CN109333768A - A kind of manufacturing method of abnormity mica part - Google Patents
A kind of manufacturing method of abnormity mica part Download PDFInfo
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- CN109333768A CN109333768A CN201811215807.1A CN201811215807A CN109333768A CN 109333768 A CN109333768 A CN 109333768A CN 201811215807 A CN201811215807 A CN 201811215807A CN 109333768 A CN109333768 A CN 109333768A
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- mica
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- pin
- mica part
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B3/00—Producing shaped articles from the material by using presses; Presses specially adapted therefor
- B28B3/02—Producing shaped articles from the material by using presses; Presses specially adapted therefor wherein a ram exerts pressure on the material in a moulding space; Ram heads of special form
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- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Mechanical Engineering (AREA)
- Casting Or Compression Moulding Of Plastics Or The Like (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses a kind of manufacturing methods of mica special-shaped part, the natural dolomite powder of different fineness or artificial mica synthesis powder and short glass fiber are sufficiently mixed, obtain ingredient, inorganic binder is dissolved in stir in pure water of the temperature greater than 50 DEG C, inorganic binder aqueous solution is made, ingredient and aqueous solution are sufficiently mixed, obtain mixture, quality needed for mixture Evian mother's part is weighed, it is then fitted into assembled mold, mold is packed into press machine, start press machine and applies pressure to mold, the gradually pressure that repeatedly pressed repeatedly reaches technique required pressure and is kept for certain time, press pressure relief is taken out into mold, remove external mold, it will be in internal model, lower locking, internal model is put into tunnel type baking oven and is dried by different warm areas, heating, solidification, it anneals disposable stream treatment, folding will except internal model clamping screw The mica part of own solidified forming is put into 45~55c0Baking oven in, carried out when reaching batch eliminate internal stress processing after carry out damp-proof treatment again.
Description
Technical field
The present invention relates to a kind of manufacturing methods of special-shaped mica part, in particular to it is Celsius that a kind of operating temperature reaches 500
The manufacturing method of degree and 1000 degrees Celsius of special-shaped mica part.
Background technique
Using mica as abnormity mica part made of substrate, due to good resistance to compression, anti-folding, anti-corrosion, shock resistance and
Thunder-lightning, arc protection, height insulation, low temperature resistant (- 60 DEG C) are hereinafter, 250 DEG C of high temperature resistant equal excellent performances, are widely used in navigating
It, aviation, military project, nuclear power, radar electrical power trans mission/distribution system, lightning protection electrical engineering and submarine, automobile, shipbuilding, super-pressure transmission net etc.
High-tech applications.With the fast development of new and high technology, application field can more extensively.
This special-shaped mica part of prior art manufacture is molten through dry exclusion with individual mica paper dipping organic siliconresin
It is overlapped one by one after agent by thickness requirement (usually hundreds of Zhang Naizhi numbers thousand are opened), is sent into hot press the compacting passed through about 24 hours
Process is made the plate for manufacturing special-shaped mica part, then plate is cut into polygon block by outer dimension, is then added by machine
Work center carries out multiple programs and fabricates, and there are many deficiencies for this manufacturing method, mainly:
1, process is complicated and period length, waste of raw materials are big, and manufacturing cost is high;
2, plate is to open single layer mica paper by hundreds of Zhang Naizhi numbers thousand to suppress, and is easily layered in processing, any one adds
Work process all can make part rejection to preceding cutting most abandoning due to layering;
3, binder is organic siliconresin, and long-term operating temperature is of limited application less than 250 DEG C.
It is especially different to high temperature resistant in order to adapt to demand of the modern science and technology to high-temperature insulation material of high speed development
The demand of shape mica part, the manufacturing method for providing a kind of special-shaped mica part are particularly important.
