CN109279571A - A kind of hydrophobic surface micro-structure and preparation method - Google Patents
A kind of hydrophobic surface micro-structure and preparation method Download PDFInfo
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- CN109279571A CN109279571A CN201811093202.XA CN201811093202A CN109279571A CN 109279571 A CN109279571 A CN 109279571A CN 201811093202 A CN201811093202 A CN 201811093202A CN 109279571 A CN109279571 A CN 109279571A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81C—PROCESSES OR APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OR TREATMENT OF MICROSTRUCTURAL DEVICES OR SYSTEMS
- B81C1/00—Manufacture or treatment of devices or systems in or on a substrate
- B81C1/00015—Manufacture or treatment of devices or systems in or on a substrate for manufacturing microsystems
- B81C1/00023—Manufacture or treatment of devices or systems in or on a substrate for manufacturing microsystems without movable or flexible elements
- B81C1/00111—Tips, pillars, i.e. raised structures
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23P—METAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
- B23P15/00—Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81B—MICROSTRUCTURAL DEVICES OR SYSTEMS, e.g. MICROMECHANICAL DEVICES
- B81B1/00—Devices without movable or flexible elements, e.g. microcapillary devices
- B81B1/006—Microdevices formed as a single homogeneous piece, i.e. wherein the mechanical function is obtained by the use of the device, e.g. cutters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81C—PROCESSES OR APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OR TREATMENT OF MICROSTRUCTURAL DEVICES OR SYSTEMS
- B81C1/00—Manufacture or treatment of devices or systems in or on a substrate
- B81C1/00436—Shaping materials, i.e. techniques for structuring the substrate or the layers on the substrate
- B81C1/00444—Surface micromachining, i.e. structuring layers on the substrate
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Abstract
The invention discloses a kind of hydrophobic surface micro-structure and preparation methods, comprising the following steps: step 1.1, cleans object to be processed surface;Step 1.2, skew wall array microstructure is processed in matrix surface using micro- milling process;Using five-axle linkage high speed microfabrication center, it is realized by horizontal, vertical both direction feed processing, i.e. respectively laterally and longitudinal milling with 30 ° of point of a knife angle V-shapeds engraving milling cutters and 60 ° of point of a knife angle V-types engraving milling cutters, the hydrophobic surface micro-structure can be obtained;Step 1.3, polishing object to be processed surface, and complete then to dry at further cleaning in polishing.Go out skew wall array type micro-structure as hydrophobic surface using the advantage fabrication design of micro-cutting technology, the hydrophobic surface shape for compensating for existing chemical method production is difficult to control, surface alignment it is difficult to predict, it is difficult to realize microstructure design, there is the defects of chemical element residual.
Description
Technical field
The present invention relates to a kind of in particular to a kind of hydrophobic surface micro-structure of material surface micro-structure and preparation methods, belong to
In the hydrophobic technical field of microfabrication lifting workpieces.
Background technique
Hydrophobic surface is because having automatically cleaning, drag reduction and the performances such as wear-resistant, in the fields such as liquid conveying, building, ship, clothes
There are boundless application prospect, the large-scale industrial application of hydrophobic surface, it will convenience is brought to people's production and living,
Very big power is created for human development.For example, most common pan of cooking in people's life, often does after meal, edible oil is all
Meeting legacy part is in pot.This causes very big difficulty to cleaning, and people is forced to clean using dish washing liquid.And dish washing liquid contains
There are many surfactants, these substances enter after body, intracorporal eubolism can be interfered, usually often in contact with dish washing liquid
People, the incidence of colorectal cancer is very high;Some businessmans do not allow perishable to guarantee dish washing liquid, can add formaldehyde as anti-corrosion yet
Agent, although eating a small amount of formaldehyde not will cause acute poisoning, long-time service just will appear severe stomachache, vomiting and stupor etc.
Symptom.If hydrophobic surface is applied to the bottom of a pan, this hidden danger can be solved using its oleophobic property, remove people easily
The bottom of a pan surface and oil contaminant.
