CN109275972A - Nana intelligent element fabric health clothing - Google Patents
Nana intelligent element fabric health clothing Download PDFInfo
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- CN109275972A CN109275972A CN201811112308.XA CN201811112308A CN109275972A CN 109275972 A CN109275972 A CN 109275972A CN 201811112308 A CN201811112308 A CN 201811112308A CN 109275972 A CN109275972 A CN 109275972A
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D2400/00—Functions or special features of garments
- A41D2400/10—Heat retention or warming
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D2400/00—Functions or special features of garments
- A41D2400/32—Therapeutic use
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- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of nana intelligent element fabric health clothings.It is to belong to intelligent health-care and take fabric to weave production technical field.It is the ceramic nano powder for dissolving out release element negative ion far-infrared drug abuse filter poison naturally by the natural ore element, intelligent phase-changing and temperature-regulating fiber capsule of nano composite material nanometer powder, anti electromagnetic wave magnetic therapy gram mite antibacterial anti-infection composite fibre ceramic nano powder, water repellent moisture-inhibiting temperature regulate and control light guide induction composite fibre ceramic nano powder composition.This intelligent health-care clothes be it is a kind of can automatically according to collaterals of human, acupuncture point, Pi Wen, painful area resistance value, heart rate, blood pressure etc. variation and discharging dissolution automatically has effects that various elements, anion necessary to the human body of special treatment, vitamin, protein, amino acid, multiple active enzymes, ferment etc. reach collection warming, intelligent thermoregulating, water repellent moisture-inhibiting, take drugs filter poison, gram mite antibacterial, physical therapy, protection, efficiency health-care are in integrated novel nano intelligence element fabric health clothing.
Description
Technical field
The invention discloses a kind of nana intelligent element fabric health clothings.It is to belong to intelligent health-care and take fabric to weave life
Produce technical field.
Background technique
Nana intelligent element fabric health clothing be it is a kind of can be automatically according to collaterals of human, acupuncture point, Pi Wen, painful area
The variation of resistance value, heart rate, blood pressure etc. and discharging dissolution automatically has effects that the natural superfine of special treatment micro- mineral element fibre
Nanoparticle is tieed up, partial size is in 0.1-0.5um particle refinement below in fabric.And these element fibers all have
Effect with fortune charge-site.Firmly can adsorb natural mineral element and cellulose macromolecule to be made has centainly securely
Property and persistent effect element fiber.The modes such as this percutaneous skin temperature of element fiber and successive friction are constantly released
Various elements, anion, vitamin, protein, amino acid, multiple active enzymes, ferment necessary to dissolution human body etc. is put to reach
Collection is warming, protects, is beautiful, and physical therapy, health-care efficacy are in the novel intelligent element fabric health clothing of one.It concentrates current material
Material is learned, microcirculation in human body medicine, microelement medicine, cytology, preventive medicine, life science, Intellectual garment, biology, far infrared
The scientific achievement of a variety of scientific domains such as magnetic therapy.
Summary of the invention
The purpose of the present invention is to provide a kind of nana intelligent element fabric health clothings.
The technical solution of the invention is as follows:
1, a kind of nana intelligent element fabric health clothing, it is characterized in that the natural ore element dissolves out release member naturally
Plain negative ion far-infrared, which is taken drugs, filters malicious ceramic nano powder by following quality proportioning composition %
SiO 2-ceramic nano powder 2-6；Titanium dioxide ceramic nano powder 2-6；
Iron oxide ceramics nano powder 2-6；Aluminium oxide ceramics nano powder 2-6；
Chinese medicine stone ceramic nano powder 2-6；Zeolite ceramic nano powder 2-6；
Tourmaline ceramic nano powder 4-12；
Di-iron trioxide Fe2O3 ceramic nano powder 2-6；
Ferroso-ferric oxide Fe3O4 ceramic nano powder 3-9；
Poly- phthalein amine -6(PA6) add to 100.