Summary of the invention
The object of the present invention is to provide a kind of manufacturing method of special-shaped mica part, processing week simple with manufacturing process
Phase is short, will not be layered, be broken in process, high yield rate, the advantages that loss is few.The present invention is opposite due to forming solidification temperature
It is low, not only save the excellent performance of conventional machining process product obtained, and long-term operating temperature can be improved to 500~
1000 DEG C or more.
The invention discloses a kind of manufacturing methods of special-shaped mica part, are at normal temperature pressed and molded blank, wherein adopt
With water-soluble binder, curing process is completed by tunnel type baking oven, solidification temperature is less than 250 DEG C, curing process of the invention
Disposably to be completed by time, temperature in tunnel type baking oven by intelligent control, can continuity continuous productive process, since solidification temperature is small
In 250 DEG C, the crystal and physicochemical property of natural mica are remained intact, heat resistance superelevation, the present invention specifically includes the following steps:
S1: ingredient: by weight, 85-95 parts of mica powder for selecting different meshes take length to be less than the short glass fibre of 10mm
10 parts, mica powder and short glass fibre are mixed evenly;Glass using length less than 10mm is tieed up, with mica powder hybrid shaping
Afterwards, impact resistance and mechanical strength are all significantly increased;
S2: water-soluble binder preparation: by mass, by mass, 5-15 parts of phosphoric acid dihydro amine, tetraboric acid amine 4- are taken
14 parts, water temperature at 76-86 parts of pure water of 50 DEG C or more, stir evenly abundant dissolution;Select pure water that can overcome because of water quality
Difference is on influence caused by product electric property;
S3: manufacture mold: being made internal model by raw material of polyflon, which presses mica part to be manufactured
Shape and size injection moulding cavity plate and punch-pin;External mold is made with carbon steel, the inner cavity of the external mold and internal model outer dimension at
Dynamic cooperation, is made compacting punch-pin with carbon steel, it is smaller than the Male Die Size of internal model that this is pressed into Male Die Size;Mold is with poly- four
Fluorine ethylene injection molding, duplication are easy, week conversion suitable for mass production, and are met mica part simultaneously and wanted to solidification temperature
It asks, external mold is made of common carbon steel, is reduced costs, and is played a protective role to internal model, and the tensile strength of internal model is improved;
S4: it molding: by weight, takes ingredient and water-soluble binder to be stirred, obtains mixture, external mold is fixed on
On press bench, the cavity plate of internal model is placed in external mold cavity, compacting is placed in the cavity plate of internal model with punch-pin, closure
Press machine, by the punch-pin of internal model be fixed on press machine it is horizontal on, open press, mixture is poured into the cavity plate core cavity of internal model,
Cracking pressure machine, presses repeatedly, then starts anti-liftout attachment, takes out internal model;Molding compacting is to carry out at normal temperature, and compacting is set
Standby is four column press for selecting general generation to have anti-liftout attachment;
S5: curing process: closing up locking for the punch-pin of the internal model of taking-up and internal model, put it into tunnel drier into
Row is dry, heating, solidification and annealing operation, then takes out mica part and is put into baking oven, and oven temperature is maintained at 50-60 DEG C, and
After carry out eliminate internal stress processing;The temperature for the tunnel type baking oven that the present invention uses, time are by intelligent control technology come real
It is existing, can continuity continuous productive process, heat-insulated asbestos cloth is housed between different warm areas in baking oven, hot-air channelling can be prevented;Through
After crossing the processing of elimination internal stress, mica part will not deform in storage, transport, use process;
S6: damp-proof treatment: by mass, taking 10-20 parts of 80-90 parts of marketable gasolines and 255 polymethylphenyl siloxane fluid to be mixed,
It will be impregnated through S5 treated mica part wherein, after removing filter dry, after spontaneously drying at normal temperature, in 60-80 DEG C of baking oven
Final mica part is obtained after middle baking.After damp-proof treatment, mica part is in storage, transportational process, in relative humidity
When greater than 90%, product itself performance is not affected.
Further, the mica powder particle size range that ingredient of the invention uses takes three kinds or more for -20 mesh~-120 mesh
The mica powder of different meshes is mixed, and granularity is preferably taken are as follows: 30 parts of -20 20 parts of mesh, 40 parts of -80 mesh and -120 mesh, it is above
By mass, varigrained mica powder has been sufficient filling with mutual gap, it is close to increase mica part in bonding
Degree.
