CN109264772A - It is a kind of to prepare four basic lead sulphate quick reaction devices - Google Patents
It is a kind of to prepare four basic lead sulphate quick reaction devices Download PDFInfo
- Publication number
- CN109264772A CN109264772A CN201811180637.8A CN201811180637A CN109264772A CN 109264772 A CN109264772 A CN 109264772A CN 201811180637 A CN201811180637 A CN 201811180637A CN 109264772 A CN109264772 A CN 109264772A
- Authority
- CN
- China
- Prior art keywords
- hothouse
- side wall
- basic lead
- spiral
- temperature control
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 20
- KEQXNNJHMWSZHK-UHFFFAOYSA-L 1,3,2,4$l^{2}-dioxathiaplumbetane 2,2-dioxide Chemical compound [Pb+2].[O-]S([O-])(=O)=O KEQXNNJHMWSZHK-UHFFFAOYSA-L 0.000 title claims abstract description 14
- 238000003756 stirring Methods 0.000 claims abstract description 34
- 239000007788 liquid Substances 0.000 claims abstract description 21
- 230000005540 biological transmission Effects 0.000 claims abstract description 20
- 235000009074 Phytolacca americana Nutrition 0.000 claims description 8
- 240000007643 Phytolacca americana Species 0.000 claims description 8
- 238000009434 installation Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- PIJPYDMVFNTHIP-UHFFFAOYSA-L Lead sulfate Chemical compound [PbH4+2].[O-]S([O-])(=O)=O PIJPYDMVFNTHIP-UHFFFAOYSA-L 0.000 abstract description 11
- 238000001035 drying Methods 0.000 abstract description 7
- 150000003467 sulfuric acid derivatives Chemical class 0.000 abstract description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 18
- 239000003381 stabilizer Substances 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 3
- 230000005712 crystallization Effects 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000006011 modification reaction Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000005864 Sulphur Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000003017 thermal stabilizer Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G21/00—Compounds of lead
- C01G21/20—Sulfates
Abstract
Four basic lead sulphate quick reaction devices are prepared the invention discloses a kind of, including pedestal and support frame, the side of pedestal is arranged in support frame as described above, the upper surface of the spiral liquid feeding device is communicated with feed liquor bucket, the other side of the Temperature control stirrer shell is equipped with temperature display, the output axis connection of stir chamber and motor one is run through in one end of the shaft, the side wall of the shaft is connected with stirring rod, the inner cavity of the stir chamber is provided with temperature monitoring, hothouse is provided with below the transmission device, the upper surface of the hothouse is connected with feed hopper, the inner wall of the hothouse is fixedly installed with splicing plate, the side of the hothouse is provided with pressure fan, the side of the pressure fan connects having heaters, the side wall of the air distributor is equipped with air supply tube.The present invention solves the problems, such as that existing four basic lead sulphates reaction unit easily causes crystal fineness uneven and lead sulfate plane of crystal uneven drying easily occurs.
Description
Technical field
The present invention relates to equipment of industrial product technical fields, specially a kind of to prepare four basic lead sulphate fast reactions dress
It sets.
Background technique
Four basic lead sulphates (abbreviation 4BS) are a kind of most common basic lead salt heat stabilizers, it can provide good
Thermal stability, electrical insulating property and good resistance to extractable, Lead salt thermal stabilizer are the thermostabilizations that polrvinyl chloride product uses earliest
Agent, it is now still a large amount of to use.The stabilizer is generally all with the ability of very strong combination hydrogen chloride, the knot of lead oxide and hydrogen chloride
Close it is very capable, but if will cause color articles as stabilizer, thus people just developed it is a series of with slag
Lead salt is used as heat stabilizer, and base lead salt is current most widely used lead stabilizer, but existing four alkali formula sulphur
There are the following problems for lead plumbate reaction unit: first is the existing agitating device for generating sulfuric acid leading crystal, since stirring is uneven, Yi Zao
At the phenomenon of crystal fineness unevenness；Second is existing four basic lead sulphates reaction unit when handling sulfuric acid leading crystal, is easily gone out
The problem of existing lead sulfate plane of crystal uneven drying.