The preparation method mechanism of action:
By formula by above-mentioned natural crystal raw material, through crushing, mixing, sieving in sintering, the heat preservation 1-by 1200-1400 DEG C
3h, then superfine 2200-2400 mesh of mistake is regrinded in quenching, and nano powder of the partial size at 0.05-5 μm is just made, and there is dissolution to release
It puts element anion and takes drugs and filter malicious anti-electromagnetic wave pollution, and have that magnetotherapy effect is radiation infrared to go deep into subcutaneous 3-5cm, give
Human body cell vigor is given, is promoted blood circulation, is improved the immunity of the human body, the far-infrared ceramic nanometer with higher health-benefiting
Powder, with the compound obtained compound of poly- phthalein amine -6, it is a kind of far-infrared health care function element fabric of yarn.It is this
Element fiber mystery effect is that human body microelement-supplementing and have good adsorption function.Containing a large amount of more in element fiber
Kind the essential trace elements of the human body, these microelements can be used as the warehouse of needed by human body trace-element anion far infrared, shape
At trace-element anion far infrared storage source, the trace-element anion far infrared of needed by human body is replenished in time, adjusts human body
Balance.Element in element fiber is penetrated into body by pore, absorbs ambient enviroment and people by direct contact with the skin
The energy of body itself radiation, accelerates blood circulation, telangiectasis, the self-disciplining movement of circulation, so as to improve microcirculation,
Promote normal metabolism and physiological function, excludes at any time various caused by microcirculation is unsmooth and the intracorporal toxin of people
Illness.
2, a kind of nana intelligent element fabric health clothing, it is characterized in that: the intelligence phase-changing and temperature-regulating fiber nanometer is micro-
Capsule method composite material ceramic nano powder forms % by following quality proportioning
Inorganic wall material has calcium silicates 2-6；Nano silver antimicrobials 2-6；
Positive 12 eicosane 2-6；Positive 15 docosane 2-6；
Paraffin 2-6；Natural cocoa butter fat acid blend 2-6；
Polycaprolactone glycol PEL 2-6；Shape memory polyurethane/TiO2-SiO22—6；
One or more of bisphenol-A, Lauxite, polyurethane, fragrant adoption peptamine add to 100.
Preparation method and the mechanism of action:
Nana intelligent textile may be by nano material and obtain intelligence, it is also possible to by intelligent fiber or arrange acquisition
Intelligence.
Nano capsule is a kind of small " container " with the capsule heart, and the diameter of Nano capsule is usually at 1 μm or less.Due to receiving
The performances such as the slow release of rice glue capsule and targeting are superior to microcapsules, have been used for field of medicaments.The partial size of Nano capsule is small, compares table
Area is big, can be preferably compound with high polymer material, and the application field of Nano capsule is widened constantly in recent years.Phase transformation material
Nano capsule is expected other than having the advantages that general Nano capsule, also has the function of that intelligence adjusts temperature, can be used for temperature adjustment fibre
Dimension field.
Nano capsule is prepared using mini-emulsion polymerization mode, the stable drop constituted with sub-micron (50-500nm) drop
Dispersion is known as miniemulsion, and corresponding drop claims core polymerization to be known as mini-emulsion polymerization.In compound emulsifying agent (such as hexadecanol and ten
Sodium dialkyl sulfate) under collective effect, droplet nucleation becomes emulsion polymerization major way.
In miniemulsion, the key that submicron droplets are stabilized is to incorporate the chemical combination of a small amount of high hydrophobicity in dispersed phase
Object, also known as co-stabilizer or co-stabilizer.In essence, their effect is to generate osmotic pressure, and on-surface-active.
The main component of miniemulsion has: continuous phase (water), dispersed phase (oil or monomer), emulsifier and co-stabilizer；When it is used to polymerize
When, it further include the other components such as initiator, relative nonlinear error.Miniemulsion is thermodynamics meta-stable system, cannot be certainly
Hair is formed, it is necessary to be overcome oily phase cohesive energy by mechanical work and be formed the surface energy of drop, be allowed to be dispersed in water.Due to dispersion
Low efficiency must use high-intensitive homogenizer when dispersion prepares sub-micron miniemulsion.
The preparation of miniemulsion generally includes three steps: 1. emulsifier (is soluble in the aqueous phase, co-stabilizer is dissolved in list by pre-emulsification
Body)；2. emulsification (mixes above-mentioned solution, be uniformly mixed by mechanical stirring)；3. (said mixture passes through fine crankshaft
The homogenization of efficient homogenizer, is dispersed into sub-micron monomer droplet for monomer).