Further, when the operating temperature of mica part to be manufactured is 500 DEG C, using natural muscovite powder, when wait make
The operating temperature for the mica part made is 1000 DEG C, using artificial mica synthesis powder.
Further, in the S3 to be pressed into Male Die Size 0.1mm smaller than the Male Die Size of internal model, and this be pressed into it is convex
Mould surface chromium plating.
Further, for the internal model by being made with polyflon of raw material, the external mold and compacting punch-pin are equal
By being made of carbon steel.
Further, several gas vents are uniformly provided on the contact surface of the punch-pin of the internal model and mica part to be manufactured.
Detailed description of the invention
Fig. 1 is flow diagram of the invention;
Fig. 2 is the cavity plate and punch-pin schematic diagram of internal model of the invention;
Fig. 3 is external mold schematic diagram of the invention;
Fig. 4 is curing process heating curve figure of the present invention;
Fig. 5 is that the present invention eliminates internal stress processing heating curve figure;
Fig. 6 is damp-proof treatment technique heating curve figure of the present invention.
Specific embodiment
The present invention is further explained with reference to the accompanying drawings and examples.
The present invention selects varigrained natural mica powder or artificial mica synthesis powder to mix with short glass fibre, using nothing
Blank, is pressed and molded by the bonding of machine water-soluble binder at normal temperature, completes curing process by intelligent tunnel formula dryer.Tool
Have that solidification temperature is low, manufacturing process is simple, at low cost, free of contamination feature.
Embodiment
As shown in Figure 1, the present embodiment is completed by following technology path:
S1: ingredient: selection granularity is 20 parts of -20 mesh mica powder, 40 parts of -8 mesh mica powder and -120 mesh micas by weight
It 30 parts of powder, takes length less than 10 parts of short glass fibre of 10mm, all ingredients is stirred evenly;Existed using varigrained mica powder
When bonding, it has been sufficient filling with mutual gap, has increased mica parts density, mica powder and short glass fibre are sufficiently mixed institute
The mechanical strength of mica part include that toughness, bending resistance, impact resistance are all significantly increased.When the work of mica part
When temperature is less than 500 DEG C, using natural mica powder, when the operating temperature of mica part is 500~1000 DEG C, using artificial
Compound mica.
S2: water-soluble binder preparation: taking 10 parts of phosphoric acid dihydro amine, and 9 parts of tetraboric acid amine, water temperature is pure at 50 DEG C or more
81 parts of water, stir evenly abundant dissolution;Inorganic binder used is pure aqueous solution, when volatilization will not as toluene, dimethylbenzene,
The organic solvents such as formaldehyde generate pernicious gas like that, and damage operator's health pollutes environment, will not be because of water quality differentia influence
Product itself performance;
S3: mold manufacture: as shown in Figures 2 and 3, internal model is made by raw material of polytetrafluoroethylene resin, internal model core cavity is pressed
The geometry and size injection moulding cavity plate 1 and punch-pin 2 of mica part 3, die cavity surrounding should shape back there are 50cm frame
Frame quadrangle is drilled with the through-hole that diameter is 13mm, and punch-pin 2 and product contact surface should be evenly distributed with the gas vent that several diameters are 1mm;With general
External mold, lower through-hole on external mold is made in logical carbon steel, and the outer mold cavity and internal model outer dimension are made at dynamic cooperation of ordinary carbon steel
With the compacting punch-pin of the small 0.1mm of 2 size of punch-pin of internal model, chrome-faced 0.1mm;Internal model is molded using polyflon
Molding, duplication are easy, use suitable for mass production, and meet requirement of the mica part to solidification temperature simultaneously, and external mold is with common
Structural carbon steel is made, and mould structure is simple, reduces costs, and in pressing process, plays a protective role, improves to internal model
The tensile strength of internal model;
S4: it forming: completes at normal temperature, unit area pressure will reach 200kg/cm2More than;
S4-1,85 parts of the ingredient stirred evenly and 15 parts of water soluble adhesive mixings are taken, obtains mixture;
S4-2, by above-mentioned mixture, weigh by the quality of mica part to be manufactured, when weighing should add 12% moisture content
With 1% loss;The specific gravity of the mica part of the present embodiment is 2.38~2.4g/cm3;
S4-3, the external mold made of ordinary carbon steel is fixed on press bench, and internal model cavity plate is placed on outside
In mould cavity, by compacting with punch-pin be placed in cavity plate in, clossing pressure machine, by compacting with punch-pin be fixed on press machine it is horizontal on, open
Open press;The press machine is 500 ton of four column universal press;