Research shows that micrometer structure, the multiple-rank arrangement and low-surface-energy material collective effect of nanostructure composition can make material
There is hydrophobicity on material surface.And the method for having production hydrophobic surface includes chemical method, special process method, all there is larger limitation.
Although chemical method has high-efficient, easy realization, can obtain the micro-architecture surface of nanoscale, and may be implemented extensive
The advantages of production, but its surface shape be difficult to control, surface alignment it is difficult to predict, it is difficult to realize microstructure design;And it is extraordinary
The defects of it can only be metal that processing method, which then has rapidoprint, and process equipment is expensive, and machining accuracy is limited.And both are processed
Method all leaving there may be harmful chemical element, if being applied to pan bottom or living closely related production with people
Product, it will subtle harm is caused to human body.
Summary of the invention
Present invention is primarily aimed at provide a kind of hydrophobic surface micro-structure, preparation method and application to make up existing dredge
The deficiency of water surface, it is more preferable to promote material surface hydrophobicity.
To achieve the above objectives, the present invention devises a kind of skew wall array type surface micro-structure, including a base to the present invention
Body, the boss being arranged successively equipped with multiple along matrix longitudinal direction and laterally on the matrix, the cross section of the boss
For the square that area from top to bottom is gradually reduced, longitudinal section is isosceles trapezoid;And there is certain spacing between adjacent lands.
Further, the skew wall angle of the boss is 60 °~75 °.
As shown in figure 3, the height of the boss is 100 μm.
Further, the spacing of the boss is 100 μm.
Further, the width maximum of the boss is 75~150 μm.
Further, the contact angle of the skew wall array of boss (wear at gas, liquid, solid three-phase intersection point by made liquid-vapor interface tangent line
The angle between liquid and solid-liquid boundary line is crossed, is hydrophobic measurement index) increase as micro-structure spacing increases, with
Micro-structure boss (square column) width increase and reduce;And the presence of skew wall greatly reduces size on contact angle influence.
The preparation method of the hydrophobic surface micro-structure, comprising the following steps:
Step 1.1, object to be processed surface is cleaned, object to be processed is individually placed to be cleaned by ultrasonic one in acetone and ethyl alcohol
The section time;
Step 1.2, skew wall array microstructure is processed using micro- milling process;
Using five-axle linkage high speed microfabrication center, speed of mainshaft n=20000rpm, feed speed f=60mm/ are set
Min, axial cutting depth are ap=0.05mm, radial cutting depth are cutter diameter;Pass through horizontal, vertical both direction feed processing
It realizes, i.e., respectively laterally and longitudinal direction milling with 30 ° of point of a knife angle V-shapeds engraving milling cutters and 60 ° of point of a knife angle V-types engraving milling cutters,
The hydrophobic surface micro-structure can be obtained;
Step 1.3, polishing object to be processed surface,
Abrasive paper for metallograph number used is 800~1200 mesh, is later put the workpiece in workpiece to be machined in alcohol, in room temperature
It is lower to be cleaned by ultrasonic sample for a period of time with ultrasonic washing instrument;Finally, rinsing specimen surface with deionized water, at room temperature
Natural air drying.
In order to guarantee machining accuracy, model 2360-p, point of a knife angle is 60 ° for use 1, and point of a knife width is 0.02mm's
V-type carves milling cutter and 1 model 2330-p, and point of a knife angle is 30 °, and the V-type that point of a knife width is 0.02mm carves milling cutter.
The medicine have the advantages that
Go out skew wall array type micro-structure as hydrophobic surface using the advantage fabrication design of micro-cutting technology, compensates for existing
Chemical method production hydrophobic surface shape be difficult to control, surface alignment it is difficult to predict, it is difficult to realize microstructure design, there is chemistry
The defects of element remains.And special process method processing hydrophobic surface material can only be metal, process equipment is expensive, processing essence
The deficiencies of degree is limited.And preparation method is simple, low in cost, hydrophobic effect is significant, can be widely applied to close with human lives
Relevant product.