Summary of the invention
Four basic lead sulphate quick reaction devices are prepared the purpose of the present invention is to provide a kind of, to solve above-mentioned background skill
The existing four basic lead sulphates reaction unit proposed in art easily causes crystal fineness uneven and lead sulfate plane of crystal easily occurs
The problem of uneven drying.
In order to solve the above technical problems, the invention provides the following technical scheme: a kind of to prepare four basic lead sulphates quickly anti-
Device, including pedestal and support frame are answered, the side of pedestal is arranged in support frame as described above, and the upper surface of the pedestal is connected with spiral
Liquid feeding device, the upper surface of the spiral liquid feeding device are communicated with feed liquor bucket, and the upper surface of support frame as described above is fixedly installed with temperature control and stirs
Device shell is mixed, the side of the Temperature control stirrer shell is connected with feed inlet, the other side installation of the Temperature control stirrer shell
There is a temperature display, the Temperature control stirrer shell is internally provided with stir chamber, on the inside of the Temperature control stirrer shell
Side is provided with motor one, and the inside of the stir chamber is equipped with shaft, and one end of the shaft is through stir chamber and motor one
Axis connection is exported, the side wall of the shaft is connected with stirring rod, and the inner cavity of the stir chamber is provided with temperature monitoring, the temperature
The lower end surface of control blender shell is connected with filter plate, and transmission device, the transmission device are provided with below the filter plate
Lower section be provided with hothouse, the upper surface of the hothouse is connected with feed hopper, and the inner wall of the hothouse is fixedly installed with
Splicing plate, the side of the hothouse are provided with pressure fan, and the side of the pressure fan connects having heaters, the heater
Side wall is equipped with air distributor, and the side wall of the air distributor is equipped with air supply tube, the side of the air supply tube and hothouse
Wall is fixedly connected.
Preferably, the spiral liquid feeding device includes spiral transmission blade and driving motor, the spiral transmission blade setting
Connect in one end of the inside of spiral liquid feeding device, the spiral transmission blade through the output shaft of spiral liquid feeding device and driving motor
It connects, the side wall of the stirring rod is provided with poke hole, and the quantity of the poke hole is set as three.
Preferably, the transmission device includes fixing seat, and the side wall of the fixing seat is provided with motor two, the fixing seat
Inner cavity be connected with rotation axis, the output axis connection of fixing seat and motor two, the rotation axis are run through in one end of the rotation axis
Side wall be provided with conveyer belt, the quantity of the splicing plate sets at least to two, and the tilt angle of the splicing plate installation exists
Between 30 ° to 35 °.
Preferably, the quantity of the air supply tube is set as three, and is evenly spaced on.
Preferably, it is electrically connected between the temperature monitoring and temperature display.
Compared with prior art, the beneficial effects of the present invention are:
1. lead powder is put into stir chamber by feed inlet first, distilled water is sent by spiral liquid feeding device by the present invention
In stir chamber, dilute sulfuric acid is then added according to a certain percentage, opens motor one at this time, then motor one drives shaft rotation,
By the way that stirring rod is fixedly connected on shaft side wall, mixing liquid, under the action of poke hole, Neng Goubao can be continuously agitated
Card stirs uniform, solves the problems, such as that fineness is uneven when lead sulfate crystallization.
2. by addition filter plate, can residue after filtering for crystallizing, under the action of transmission device, by sulfuric acid leading crystal
It is sent into hothouse, opens pressure fan and heater, the hot wind of generation, under the action of air distributor, by air-supply at this time
Pipe, into inside hothouse, by the way that splicing plate is fixedly mounted in the inner cavity of hothouse, it is dry that sulfuric acid leading crystal is capable of falling into for substep
Dry interior can uniformly dry lead sulfate plane of crystal by setting three for the quantity of air supply tube, solve four alkali formulas
Easily there is the problem of lead sulfate plane of crystal uneven drying in lead sulfate reaction unit.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of entirety of the embodiment of the present invention；
Fig. 2 is the structural schematic diagram of stirring rod of the embodiment of the present invention；
Fig. 3 is the side view of transmission device of the embodiment of the present invention.
