CN109264805A - A kind of equipment and its processing method of efficient process waste water containing carbonyl - Google Patents

A kind of equipment and its processing method of efficient process waste water containing carbonyl Download PDF

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Publication number
CN109264805A
CN109264805A CN201811378000.XA CN201811378000A CN109264805A CN 109264805 A CN109264805 A CN 109264805A CN 201811378000 A CN201811378000 A CN 201811378000A CN 109264805 A CN109264805 A CN 109264805A
Authority
CN
China
Prior art keywords
waste water
water containing
containing carbonyl
evaporator
carbonyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811378000.XA
Other languages
Chinese (zh)
Inventor
肖冬明
马国生
甄超兴
刘洪彪
罗世铭
李登瑞
王金鹏
王强
沈宝华
王大窝
王良
许全涛
李智文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jinchuan Group Co Ltd
Original Assignee
Jinchuan Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jinchuan Group Co Ltd filed Critical Jinchuan Group Co Ltd
Priority to CN201811378000.XA priority Critical patent/CN109264805A/en
Publication of CN109264805A publication Critical patent/CN109264805A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048Purification of waste water by evaporation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/043Details
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/66Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/72Treatment of water, waste water, or sewage by oxidation
    • C02F1/722Oxidation by peroxides
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00Controlling or monitoring parameters in water treatment
    • C02F2209/06Controlling or monitoring parameters in water treatment pH
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00Controlling or monitoring parameters in water treatment
    • C02F2209/42Liquid level
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00General aspects of water treatment
    • C02F2301/04Flow arrangements
    • C02F2301/043Treatment of partial or bypass streams
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/14Maintenance of water treatment installations

Abstract

The invention belongs to carbonyl technical field of metallurgical production, more particularly to the equipment and its processing method of a kind of efficient process waste water containing carbonyl, the device includes waste tank, the evaporator of waste water containing carbonyl, tubular heat exchanger, gas purifier and powder disinfection storehouse, it is connected between the waste tank and the evaporator of waste water containing carbonyl with stainless steel tube, the base of evaporator of waste water containing carbonyl is connected with tubular heat exchanger, the metal diaphragm pump group being arranged in parallel and cut-off valve group are installed on stainless steel tube, the evaporator side of waste water containing carbonyl is equipped with gas purifier, gas purifier lower end is connected with powder disinfection storehouse.The present invention takes carbonyl compound out of decomposition by way of it will contain the evaporation of carbonyl waste water, relatively before processing mode, treatment process is highly-safe, and effect is obvious;It is handled in addition, remaining after evaporation liquid is directed at conditioning tank by this processing method, the indexs such as liquid pH value, carbonyl compound content meet environmental requirement after processing.

