CN109266428A - A kind of olive lubricating oil and preparation method thereof - Google Patents

A kind of olive lubricating oil and preparation method thereof Download PDF

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Publication number
CN109266428A
CN109266428A CN201811039903.5A CN201811039903A CN109266428A CN 109266428 A CN109266428 A CN 109266428A CN 201811039903 A CN201811039903 A CN 201811039903A CN 109266428 A CN109266428 A CN 109266428A
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olive
parts
lubricating oil
oil
obtains
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赵春艳
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Sichuan Yizhang Agricultural Development Co Ltd
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Sichuan Yizhang Agricultural Development Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/022—Ethene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/024—Propene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/026—Butene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/04—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing aromatic monomers, e.g. styrene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/06—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/401—Fatty vegetable or animal oils used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084—Acrylate; Methacrylate
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/08—Halogenated waxes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/02—Unspecified siloxanes; Silicones
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16—Antiseptic; (micro) biocidal or bactericidal

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of olive lubricating oil and preparation method thereof, a kind of raw material components and its parts by weight of olive lubricating oil are as follows: 125~170 parts of olive oil-base fluid, 2~6 parts of viscosity index improver, 2~5 parts of preservative, 2~5 parts of crystalline flake graphite, 2~5 parts of fungicide, 2~5 parts of defoaming agent, 2~8 parts of oiliness improver, 2~6 parts of antiwear additive, 2~5 parts of extreme pressure agent and 180~220 parts of water.Beneficial effect is: compared with conventional lubrication oil, resource is richer, and renewable is strong, and resource utilization is higher, and environmental-protecting performance is more preferable, and manufacturing cost is low；Manufacturing process is simple, significantly reduces labor intensity of workers, has biggish economic value.

