CN109319907A - Blending tank is used in a kind of production of stalk flocculant - Google Patents
Blending tank is used in a kind of production of stalk flocculant Download PDFInfo
- Publication number
- CN109319907A CN109319907A CN201811173392.6A CN201811173392A CN109319907A CN 109319907 A CN109319907 A CN 109319907A CN 201811173392 A CN201811173392 A CN 201811173392A CN 109319907 A CN109319907 A CN 109319907A
- Authority
- CN
- China
- Prior art keywords
- homogeneous
- blending tank
- funnel
- stalk
- hinged
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
Abstract
A kind of stalk flocculant production blending tank, is respectively equipped with the top controlled respectively by upper and lower telescopic hydraulic cylinder, low pressure sealing cover in the upper and lower end of blending tank；Heat transfer medium is full of in the collet of the homogeneous mixing warehouse of blending tank；It is successively arranged the crossbeam being fixedly connected, inclined liquid feeding pipeline, horizontal liquid separation filter funnel and homogeneous system from top to bottom inside homogeneous mixing bunker body, the center of the backings of liquid separation filter funnel connects funnel shaft by bearing, and funnel shaft and upper beam are affixed；Separatory funnel is driven by waterproof machine to be rotated relative to funnel shaft, and top and bottom of the funnel shaft inside liquid separation filter funnel are respectively connected with a funnel stirring blade；The liquid feeding end of liquid feeding pipeline is connect with external liquid feeding source；Homogeneous system include rotationally be set with a pair of of homogeneous axis have on a pair of of homogeneous impeller group, a pair of of homogeneous axis drives by a pair of of homogeneous driving mechanism.The mixing jar structure is simple, mixing efficiency is high, effect is good.
Description
Technical field
The invention belongs to field of environment protection equipment, and in particular to blending tank is used in a kind of production of stalk flocculant.
Background technique
With the fast development of national economy, demand of the enterprise to stalk flocculant increases year by year, has also therefore driven phase
Close the growth of flocculant industry.Currently, existing stalk flocculant blending tank agitating mode mostly uses base soln greatly and adds
Add agent to input in agitator together, mixing is stirred by agitating shaft and stirrer paddle, but existing mixing stirring device
Have the shortcomings that structure is complicated, mixing efficiency is low and mixed effect is poor.
Summary of the invention
In view of the above existing problems in the prior art, the present invention provides a kind of stalk flocculant production blending tanks, this is mixed
Conjunction jar structure is simple, mixing efficiency is high, and mixing effect is ideal.
To achieve the goals above, the present invention provides a kind of stalk flocculant production blending tank, including blending tank, fixation
It is connected to multiple supporting steel frames of blending tank lower outside, upper connection is cranked arm, lower connection is cranked arm, upper telescopic oil cylinder and lower flexible oil
Cylinder；
The upper pressure sealing cover of sealing blending tank is separately provided in the upper open end and lower open end of blending tank
With low pressure sealing cover；Described upper one end cranked arm that connects is fixedly connected with the upper surface of upper pressure sealing cover, the other end
It is hinged with the hinged seat that is fixedly connected on the outside of blending tank upper end；Outside the hinged end that one end of upper telescopic oil cylinder and upper connection are cranked arm
Side is hinged, hinged in the middle part of the can body of the other end and blending tank, with controlled by expanding-contracting action upper pressure sealing cover lid conjunction or
It opens；Described lower one end for cranking arm of connecting is fixedly connected with the lower end surface of low pressure sealing cover, the other end be fixedly connected on
The hinged seat of blending tank lower end outside is hinged；One end of lower telescopic oil cylinder and the lower hinged end outside cranked arm that connects are hinged, another
End and the can body middle part of blending tank are hinged, close or open to control the lid of low pressure sealing cover by expanding-contracting action；
The blending tank includes jacket structured homogeneous mixing warehouse, is situated between in the collet of homogeneous mixing warehouse full of heat transfer
Matter, homogeneous mixing warehouse are externally connected to the heat medium pipeline being connected to its jacket space, the other end of heat medium pipeline with
The connection of thermal medium source of supply；
It is disposed with the crossbeam radially extended, the liquid-feeding tube being obliquely installed from top to bottom inside homogeneous mixing bunker body
Road, it is horizontal positioned and can relative homogeneous mixing warehouse rotation liquid separation filter funnel and homogeneous system, the both ends of crossbeam respectively with
The opposite sides of side wall is fixedly connected in homogeneous mixing bunker body；The bottom plate of liquid separation filter funnel is outwardly provided with multiple throughout it
Aperture, and the rotation center of bottom plate is connected with funnel shaft by bearing collet, funnel shaft upwardly extend and with upper beam
Middle part is fixedly connected；The outlet end of liquid feeding pipeline is located above liquid separation filter funnel, and liquid feeding end is pierced by homogeneous mixing warehouse
It is connect after side wall with liquid feeding source；
Ground is provided with several side-wall holes on the side wall of liquid separation filter funnel, in the upper end of liquid separation filter funnel
External fixing sleeve is equipped with outer gear ring；Waterproof machine is fixedly connected with corresponding to outer gear ring on the inner sidewall of homogeneous mixing warehouse,
Funnel gear is equipped on the output shaft of waterproof machine, funnel gear is engaged with outer gear ring；Funnel shaft is in liquid separation filter funnel
Internal top and bottom are respectively connected with the funnel stirring blade of one with the cooperation of inside upper end and lower end internal clearance；
Homogeneous system includes that pair of parellel setting is rotationally set in homogeneous axis, a pair of of homogeneous axis at middle part respectively
There is corresponding a pair of of homogeneous impeller group, homogeneous impeller group is made of multiple high speed homogenization impellers, in a pair of of homogeneous impeller group
It is engaged between high speed homogenization impeller；The opposite both ends of a pair of of homogeneous axis are rotationally pierced by after homogeneous mixing warehouse respectively respectively
It is connect with the output section for the homogeneous driving mechanism for being fixedly connected on homogeneous mixing bunker body both sides external；Homogeneous axis is far from driving machine
The other end of structure is rotatablely connected by closed type thrust bearing with the inner sidewall of homogeneous mixing warehouse.