Description

A kind of equipment and its processing method of efficient process waste water containing carbonyl
Technical field
The invention belongs to carbonyl technical field of metallurgical production, and in particular to a kind of equipment of efficient process waste water containing carbonyl and its Processing method.
Background technique
During carbonyl compound production, it can be generated when clearing up storage tank, evaporator etc. and contacting the container of carbonyl compound big Waste water containing carbonyl is measured, due to the feature that the risk of wastewater treatment process containing carbonyl is high, treating method is few, is deposited for a long time to wastewater storage tank, is Production brings biggish security risk.
Therefore the processing waste water containing carbonyl for capableing of safety non-pollution is particularly important.
Summary of the invention
For above-mentioned problems of the prior art and deficiency, the present invention provides a kind of setting for efficient process waste water containing carbonyl It is standby.
Another object of the present invention is to provide a kind of methods using above equipment processing waste water containing carbonyl.
To achieve the above object, the invention provides the following technical scheme:
A kind of equipment of efficient process waste water containing carbonyl, including waste tank, waste water containing carbonyl evaporator, tubular heat exchanger, gas Clarifier and powder disinfection storehouse are connected between the waste tank and the evaporator of waste water containing carbonyl with stainless steel tube, waste water containing carbonyl Base of evaporator is connected with tubular heat exchanger, and the metal diaphragm pump group being arranged in parallel and shut-off valve are equipped on stainless steel tube Group, the evaporator side of waste water containing carbonyl are equipped with gas purifier, pass through pipeline and gas purification at the top of the evaporator of waste water containing carbonyl Device connection, gas purifier lower end is connected with powder disinfection storehouse.
Further, the metal diaphragm pump group is made of the first metal diaphragm pump and the second metal diaphragm pump, cut-off Valve group is made of the first shut-off valve and the second shut-off valve, and by-passing valve is equipped between the first shut-off valve and the second shut-off valve and is connected.
Further, the waste water containing carbonyl evaporator side is equipped with liquidometer, and the input duct of liquidometer, which extends to, to be contained The bottom of carbonyl waste water evaporator.
Further, the bottom side of the evaporator of waste water containing carbonyl is also connected with conditioning tank, the evaporator of waste water containing carbonyl The pipeline connecting with conditioning tank is equipped with conditioning tank inlet valve.
Further, the metallic dust of gas purifier discharge is periodically released after entering powder disinfection storehouse.
Further, the side of the evaporator of waste water containing carbonyl is equipped with manhole.
A method of using efficient process waste water containing carbonyl equipment handle waste water containing carbonyl, this method as steps described below into Row:
Step 1: gas purifier temperature of each section being put into, after temperature rises to set temperature, uses one group of metal diaphragm pump and one Group shut-off valve turns the extremely evaporator of waste water containing carbonyl of waste water containing carbonyl deposited to waste tank, observes the level readings of liquidometer at any time, The first metal diaphragm pump and the second metal diaphragm pump are deactivated when the liquid level of liquidometer reaches 85%, close corresponding first cut-off Valve and the second shut-off valve;
Step 2: opening hot nitrogen inlet valve, come into operation tubular heat exchanger, is passed through hot nitrogen into the evaporator of waste water containing carbonyl, evaporates Time 5h, gas enter gas purifier and carry out 220 DEG C of pyrolytics, and metallic dust is put by powder disinfection storehouse disinfection qualification Out, gas decomposites CO gas and enters CO gas holder;
Step 3: unlatching conditioning tank inlet valve will contain evaporation remaining liq in carbonyl waste water evaporator and drain into conditioning tank, in conditioning tank It is finally being aoxidized with hydrogen peroxide, finally adjusting pH value to 7-8 drains into production drainage pipeline
Compared with prior art, the beneficial effects of the present invention are:
The present invention takes carbonyl compound out of decompositions by way of it will contain the evaporation of carbonyl waste water, relatively before processing mode, it is processed Journey is highly-safe, and effect is obvious;It is handled in addition, remaining after evaporation liquid is directed at conditioning tank by this processing method, liquid after processing The indexs such as pH value, carbonyl compound content meet environmental requirement.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention;
In figure: 1. waste tanks, 2. evaporators of waste water containing carbonyl, 3. tubular heat exchangers, 4. gas purifiers, the disinfection of 5. powders Storehouse, 6. first metal diaphragm pumps, 7. first shut-off valves, 8. second metal diaphragm pumps, 9. second shut-off valves, 10. by-passing valves, 11. Liquidometer, 12. conditioning tanks, 13. manholes, 14. hot nitrogen inlet valves, 15. conditioning tank inlet valves, 16. stainless steel tubes.
Specific embodiment
The following describes the present invention in detail with reference to the accompanying drawings and specific embodiments.
As shown in Figure 1, a kind of equipment of efficient process waste water containing carbonyl, including waste tank 1, waste water containing carbonyl evaporator 2, column Pipe heat exchanger 3, gas purifier 4 and powder disinfection storehouse 5 use stainless steel tube between waste tank 1 and the evaporator of waste water containing carbonyl 2 16 connections, 2 bottom of the evaporator of waste water containing carbonyl is connected with tubular heat exchanger 3, the gold being arranged in parallel is equipped on stainless steel tube 16 Belong to diaphragm pump group and cut-off valve group, metal diaphragm pump group are made of the first metal diaphragm pump 6 and the second metal diaphragm pump 8, ends Valve group is made of the first shut-off valve 7 and the second shut-off valve 9, and by-passing valve 10 is equipped between the first shut-off valve 7 and the second shut-off valve 9 and is connected It connecing, 2 side of the evaporator of waste water containing carbonyl is equipped with gas purifier 4, and 4 lower end of gas purifier is connected with powder disinfection storehouse 5, contain carbonyl 2 side of waste water evaporator is equipped with liquidometer 11, and the input duct of liquidometer 11 extends to the bottom of the evaporator of waste water containing carbonyl 2, contains The bottom side of carbonyl waste water evaporator 2 is also connected with conditioning tank 12, on the pipeline that the evaporator of waste water containing carbonyl 2 is connect with conditioning tank 12 Equipped with conditioning tank inlet valve 15, it is connect by pipeline with gas purifier 4 at the top of the evaporator of waste water containing carbonyl 2,4 row of gas purifier Metallic dust out is periodically released after entering powder disinfection storehouse 5, and the side of the evaporator of waste water containing carbonyl 2 is equipped with manhole 13.
A method of using efficient process waste water containing carbonyl equipment handle waste water containing carbonyl, this method as steps described below into Row:
Step 1: 4 temperature of each section of gas purifier being put into, after temperature rises to set temperature, uses one group of metal diaphragm pump and one Group shut-off valve turns the waste water containing carbonyl deposited to waste tank 1 to the evaporator of waste water containing carbonyl 2, and the liquid level for observing liquidometer 11 at any time is read Number deactivates the first metal diaphragm pump 6 and the second metal diaphragm pump 8 when the liquid level of liquidometer 11 reaches 85%, closes corresponding the One shut-off valve 7 and the second shut-off valve 9;
Step 2: hot nitrogen inlet valve 14 is opened, come into operation tubular heat exchanger 3, it is passed through hot nitrogen into the evaporator of waste water containing carbonyl 2, Evaporation time 5h, gas enter gas purifier 4 and carry out 220 DEG C of pyrolytics, and metallic dust is closed by the disinfection of powder disinfection storehouse 5 Lattice are released, and gas decomposites CO gas and enters CO gas holder;
Step 3: unlatching conditioning tank inlet valve 15 will contain evaporation remaining liq in carbonyl waste water evaporator 2 and drain into conditioning tank 12, adjust Section is finally being aoxidized in pond 12 with hydrogen peroxide, and finally adjusting pH value to 7-8 drains into production drainage pipeline.