Surfaces of complex shape micro-structure can be accurately controlled using the skew wall array type hydrophobic surface that the present invention designs, wherein
The presence of skew wall structure will increase water droplet in the contact angle of micro-structure surface than other structures, and reduce microstructure size parameter pair
The influence of contact angle has the effect of highly significant to promotion material surface hydrophobicity.
Detailed description of the invention
The accompanying drawings constituting a part of this application is used to provide further understanding of the present application, and the application's shows
Meaning property embodiment and its explanation are not constituted an undue limitation on the present application for explaining the application.
Fig. 1, Fig. 2 are skew wall array microstructure schematic diagrames;
Fig. 3 is the microcosmic schematic diagram of hydrophobic surface;
Fig. 4, Fig. 5 are the observation schematic diagrames of contact angle.
Specific embodiment
It is noted that following detailed description is all illustrative, it is intended to provide further instruction to the application.Unless another
It indicates, all technical and scientific terms used herein has usual with the application person of an ordinary skill in the technical field
The identical meanings of understanding.
It should be noted that term used herein above is merely to describe specific embodiment, and be not intended to restricted root
According to the illustrative embodiments of the application.As used herein, unless the context clearly indicates otherwise, otherwise singular
Also it is intended to include plural form, additionally, it should be understood that, when in the present specification using term "comprising" and/or " packet
Include " when, indicate existing characteristics, step, operation, device, component and/or their combination;
As background technique is introduced, the method for having production hydrophobic surface includes chemical method, special process method, is all deposited
In larger limitation.Although chemical method has high-efficient, the easy micro-architecture surface realized, can obtain nanoscale, and can
With realize large-scale production the advantages of, but its surface shape be difficult to control, surface alignment it is difficult to predict, it is difficult to realize micro-structure
Design;And the defects of it can only be metal that special process method, which then has rapidoprint, and process equipment is expensive, and machining accuracy is limited.
And both processing methods all leaving there may be harmful chemical element, if being applied to pan bottom or living with people close
Cut relevant product, it will subtle harm is caused to human body, with the research of micro Process mechanism, turning, Milling Process
The raising of precision, milling cutter size are gradually reduced, and processing micron-scale micro-structure with micro-cutting method, to promote its hydrophobic
Property is possibly realized.It is high that there is machining accuracy using the hydrophobic surface that micro-cutting technology processes, and can accurately control complicated shape
The advantages that surface micro-structure shape, the Product Green processed is nuisanceless.
Have machining accuracy high using the skew wall groove microstructure that Investigation of Mechanical Micro-cutting Technology design processes, tries out material
Extensively, surfaces of complex shape microstructure aspects can be accurately controlled, the advantages that Product Green processed is nuisanceless.Compensate for existing dredge
The deficiency of water surface.And the skew wall groove microstructure designed based on Investigation of Mechanical Micro-cutting Technology is proved through experimental study, Neng Gou great
It is angle of the made gas-liquid interface tangent line across liquid and solid-liquid boundary line at gas, liquid, solid three-phase intersection point that width, which is promoted,
And then promote material surface hydrophobicity.
In a kind of typical embodiment of the application, as shown in Figure 1, the present invention devises a kind of skew wall array type surface
Micro-structure, including a matrix, the boss being arranged successively equipped with multiple along matrix longitudinal direction and laterally on the matrix, institute
The cross section for the boss stated is the square that area is gradually reduced from top to bottom, and longitudinal section is isosceles trapezoid;And adjacent lands
Between have certain spacing.
As shown in Fig. 2, the skew wall angle γ of boss is 60 °~75 °;Skew wall angle described here refers to the skew wall of boss
With the angle of bottom;Since the cross section of boss is the square that area is gradually reduced from top to bottom, side wall and bottom
An angle is formd, which is skew wall angle;Wherein the presence of skew wall structure will increase water droplet in micro- knot than other structures
The contact angle on structure surface, and reduce influence of the microstructure size parameter to contact angle, have very to material surface hydrophobicity is promoted
Significant effect.