As a preference, the homogeneous driving mechanism is formed by connecting by homogeneous driving motor with retarder.
Further, further include control cabinet in order to facilitate centralized control, speed probe is set on retarder, thermal medium supplies
Ying Yuan and liquid feeding source are respectively the thermal medium transfer pump connecting with thermal medium source and the fluid filling pump connecting with liquid source；
Control cabinet connects with homogeneous driving motor, speed probe, thermal medium transfer pump, fluid filling pump and waterproof machine respectively
It connects.
As a preference, the supporting steel frame quantity is 3 groups, and it is evenly distributed on the outside of blending tank；
The wall thickness of the homogeneous mixing bunker is 2mm~50mm；
The liquid separation filter funnel is located at the position of homogeneous mixing bunker waist 25mm~55mm on the upper side；
The liquid-adding device and horizontal direction angle are between 10 °~32 °；
Funnel stirring blade is by the radial direction between the annulus being set on the outside of funnel shaft and connection annulus and funnel shaft
Connecting rod composition.
It further, further include the homogeneity detector being arranged in inside homogeneous mixing bunker for the ease of detecting homogeneous degree,
Homogeneity detector is connect with control cabinet.
Further, in order to improve homogenizing effect, high speed homogenization impeller quantity is 10, between adjacent high speed homogenization impeller etc.
Distance arrangement, and spacing, between 5mm~12mm, high speed homogenization impeller shape is in ratchet-like.
Further, for the ease of radiating to oil cylinder,
Fixing sleeve is equipped with fixed sleeving on the piston rod A of the lower telescopic oil cylinder, and the circumferential direction of fixed sleeving is evenly arranged with
Multiple fin deployment rods are articulated and connected between the inner end and fixed sleeving of fin deployment rod by deployment rod shaft；
The cylinder barrel A of the lower telescopic oil cylinder is circumferentially evenly arranged with multiple oil cylinder fins, oil cylinder close to one end of piston rod A
It is arranged in a one-to-one correspondence between fin and fin deployment rod, the bottom end of fin deployment rod is hinged by fin lower shaft and cylinder barrel A, top
It holds hinged with the outer end of fin deployment rod.
Further, in order to improve heat dissipation effect, the quantity of the fin deployment rod and oil cylinder fin is 6, the oil cylinder wing
The material of piece is thin plate stainless steel material.
Further, the high speed homogenization impeller good in order to the homogenizing effect that gets a promotion, the high speed homogenization impeller is by high score
Sub- material is made, by mass percentage content meter, and constituent is as follows:
Methyl ester derivative 30%~65%, thiophosphate analog derivative 25%~60%, mixed aid be 1%~
5%, crosslinking agent is 1%~5%, O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45%, (T-
4)-bis- (diethyldithiocar bamic acid-S, S') zinc 2%~15%.
Further, the high speed homogenization impeller good in order to the homogenizing effect that gets a promotion, the preparation method of high speed homogenization impeller
It comprises the steps of:
Step 1: the ultrapure water 22%~32% that conductivity is 1.25 μ of μ S/cm~3.15 S/cm is added in a kettle, opens
Blender in dynamic reaction kettle, revolving speed are 125rpm~375rpm, start heat pump, make reactor temperature rise to 75 DEG C~
185℃；Successively methylate ester derivative 30%~65%, mixed aid are 1%~5%, and stirring is adjusted to being completely dissolved
PH value be 5.5~8.5, be added thiophosphate analog derivative 25%~60%, by agitator speed be adjusted to 255rpm~
315rpm, temperature are 90 DEG C~395 DEG C；
Step 2: O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45% is added, (T-4)-is bis-
(diethyldithiocar bamic acid-S, S') zinc 2%~15% is uniformly mixed；
Step 3: it is 1~5% that crosslinking agent, which is added, and agitator speed is 75rpm~235rpm, and temperature is 90 DEG C~265 DEG C,
It keeps this state 5~25 hours, discharges, entering molding press can be prepared by high speed homogenization impeller.
In the present invention, upper pressure sealing cover and low pressure sealing cover pass through upper telescopic oil cylinder and lower telescopic oil cylinder respectively
Folding control is carried out, the degree of automation of the blending tank can be improved.Waterproof machine is driven through funnel gear driving outer gear ring and turns
It is dynamic, and then liquid separation filter funnel is driven to be rotated in filtering, filter effect and efficiency not only can be improved, but also
The liquid additive being added can be made uniformly mix with material to be processed and stir in advance, a pair of of homogeneous wave in homogeneous system
Wheel group by uniform driving mechanism driving do high speed move toward one another, mixing effect can not only be improved, and can promote additive with to
Handle the reaction between material.The apparatus structure is simple, stirring efficiency is high, and homogenizing effect is ideal.