In order to avoid homogenization destroys polymer particle, mini-emulsion polymerization is often divided to fine crankshaft and two stages of polymerization,
Polymerization stage, system only need lower be stirred.
Specific capsule of nano preparation:
It selects fusing point for 35 DEG C of paraffin, prepares paraffin solution A 35 DEG C of environment temperature or more (guarantee paraffin is liquid), with wall
The mass ratio of material bisphenol-A is 2:10, and the A for adding emulsifier SPAN80 to be dissolved in formation 4:1:10 in toluene solution a small amount of bisphenol-A is molten
Minute quantity curing agent and core material solution are mixed to form B solution, solution A are slowly added to mix and be stirred with B solution by liquid
(800r/min), tentatively generation microcapsules reduce mixing speed after 1-2min to 400r/min or so, foot are added into reaction pot
It measures curing agent (wall material: curing agent=10:1), and improves mixing speed to 900r/min, phase-change microcapsule is formed after 20-30min.
At this moment TWEEN80 is added into reaction pot to be separated unreacted monomer repeatedly, is taken away upper layer impurity with extracting device, most
After can add 1%-1.5% normal saline solution auxiliary purification microcapsules.
3, a kind of nana intelligent element fabric health clothing, it is characterized in that: the anti electromagnetic wave magnetic therapy gram mite antibacterial is anti-
Composite fibre Cypress ethereal oil ceramic nano powder is infected, forms % by following quality proportioning
Permanent magnet nano powder 2-6；Ferroso-ferric oxide Fe3O42—6；
Chitin nano powder 2-6；Chitosan nano rice flour 2-6；
Natural kawo fiber 2-6；Polylactic acid 2-6；
Enuatrol SD 2-6；Polyethylene glycol PEG 2-6；
Polyaniline PANI 2-6；Polypyrrole PPy 2-6；
Poly-vinyl alcohol solution adds to 100.
The preparation of magnetic polymer nana intelligent textile:
Magnetic nanoparticle is added in high polymer fibre matrix, obtained magnetic nano composite fibre shows unique magnetic
Property region dependence, can be used for manufacturing the protective garment of intelligent fiber and military front line staff, it can also be used in terms of healthy medical care.This
Outside, magnetic infiltration, sensor, electronic device, information storage, magnetic imaging, static low frequency magnetic screen and magnetic induction magnetic photon
Also there is potential application value in equipment.By the way that Fe is added in poly-vinyl alcohol solution3O4Fluid, preparation disperse more uniform magnetic
Property nano-composite fiber, and arrange fiber alignment by externally-applied magnetic field, be prepared for that uniformity is preferable, magnetic good Nanowire
Dimension.
Nanometer Fe is prepared for titration Hydrolyze method3O4Particle, by selecting suitable dispersing agent and using ultrasonic wave dispersion
Method prepares the preferable water-based magnetic fluid of stability in gravitational field and magnetic field.With Electrospinning, it is with polyvinyl alcohol
Raw material is produced containing Fe3O4(diameter is in 100-300nm ranges) polyvinyl alcohol nano of magnetic nanoparticle.
4, a kind of nana intelligent element fabric health clothing, it is characterized in that: the water repellent moisture-inhibiting temperature regulates and controls light guide sense
Physical therapy composite fibre ceramic nano powder is answered, forms % by following quality proportioning
Shape Memory Polymer SMP 2-6；Aqueous inorganic salts 2-6；
Long chain hydrocarbon 2-6；Polyethylene glycol 2-6；
Glass optical fiber 2-6；Fatty acid 2-6；
Silica fibre 2-6；Neoprene 2-6；
Polyvinyl chloride 2-6；Polyurethane 2-6；
Acrylic acid 2-6；Zirconium carbide adds to 100.
The intelligent clothing first has to rely on intelligentized textile material as main body, these intelligentized textile materials are logical
Often with there are the functions such as induction, memory, adjusting, transmission and storage, and adaptability can be made according to the variation of environment and human body
Adjustment and reaction, to reach the scheduled design effect of intelligent clothing.