Description

A kind of olive lubricating oil and preparation method thereof
Technical field
The present invention relates to technical field of lubricating oil, more particularly to a kind of olive lubricating oil and preparation method thereof.
Background technique
Be increasingly enhanced environmental crisis consciousness, a large amount of lubricating oil in production, use and discharge process due to infiltration, Leak, overflow and deal with improperly, and caused by pollution problem be increasingly taken seriously, from the point of view of the trend of development, have biology The environment-friendly lubricating oil and its additive of degradability will replace existing lubricating oil.
Olive is Oleaceae Olea aiphyllium, is world-renowned woody oleiferous plants and fruit tree species, cultivation product Kind has higher edible value, containing abundant high-quality edible plant oil --- olive oil, in recent years, with the continuous increasing of environmental consciousness By force, technology of the olive in terms of lubricating oil is also constantly being carried out, and since its manufacturing cost is low, using effect is good, prepares difficulty Low advantage, by the extensive concern of lubricating oil producer, but a kind of preparation method of traditional olive lubricating oil exists, system The problems such as standby difficulty is big, long processing time, oil product is poor, therefore we need further on the basis of existing improved.
Summary of the invention
The object of the invention is that providing a kind of olive lubricating oil and preparation method thereof to solve the above-mentioned problems.
The present invention through the following technical solutions to achieve the above objectives:
A kind of olive lubricating oil, the raw material components and its parts by weight of the olive lubricating oil are as follows: olive oil-base fluid 125~170 parts, 2~6 parts of viscosity index improver, 2~5 parts of preservative, 2~5 parts of crystalline flake graphite, 2~5 parts of fungicide, defoaming 2~5 parts of agent, 2~8 parts of oiliness improver, 2~6 parts of antiwear additive, 2~5 parts of extreme pressure agent and 180~220 parts of water.
Further, the viscosity index improver be ethylenebis stearic amide, hy drogenated styrene-diene copolymer, One or more of polymethacrylates, ethylene propylene copolymer, polyisobutene.
Further, the defoaming agent is polyether-modified silicon.
Further, the oiliness improver is palmitinic acid.
Further, the fungicide concrete model is F-022.
Further, the antiwear additive is one or more of vulcanization grease, phosphate, metal dithiophosphate.
Further, the extreme pressure agent is chlorinated paraffin.
The present invention also provides a kind of preparation methods of olive lubricating oil, the production applied to above-mentioned olive lubricating oil In, comprising the following steps:
Step 1: fresh olive is selected in olive pretreatment, obtains cleaning olive after cleaning removal of impurities, by wash oil Olive, which is put into juice extractor, carries out juicing processing, obtains pulp, antioxidant and demulsifier will be added in pulp, at 10-25 DEG C 1-1.5h is stirred with 120-300r/min, obtains mixing pulp；
Step 2: mixing pulp is poured on oil press and is squeezed by squeezing, and pressing temperature is 10-20 DEG C, pressure 30- 40MPa, the time of pressure process are 20-50 minutes, and the dwell time is 40-80 minutes, obtain juice；
Step 3: filtering, juice are filtered using flame filter press, and flame filter press uses 300-500 mesh filter cloth, filtration pressure Power 0.1-0.3MPa obtains oiliness mixed liquor；
Step 4: separation by oiliness mixed liquor at standing 7-10 hours of 15-20 DEG C, is layered grease, utilizes suction machine Surface layer oil is mutually drawn, olive oil-base fluid is obtained；
Step 5: Hybrid Heating, by etc. the stearic acid of parts by weight, dihydroxy stearic acid Hybrid Heating, be heated to 60~65 It after DEG C, is gradually added into olive oil matrix obtained in step 4, persistently stirs 10~15 minutes and mix olive to get to preliminary Oil；
Step 6: stirring preparation is added after the primary mixed olive oil of gained in step 5 is heated to 40~45 DEG C by phase Answer preservative, viscosity index improver, crystalline flake graphite, fungicide, defoaming agent, oiliness improver, antiwear additive, the extreme pressure agent of parts by weight And water, 30~50min, which is stirred, under the revolving speed of 35~40r/min obtains a kind of olive lubricating oil.
The beneficial effects of the present invention are: compared with conventional lubrication oil, resource is richer, and renewable is strong, resource benefit Higher with rate, environmental-protecting performance is more preferable, and manufacturing cost is low；Manufacturing process is simple, significantly reduces labor intensity of workers, has biggish Economic value.
Specific embodiment
Below with reference to embodiment, the invention will be further described:
Embodiment one:
A kind of olive lubricating oil, the raw material components and its parts by weight of the olive lubricating oil are as follows: olive oil-base fluid 125 parts, 2 parts of viscosity index improver, 2 parts of preservative, 2 parts of crystalline flake graphite, 2 parts of fungicide, 3 parts of defoaming agent, 4 parts of oiliness improver, 3 parts of antiwear additive, 4 parts of extreme pressure agent and 180 parts of water.
In the present embodiment, the viscosity index improver is ethylenebis stearic amide.
In the present embodiment, the defoaming agent is polyether-modified silicon.
In the present embodiment, the oiliness improver is palmitinic acid.
In the present embodiment, the fungicide concrete model is F-022.
In the present embodiment, the antiwear additive is vulcanization grease.
In the present embodiment, the extreme pressure agent is chlorinated paraffin.
The present invention also provides a kind of preparation methods of olive lubricating oil of oil, the production applied to above-mentioned olive lubricating oil In, comprising the following steps:
Step 1: fresh olive is selected in olive pretreatment, obtains cleaning olive after cleaning removal of impurities, by wash oil Olive, which is put into juice extractor, carries out juicing processing, obtains pulp, and antioxidant and demulsifier will be added in pulp, 10 DEG C with 180r/min stirs 1h, obtains mixing pulp；
Step 2: mixing pulp is poured on oil press and is squeezed by squeezing, and pressing temperature is 10 DEG C, and pressure 30MPa adds The time for pressing through journey is 20 minutes, and the dwell time is 50 minutes, obtains juice；
Step 3: filtering, juice are filtered using flame filter press, and flame filter press uses 350 mesh filter clothes, filter pressure 0.2MPa obtains oiliness mixed liquor；