Detailed description of the invention
Fig. 1 is structural schematic diagram of the invention；
Fig. 2 is the structural schematic diagram of blending tank in the present invention；
Fig. 3 is the structural schematic diagram of liquid separation filter funnel in the present invention；
Fig. 4 is the structural schematic diagram of homogeneous system in the present invention；
Fig. 5 is the structural schematic diagram of lower telescopic oil cylinder in the present invention；
Fig. 6 is O- ethyl O- in the present invention (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate accounting to improving uniformity
The influence graph of relation of rate；
Fig. 7 is methyl ester derivative molecular characterization schematic diagram in the present invention；
Fig. 8 is group thiophosphate derivative molecular structure feature schematic diagram in the present invention；
Fig. 9 is oxysilane substance molecular characterization schematic diagram in the present invention.
In figure: 1, supporting steel frame, 2, blending tank, 2-1, homogeneous mixing bunker, 2-2, liquid separation filter funnel, 2-2-1, side wall are opened
Hole, 2-2-2, outer gear ring, 2-2-3, funnel gear, 2-2-4, waterproof machine, 2-2-5, funnel stirring blade, 2-2-6, bearing bottom
Support, 2-3, liquid feeding pipeline, 2-4, homogeneous system, 2-4-1, homogeneous driving motor, 2-4-2, retarder, 2-4-3, homogeneous axis,
2-4-4, closed type thrust bearing, 2-4-5, high speed homogenization impeller, 2-5, homogeneity detector, 3, upper pressure sealing cover, 4, on
Connection is cranked arm, 5, upper telescopic oil cylinder, 6, low pressure sealing cover, 7, lower telescopic oil cylinder, 7-1, cylinder barrel A, 7-2, fin lower shaft, 7-
3, oil cylinder fin, 7-4, fixed sleeving, 7-5, piston rod A, 7-6, fin deployment rod, 7-7, deployment rod shaft, 8, control cabinet, 9,
Crossbeam, 10, funnel shaft.
Specific embodiment
The invention will be further described below.
As shown in Figures 1 to 5, a kind of stalk flocculant production blending tank, including blending tank 2, it is fixedly connected on mixing
Multiple supporting steel frames 1 of 2 lower outside of tank, upper connection crank arm 4, lower connection is cranked arm 9, upper telescopic oil cylinder 5 and lower telescopic oil cylinder 7；
The upper pressure sealing of sealing blending tank 2 is separately provided in the upper open end and lower open end of blending tank 2
Lid 3 and low pressure sealing cover 6；Crank arm 4 one end of the upper connection is fixedly connected with the upper surface of upper pressure sealing cover 3,
The other end and the hinged seat being fixedly connected on the outside of 2 upper end of blending tank are hinged；One end of upper telescopic oil cylinder 5 and upper connection crank arm 4
Hinged end on the outside of it is hinged, it is hinged in the middle part of the can body of the other end and blending tank 2, sealed with controlling upper pressure by expanding-contracting action
The lid of lid 3 is closed or is opened；Crank arm 9 one end of the lower connection is fixedly connected with the lower end surface of low pressure sealing cover 6, another
The hinged seat for holding and being fixedly connected on 2 lower end outside of blending tank is hinged；One end of lower telescopic oil cylinder 7 and it is lower connection crank arm 9 hinge
It is hinged to connect end outside, it is hinged in the middle part of the can body of the other end and blending tank 2, to control low pressure sealing cover 6 by expanding-contracting action
Lid close or open；
The blending tank 2 includes jacket structured homogeneous mixing warehouse 2-1, is full of in the collet of homogeneous mixing warehouse 2-1
Heat transfer medium, homogeneous mixing warehouse 2-1's is externally connected to the heat medium pipeline being connected to its jacket space, heat medium pipeline
The other end is connect with thermal medium source of supply；
It is disposed with the crossbeam 9 radially extended, the liquid feeding being obliquely installed from top to bottom inside homogeneous mixing warehouse 2-1
Pipeline 2-3, it is horizontal positioned and can relative homogeneous mixing warehouse 2-1 rotation liquid separation filter funnel 2-2 and homogeneous system 2-4, it is horizontal
The both ends of beam 9 are fixedly connected with the opposite sides of homogeneous mixing warehouse 2-1 inner sidewall respectively；The bottom plate of liquid separation filter funnel 2-2
Multiple apertures are outwardly provided with throughout it, and the rotation center of bottom plate is connected with funnel shaft 10 by bearing collet 2-2-6,
Funnel shaft 10 is upwardly extended and is fixedly connected with the middle part of upper beam 9；The outlet end of liquid feeding pipeline 2-3 is located at the leakage of liquid separation strainer
It struggles against above 2-2, liquid feeding end is connect after being pierced by the side wall of homogeneous mixing warehouse 2-1 with liquid feeding source；
Ground is provided with several side-wall holes 2-2-1 on the side wall of liquid separation filter funnel 2-2, is leaked in liquid separation strainer
Fixing sleeve is equipped with outer gear ring 2-2-2 outside the upper end of bucket 2-2；Outer gear ring 2- is corresponded on the inner sidewall of homogeneous mixing warehouse 2-1
It is fixedly connected with to 2-2 waterproof machine 2-2-4, funnel gear 2-2-3, funnel are equipped on the output shaft of waterproof machine 2-2-4
Gear 2-2-3 is engaged with outer gear ring 2-2-2；Top and bottom of the funnel shaft 10 inside liquid separation filter funnel 2-2 respectively connect
There are the funnel stirring blade 2-2-5 of one with the cooperation of inside upper end and lower end internal clearance；
Homogeneous system 2-4 includes that pair of parellel is arranged in homogeneous axis 2-4-3, a pair of homogeneous axis 2-4-3 in middle part
It is not set with corresponding a pair of of homogeneous impeller group rotationally, homogeneous impeller group is made of multiple high speed homogenization impeller 2-4-5,
It is engaged between high speed homogenization impeller 2-4-5 in a pair of of homogeneous impeller group；It a pair of of homogeneous axis 2-4-3 opposite both ends respectively can
It is rotationally pierced by after homogeneous mixing warehouse 2-1 and is driven respectively with the homogeneous for being fixedly connected on homogeneous mixing warehouse 2-1 both sides external
The output section of mechanism connects；Homogeneous axis 2-4-3 passes through closed type thrust bearing 2-4-4 and homogeneous far from the other end of driving mechanism
Mix the inner sidewall rotation connection of warehouse 2-1.