In figure: 1, pedestal；2, spiral liquid feeding device；3, support frame；4, feed liquor bucket；5, feed inlet；6, Temperature control stirrer shell；
7, motor one；8, stir chamber；9, temperature monitoring；10, temperature display；11, shaft；12, stirring rod；13, filter plate；14,
Transmission device；15, feed hopper；16, air distributor；17, heater；18, pressure fan；19, air supply tube；20, hothouse；21,
Splicing plate；22, fixing seat；23, conveyer belt；24, rotation axis；25, motor two.
Specific embodiment
It easily causes crystal fineness uneven in order to solve existing four basic lead sulphates reaction unit and lead sulfate crystalline substance easily occurs
The problem of body surface face uneven drying, prepares four basic lead sulphate quick reaction devices the embodiment of the invention provides a kind of.Under
Face will combine the attached drawing in the embodiment of the present invention, and technical scheme in the embodiment of the invention is clearly and completely described, show
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1
Fig. 1-3 is please referred to, present embodiments provides and a kind of prepares four basic lead sulphate quick reaction devices, including pedestal 1
With support frame 3, the side of pedestal 1 is arranged in support frame 3, and the upper surface of pedestal 1 is connected with spiral liquid feeding device 2, spiral liquid feeding device 2
Blade and driving motor are transmitted including spiral, the inside of spiral liquid feeding device 2 is arranged in spiral transmission blade, and spiral transmits blade
The output axis connection of spiral liquid feeding device 2 and driving motor is run through in one end, and the upper surface of spiral liquid feeding device 2 is communicated with feed liquor bucket 4, props up
The upper surface of support 3 is fixedly installed with Temperature control stirrer shell 6, and the side of Temperature control stirrer shell 6 is connected with feed inlet 5, temperature
The other side of control blender shell 6 is equipped with temperature display 10, and Temperature control stirrer shell 6 is internally provided with stir chamber 8, temperature
Motor 1 is provided between control blender shell 6 and stir chamber 8, the inside of stir chamber 8 is equipped with shaft 11, and the one of shaft 11
The output axis connection of stir chamber 8 and motor 1 is run through at end, and the side wall of shaft 11 is connected with stirring rod 12, the side wall of stirring rod 12
It is provided with poke hole, the quantity of poke hole is set as three, and the inner cavity of stir chamber 8 is provided with temperature monitoring 9, Temperature control stirrer
The lower end surface of shell 6 is connected with filter plate 13, and the lower section of filter plate 13 is provided with transmission device 14, and transmission device 14 includes fixing
Seat 22, the side wall of fixing seat 22 is provided with motor 2 25, and the inner cavity of fixing seat 22 is connected with rotation axis 24, one end of rotation axis 24
Through the output axis connection of fixing seat 22 and motor 2 25, the side wall of rotation axis 24 is provided with conveyer belt 23, transmission device 14
Lower section is provided with hothouse 20, and the upper surface of hothouse 20 is connected with feed hopper 15, and the inner wall of hothouse 20, which is fixedly installed with, to be connect
Flitch 21, the quantity of splicing plate 21 set at least to two, and the tilt angle that splicing plate 21 is installed is dry between 30 ° to 35 °
The side of room 20 is provided with pressure fan 18, and the side of pressure fan 18 connects having heaters 17, and the side wall installation of heater 17 is free
Gas distributor 16, the side wall of air distributor 16 are equipped with air supply tube 19, and the quantity of air supply tube 19 is set as three, and uniformly between
Every distribution, air supply tube 19 is fixedly connected with the side wall of hothouse 20.
In the present embodiment, in the work of four basic lead sulphate quick reaction devices, lead powder is put by feed inlet 5 first
In stir chamber 8, distilled water is sent into stir chamber 8 by spiral liquid feeding device 2, dilute sulfuric acid is then added according to a certain percentage,
Motor 1 is opened at this time, then motor 1 drives shaft 11 to rotate, by the way that stirring rod 12 is fixedly connected on 11 side wall of shaft,
It can be continuously agitated mixing liquid, under the action of poke hole, can guarantee the uniform of stirring, when solving lead sulfate crystallization
The problem of fineness unevenness, by adding filter plate 13, can residue after filtering for crystallizing, sulfuric acid leading crystal falls into conveyer belt at this time
On 23, it is then turned on motor 2 25, drives rotation axis 24 to move by motor 2 25, and then conveyer belt 23 is driven to move, is passing
Under the action of sending device 14, sulfuric acid leading crystal is sent into hothouse 20, opens pressure fan 18 and heater 17 at this time, preferably
Pressure fan 18 and the model of heater 17 are respectively Y5-47II and A55TH, the hot wind of generation, in the effect of air distributor 16
Under, the model KQF-III of preferable air distributor 16, by air supply tube 19, into inside hothouse 20, by drying
The inner cavity of room 20 is fixedly mounted splicing plate 21, and sulfuric acid leading crystal is capable of the falling into hothouse 20 of substep, by by air supply tube 19
Quantity be set as three, can uniformly dry lead sulfate plane of crystal, solve four basic lead sulphate reaction units and easily go out
The problem of existing lead sulfate plane of crystal uneven drying.
Embodiment 2
Referring to Fig. 1, being electrically connected between temperature monitoring 9 and temperature display 10, the type of preferable temperature monitoring 9
Number it is M344830, by addition temperature monitoring 9 and temperature display 10, is capable of the temperature of real-time monitoring stir chamber 8, prevents
Because temperature is too low or excessively high, the crystallization of sulfuric acid leading crystal is influenced.
In this practical description, it should be noted that the orientation of the instructions such as term "vertical", "upper", "lower", "horizontal" or
Person's positional relationship is orientation based on the figure or positional relationship, is merely for convenience of this practical and simplified description of description,
Rather than the device or element of instruction or hint meaning must have a particular orientation, and are constructed and grasped with specific orientation
Make, therefore should not be understood as the limitation practical to this.
In this practical description, it is also necessary to explanation, unless otherwise specific regulation and limitation, term " setting ", " peace
Dress ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integrally
Connection, can be mechanical connection, is also possible to be electrically connected, can be and be directly connected to, and be also possible to be connected by intermediary, can
To be the connection inside two elements.For the ordinary skill in the art, can understand as the case may be above-mentioned
Concrete meaning of the term in this is practical.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (5)
1. a kind of prepare four basic lead sulphate quick reaction devices, it is characterised in that: described including pedestal (1) and support frame (3)
Support frame (3) is arranged in the side of pedestal (1), and the upper surface of the pedestal (1) is connected with spiral liquid feeding device (2), the spiral
The upper surface of liquid feeding device (2) is equipped with feed liquor bucket (4), and the upper surface of support frame as described above (3) is fixedly installed with outside Temperature control stirrer
The side of shell (6), the Temperature control stirrer shell (6) is communicated with feed inlet (5), the Temperature control stirrer shell (6) it is another
Side is equipped with temperature display (10), and the Temperature control stirrer shell (6) is internally provided with stir chamber (8), and the temperature control is stirred
The inner upper for mixing device shell (6) is provided with motor one (7), and the inside of the stir chamber (8) is equipped with shaft (11), and described turn
The output axis connection of stir chamber (8) and motor one (7) is run through in one end of axis (11), and the side wall of the shaft (11) is connected with stirring
The inner cavity of bar (12), the stir chamber (8) is provided with temperature monitoring (9), and the lower end surface of the Temperature control stirrer shell (6) connects
It is connected to filter plate (13), is provided with transmission device (14) below the filter plate (13), the lower section of the transmission device (14)
It is provided with hothouse (20), the upper surface of the hothouse (20) is connected with feed hopper (15), the inner wall of the hothouse (20)
It being fixedly installed with splicing plate (21), the side of the hothouse (20) is provided with pressure fan (18), and the one of the pressure fan (18)
Side connects having heaters (17), and the side wall of the heater (17) is equipped with air distributor (16), the air distributor
(16) side wall is equipped with air supply tube (19), and the air supply tube (19) is fixedly connected with the side wall of hothouse (20).
2. a kind of four basic lead sulphate quick reaction devices are prepared according to claim 1, it is characterised in that: the spiral
Liquid feeding device (2) includes spiral transmission blade and driving motor, and the spiral transmission blade is arranged in the interior of spiral liquid feeding device (2)
The output axis connection of spiral liquid feeding device (2) and driving motor, the stirring rod are run through in the one end in portion, the spiral transmission blade
(12) side wall is provided with poke hole, and the quantity of the poke hole is set as three.
3. a kind of four basic lead sulphate quick reaction devices are prepared according to claim 1, it is characterised in that: the transmission
Device (14) includes fixing seat (22), and the side wall of the fixing seat (22) is provided with motor two (25), the fixing seat (22)
Inner cavity is connected with rotation axis (24), and one end of the rotation axis (24) connects through the output shaft of fixing seat (22) and motor two (25)
It connects, the side wall of the rotation axis (24) is provided with conveyer belt (23), and the quantity of the splicing plate (21) sets at least to two, institute
The tilt angle of splicing plate (21) installation is stated between 30 ° to 35 °.
4. a kind of four basic lead sulphate quick reaction devices are prepared according to claim 1, it is characterised in that: the air-supply
The quantity of pipe (19) is set as three, and is evenly spaced on.
5. a kind of four basic lead sulphate quick reaction devices are prepared according to claim 1, it is characterised in that: the temperature
It is electrically connected between monitor (9) and temperature display (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811180637.8A CN109264772B (en) | 2018-10-09 | 2018-10-09 | Preparation tetrabasic lead sulfate fast reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811180637.8A CN109264772B (en) | 2018-10-09 | 2018-10-09 | Preparation tetrabasic lead sulfate fast reaction device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109264772A true CN109264772A (en) | 2019-01-25 |
| CN109264772B CN109264772B (en) | 2021-03-02 |
Family
ID=65196462
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811180637.8A Active CN109264772B (en) | 2018-10-09 | 2018-10-09 | Preparation tetrabasic lead sulfate fast reaction device |
Country Status (1)
| Country | Link |
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| CN (1) | CN109264772B (en) |
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| CN103413937A (en) * | 2013-08-29 | 2013-11-27 | 天能集团江苏特种电源有限公司 | Method for synthesizing high-purity four-basic lead sulfate and application thereof |
| CN103803641A (en) * | 2012-12-17 | 2014-05-21 | 天能电池(芜湖)有限公司 | Preparation method of four-alkali sulfuric acid lead |
| CN106564941A (en) * | 2016-11-04 | 2017-04-19 | 浙江兜兰智能设备股份有限公司 | Method for preparing tetrabasic lead sulfate |
| CN107628638A (en) * | 2017-09-30 | 2018-01-26 | 浙江兜兰智能设备股份有限公司 | A kind of four basic lead sulphate productions prepare after-treatment system |
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| CN207391018U (en) * | 2017-09-30 | 2018-05-22 | 浙江兜兰智能设备股份有限公司 | A kind of four basic lead sulphate productions prepare after-treatment system |
-
2018
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| CN106564941A (en) * | 2016-11-04 | 2017-04-19 | 浙江兜兰智能设备股份有限公司 | Method for preparing tetrabasic lead sulfate |
| CN207050377U (en) * | 2017-07-21 | 2018-02-27 | 深圳市天杞园云商网络有限公司 | A kind of drying plant |
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