1. shape memory fiber and fabric.This fiber mainly mode of foundation thermoforming and cooling and shaping is formed.
When temperature of the peripheral temperature close to original thermoforming, shape memory fiber has the effect of restoring original form.It grinds for the first period
Study carefully and using it is most common be nickel alloy fiber, it is primarily processed to the coil spring shape of Pagoda-shaped, is further processed into
It is planar, it is then fixed in the interlayer of fabric.This kind of fabric applies to the thermal resistance clothes of the industries such as fire-fighting, smelting more.Work as clothes
When dress surface touches high temperature, the nickel alloy fiber in interlayer can become pagoda shape by flat shape rapidly, at two layers
Certain space is formed in fabric, is effectively reduced infringement of the high temperature source to human skin, is avoided the generation of scald accident.Furthermore lead to
Cross high molecular material and carry out molecular modification and modification, form Shape Memory Polymer SMP, can with external environment condition such as thermal energy,
Luminous energy, electric energy and chemical characteristic variation, it is automatic to change or restore form.It is tool using earliest shape memory high molecule material
Have the silk like fabric zephyr of retractility specific function, be chiefly used in the professionals such as similar dancing, gymnastics dress tights,
Shirt etc., it may also be used for the curtain of energy automatic open-close.
2. water repellent moisture permeable fabrics.The high polymers such as neoprene, polyvinyl chloride, polyurethane and acrylic acid are mostly used, are passed through
The mode of coating is in conjunction with common fabric.This kind fabric can be divided into micropore membranous type, hydrophilic coating non-porous film three categories, they
Possessed general character style is to draw coating technique by using polymer, and fabric is made to generate water-proof function, while being kept again general
The performance that fabric air-permeability is perspired, kept the temperature.The clothes made of this kind of fabric had both added protection effect, also ensured that dress used
Body-sensing comfort level.
3. temperature regulates and controls fiber.Temperature control fiber refers to can be according to environment or the fibre of human body variation automatic adjustment temperature and humidity
Dimension, generally can be divided into heat-accumulation temperature-adjustment type and conditioning type two categories.By the fabric and clothes of heat storing and heat preserving fiber process, remove
Static state constant-temperature effect with general fabric clothing is outer, also because using aqueous inorganic salts, long chain hydrocarbon, poly- second two
Liquid-solid reversible transition occurs for the phase change materials such as alcohol, fatty acid, or the absorption from environment by fiber-storage stores-is released
Thermal discharge forms between fabric and human body and is different from the external relative constant micro climate of temperature, reaches temperature and adjusts control
Effect.The fabric is used for suit earliest, has started to apply to the clothes such as cold-proof, sports now.Conditioning type is fine
Dimension mainly using the high hygroscopic property of fiber, by absorbing the hydrone that in air or human body generates, and is implementing gaseous state-liquid
State generates release when liquid-vapor converts or absorbs the principle of thermal energy, achievees the effect that constant temperature.
4. light guide incudes fiber.Also known as optical fiber or abbreviation light, it be it is a kind of can luminous energy be closed in the fibre, and
Generate the optical composite material of conduction.Optical fiber is usually the Material cladding different by two or more refractive index
Made of, one kind being core material, and another kind is skin material, and core material has conduction function, and skin material then makes luminous energy be closed core material, the folding of the two
It penetrates rate difference to be the bigger the better, i.e. the conductive performance of luminous energy is stronger.By material difference, optical fiber can be divided into inorganic light guide and have
Two class of machine light guide, no machine optical fiber includes glass optical fiber and silica fibre, and organic fiber is a kind of very thin core-skin type conjunction
At fiber, it has the characteristics that flexible, slim and graceful, intensity is big and price is lower and has certain radiation protection ability.Use optical fiber
Manufactured fabric has certain sensing function, with some signals can be transmitted after human contact, such as Environmental Chemistry biological condition
Detection, the variation of heart rate, in fight the position of soldier's injury determination, the health such as daily nursing index of children and patient is anti-
Shield clothes.