The homogeneous driving mechanism is formed by connecting by homogeneous driving motor 2-4-1 and retarder 2-4-2.
Further include control cabinet 8, speed probe is set on retarder 2-4-2, thermal medium source of supply and liquid feeding source are respectively
The thermal medium transfer pump being connect with thermal medium source and the fluid filling pump being connect with liquid source；
Control cabinet 8 respectively with homogeneous driving motor 2-4-1, speed probe, thermal medium transfer pump, fluid filling pump and anti-water power
Machine 2-2-4 connection.
1 quantity of supporting steel frame is 3 groups, and is evenly distributed on the outside of blending tank 2；
The wall thickness of the homogeneous mixing bunker 2-1 is 2mm~50mm；
The liquid separation filter funnel 2-2 is located at the position of homogeneous mixing bunker 2-1 waist 25mm~55mm on the upper side；
The liquid-adding device 2-3 and horizontal direction angle are between 10 °~32 °；
Funnel stirring blade 2-2-5 by be set in the outside of funnel shaft 10 annulus and connection annulus and funnel shaft 10 it
Between radially directed connecting link composition.
It further include homogeneity detector 2-5, homogeneity detector 2-5 and the control being arranged in inside homogeneous mixing bunker 2-1
Case 8 connects.
High speed homogenization impeller 2-4-5 quantity is 10, is spaced substantially equidistant between adjacent high speed homogenization impeller 2-4-5, and
Away between 5mm~12mm, high speed homogenization impeller 2-4-5 shape is in ratchet-like.
Fixing sleeve is equipped with fixed sleeving 7-4, the circumferential direction of fixed sleeving 7-4 on the piston rod A7-5 of the lower telescopic oil cylinder 7
Multiple fin deployment rod 7-6 are evenly arranged with, are turned between the inner end and fixed sleeving 7-4 of fin deployment rod 7-6 by deployment rod
Axis 7-7 articulated connection；
The cylinder barrel A7-1 of the lower telescopic oil cylinder 7 is circumferentially evenly arranged with multiple oil cylinder wings close to one end of piston rod A7-5
It is arranged in a one-to-one correspondence between piece 7-3, oil cylinder fin 7-3 and fin deployment rod 7-6, the bottom end of fin deployment rod 7-6 passes through fin
Lower shaft 7-2 and cylinder barrel A7-1 are hinged, and top and the outer end of fin deployment rod 7-6 are hinged.Oil cylinder fin 7-3 is with fin lower shaft
7-2 is tight and expansion of the rotary shaft realization to telescopic rod 7-5, and then reaches the mesh to radiate to lower telescopic oil cylinder 7
's.
The quantity of the fin deployment rod 7-6 and oil cylinder fin 7-3 are 6, the material of oil cylinder fin 7-3 be thin plate not
Rust steel material.
The high speed homogenization impeller 2-4-5 is made of high molecular material, by mass percentage content meter, and constituent is such as
Under:
Methyl ester derivative 30%~65%, thiophosphate analog derivative 25%~60%, mixed aid be 1%~
5%, crosslinking agent is 1%~5%, O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45%, (T-
4)-bis- (diethyldithiocar bamic acid-S, S') zinc 2%~15%.
The crosslinking agent is (phosphordithiic acid diisopropyl ester sodium, isopentyl and isopropyl) phosphorodithioate zinc salt, four
Any one in phenyl (bisphenol-A) bisphosphate.
The feature of methyl ester derivative molecular structure is as shown in fig. 7, wherein R is the alkyl that carbon atom number is 1~8.
The feature of group thiophosphate derivative molecular structure is as shown in figure 8, its molecular formula: C10H15O3PS2；Molecule
Amount: 278.343.
Mixed aid be oxysilane substance, molecular structural formula as shown in figure 9, its included molecular structure molecule
Formula are as follows: C16H20O2Si.
The preparation method of high speed homogenization impeller 2-4-5 comprises the steps of:
Step 1: the ultrapure water 22%~32% that conductivity is 1.25 μ of μ S/cm~3.15 S/cm is added in a kettle, opens
Blender in dynamic reaction kettle, revolving speed are 125rpm~375rpm, start heat pump, make reactor temperature rise to 75 DEG C~
185℃；Successively methylate ester derivative 30%~65%, mixed aid are 1%~5%, and stirring is adjusted to being completely dissolved
PH value be 5.5~8.5, be added thiophosphate analog derivative 25%~60%, by agitator speed be adjusted to 255rpm~
315rpm, temperature are 90 DEG C~395 DEG C；
Step 2: O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45% is added, (T-4)-is bis-
(diethyldithiocar bamic acid-S, S') zinc 2%~15% is uniformly mixed；
Step 3: it is 1~5% that crosslinking agent, which is added, and agitator speed is 75rpm~235rpm, and temperature is 90 DEG C~265 DEG C,
It keeps this state 5~25 hours, discharges, entering molding press can be prepared by high speed homogenization impeller 2-4-5.
