CN109304137A - A kind of precipitation reactor producing organic matter processing catalyst - Google Patents
A kind of precipitation reactor producing organic matter processing catalyst Download PDFInfo
- Publication number
- CN109304137A CN109304137A CN201710623771.XA CN201710623771A CN109304137A CN 109304137 A CN109304137 A CN 109304137A CN 201710623771 A CN201710623771 A CN 201710623771A CN 109304137 A CN109304137 A CN 109304137A
- Authority
- CN
- China
- Prior art keywords
- middle shaft
- tank body
- organic matter
- producing organic
- matter processing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000001556 precipitation Methods 0.000 title claims abstract description 22
- 239000003054 catalyst Substances 0.000 title claims abstract description 15
- 239000005416 organic matter Substances 0.000 title claims abstract description 13
- 238000012545 processing Methods 0.000 title claims abstract description 13
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000012360 testing method Methods 0.000 claims description 10
- 238000007789 sealing Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 abstract description 8
- 238000000034 method Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 4
- 230000001376 precipitating effect Effects 0.000 description 4
- 230000032683 aging Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 239000000872 buffer Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
Abstract
The present invention relates to a kind of precipitation reactors for producing organic matter processing catalyst, including motor, tank body, top cover, middle shaft, bracket and pedestal, descaler is additionally provided in the tank body, the descaler is horizontally installed in middle shaft and rotates with middle shaft, free end is contacted with inner tank wall simultaneously, rotation temperature control shield is enclosed on the outside of the tank wall, the rotation temperature control shield is connected to middle shaft by symmetrically arranged two connecting rods and can rotate with middle shaft around tank body；With homogeneous heating, the temperature difference in tank is effectively eliminated, cleans the high feature of degree.
Description
Technical field
The invention belongs to catalyst production equipment fields, and in particular to a kind of precipitating for producing organic matter processing catalyst is anti-
Answer device.
Background technique
The catalyst precipitation method need to often be carried out when producing with metallic salt and precipitating reagent in precipitation reactor, in order to ideal
In precipitation process material must protect to certain temperature, and be stirred continuously for precipitation particles, guarantee mixing, be uniformly dispersed.Precipitating
Operation is mostly intermittent.Feed way can be the method for fractional steps or cocurrent process, if several strands of materials enter band stirring simultaneously with cocurrent process
Plastic cans, continuous operation, subsequently into ageing can, the material of certain volume to be collected into, after certain temperature, time aging
Enter back into next process, ageing can intermittently operated.
Precipitation reactor has to meet process requirement, and convenient for operation, heating is convenient, well-ventilated, while can use at any time
The variation of solution colour in precipitation process, colloid consistency is visually observed, convenient for the measurement etc. of pH value.Intermittence precipitation reaction at present
There is heating unevenness in device, be easy occur the case where apparent temperature difference in the reactor, while material is easy to generate because of the temperature difference and " hang
Wall " phenomenon generates a large amount of residual in reactor wall, it is difficult to it clears up, and disadvantages mentioned above, it will have a direct impact on the catalysis produced
The performance and homogeneous degree of agent, greatly reduce the quality of product, while also improving maintenance cost.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of homogeneous heating, the temperature difference in tank can be eliminated, and is set
There is descaler to carry out the precipitation reactor of the production organic matter processing catalyst of secondary in tank.
The technical scheme adopted by the invention is as follows:
A kind of precipitation reactor producing organic matter processing catalyst, including motor, tank body, top cover, middle shaft, bracket and bottom
Seat, the motor are installed on middle shaft and stretch out top cover upper end, population and inlet tube are provided on the top cover, the middle shaft is perpendicular
Straight setting, for transfer axle position in the intracorporal part of tank, middle is equipped with horizontally disposed blender, sets at the middle shaft lower end
It is equipped with the discharge port of tank body, the branch is placed on tank body lower part, and is fixed on pedestal, it is additionally provided with descaler in the tank body,
The descaler is horizontally installed in middle shaft and rotates with middle shaft, while free end is contacted with inner tank wall, the tank body
Side-wall outer side is enclosed with rotation temperature control shield, and the rotation temperature control shield is connected to middle shaft simultaneously by symmetrically arranged two connecting rods
It can be rotated with middle shaft around tank body.
