight ratio of leaf chrysanthemum glycosides is 2:1.
As an improvement, it is respectively mixed juice weight that xanthan gum, citric acid, xylitol and stevioside glycosides are added in step (3) 2%, 0.02%, 0.05% and 0.01%.
According to the orange beverage that the preparation method is prepared, in good taste, additive is few, utmostly retains The advantages that orange nutrition.
In order to mention the adsorption efficiency of high water-absorbing resin, the present invention uses a kind of homemade absorption resin, the absorption resin For macroporous absorbent resin, the adsorbent resin preparation method thereof are as follows: use calcium chloride solution that mass fraction is 5-10% as water Phase, and the oily phase of water phase quality 30-50% is added, stirring is warming up to 80 DEG C or more and keeps the temperature 2 hours, continues to be warming up to 90 DEG C of heat preservations 10 hours, then resin was adsorbed in filtration washing, preparation;
The oil mutually includes 100 parts of butyl acetates, 10-20 parts of N, N '-methylene-bisacrylamide, 5-10 parts of benzene second Simultaneously pore-foaming agent and di-t-butyl peroxide is added in alkene, 5-10 part terephthalic acid (TPA).
Above-mentioned special absorption resin can satisfy in the case where not influencing beverage mouthfeel, only adsorbs its bitter taste, does not produce Raw side effect, adsorption effect are good.
The invention also discloses the adsorbent equipment of a kind of pair of clear liquid processing, absorption resin is equipped with inside the adsorbent equipment.It should Adsorbent equipment includes cylinder and the filter core positioned at inner barrel, and the cylinder is cylinder, and filter core is close to cylinder inboard wall, filter In-core is fixed with absorption resin, and filter core and cylinder are coaxial, and filter core can be rotated around the axial direction of cylinder, the top of the cylinder Equipped with an entrance, clear liquid enters cylinder out of entrance, goes out after being adsorbed with water-absorbing resin from the side for being located at cylinder body bottom Mouth discharge.The filter core from bottom, the filter core is interior to be equipped with the filter full of filter core, and filter is equipped with frame, and frame is equipped with admittedly Surely the net of resin is adsorbed, and clear liquid is enabled to pass through filter, is a shell around filter, filter and shell are fixed, filter Central part is a newel, and newel drives filter and housing into rotation, between shell and cylinder by the connection such as bearing so that It is relatively rotatable to each other between shell and cylinder, newel and driving device connection, in a preferred approach, driving device can be Gear.
After being adsorbed with the adsorbent equipment to clear liquid, the static defect of traditional adsorbent equipment, static suction are overcome On the one hand adsorption device is easy so that being plugged, on the one hand the contact of absorption resin and clear liquid is bad, and adsorption effect is poor.This hair Bright adsorbent equipment is fixed by filter by resin dispersion is adsorbed, and the space that absorption resin accounts for is big, but adsorbs resin distribution Compare scattered, clear liquid will not be blocked, absorption property is good.
The beneficial effects of the present invention are:
Preparation method of the present invention is simple, by filtering the bitter taste with Adsorption orange peel, improves the value of orange peel, passes through Twice homogenization, so that orange juice is more stable, the orange beverage prepared has the original flavor of orange, good mouthfeel and stability It is good.
Adsorption effect of the invention is high simultaneously, soak time is short, fruit juice and will not influence substantially without bitter taste after absorption Other effective components.
Detailed description of the invention
Fig. 1 is structural schematic diagram of the invention;
Fig. 2 is the schematic diagram of other side observation;
Fig. 3 is the schematic diagram of filter core
Marked in the figure: 1- cylinder, 101- entrance, the outlet 102-, 2- filter core, 201- filter, 202- newel, 203- tooth Wheel.
Specific embodiment
Embodiment 1
A kind of preparation method of orange beverage, including the following steps:
(1) it pre-processes: after the peeling of fresh orange, obtaining pulp and pericarp, by pulp crushing, juicing obtains new orange Juice, crosses homogenizer under normal temperature conditions, and homogenization pressure 8MP obtains homogeneous orange juice;
(2) pericarp is handled: will obtain pericarp slurry after peel crushing, the water that pericarp starches 3 times of weight is added, then adds fruit Glue enzyme and cellulase digest 80min under the conditions of 40 DEG C, and under the conditions of 80 DEG C after enzyme deactivation, filtering obtains clear liquid, by clear liquid By adsorbing resin, peel juice is obtained;Wherein, the amount for adsorbing resin is 4 times of clear liquid weight, clear liquid by absorption resin when Between be 10min;
(3) it mixes: peel juice obtained in homogeneous orange juice obtained in step (1) and step (2) is mixed to get mixing Xanthan gum, citric acid, xylitol and stevioside glycosides are added in juice, after being sufficiently mixed uniformly, homogenizer are crossed under the conditions of 40 DEG C, Matter pressure is 10MP, obtains orange juice;
(4) sterilize: orange juice obtained in step (3) sterilizes 20min under the conditions of 80 DEG C;After packaging is completed in sterilization Obtain orange beverage.
Wherein, the total amount of the pectase and cellulase of addition is that pericarp starches the 3% of weight;Be added xanthan gum, citric acid, Xylitol and stevioside glycosides are 2%, 0.02%, 0.05% and the 0.01% of mixed juice weight.
The weight ratio of a kind of preparation method of orange beverage, pectase and cellulase is 1:1.
Embodiment 2
A kind of preparation method of orange beverage, including the following steps:
(1) it pre-processes: after the peeling of fresh orange, obtaining pulp and pericarp, by pulp crushing, juicing obtains new orange Juice, crosses homogenizer under normal temperature conditions, and homogenization pressure 5MP obtains homogeneous orange juice;
(2) pericarp is handled: will obtain pericarp slurry after peel crushing, the water that pericarp starches 2 times of weight is added, then adds fruit Glue enzyme and cellulase digest 60min under the conditions of 40 DEG C, and under the conditions of 80 DEG C after enzyme deactivation, filtering obtains clear liquid, by clear liquid By adsorbing resin, peel juice is obtained;Wherein, the amount for adsorbing resin is 5 times of clear liquid weight, clear liquid by absorption resin when Between be 12min;
(3) it mixes: peel juice obtained in homogeneous orange juice obtained in step (1) and step (2) is mixed to get mixing Xanthan gum, citric acid, xylitol and stevioside glycosides are added in juice, after being sufficiently mixed uniformly, homogenizer are crossed under the conditions of 45 DEG C, Matter pressure is 7MP, obtains orange juice;
(4) sterilize: orange juice obtained in step (3) sterilizes 15min under the conditions of 85 DEG C;After packaging is completed in sterilization Obtain orange beverage.
Wherein, the total amount of the pectase and cellulase of addition is that pericarp starches the 1% of weight;Be added xanthan gum, citric acid, Xylitol and stevioside glycosides are 1%, 0.04%, 0.03% and the 0.02% of mixed juice weight.
The weight ratio of a kind of preparation method of orange beverage, pectase and cellulase is 1:1.
A kind of to remove bitter absorption resin for orange beverage, resin is that the present invention uses a kind of homemade absorption resin, institute The absorption resin stated is macroporous absorbent resin, the adsorbent resin preparation method thereof are as follows: the chlorination for being 5-10% with mass fraction The oily phase of water phase quality 30-50% is added as water phase in calcium solution, and stirring is warming up to 80 DEG C or more and keeps the temperature 2 hours, after of continuing rising Temperature keeps the temperature 10 hours to 90 DEG C, then filtration washing, and the post-processing step of preparation absorption this preparation method of resin absorption resin can Referenced patent application CN201710411666.X or other prepare the prior art of macroreticular resin.
The oil mutually includes 100 parts of butyl acetates, 10-20 parts of N, N '-methylene-bisacrylamide, 5-10 parts of benzene second Simultaneously pore-foaming agent and di-t-butyl peroxide is added in alkene, 5-10 part terephthalic acid (TPA).
The absorption resin property index being prepared is as follows:
Wherein in a preferred embodiment, the present invention discloses the adsorbent equipment to clear liquid processing, as shown in Figure 1, should Absorption resin is equipped with inside adsorbent equipment.The adsorbent equipment includes cylinder 1 and the filter core 2 inside cylinder 1, the cylinder Body is cylinder, and filter core is close to 1 inner wall of cylinder, and absorption resin is fixed in filter core, and filter core and cylinder 1 are coaxial, and filter core 2 can be around The axial rotation of cylinder, the top of the cylinder be equipped with an entrance 101, clear liquid enters cylinder out of entrance, with water suction Resin is discharged after being adsorbed from the side exit 102 for being located at cylinder body bottom.As shown in Fig. 2, the filter core from bottom, the filter core Interior to be equipped with the filter full of filter core, filter is equipped with frame, and frame is equipped with the net of fixed absorption resin, and enables to clear Liquid passes through filter, is a shell around filter, and filter and shell are fixed, and filter central part is a newel 202, and newel drives Filter and housing into rotation, by the connections such as bearing so that be relatively rotatable to each other between shell and cylinder between shell and cylinder, Newel and driving device connection.
After being adsorbed with the adsorbent equipment to clear liquid, the static defect of traditional adsorbent equipment, static suction are overcome On the one hand adsorption device is easy to be plugged, on the one hand adsorb resin and the contact of clear liquid is bad, adsorption effect is poor.Of the invention Adsorbent equipment is fixed by filter by resin dispersion is adsorbed, and the space that absorption resin accounts for is big, but adsorbs the comparison of resin distribution It dissipates, clear liquid will not be blocked, absorption property is good.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (6)