Step 4: separation by oiliness mixed liquor at standing 8 hours of 18 DEG C, is layered grease, using suction machine by surface layer It is oily mutually to draw, obtain olive oil-base fluid.
Step 5: Hybrid Heating, by etc. the stearic acid of parts by weight, dihydroxy stearic acid Hybrid Heating, after being heated to 68 DEG C, It is gradually added into olive oil matrix obtained in step 4, stirs 13 minutes persistently to get preliminary mixed olive oil is arrived；
Step 6: stirring preparation is added and will accordingly weigh after the primary mixed olive oil of gained in step 5 is heated to 42 DEG C Measure the preservative of number, viscosity index improver, crystalline flake graphite, fungicide, defoaming agent, oiliness improver, antiwear additive, extreme pressure agent and Water stirs 40min under the revolving speed of 38r/min and obtains a kind of olive lubricating oil.
Embodiment two:
A kind of olive lubricating oil, the raw material components and its parts by weight of the olive lubricating oil are as follows: olive oil-base fluid 140 parts, 3 parts of viscosity index improver, 3 parts of preservative, 3 parts of crystalline flake graphite, 3 parts of fungicide, 4 parts of defoaming agent, 5 parts of oiliness improver, 5 parts of antiwear additive, 3 parts of extreme pressure agent and 220 parts of water.
In the present embodiment, the viscosity index improver is polymethacrylates.
In the present embodiment, the defoaming agent is polyether-modified silicon.
In the present embodiment, the oiliness improver is palmitinic acid.
In the present embodiment, the fungicide concrete model is F-022.
In the present embodiment, the antiwear additive is vulcanization grease.
In the present embodiment, the extreme pressure agent is chlorinated paraffin.
The present invention also provides a kind of preparation methods of olive lubricating oil of oil, the production applied to above-mentioned olive lubricating oil In, comprising the following steps:
Step 1: fresh olive is selected in olive pretreatment, obtains cleaning olive after cleaning removal of impurities, by wash oil Olive, which is put into juice extractor, carries out juicing processing, obtains pulp, and antioxidant and demulsifier will be added in pulp, 20 DEG C with 270r/min stirs 1.3h, obtains mixing pulp；
Step 2: mixing pulp is poured on oil press and is squeezed by squeezing, and pressing temperature is 15 DEG C, and pressure 35MPa adds The time for pressing through journey is 40 minutes, and the dwell time is 60 minutes, obtains juice；
Step 3: filtering, juice are filtered using flame filter press, and flame filter press uses 450 mesh filter clothes, filter pressure 0.3MPa obtains oiliness mixed liquor；
Step 4: separation by oiliness mixed liquor at standing 8 hours of 18 DEG C, is layered grease, using suction machine by surface layer It is oily mutually to draw, obtain olive oil-base fluid.
Step 5: Hybrid Heating, by etc. the stearic acid of parts by weight, dihydroxy stearic acid Hybrid Heating, after being heated to 62 DEG C, It is gradually added into olive oil matrix obtained in step 4, stirs 14 minutes persistently to get preliminary mixed olive oil is arrived；
Step 6: stirring preparation is added and will accordingly weigh after the primary mixed olive oil of gained in step 5 is heated to 42 DEG C Measure the preservative of number, viscosity index improver, crystalline flake graphite, fungicide, defoaming agent, oiliness improver, antiwear additive, extreme pressure agent and Water stirs 50min under the revolving speed of 38r/min and obtains a kind of olive lubricating oil.
Embodiment three:
A kind of olive lubricating oil, the raw material components and its parts by weight of the olive lubricating oil are as follows: olive oil-base fluid 160 parts, 5 parts of viscosity index improver, 4 parts of preservative, 3 parts of crystalline flake graphite, 4 parts of fungicide, 5 parts of defoaming agent, 6 parts of oiliness improver, 5 parts of antiwear additive, 4 parts of extreme pressure agent and 210 parts of water.
In the present embodiment, the viscosity index improver is polyisobutene.
In the present embodiment, the defoaming agent is polyether-modified silicon.
In the present embodiment, the oiliness improver is palmitinic acid.
In the present embodiment, the fungicide concrete model is F-022.
In the present embodiment, the antiwear additive is metal dithiophosphate.
In the present embodiment, the extreme pressure agent is chlorinated paraffin.
The present invention also provides a kind of preparation methods of olive lubricating oil of oil, the production applied to above-mentioned olive lubricating oil In, comprising the following steps:
Step 1: fresh olive is selected in olive pretreatment, obtains cleaning olive after cleaning removal of impurities, by wash oil Olive, which is put into juice extractor, carries out juicing processing, obtains pulp, and antioxidant and demulsifier will be added in pulp, 17 DEG C with 220r/min stirs 1.2h, obtains mixing pulp；
Step 2: mixing pulp is poured on oil press and is squeezed by squeezing, and pressing temperature is 17 DEG C, and pressure 35MPa adds The time for pressing through journey is 30 minutes, and the dwell time is 60 minutes, obtains juice；
Step 3: filtering, juice are filtered using flame filter press, and flame filter press uses 400 mesh filter clothes, filter pressure 0.1MPa obtains oiliness mixed liquor；
Step 4: separation by oiliness mixed liquor at standing 8 hours of 17 DEG C, is layered grease, using suction machine by surface layer It is oily mutually to draw, obtain olive oil-base fluid.
Step 5: Hybrid Heating, by etc. the stearic acid of parts by weight, dihydroxy stearic acid Hybrid Heating, after being heated to 62 DEG C, It is gradually added into olive oil matrix obtained in step 4, stirs 12 minutes persistently to get preliminary mixed olive oil is arrived；
Step 6: stirring preparation is added and will accordingly weigh after the primary mixed olive oil of gained in step 5 is heated to 45 DEG C Measure the preservative of number, viscosity index improver, crystalline flake graphite, fungicide, defoaming agent, oiliness improver, antiwear additive, extreme pressure agent and Water stirs 40min under the revolving speed of 37r/min and obtains a kind of olive lubricating oil.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should Understand, the present invention is not limited to the above embodiments, and the above embodiments and description only describe originals of the invention Reason, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes and improvements It all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appending claims and equivalents circle It is fixed.