5. bionic intelligence fiber.So-called bionic intelligence fiber refers to the characteristic for imitating the certain biologies of nature, by certain
The utilization of manufacturing process enables textile material also have the function of similar certain biological self-controls and protection.Such as by lotus leaf
Surface micro-structure is conducive to the observation of this phenomenon of self-cleaning, textile technology worker with nanotechnology to fabric surface into
Row processing, forms it into tiny regular veins as micro-structure on lotus leaf, can effectively stop the delay of all kinds of particles.One
A little pollutants, the wine liquid such as splashed out, fruit juice, dust are difficult the fabric surface this by specially treated and stop, to improve
Effect that fabric keeps self clean.This fabric for being referred to as having " lotus leaf effect " is the representativeness of bionic intelligence
Achievement.Also such as, scientist has found that it is extremely similar to optical fiber after having studied the fur structure of polar bear.The hair of polar bear
Outer end is transparent, and like a tiny quartz fibre, and is opaque neural myelin close to one end of skin, surface is thick
Rough hard, centre is in hollow shape.This structure is particularly conducive to the transmission of light, it can absorb luminous energy to the maximum extent, collects
It is converted to thermal energy after to skin surface, and thermal energy is transported to by whole body by subcutaneous blood.According to this suction of polar bear fur
The principle of light accumulation of heat, containing carbonization zirconium material, " the daylight fiber " for having " extinction accumulation of heat " function is developed one kind, uses this
Clothes made of kind fiber weaving fabric, not only make it possible " thin clothing is passed the winter ", but also provide for polar expedition and exploration
Ideal dress.
It is furtherd elucidate below with reference to embodiment
Specific embodiment:
Embodiment 1: a kind of nana intelligent element fabric health clothing, it is characterized in that the natural ore element dissolves out naturally
It discharges the malicious ceramic nano powder of element negative ion far-infrared drug abuse filter and forms % by following quality proportioning
SiO 2-ceramic nano powder 2-6；Titanium dioxide ceramic nano powder 2-6；
Iron oxide ceramics nano powder 2-6；Aluminium oxide ceramics nano powder 2-6；
Chinese medicine stone ceramic nano powder 2-6；Zeolite ceramic nano powder 2-6；
Tourmaline ceramic nano powder 4-12；
Di-iron trioxide Fe2O3 ceramic nano powder 2-6；
Ferroso-ferric oxide Fe3O4 ceramic nano powder 3-9；
Poly- phthalein amine -6(PA6) add to 100.
Embodiment 2: a kind of nana intelligent element fabric health clothing, it is characterized in that: the intelligence phase-changing and temperature-regulating fiber
Capsule of nano method composite material ceramic nano powder forms % by following quality proportioning
Inorganic wall material has calcium silicates 2-6；Nano silver antimicrobials 2-6；
Positive 12 eicosane 2-6；Positive 15 docosane 2-6；
Paraffin 2-6；Natural cocoa butter fat acid blend 2-6；
Polycaprolactone glycol PEL 2-6；Shape memory polyurethane/TiO2-SiO22—6；
One or more of bisphenol-A, Lauxite, polyurethane, fragrant adoption peptamine add to 100.
Embodiment 3: a kind of nana intelligent element fabric health clothing, it is characterized in that: the anti electromagnetic wave magnetic therapy gram mite
Antibacterial anti-infection composite fibre Cypress ethereal oil ceramic nano powder forms % by following quality proportioning
Permanent magnet nano powder 2-6；Ferroso-ferric oxide Fe3O4 2—6；
Chitin nano powder 2-6；Chitosan nano rice flour 2-6；
Natural kawo fiber 2-6；Polylactic acid 2-6；
Enuatrol SD 2-6；Polyethylene glycol PEG 2-6；
Polyaniline PANI 2-6；Polypyrrole PPy 2-6；
Poly-vinyl alcohol solution adds to 100.
Embodiment 4: a kind of nana intelligent element fabric health clothing, it is characterized in that: the water repellent moisture-inhibiting temperature regulates and controls
Light guide incudes physical therapy composite fibre ceramic nano powder, forms % by following quality proportioning
Shape Memory Polymer SMP 2-6；Aqueous inorganic salts 2-6；
Long chain hydrocarbon 2-6；Polyethylene glycol 2-6；
Glass optical fiber 2-6；Fatty acid 2-6；
Silica fibre 2-6；Neoprene 2-6；
Polyvinyl chloride 2-6；Polyurethane 2-6；
Acrylic acid 2-6；Zirconium carbide adds to 100.