Claims (7)

1. a kind of equipment of efficient process waste water containing carbonyl, including the heat exchange of waste tank (1), the evaporator of waste water containing carbonyl (2), shell and tube Device (3), gas purifier (4) and powder disinfection storehouse (5), which is characterized in that the waste tank (1) and waste water containing carbonyl is evaporated It is connected between device (2) with stainless steel tube (16), the evaporator of waste water containing carbonyl (2) bottom is connected with tubular heat exchanger (3), stainless steel The metal diaphragm pump group being arranged in parallel and cut-off valve group are installed, the evaporator of waste water containing carbonyl (2) side is equipped on pipe (16) Gas purifier (4), the evaporator of waste water containing carbonyl (2) top are connect by pipeline with gas purifier (4), gas purifier (4) Lower end is connected with powder disinfection storehouse (5).
2. a kind of equipment of efficient process waste water containing carbonyl as described in claim 1, which is characterized in that the metal diaphragm pump Group is made of the first metal diaphragm pump (6) and the second metal diaphragm pump (8), ends valve group by the first shut-off valve (7) and second section Only valve (9) forms, and by-passing valve (10) are equipped between the first shut-off valve (7) and the second shut-off valve (9) and are connected.
3. a kind of equipment of efficient process waste water containing carbonyl as claimed in claim 2, which is characterized in that the waste water containing carbonyl steams It sends out device (2) side and is equipped with liquidometer (11), the input duct of liquidometer (11) extends to the bottom of the evaporator of waste water containing carbonyl (2).
4. a kind of equipment of efficient process waste water containing carbonyl as claimed in claim 3, which is characterized in that the waste water containing carbonyl steams The bottom side of hair device (2) is also connected with conditioning tank (12), on the pipeline that the evaporator of waste water containing carbonyl (2) is connect with conditioning tank (12) Equipped with conditioning tank inlet valve (15).
5. a kind of equipment of efficient process waste water containing carbonyl as claimed in claim 4, which is characterized in that the gas purifier (4) metallic dust being discharged enters powder disinfection storehouse (5) and periodically releases afterwards.
6. a kind of equipment of efficient process waste water containing carbonyl as claimed in claim 5, which is characterized in that the waste water containing carbonyl steams The side for sending out device (2) is equipped with manhole (13).
7. a kind of method of equipment processing waste water containing carbonyl using a kind of efficient process waste water containing carbonyl as claimed in claim 6, It is characterized in that, this method carries out as steps described below:
Step 1: gas purifier (4) temperature of each section is put into, after temperature rises to set temperature, using one group of metal diaphragm pump and One group of shut-off valve turns the waste water containing carbonyl deposited to waste tank (1) to the evaporator of waste water containing carbonyl (2), observes liquidometer (11) at any time Level readings, when the liquid level of liquidometer (11) reaches 85% deactivate the first metal diaphragm pump (6) and the second metal diaphragm pump (8), corresponding first shut-off valve (7) and the second shut-off valve (9) are closed;
Step 2: opening hot nitrogen inlet valve (14), the tubular heat exchanger that comes into operation (3), be passed through into the evaporator of waste water containing carbonyl (2) Hot nitrogen, evaporation time 5h, gas enter gas purifier (4) and carry out 220 DEG C of pyrolytics, and metallic dust is sterilized by powder Storehouse (5) disinfection is qualified to release, and gas decomposites CO gas and enters CO gas holder;
Step 3: unlatching conditioning tank inlet valve (15) will contain evaporation remaining liq in carbonyl waste water evaporator (2) and drain into conditioning tank (12), it is finally being aoxidized in conditioning tank (12) with hydrogen peroxide, finally adjusting pH value to 7-8 drains into production downcomer Road.
CN201811378000.XA 2018-11-19 2018-11-19 A kind of equipment and its processing method of efficient process waste water containing carbonyl Pending CN109264805A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811378000.XA CN109264805A (en) 2018-11-19 2018-11-19 A kind of equipment and its processing method of efficient process waste water containing carbonyl