S4-4, the mixture after weighing is poured into the cavity plate core cavity using polyflon as internal model made of raw material
In;
S4-5, starting press machine, press 4~5 times repeatedly, are separated by 1 minute every time, pressure 200kg/cm2, kept for 10 points
Cracking pressure machine after clock starts anti-liftout attachment, takes out the cavity plate of internal model;
S5: curing process:
The cavity plate of internal model and the punch-pin of internal model that S5-1, S4-5 take out close up, and quadrangle is locked with 12mm bolt;
S5-2, the mica part that will be locked in internal model, are put into tunnel type dryer and are dried, heat, solidifying, moving back
Fiery continuous productive process, the time of drying, temperature should strictly be operated by the regulation of figure four;The tunnel drier of the curing process when
Between, temperature disposably completed by intelligent control, can continuity continuous productive process;Heat-insulated stone is housed between different warm areas in dryer
Cotton can prevent hot-air channelling.Less than 250 DEG C, the crystal and physicochemical property of natural mica remain intact solidification temperature, bonding
Agent is inorganic binder, and long-term operating temperature can achieve 500 DEG C and 1000 DEG C.
S6: internal stress processing is eliminated:
S6-1: it takes out the mica part that oneself is fully cured and is put into baking oven, oven temperature is maintained at 50~60 DEG C;
S6-2: it after reaching certain batch, carries out eliminating internal stress processing by the requirement of figure five;Through eliminating internal stress processing
Mica part is in storage, transportational process, and when environment temperature is greater than -600C or is greater than 800C, mica part will not be deformed.
S7: damp-proof treatment:
S7-1: using 80-90 parts of 95# gasoline, and 255 10-20 parts of polymethylphenyl siloxane fluids are mixed into solution, will eliminate by internal stress
The mica part of processing impregnates 10 minutes;
S7-2: the mica part after immersion is removed filter dry, and is spontaneously dried 12-24 hours at normal temperature;
S7-3: being put into baking oven, when volume reaches baking oven volume 2/3rds, is handled according to the requirement of Fig. 6.Through
The mica part of damp-proof treatment is in storage, transport, use process, when ambient humidity is greater than 95%, mica part itself
Various performances will not reduce.
The elimination internal stress processing of the present embodiment and the baking oven of damp-proof treatment are a conventional ovens for exhaust apparatus.
By the mica part of embodiment of the present invention manufacture and the mica part of prior art manufacture, through at 500 degrees Celsius
Under conditions of roast 2 hours after, main performance comparison be shown in Table 1;
Table 1: the measured value after 500 DEG C roast 2 hours
It can be seen that under conditions of 500 degrees Celsius from 1 column data of table, only by 2 hours short, by the prior art
The mica part of manufacture main application performance the sixth of the twelve Earthly Branches completely loses, and still maintains excellent insulating properties by mica part of the invention
It can be with good mechanical strength.
Claims (7)
1. a kind of manufacturing method of special-shaped mica part according to claim 1, it is characterised in that: the following steps are included:
S1: ingredient: by weight, 85-95 parts of mica powder for selecting different meshes take length to be less than the short glass fibre 10 of 10mm
Part, mica powder and short glass fibre are mixed evenly;
S2: water-soluble binder preparation: by mass, take 5-15 parts of phosphoric acid dihydro amine, 4-14 parts of tetraboric acid amine, water temperature at 50 DEG C
76-86 parts of above pure water, stirs evenly abundant dissolution;
S3: it manufacture mold: is manufactured including internal model manufacture, external mold manufacture and compacting with punch-pin, the core cavity of the internal model is by be manufactured
Mica part shape and size injection moulding cavity plate and punch-pin, which is equipped with the inner cavity for placing internal model cavity plate and should
At dynamic cooperation, the size of the compacting punch-pin is less than the Male Die Size of internal model for the inner cavity of external mold and internal model outer dimension;
S4: it molding: by weight, takes ingredient and water-soluble binder to be stirred, obtains mixture, external mold is fixed on pressure
On machine worktable, the cavity plate of internal model is placed in outer mold cavity, compacting is placed in the cavity plate of internal model with punch-pin, clossing pressure
Machine, by compacting with punch-pin be fixed on press machine it is horizontal on, open press, mixture is poured into the cavity plate core cavity of internal model, open
Press machine presses repeatedly, then starts anti-liftout attachment, takes out internal model;
S5: curing process: the punch-pin of the internal model of taking-up and internal model is closed up into locking, puts it into tunnel drier and is done
Dry, heating, solidification and annealing operation then take out mica part and are toasted and eliminated internal stress operation.