Claims (9)

1. a kind of olive lubricating oil, it is characterised in that: a kind of raw material components and its parts by weight of olive lubricating oil Are as follows: 125~170 parts of olive oil-base fluid, 2~6 parts of viscosity index improver, 2~5 parts of preservative, 2~5 parts of crystalline flake graphite, sterilization 2~5 parts of agent, 2~5 parts of defoaming agent, 2~8 parts of oiliness improver, 2~6 parts of antiwear additive, 2~5 parts of extreme pressure agent and 180~220 parts of water.
2. a kind of olive lubricating oil according to claim 1, it is characterised in that: the viscosity index improver is sub- second The double stearic amide of base, hy drogenated styrene-diene copolymer, polymethacrylates, ethylene propylene copolymer, in polyisobutene One or more.
3. a kind of olive lubricating oil according to claim 1, it is characterised in that: the defoaming agent is polyether-modified silicon.
4. a kind of olive lubricating oil according to claim 1, it is characterised in that: the preservative is sodium Diacetate.
5. a kind of olive lubricating oil according to claim 1, it is characterised in that: the oiliness improver is palmitinic acid.
6. a kind of olive lubricating oil according to claim 1, it is characterised in that: the fungicide concrete model is F- 022。
7. a kind of olive lubricating oil according to claim 1, it is characterised in that: the antiwear additive is vulcanization grease, phosphorus One or more of acid esters, metal dithiophosphate.
8. a kind of olive lubricating oil according to claim 1, it is characterised in that: the extreme pressure agent is chlorinated paraffin.
9. a kind of preparation method of olive lubricating oil is lubricated applied to olive described in any one of claim 1 to 8 In the production of oil, it is characterised in that: the following steps are included:
Step 1: fresh olive is selected in olive pretreatment, obtains cleaning olive after cleaning removal of impurities, by clean olive Be put into juice extractor and carry out juicing processing, obtain pulp, antioxidant and demulsifier will be added in pulp, 10-25 DEG C with 120-300r/min stirs 1-1.5h, obtains mixing pulp；
Step 2: mixing pulp is poured on oil press and is squeezed by squeezing, and pressing temperature is 10-20 DEG C, pressure 30-40MPa, The time of pressure process is 20-50 minutes, and the dwell time is 40-80 minutes, obtains juice；
Step 3: filtering, juice are filtered using flame filter press, and flame filter press uses 300-500 mesh filter cloth, filter pressure 0.1-0.3MPa obtains oiliness mixed liquor；
Step 4: separation by oiliness mixed liquor at standing 7-10 hours of 15-20 DEG C, is layered grease, using suction machine by table Layer oil is mutually drawn, and olive oil-base fluid is obtained；
Step 5: Hybrid Heating, by etc. the stearic acid of parts by weight, dihydroxy stearic acid Hybrid Heating, after being heated to 60~65 DEG C, It is gradually added into olive oil matrix obtained in step 4, stirs 10~15 minutes persistently to get preliminary mixed olive oil is arrived；
Step 6: stirring preparation is added and will accordingly weigh after the primary mixed olive oil of gained in step 5 is heated to 40~45 DEG C Measure the preservative of number, viscosity index improver, crystalline flake graphite, fungicide, defoaming agent, oiliness improver, antiwear additive, extreme pressure agent and Water stirs 30~50min under the revolving speed of 35~40r/min and obtains olive lubricating oil.
CN201811039903.5A 2018-09-06 2018-09-06 A kind of olive lubricating oil and preparation method thereof Pending CN109266428A (en)

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Application Number Priority Date Filing Date Title
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CN109266428A true CN109266428A (en) 2019-01-25

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Application publication date: 20190125