As shown in Fig. 2, the height h of boss is 100 μm.
As shown in Figure 1, boss spacing b (spacing described here, which refers to, is formed by clearance distance between adjacent lands,
It is specific as shown in the figure) it is 100 μm.
As shown in Figure 1, the bottom width of boss is 75~150 μm.
As shown in figure 3, contact angle (the made liquid-vapor interface at gas, liquid, solid three-phase intersection point of the skew wall array of above-mentioned boss
Angle of the tangent line across liquid and solid-liquid boundary line, is hydrophobic measurement index) increase as micro-structure spacing increases
Greatly, reduce as micro-structure boss (square column) width increases;And the presence of skew wall subtracts size significantly on contact angle influence
It is small.
Micro- Milling Process technology used in the present invention can be completed on microfabrication center.
Below with reference to experiment embodiment, the present invention is further described.
1. Preparatory work of experiment
(1) selection: the selection of material is that rapidoprint is PMMA (acrylic).PMMA has preferable mechanical performance, normal
Under temperature, hardness is higher, has biggish tension, resistance to compression, counter-bending and impact strength, in addition there are preferable wear-resisting properties.
PMMA also has good moulding process, very easily can process various shape by the methods of injection molding, thermoforming.This
Outside, there are also good suitability for secondary processing by PMMA, therefore can guarantee its accurate machining accuracy by micro- milling, to reduce
The factors such as mismachining tolerance or surface defect are influenced caused by contact angle.
(2) laboratory apparatus: micro-structure machining experiment is completed on KERN-2522 five-axle linkage high speed microfabrication center
's.The maximum speed of the machining center is 50000rpm, and Workpiece Machining Accuracy is ± 2.5 μm, equipped with laser tool setting gauge, is used
Digital control system be HEIDENHAIN ITNC 530.
2. design processing skew wall array surface micro-structure, the factors pair such as research square column (boss) width, spacing, skew wall angle
The influence of contact angle.Microstructure size is determined according to tool dimension, machine finish, expectancy theory research size, micro- knot
Structure dimensional parameters are as follows:
Skew wall array microstructure dimensional parameters:
Skew wall array microstructure sample designs 8 groups altogether.Boss bottom width is 75 μm, 100 μm, 125 μm, 150 μm, spacing
It is 100 μm, skew wall angle is respectively 60 ° and 75 °.
3. processing skew wall array.
Skew wall array microstructure is by horizontal, vertical both direction feed processing realization, the main cutting that setting micro-structure is processed
Parameter are as follows: speed of mainshaft n=20000rpm, feed speed f=60mm/min, axial cutting depth is with ap=0.05mm, it is radial
Cutting depth is cutter diameter.With 30 ° of point of a knife angle V-shaped engraving milling cutters and 60 ° of point of a knife angle V-type engraving milling cutter laterally longitudinal millings
It cuts, the structure of design can be obtained.In order to guarantee that the V-type that point of a knife angle is 60 ° is carved milling cutter and 1 knife by machining accuracy, use 1
The V-type that wedge angle degree is 30 ° carves the sample that milling cutter processes design.Such as attached drawing 1.
4.PMMA sample can generate a large amount of burrs in process, after processing is completed, need to carry out unhairing to specimen surface
Thorn processing, to eliminate influence of the burr to contact angle.Firstly, the light brush workpiece surface of ultra-fine hairbrush for being 0.05mm with diameter, goes
Except most of burrs.Then, it puts the workpiece in alcohol, at room temperature with the ultrasonic cleaning examination of KX-1620TR ultrasonic washing instrument
Sample 30 minutes.Finally, rinsing specimen surface, under room temperature natural air drying with deionized water.