2. a kind of manufacturing method of special-shaped mica part according to claim 1, it is characterised in that: the mica that ingredient uses
Powder Particle Size range is -20 mesh~-120 mesh, takes three kinds and the mica powder of the above different meshes is mixed.
3. a kind of manufacturing method of abnormity mica part described in -2 any one according to claim 1, it is characterised in that: when to
The operating temperature of the mica part of manufacture is 500 DEG C, using natural muscovite powder, when the operating temperature of mica part to be manufactured
It is 1000 DEG C, using artificial mica synthesis powder.
4. a kind of manufacturing method of special-shaped mica part according to claim 1, it is characterised in that: the compacting in the S3
It is 0.1mm smaller than the Male Die Size of internal model with Male Die Size, and this is pressed into convex mould surface chromium plating.
5. a kind of manufacturing method of special-shaped mica part according to claim 1, it is characterised in that: the internal model is with poly-
Tetrafluoroethylene resin is made of raw material, and the external mold and compacting are to be made of carbon steel with punch-pin.
6. a kind of manufacturing method of special-shaped mica part according to claim 1, it is characterised in that: the punch-pin of the internal model
Several gas vents are uniformly provided with on the contact surface of mica part to be manufactured.
7. a kind of manufacturing method of special-shaped mica part according to claim 1, it is characterised in that: further include:
S6: damp-proof treatment: by mass, taking 10-20 parts of 80-90 parts of marketable gasolines and 255 polymethylphenyl siloxane fluid to be mixed, will be through
S5 treated mica part impregnates wherein, after removing filter dry, after spontaneously drying at normal temperature, dries in 60-80 DEG C of baking oven
Final mica part is obtained after roasting.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111875412A (en) * | 2020-06-15 | 2020-11-03 | 嘉兴市荔禾实业有限公司 | Conical mica tube and processing technology thereof |
CN111976037A (en) * | 2020-06-30 | 2020-11-24 | 湖北平安电工股份有限公司 | Method for producing mica special-shaped piece |
CN114013153A (en) * | 2021-02-18 | 2022-02-08 | 湖北平安电工科技股份公司 | Mica special-shaped piece forming process containing organic silicon adhesive |
CN114274597A (en) * | 2021-02-18 | 2022-04-05 | 湖北平安电工科技股份公司 | Mica special-shaped piece for lithium battery assembly and processing method |
CN114312604A (en) * | 2022-03-11 | 2022-04-12 | 浙江荣泰电工器材股份有限公司 | Upper cover thermal runaway protection mica structural member for new energy automobile and preparation method thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111875412A (en) * | 2020-06-15 | 2020-11-03 | 嘉兴市荔禾实业有限公司 | Conical mica tube and processing technology thereof |
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CN114013153A (en) * | 2021-02-18 | 2022-02-08 | 湖北平安电工科技股份公司 | Mica special-shaped piece forming process containing organic silicon adhesive |
CN114274597A (en) * | 2021-02-18 | 2022-04-05 | 湖北平安电工科技股份公司 | Mica special-shaped piece for lithium battery assembly and processing method |
CN114312604A (en) * | 2022-03-11 | 2022-04-12 | 浙江荣泰电工器材股份有限公司 | Upper cover thermal runaway protection mica structural member for new energy automobile and preparation method thereof |
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