As further improved technical solution, the top cover and tank body closure joint are equipped with sealing ring.
As further improved technical solution, the test bar for protruding into tank interior, the inspection are provided at the population
Surveying stick point, there are two the detectors for testing ph value and temperature respectively.
As further improved technical solution, the connecting rod and rotation temperature control shield junction are equipped with cushion collar.
As further improved technical solution, the connecting rod and transfer shaft connection place are equipped with axle sleeve.
Advantageous effects of the invention are as follows:
The present invention provides a kind of homogeneous heatings, can eliminate the temperature difference in pipe, and are equipped with descaler and carry out secondary in tank
Production organic matter processing catalyst precipitation reactor.
(1) using rotation temperature control shield, so as to guarantee that the degree of heat in reactor is identical, that is, it can guarantee that heating is equal
It is even, effectively eliminate the temperature difference in reactor, it is therefore prevented that " wall built-up " phenomenon of material reaction, heating effect is more preferable, material reaction
More preferably.
(2) it is equipped with descaler, further solves the problem of precipitation reactor bottom is easy residual reactants, is realized clear
Clean production, easy to maintenance, simple rinse can keep the clean of reactor wall, reduce manual cleaning and maintenance at
This.
(3) structure is simple, easy to use, entire precipitation reactor it is highly-safe, design rationally, it is functional.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is overlooking structure diagram of the invention；
Appended drawing reference: 1, motor；2, tank body；3, top cover；4, middle shaft；5, sealing ring；6, population；7, discharge port；8, pedestal；9,
Bracket；10, temperature control shield is rotated；11, connecting rod；12, inlet tube；13, blender；14, descaler；15, test bar；16, it buffers
Set；17, axle sleeve.
Specific embodiment
The invention will be further elaborated with reference to the accompanying drawings and detailed description.
A kind of precipitation reactor for producing organic matter processing catalyst as shown in the figure, including motor 1, tank body 2, top cover 3,
Middle shaft 4, bracket 9 and pedestal 8, the motor 1 are installed on middle shaft 4 and stretch out 3 upper end of top cover, and someone is arranged on the top cover 3
Mouth 6 and inlet tube 12, the middle shaft 4 are vertically arranged, and middle shaft 4 is located at the part in tank body 2, and middle is equipped with level
The blender 13 of setting, the discharge port 7 of tank body 2 is provided at middle 4 lower end of shaft, and the bracket 9 is placed under tank body 2
Portion, and be fixed on pedestal 8, descaler 14 is additionally provided in the tank body 2, the descaler 14 is horizontally installed in middle shaft 4
And rotated with middle shaft 4, while free end is contacted with 2 inner wall of tank body, 2 side-wall outer side of tank body is enclosed with rotation temperature control shield
10, the rotation temperature control shield 10 is connected to middle shaft 4 by symmetrically arranged two connecting rods 11 and can surround with middle shaft 4
Tank body 2 rotates.
The top cover 3 is closed joint with tank body 2 and is equipped with sealing ring 5.
It is provided with the test bar 15 protruded into inside tank body 2 at the population 6, the test bar 15 divides that there are two test respectively
The detector of ph value and temperature.
The connecting rod 11 is equipped with cushion collar 16 with rotation 10 junction of temperature control shield.
The connecting rod 11 is equipped with axle sleeve 17 with middle 4 junction of shaft.