1. a kind of preparation method of orange beverage, which is characterized in that including the following steps:
(1) it pre-processes: after the peeling of fresh orange, obtaining pulp and pericarp, by pulp crushing, juicing obtains new fresh orange-juice, mistake Homogenizer obtains homogeneous orange juice;
(2) pericarp is handled: will obtain pericarp slurry after peel crushing, the water that pericarp starches 2-3 times of weight is added, then adds pectin Enzyme and cellulase digest 60-80min under the conditions of 40 DEG C, enzyme deactivation under the conditions of 80 DEG C, and filtering obtains clear liquid, adjust clear liquid PH value obtains peel juice by clear liquid by absorption resin;Wherein, the amount for adsorbing resin is 4-5 times of clear liquid weight, absorption temperature Degree is 12 DEG C -15 DEG C, pH value 7.5, and clear liquid is 10-20min by the time of absorption resin;
(3) it mixes: peel juice obtained in homogeneous orange juice obtained in step (1) and step (2) being mixed to get mixed juice, is added Enter xanthan gum, citric acid, xylitol and stevioside glycosides, after being sufficiently mixed uniformly, crosses homogenizer, obtain orange juice;
(4) sterilize: orange beverage can be obtained in packaging after the sterilization of orange juice obtained in step (3);
Wherein, the total amount of the pectase and cellulase of addition is the 1-3% that pericarp starches weight;Xanthan gum, citric acid, wood is added Sugar alcohol and stevioside glycosides respectively are 1-2%, 0.02-0.04%, 0.03-0.05% and 0.01- of mixed juice weight 0.02%.
2. the preparation method of orange beverage according to claim 1, the adsorbent resin preparation method thereof are as follows: with mass fraction be 5- The oily phase of water phase quality 30-50% is added as water phase in 10% calcium chloride solution, and stirring is warming up to 80 DEG C or more and keeps the temperature 2 Hour, continue to be warming up to 90 DEG C of heat preservations 10 hours, then filtration washing, obtains absorption resin;
The oil mutually includes 100 parts of butyl acetates, 10-20 parts of N, N '-methylene-bisacrylamide, 5-10 part styrene, 5-10 Simultaneously pore-foaming agent and di-t-butyl peroxide is added in part terephthalic acid (TPA).
3. the preparation method of orange beverage according to claim 1, step (1) homogeneous is progress, homogenization pressure at normal temperature For 5-8MP;Step (2) homogeneous carries out under the conditions of 40-45 DEG C, homogenization pressure 7-10MP.
4. the preparation method of orange beverage according to claim 1, which is characterized in that the weight ratio of pectase and cellulase For 1:1.
5. the preparation method of orange beverage according to claim 1, which is characterized in that the citric acid being added in step (3) Weight ratio with stevioside glycosides is 2:1.
6. a kind of preparation method of orange beverage according to claim 1 or 3, which is characterized in that be added in step (3) yellow Virgin rubber, citric acid, xylitol and stevioside glycosides are respectively 2%, 0.02%, 0.05% and the 0.01% of mixed juice weight.
CN201811195138.6A 2018-10-15 2018-10-15 A kind of preparation method of orange beverage Pending CN109363020A (en)