Claims (4)
1. a kind of nana intelligent element fabric health clothing, it is characterized in that the natural ore element dissolves out release member naturally
Plain negative ion far-infrared, which is taken drugs, filters malicious ceramic nano powder by following quality proportioning composition %
SiO 2-ceramic nano powder 2-6；Titanium dioxide ceramic nano powder 2-6；
Iron oxide ceramics nano powder 2-6；Aluminium oxide ceramics nano powder 2-6；
Chinese medicine stone ceramic nano powder 2-6；Zeolite ceramic nano powder 2-6；
Tourmaline ceramic nano powder 4-12；
Di-iron trioxide Fe2O3 ceramic nano powder 2-6；
Ferroso-ferric oxide Fe3O4 ceramic nano powder 3-9；
Poly- phthalein amine -6(PA6) add to 100.
2. a kind of nana intelligent element fabric health clothing, it is characterized in that: the intelligence phase-changing and temperature-regulating fiber capsule of nano
Method composite material ceramic nano powder forms % by following quality proportioning
Inorganic wall material has calcium silicates 2-6；Nano silver antimicrobials 2-6；
Positive 12 eicosane 2-6；Positive 15 docosane 2-6；
Paraffin 2-6；Natural cocoa butter fat acid blend 2-6；
Polycaprolactone glycol PEL 2-6；Shape memory polyurethane/TiO2-SiO22—6；
One or more of bisphenol-A, Lauxite, polyurethane, fragrant adoption peptamine add to 100.
3. a kind of nana intelligent element fabric health clothing, it is characterized in that: the anti electromagnetic wave magnetic therapy gram mite antibacterial anti-infection
Composite fibre Cypress ethereal oil ceramic nano powder forms % by following quality proportioning
Permanent magnet nano powder 2-6；Ferroso-ferric oxide Fe3O4 2—6；
Chitin nano powder 2-6；Chitosan nano rice flour 2-6；
Natural kawo fiber 2-6；Polylactic acid 2-6；
Enuatrol SD 2-6；Polyethylene glycol PEG 2-6；
Polyaniline PANI 2-6；Polypyrrole PPy 2-6；
Poly-vinyl alcohol solution adds to 100.
4. a kind of nana intelligent element fabric health clothing, it is characterized in that: water repellent moisture-inhibiting temperature regulation light guide induction reason
Composite fibre ceramic nano powder is treated, forms % by following quality proportioning
Shape Memory Polymer SMP 2-6；Aqueous inorganic salts 2-6；
Long chain hydrocarbon 2-6；Polyethylene glycol 2-6；
Glass optical fiber 2-6；Fatty acid 2-6；
Silica fibre 2-6；Neoprene 2-6；
Polyvinyl chloride 2-6；Polyurethane 2-6；
Acrylic acid 2-6；Zirconium carbide adds to 100.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811112308.XA CN109275972A (en) | 2018-09-25 | 2018-09-25 | Nana intelligent element fabric health clothing |
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| CN201811112308.XA CN109275972A (en) | 2018-09-25 | 2018-09-25 | Nana intelligent element fabric health clothing |
Publications (1)
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| CN109275972A true CN109275972A (en) | 2019-01-29 |
Family
ID=65181577
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| CN201811112308.XA Withdrawn CN109275972A (en) | 2018-09-25 | 2018-09-25 | Nana intelligent element fabric health clothing |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113186647A (en) * | 2021-04-21 | 2021-07-30 | 上海工程技术大学 | Polypyrrole/zirconium carbide/polyurethane composite fiber membrane and preparation method and application thereof |
| CN113429937A (en) * | 2021-05-17 | 2021-09-24 | 中国地质大学（武汉） | Energy-saving temperature-control phase-change microcapsule for wall and preparation method thereof |
| CN115087416A (en) * | 2019-11-08 | 2022-09-20 | 健康小环境有限公司 | System of panty liner and sanitary napkin |
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| CN113429937A (en) * | 2021-05-17 | 2021-09-24 | 中国地质大学（武汉） | Energy-saving temperature-control phase-change microcapsule for wall and preparation method thereof |
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