Following embodiment further illustrates the contents of the present invention, and as high speed homogenization impeller 2-4-5, it is weight of the invention
Component is wanted, due to its presence, increases the service life of integral device, it is played for the safety of integral device, even running
Key effect.For this purpose, by it is following be embodiment, further verify the component of the present invention, what is shown is higher than
The physical characteristic of other related patents.
Embodiment 1
High speed homogenization impeller 2-4-5 of the present invention, and content meter by mass percentage are manufactured according to the following steps:
Step 1: the ultrapure water 22% that conductivity is 1.25 μ S/cm being added in a kettle, starts blender in reaction kettle,
Revolving speed is 125rpm, starts heat pump, reactor temperature is made to rise to 75 DEG C；Successively methylate ester derivative 30% mixes
Closing auxiliary agent is 1%, and to being completely dissolved, adjusting pH value is 5.5 for stirring, thiophosphate analog derivative 25% is added, by blender
Revolving speed is adjusted to 255rpm, and temperature is 90 DEG C；
Step 2: O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45% is added, (T-4)-is bis-
(diethyldithiocar bamic acid-S, S') zinc 2% is uniformly mixed；
Step 3: it is 1% that crosslinking agent, which is added, agitator speed 75rpm, and temperature is 90 DEG C, keeps this state 5 hours, out
Material, entering molding press can be prepared by high speed homogenization impeller 2-4-5.
Embodiment 2
High speed homogenization impeller 2-4-5 of the present invention, and content meter by mass percentage are manufactured according to the following steps:
Step 1: the ultrapure water 32% that conductivity is 3.15 μ S/cm being added in a kettle, starts blender in reaction kettle,
Revolving speed is 375rpm, starts heat pump, reactor temperature is made to rise to 185 DEG C；Successively methylate ester derivative 65% mixes
Closing auxiliary agent is 5%, and to being completely dissolved, adjusting pH value is 8.5 for stirring, thiophosphate analog derivative 60% is added, by blender
Revolving speed is adjusted to 315rpm, and temperature is 395 DEG C；
Step 2: O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 45%, (T-4)-bis- (diethyls is added
Base aminodithioformic acid-S, S') zinc 15% be uniformly mixed；
Step 3: it is 5% that crosslinking agent, which is added, agitator speed 235rpm, and temperature is 265 DEG C, keeps this state 25 small
When, discharging, entering molding press can be prepared by high speed homogenization impeller 2-4-5.
Embodiment 3
High speed homogenization impeller 2-4-5 of the present invention, and content meter by mass percentage are manufactured according to the following steps:
Step 1: the ultrapure water 29% that conductivity is 1.315 μ S/cm, stirring in starting reaction kettle are added in a kettle
Device, revolving speed 178rpm start heat pump, reactor temperature are made to rise to 85 DEG C；Successively methylate ester derivative 39%,
Mixed aid is 4%, and to being completely dissolved, adjusting pH value is 5.8 for stirring, and thiophosphate analog derivative 40% is added, will stir
Device revolving speed is adjusted to 300rpm, and temperature is 90 DEG C；
Step 2: O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 40%, (T-4)-bis- (diethyls is added
Base aminodithioformic acid-S, S') zinc 10% be uniformly mixed；
Step 3: it is 3% that crosslinking agent, which is added, agitator speed 90rpm, and temperature is 91 DEG C, keeps this state 8 hours, out
Material, entering molding press can be prepared by high speed homogenization impeller 2-4-5.
Reference examples
Reference examples are that the high speed homogenization impeller of certain commercially available brand is used for the service condition of oil product mixing assorting room.
High speed homogenization impeller described in high speed homogenization impeller 2-4-5 and reference examples that Examples 1 to 3 prepares is used for
The service condition of oil product mixed process compares, and with volume resistivity, oil from spending, reduce sticky rate, mixture homogeneity
Enhancing rate is that technical indicator is counted, and the results are shown in Table 1:
Table 1 is service condition of the high speed homogenization impeller described in Examples 1 to 3 and reference examples for oil product mixed process
The comparing result of parameters, as seen from Table 1, high speed homogenization impeller 2-4-5 of the present invention, volume resistivity, oil from
It spends, reduce sticky rate, mixture homogeneity enhancing rate is above the product that the prior art produces.
In addition, as shown in fig. 6, being O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate accounting to the uniformity
Promote the influence relational graph of rate.Find out in figure, as the important component of high speed homogenization impeller 2-4-5 material, incorporation pair
Enhancing product performance, it is vital to play the role of, and mixes its ingredient in terms of improving uniformity rate substantially better than existing production
Product.
The device working method including the following steps:
Step 1: low pressure sealing cover 6 implements slow liter, and be fitted with blending tank 2 under the action of lower telescopic oil cylinder 7,
Realize sealing；Treating material is entered in blending tank 2 by conduit, upper pressure sealing cover 3 cranks arm 4 by connection, and
Under the action of upper telescopic oil cylinder 5, slow drop is implemented to upper pressure sealing cover 3, and be fitted with blending tank 2, realize sealing；
Step 2: in blending tank 2, treating material enters liquid separation filter funnel 2-2 by liquid feeding pipeline 2-3, due to adding
Liquid pipeline 2-3 is obliquely installed, and the material of entrance acts on liquid separation filter funnel 2-2, is filtered the side liquid separation filter funnel 2-2
The rotation of operation side, is filtered by the liquid separation filter funnel 2-2 rotated, filter effect can be made more preferable；Two homogeneous driving mechanisms
It drives two a pair of of homogeneous impeller groups to move toward one another, is engaged between the high speed homogenization impeller in a pair of of homogeneous impeller group, object can be made
Material reaches homogenizing effect, and then enters the lower part homogeneous mixing bunker 2-1；Homogeneity detector 2-5 is to entrance homogeneous mixing bunker 2-1
The homogeneity of the material of lower part makes induction and reacts and detected；When homogeneity does not meet examination criteria, homogeneity detection
Device 2-5 issues electric signal to control cabinet 8, and controller 8 is alarmed by alarm connected to it.