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Application Number Priority Date Filing Date Title
CN201811378000.XA CN109264805A (en) 2018-11-19 2018-11-19 A kind of equipment and its processing method of efficient process waste water containing carbonyl

Publications (1)

Publication Number Publication Date
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06198275A (en) * 1992-12-28 1994-07-19 Ogawa Kankyo Kenkyusho:Kk Method and device for waste liquid treatment
CN1821115A (en) * 2006-03-17 2006-08-23 金川集团有限公司 Method for treating industrial waste water containing carbonyl compound
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CN103496755A (en) * 2013-09-18 2014-01-08 天脊煤化工集团股份有限公司 Method and device for treating coal chemical industry production sewage
CN103663824A (en) * 2012-09-14 2014-03-26 苏州工业园区七星电子有限公司 Wastewater treatment method and device
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CN106007134A (en) * 2016-05-27 2016-10-12 北京国电富通科技发展有限责任公司 Purifying salt production system and method for synchronous removal of organic matters through evaporative crystallization of high-salinity organic wastewater
CN205676189U (en) * 2016-05-30 2016-11-09 崇越科技股份有限公司 Volatility Waste Water Treatment
CN106396223A (en) * 2016-06-13 2017-02-15 王华兵 Treatment process for phenolic water
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* Cited by examiner, † Cited by third party
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CN1821115A (en) * 2006-03-17 2006-08-23 金川集团有限公司 Method for treating industrial waste water containing carbonyl compound
CN201095612Y (en) * 2007-10-15 2008-08-06 骆志杰 Treatment device for coal gas producer sewage containing phenol and cyanogen
CN101209875A (en) * 2007-12-25 2008-07-02 金川集团有限公司 Method for processing wastewater containing carbonyl iron
CN102642971A (en) * 2012-05-03 2012-08-22 太原理工大学 Coking wastewater treatment process
CN103663824A (en) * 2012-09-14 2014-03-26 苏州工业园区七星电子有限公司 Wastewater treatment method and device
CN103496755A (en) * 2013-09-18 2014-01-08 天脊煤化工集团股份有限公司 Method and device for treating coal chemical industry production sewage
CN203609882U (en) * 2013-12-14 2014-05-28 金川集团股份有限公司 Evaporating device for liquid carbonyl compound
CN106007134A (en) * 2016-05-27 2016-10-12 北京国电富通科技发展有限责任公司 Purifying salt production system and method for synchronous removal of organic matters through evaporative crystallization of high-salinity organic wastewater
CN205676189U (en) * 2016-05-30 2016-11-09 崇越科技股份有限公司 Volatility Waste Water Treatment
CN106396223A (en) * 2016-06-13 2017-02-15 王华兵 Treatment process for phenolic water
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Application publication date: 20190125

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