5. being obtained after analysis using the contact angle on contact angle measurement measurement different parameters lower sloped walls array microstructure surface
Conclusion: square column array microstructure can make water droplet its surface contact angle increase, contact angle with micro-structure spacing increase and
Increase, reduces as boss (square column) width increases.The presence of skew wall structure will increase water droplet in the contact of micro-structure surface
Angle, in addition, the presence of skew wall makes microstructure size parameter influence to reduce on contact angle.
The above method can be also used for the hydrophobic structure of preparation other structures.
Above-mentioned, although the foregoing specific embodiments of the present invention is described with reference to the accompanying drawings, not protects model to the present invention
The limitation enclosed, those skilled in the art should understand that, based on the technical solutions of the present invention, those skilled in the art are not
Need to make the creative labor the various modifications or changes that can be made still within protection scope of the present invention.
Claims (10)
1. a kind of preparation method of hydrophobic surface micro-structure, which comprises the following steps:
Step 1.1, object to be processed surface is cleaned;
Step 1.2, skew wall array microstructure is processed in matrix surface using micro- milling process;
Using five-axle linkage high speed microfabrication center, realized by horizontal, vertical both direction feed processing, i.e., with 30 ° of nose angles
It spends V-shaped engraving milling cutter and 60 ° of point of a knife angle V-types engraving milling cutters respectively laterally and longitudinal milling, can be obtained described hydrophobic
Surface micro-structure;
Step 1.3, polishing object to be processed surface, and complete then to dry at further cleaning in polishing.
2. a kind of preparation method of hydrophobic surface micro-structure as described in claim 1, which is characterized in that in step 1.1, cleaning
Point mode is to be individually placed to object to be processed to be cleaned by ultrasonic a period of time in acetone and ethyl alcohol.
3. a kind of preparation method of hydrophobic surface micro-structure as described in claim 1, which is characterized in that in step 1.3: used
Abrasive paper for metallograph polishes to processing object surface, later puts the workpiece in workpiece to be machined in alcohol, at room temperature with super
Sound wave cleaning device is cleaned by ultrasonic sample for a period of time;Finally, rinsing specimen surface, at room temperature natural wind with deionized water
It is dry.
4. a kind of preparation method of hydrophobic surface micro-structure as described in claim 1, which is characterized in that in step 1.2
Using 1 model 2360-p, point of a knife angle is 60 °, and the V-type that point of a knife width is 0.02mm carves milling cutter and 1 model
For 2330-p, point of a knife angle is 30 °, and the V-type that point of a knife width is 0.02mm carves milling cutter.
5. a kind of hydrophobic surface micro-structure is made using any preparation method of claim 7-8.
6. hydrophobic surface micro-structure as claimed in claim 5, which is characterized in that it is skew wall array type hydrophobic surface micro-structure,
It includes a matrix, the boss being arranged successively equipped with multiple along matrix longitudinal direction and laterally on the matrix, described
The cross section of boss is the square that area is gradually reduced from top to bottom, and longitudinal section is isosceles trapezoid;And between adjacent lands
There is certain spacing.
7. hydrophobic surface micro-structure as claimed in claim 5, which is characterized in that the skew wall angle of the boss be 60 °~
75°。
8. hydrophobic surface micro-structure as claimed in claim 5, which is characterized in that the height of the boss is 100 μm;It is described
The spacing of boss is 100 μm.
9. hydrophobic surface micro-structure as claimed in claim 5, which is characterized in that the width of the boss is 75~150 μm.
10. hydrophobic surface micro-structure as claimed in claim 5, which is characterized in that the contact angle of the skew wall array of boss with
Micro-structure spacing increases and increases, and reduces as micro-structure projection width increases;And the presence of skew wall makes size to contact
Angle influences to greatly reduce.
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CN110318902A (en) * | 2019-04-23 | 2019-10-11 | 天津大学 | Hydrophobic type cylinder jacket outer surface structure and hydrophobic type cylinder jacket |
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Application publication date: 20190129 |