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Application Number Priority Date Filing Date Title
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030064144A1 (en) * 1998-12-10 2003-04-03 Chu Osvaldo A. Juice processing incorporating resin treatment
CN1915113A (en) * 2005-06-29 2007-02-21 热带产品公司 Citrus peel juice
CN102164511A (en) * 2008-08-29 2011-08-24 热带产品公司 Naturally sweetened juice beverage products
CN102190753A (en) * 2010-03-19 2011-09-21 周家付 Preparation method for macroporous weak-acidic cation exchange resin

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030064144A1 (en) * 1998-12-10 2003-04-03 Chu Osvaldo A. Juice processing incorporating resin treatment
CN1915113A (en) * 2005-06-29 2007-02-21 热带产品公司 Citrus peel juice
CN102164511A (en) * 2008-08-29 2011-08-24 热带产品公司 Naturally sweetened juice beverage products
CN102190753A (en) * 2010-03-19 2011-09-21 周家付 Preparation method for macroporous weak-acidic cation exchange resin

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
[英]G.G.伯奇等主编: "《酶与食品加工》", 31 March 1991, 轻工业出版社 *
何天白等: "《功能高分子与新技术》", 31 January 2001, 化学工业出版社材料科学与工程出版中心 *
周皓等: ""PET瓶装橙汁饮料沉淀机理与预防"", 《PET瓶装橙汁饮料沉淀机理与预防》 *
张光华编: "《水处理化学品制备与应用指南》", 30 October 2003, 中国石化出版社出版发行 *

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Application publication date: 20190222