In use, shaft 4 and external rotation temperature control shield 10 rotate in the drive of motor 1, rotation temperature control shield 10 is as needed
It adjusts suitable temperature to heat inside reactor, material enters in precipitation reactor from inlet tube 12 to be reacted, together
When the situation in reactor can be monitored by test bar 15 and population 6, to adjust the temperature etc. of heating, bottom in real time
The descaler 14 in portion effectively prevents due to gravity there are also caused by flow gradients, and reactor bottom precipitating ensure that it
Good spatter property and reactivity worth.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art
Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (5)
1. a kind of precipitation reactor for producing organic matter processing catalyst, including motor (1), tank body (2), top cover (3), middle shaft
(4), bracket (9) and pedestal (8), the motor (1) is installed on middle shaft (4) and stretches out top cover (3) upper end, on the top cover (3)
It is provided with population (6) and inlet tube (12), the middle shaft (4) is vertically arranged, and middle shaft (4) is located at the part in tank body (2),
Middle is equipped with horizontally disposed blender (13), and the discharge port (7) of tank body (2) is provided at middle shaft (4) lower end,
The bracket (9) is placed in tank body (2) lower part, and is fixed on pedestal (8), which is characterized in that is additionally provided with and removes in the tank body (2)
Dirty device (14), the descaler (14) is horizontally installed on middle shaft (4) and rotates with middle shaft (4), while free end and tank
The contact of body (2) inner wall, tank body (2) side-wall outer side are enclosed with rotation temperature control shield (10), and the rotation temperature control shield (10) passes through
Symmetrically arranged two connecting rods (11) are connected to middle shaft (4) and can rotate with middle shaft (4) around tank body (2).
2. a kind of precipitation reactor for producing organic matter processing catalyst according to claim 1, which is characterized in that described
Top cover (3) and tank body (2) closure joint are equipped with sealing ring (5).
3. a kind of precipitation reactor for producing organic matter processing catalyst according to claim 1, which is characterized in that described
It is provided at population (6) and protrudes into the internal test bar (15) of tank body (2), there are two test ph value respectively for the test bar (15) point
With the detector of temperature.
4. a kind of precipitation reactor for producing organic matter processing catalyst according to claim 1, which is characterized in that described
Connecting rod (11) and rotation temperature control shield junction are equipped with cushion collar (16).
5. a kind of precipitation reactor for producing organic matter processing catalyst according to claim 4, which is characterized in that described
Connecting rod (11) and middle shaft (4) junction are equipped with axle sleeve (17).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710623771.XA CN109304137A (en) | 2017-07-27 | 2017-07-27 | A kind of precipitation reactor producing organic matter processing catalyst |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710623771.XA CN109304137A (en) | 2017-07-27 | 2017-07-27 | A kind of precipitation reactor producing organic matter processing catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109304137A true CN109304137A (en) | 2019-02-05 |
Family
ID=65202644
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710623771.XA Pending CN109304137A (en) | 2017-07-27 | 2017-07-27 | A kind of precipitation reactor producing organic matter processing catalyst |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109304137A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110078252A (en) * | 2019-04-16 | 2019-08-02 | 无锡泽邦环保科技有限公司 | A kind of efficient air-floating precipitating integrated device |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103801282A (en) * | 2012-11-12 | 2014-05-21 | 中国科学院大连化学物理研究所 | Solid base catalyst as well as preparation and application thereof |