Step 3: in liquid separation filter funnel 2-2, waterproof machine 2-2-4 is operated after powering on, and drives funnel
Gear 2-2-3 rotation, and then the rotation of funnel gear 2-2-3 driving outer gear ring 2-2-2 is to realize liquid separation filter funnel 2-2 around leakage
The operating for the shaft 10 that struggles against；Funnel paddle 2-2-5 is fixed, opposite with funnel paddle 2-2-5 in liquid separation filter funnel 2-2
Under the stirring action of movement, reach the uniform stirring to material；Material is after stirring, from the bottom plate of liquid separation filter funnel 2-2
And it is flowed out in side-wall hole 2-2-1；
Step 4: in lower telescopic oil cylinder 7, when piston rod A 7-5 is moved downward, driving fixed sleeving 7-4 to move down, into
And oil cylinder fin 7-3 expansion is driven by fin deployment rod 7-6；When piston rod A 7-5 is moved upwards, fixed sleeving is driven
7-4 is moved up, and then drives oil cylinder fin 7-3 to shrink by fin deployment rod 7-6；The expansion and contraction of oil cylinder fin 7-3 is realized
Cooling to lower telescopic oil cylinder 7.
Claims (10)
1. a kind of stalk flocculant production blending tank, including blending tank (2) and is fixedly connected on blending tank (2) lower outside
Multiple supporting steel frames (1), which is characterized in that further include it is upper connection crank arm (4), it is lower connection crank arm (9), upper telescopic oil cylinder (5) and
Lower telescopic oil cylinder (7)；
The upper pressure sealing of sealing blending tank (2) is separately provided in the upper open end and lower open end of blending tank (2)
Cover (3) and low pressure sealing cover (6)；Described upper one end of (4) of cranking arm that connects is consolidated with the upper surface of upper pressure sealing cover (3)
Fixed connection, the other end and the hinged seat being fixedly connected on the outside of blending tank (2) upper end are hinged；One end of upper telescopic oil cylinder (5) with
Upper connection crank arm (4) hinged end on the outside of it is hinged, it is hinged in the middle part of the can body of the other end and blending tank (2), to pass through expanding-contracting action
The lid for controlling upper pressure sealing cover (3) is closed or is opened；It is described it is lower connection crank arm (9) one end and low pressure sealing cover (6)
Lower end surface be fixedly connected, the other end and the hinged seat for being fixedly connected on blending tank (2) lower end outside are hinged；Lower telescopic oil cylinder
(7) one end and lower connection crank arm (9) hinged end on the outside of it is hinged, it is hinged in the middle part of the can body of the other end and blending tank (2), with logical
The lid for crossing flexible action control low pressure sealing cover (6) is closed or is opened；
The blending tank (2) includes jacket structured homogeneous mixing warehouse (2-1), is filled in the collet of homogeneous mixing warehouse (2-1)
Full heat transfer medium, homogeneous mixing warehouse (2-1) are externally connected to the heat medium pipeline being connected to its jacket space, thermal medium pipe
The other end on road is connect with thermal medium source of supply；
The liquid feeding that radially extend crossbeam (9), is obliquely installed is disposed with inside the homogeneous mixing warehouse (2-1) from top to bottom
Pipeline (2-3), it is horizontal positioned and can relative homogeneous mixing warehouse (2-1) rotation liquid separation filter funnel (2-2) and homogeneous system
(2-4), the both ends of crossbeam (9) are fixedly connected with the opposite sides of homogeneous mixing warehouse (2-1) inner sidewall respectively；The leakage of liquid separation strainer
The bottom plate of bucket (2-2) is outwardly provided with multiple apertures throughout it, and the rotation center of bottom plate is connected by bearing collet (2-2-6)
Be connected to funnel shaft (10), funnel shaft (10) upwardly extend and be fixedly connected in the middle part of upper beam (9)；Liquid feeding pipeline (2-
3) outlet end is located above liquid separation filter funnel (2-2), and liquid feeding end is pierced by after the side wall of homogeneous mixing warehouse (2-1) and adds
The connection of liquid source；
Ground is provided with several side-wall holes (2-2-1) on the side wall of liquid separation filter funnel (2-2), is leaked in liquid separation strainer
Fixing sleeve is equipped with outer gear ring (2-2-2) outside the upper end of bucket (2-2)；It is corresponding outer on the inner sidewall of homogeneous mixing warehouse (2-1)
It is fixedly connected with waterproof machine (2-2-4) to gear ring (2-2-2), is equipped with funnel tooth on the output shaft of waterproof machine (2-2-4)
It takes turns (2-2-3), funnel gear (2-2-3) is engaged with outer gear ring (2-2-2)；Funnel shaft (10) is at liquid separation filter funnel (2-2)
Internal top and bottom are respectively connected with the funnel stirring blade (2-2- of one with the cooperation of inside upper end and lower end internal clearance
5)；
Homogeneous system (2-4) includes that pair of parellel is arranged in homogeneous axis (2-4-3), a pair of of homogeneous axis (2-4-3) at middle part
It is rotationally set with corresponding a pair of of homogeneous impeller group respectively, homogeneous impeller group is by multiple high speed homogenization impellers (2-4-5)
It forms, is engaged between the high speed homogenization impeller (2-4-5) in a pair of of homogeneous impeller group；A pair of of homogeneous axis (2-4-3) is opposite
Both ends be rotationally pierced by after homogeneous mixing warehouse (2-1) respectively respectively with to be fixedly connected on homogeneous mixing warehouse (2-1) external
The output section of the homogeneous driving mechanism of two sides connects；Homogeneous axis (2-4-3) is pushed away far from the other end of driving mechanism by enclosed
Power bearing (2-4-4) is rotatablely connected with the inner sidewall of homogeneous mixing warehouse (2-1).
2. a kind of stalk flocculant production blending tank according to claim 1, which is characterized in that the homogeneous driving machine
Structure is formed by connecting by homogeneous driving motor (2-4-1) and retarder (2-4-2).
3. a kind of stalk flocculant production blending tank according to claim 1 or 2, which is characterized in that further include control
Case (8), speed probe is arranged on retarder (2-4-2), and thermal medium source of supply and liquid feeding source are respectively to connect with thermal medium source
Thermal medium transfer pump and the fluid filling pump that is connect with liquid source；
Control cabinet (8) respectively with homogeneous driving motor (2-4-1), speed probe, thermal medium transfer pump, fluid filling pump and anti-water power
Machine (2-2-4) connection.
4. a kind of stalk flocculant production blending tank according to claim 3, which is characterized in that the supporting steel frame
(1) quantity is 3 groups, and is evenly distributed on the outside of blending tank (2)；
The wall thickness of the homogeneous mixing bunker (2-1) is 2mm~50mm；
The liquid separation filter funnel (2-2) is located at the position of homogeneous mixing bunker (2-1) waist 25mm~55mm on the upper side；
The liquid-adding device (2-3) and horizontal direction angle are between 10 °~32 °；
Funnel stirring blade (2-2-5) is by the annulus and connection annulus that are set on the outside of funnel shaft (10) and funnel shaft (10)
Between radially directed connecting link composition.
5. a kind of stalk flocculant production blending tank according to claim 4, which is characterized in that further include being arranged equal
The internal homogeneity detector (2-5) of matter mixing bunker (2-1), homogeneity detector (2-5) are connect with control cabinet (8).
6. a kind of stalk flocculant production blending tank according to claim 5, which is characterized in that high speed homogenization impeller
(2-4-5) quantity is 10, is spaced substantially equidistant between adjacent high speed homogenization impeller (2-4-5), and spacing 5mm~12mm it
Between, high speed homogenization impeller (2-4-5) shape is in ratchet-like.
7. a kind of stalk flocculant production blending tank according to claim 6, which is characterized in that the lower telescopic oil cylinder
(7) fixing sleeve is equipped with fixed sleeving (7-4) on piston rod A (7-5), and the circumferential direction of fixed sleeving (7-4) is evenly arranged with multiple
Fin deployment rod (7-6) is cut with scissors between the inner end and fixed sleeving (7-4) of fin deployment rod (7-6) by deployment rod shaft (7-7)
It connects in succession；
The cylinder barrel A (7-1) of the lower telescopic oil cylinder (7) is circumferentially evenly arranged with multiple oil cylinders close to the one end of piston rod A (7-5)
Fin (7-3) is arranged in a one-to-one correspondence between oil cylinder fin (7-3) and fin deployment rod (7-6), the bottom of fin deployment rod (7-6)
Hingedly by fin lower shaft (7-2) and cylinder barrel A (7-1), top and the outer end of fin deployment rod (7-6) are hinged at end.
8. a kind of stalk flocculant production blending tank according to claim 7, which is characterized in that the fin deployment rod
The quantity of (7-6) and oil cylinder fin (7-3) is 6, and the material of oil cylinder fin (7-3) is thin plate stainless steel material.
9. a kind of stalk flocculant production blending tank according to claim 7, which is characterized in that the high speed homogenization wave
Wheel (2-4-5) is made of high molecular material, and content meter, constituent are as follows by mass percentage:
Methyl ester derivative 30%~65%, thiophosphate analog derivative 25%~60%, mixed aid are 1%~5%,
Crosslinking agent is 1%~5%, O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45%, and (T-4)-is bis-
(diethyldithiocar bamic acid-S, S') zinc 2%~15%.
10. a kind of stalk flocculant production blending tank according to claim 7, which is characterized in that high speed homogenization impeller
The preparation method of (2-4-5) comprises the steps of:
Step 1: being added the ultrapure water 22%~32% that conductivity is 1.25 μ of μ S/cm~3.15 S/cm in a kettle, and starting is anti-
Blender in kettle is answered, revolving speed is 125rpm~375rpm, starts heat pump, reactor temperature is made to rise to 75 DEG C~185 DEG C；
Successively methylate ester derivative 30%~65%, mixed aid are 1%~5%, and to being completely dissolved, adjusting pH value is for stirring
5.5~8.5, thiophosphate analog derivative 25%~60% is added, agitator speed is adjusted to 255rpm~315rpm, temperature
It is 90 DEG C~395 DEG C；
Step 2: O- ethyl O- (4- methyl mercapto phenyl) S- propyl disulfide substituted phosphate 15%~45%, (T-4)-bis- (two is added
Diethyldithiocar bamic acid-S, S') zinc 2%~15% be uniformly mixed；
Step 3: it is 1~5% that crosslinking agent, which is added, and agitator speed is 75rpm~235rpm, and temperature is 90 DEG C~265 DEG C, is kept
This state 5~25 hours, discharging, entering molding press can be prepared by high speed homogenization impeller (2-4-5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811173392.6A CN109319907A (en) | 2018-10-09 | 2018-10-09 | Blending tank is used in a kind of production of stalk flocculant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811173392.6A CN109319907A (en) | 2018-10-09 | 2018-10-09 | Blending tank is used in a kind of production of stalk flocculant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109319907A true CN109319907A (en) | 2019-02-12 |
Family
ID=65261730
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811173392.6A Withdrawn CN109319907A (en) | 2018-10-09 | 2018-10-09 | Blending tank is used in a kind of production of stalk flocculant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109319907A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516898A (en) * | 2020-12-30 | 2021-03-19 | 徐州工程学院 | Hydraulic oil mixing tank of tunnel expanding machine and using method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20060094735A (en) * | 2005-02-25 | 2006-08-30 | 명원환경 주식회사 | The equipment to recycle sludge from sewage and wastwwater |
| CN203307613U (en) * | 2013-04-28 | 2013-11-27 | 巢湖市翔宇渔具有限公司 | High-temperature reaction kettle for dyeing fishing net |
| CN207342536U (en) * | 2017-09-28 | 2018-05-11 | 上海晋升塑料科技有限公司 | Mixed stirring device |
| CN207786421U (en) * | 2017-11-15 | 2018-08-31 | 浙江万科建材有限公司 | A kind of mixed stirring device of concrete additive production |
| CN207805530U (en) * | 2017-12-29 | 2018-09-04 | 刘昌福 | A kind of powder liquid drug mixed stirring device |
| CN108585436A (en) * | 2018-03-19 | 2018-09-28 | 徐州工程学院 | A kind of bed mud pre-processing device |
-
2018
- 2018-10-09 CN CN201811173392.6A patent/CN109319907A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20060094735A (en) * | 2005-02-25 | 2006-08-30 | 명원환경 주식회사 | The equipment to recycle sludge from sewage and wastwwater |
| CN203307613U (en) * | 2013-04-28 | 2013-11-27 | 巢湖市翔宇渔具有限公司 | High-temperature reaction kettle for dyeing fishing net |
| CN207342536U (en) * | 2017-09-28 | 2018-05-11 | 上海晋升塑料科技有限公司 | Mixed stirring device |
| CN207786421U (en) * | 2017-11-15 | 2018-08-31 | 浙江万科建材有限公司 | A kind of mixed stirring device of concrete additive production |
| CN207805530U (en) * | 2017-12-29 | 2018-09-04 | 刘昌福 | A kind of powder liquid drug mixed stirring device |
| CN108585436A (en) * | 2018-03-19 | 2018-09-28 | 徐州工程学院 | A kind of bed mud pre-processing device |
Non-Patent Citations (1)
| Title |
|---|
| 杨晓惠等: "《固液分离原理与工业水处理装置》", 31 January 2017, 电子科技大学出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516898A (en) * | 2020-12-30 | 2021-03-19 | 徐州工程学院 | Hydraulic oil mixing tank of tunnel expanding machine and using method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109438581A (en) | Tank is pre-processed in a kind of processing of production of corn starch | |
| CN109351274A (en) | Agitator tank in a kind of carbon tetrachloride processing system | |
| CN109319907A (en) | Blending tank is used in a kind of production of stalk flocculant | |
| CN109331678A (en) | A kind of underground water duct expanding machine hydraulic oil blending tank | |
| CN109354237A (en) | A kind of residents in rural community device for treating leachate | |
| CN109317035A (en) | Agitator tank in a kind of manganese slag disposal system | |
| CN109289667A (en) | Agitator tank in a kind of heavy metal-polluted soil lead zinc processing system | |
| CN107927864A (en) | A kind of water-cooled fermented feed processing cooling device | |
| CN206897224U (en) | A kind of new and effective pitch paying mixer | |
| CN109231552A (en) | Sewage-treatment plant in a kind of more milk with probiotics production | |
| CN207591724U (en) | A kind of vertical mixing tank | |
| CN109317034A (en) | One kind is for nutrient solution mixing arrangement in camplotheca acuminata plantation | |
| CN109225026A (en) | A kind of high salt equipment for treating water from mine | |
| CN109173892A (en) | A kind of underground engineering wastewater treatment equipment | |
| CN212189059U (en) | Kettle type stirring reactor | |
| CN109277016A (en) | A kind of control system of subway engineering construction wastewater treatment equipment | |
| CN109231551A (en) | A kind of lake water pollution sludge handling device | |
| CN109231386A (en) | A kind of distributed countryside sewage treatment equipment in remote districts | |
| CN219559428U (en) | Mixing device for electrolyte production | |
| CN215428988U (en) | Chemical polymerization kettle with automatic feeding device | |
| CN219441675U (en) | High-efficient reation kettle | |
| CN109231553A (en) | A kind of small watershed heavy metal pollution of water body emergency treatment device | |
| CN219922903U (en) | Bulk drug reation kettle suitable for alkylation reaction | |
| CN109250843A (en) | Sewage-treatment plant in a kind of alcohol production process | |
| CN212925041U (en) | High protein type biological feed control by temperature change fermenting installation |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| CB02 | Change of applicant information |
Address after: 221000 Science and Technology Park of Xuzhou University of Engineering, No. 18 South Third Ring Road, Quanshan District, Xuzhou City, Jiangsu Province (Xuzhou 2.5 Industrial Park) Applicant after: XUZHOU University OF TECHNOLOGY Address before: 221000 University Science Park, Xuzhou Institute of Engineering, No. 18 South Third Ring Road, Quanshan District, Xuzhou City, Jiangsu Province Applicant before: XUZHOU University OF TECHNOLOGY |
|
| CB02 | Change of applicant information | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190212 |
|
| WW01 | Invention patent application withdrawn after publication |