| CN203971943U (en) * | 2014-07-30 | 2014-12-03 | 杭州凯斯特化工有限公司 | Reactor |
| CN204214146U (en) * | 2014-08-28 | 2015-03-18 | 杭州协红科技咨询有限公司 | A kind of heater of rotary moveable formula liquid reserve tank |
| CN204519282U (en) * | 2015-04-12 | 2015-08-05 | 阮霞伟 | A kind of stir-fry Chinese chestnut baking machine |
| CN204888613U (en) * | 2015-08-23 | 2015-12-23 | 安溪县贤彩茶叶机械有限公司 | Environmental protection tea roasting machine |
| CN105413214A (en) * | 2016-01-11 | 2016-03-23 | 宜诺珐玛（天津）科技有限公司 | Segmented high-concentration falling film concentrating device |
| CN205300231U (en) * | 2016-01-18 | 2016-06-08 | 山东鑫海科技股份有限公司 | High -efficient centrifugal nickel powder heavily melts electric kiln |
| CN207085915U (en) * | 2017-07-27 | 2018-03-13 | 南京威安新材料科技有限公司 | A kind of precipitation reactor for producing organic matter processing catalyst |
-
2017
- 2017-07-27 CN CN201710623771.XA patent/CN109304137A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103801282A (en) * | 2012-11-12 | 2014-05-21 | 中国科学院大连化学物理研究所 | Solid base catalyst as well as preparation and application thereof |
| CN203971943U (en) * | 2014-07-30 | 2014-12-03 | 杭州凯斯特化工有限公司 | Reactor |
| CN204214146U (en) * | 2014-08-28 | 2015-03-18 | 杭州协红科技咨询有限公司 | A kind of heater of rotary moveable formula liquid reserve tank |
| CN204519282U (en) * | 2015-04-12 | 2015-08-05 | 阮霞伟 | A kind of stir-fry Chinese chestnut baking machine |
| CN204888613U (en) * | 2015-08-23 | 2015-12-23 | 安溪县贤彩茶叶机械有限公司 | Environmental protection tea roasting machine |
| CN105413214A (en) * | 2016-01-11 | 2016-03-23 | 宜诺珐玛（天津）科技有限公司 | Segmented high-concentration falling film concentrating device |
| CN205300231U (en) * | 2016-01-18 | 2016-06-08 | 山东鑫海科技股份有限公司 | High -efficient centrifugal nickel powder heavily melts electric kiln |
| CN207085915U (en) * | 2017-07-27 | 2018-03-13 | 南京威安新材料科技有限公司 | A kind of precipitation reactor for producing organic matter processing catalyst |
Non-Patent Citations (1)
| Title |
|---|
| 成都科技大学等: "《化工轻工设备机械基础》", 成都：成都科技大学出版社, pages: 358 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110078252A (en) * | 2019-04-16 | 2019-08-02 | 无锡泽邦环保科技有限公司 | A kind of efficient air-floating precipitating integrated device |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN205914110U (en) | Novel high -efficient fluid reservoir that mixes | |
| CN204522975U (en) | A kind of device for raw material generation chemical reaction | |
| CN109304137A (en) | A kind of precipitation reactor producing organic matter processing catalyst | |
| CN206308352U (en) | A kind of new terramycin fermentation tank | |
| CN207085915U (en) | A kind of precipitation reactor for producing organic matter processing catalyst | |
| CN206255450U (en) | A kind of storage tank for paint production | |
| CN208340561U (en) | New coating production line | |
| CN208194218U (en) | A kind of accelerator stirred tank of band automation Dropping feeder | |
| CN206604487U (en) | A kind of novel furan production of resins reactor | |
| CN207941530U (en) | A kind of reaction kettle for m-phthaloyl chloride production | |
| CN107384747A (en) | A kind of reactor with flexible rabbling mechanism | |
| CN205269630U (en) | Chemical reaction tank | |
| CN205042480U (en) | Chemical synthesis device | |
| CN203830009U (en) | Reaction kettle | |
| CN208928141U (en) | A kind of Chemical Manufacture stirred tank reactor convenient for removal of impurities | |
| CN1623691B (en) | Washing apparatus for sealed container and it cleaning process | |
| CN218296738U (en) | Novel mechanism for automatic quantitative feeding of ferrous chloride cracking furnace | |
| CN208928150U (en) | A kind of synthesis rosin resin reaction kettle | |
| US20030007911A1 (en) | Hydrophobic silica system | |
| CN209501672U (en) | A kind of novel rearrangement reaction kettle | |
| CN211800197U (en) | Chemical raw material stirring device | |
| CN207336132U (en) | A kind of sampler | |
| CN210206764U (en) | Coating reaction device | |
| CN219964885U (en) | Solid-liquid reaction kettle | |
| CN207143225U (en) | A kind of reactor for preventing biology enzyme to be lost in |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |