CN109260815A - A kind of organosilicon slag slurry processing method - Google Patents
A kind of organosilicon slag slurry processing method Download PDFInfo
- Publication number
- CN109260815A CN109260815A CN201811121262.8A CN201811121262A CN109260815A CN 109260815 A CN109260815 A CN 109260815A CN 201811121262 A CN201811121262 A CN 201811121262A CN 109260815 A CN109260815 A CN 109260815A
- Authority
- CN
- China
- Prior art keywords
- tank body
- slag slurry
- organosilicon slag
- cylinder
- screw rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/001—Filters in combination with devices for the removal of gas, air purge systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/003—Filters in combination with devices for the removal of liquids
- B01D36/006—Purge means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/44—Mixers with shaking, oscillating, or vibrating mechanisms with stirrers performing an oscillatory, vibratory or shaking movement
- B01F31/443—Mixers with shaking, oscillating, or vibrating mechanisms with stirrers performing an oscillatory, vibratory or shaking movement performing a superposed additional movement other than oscillation, vibration or shaking
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention belongs to technical field of organic silicon production, specifically a kind of organosilicon slag slurry processing method, processing unit used in this method includes cover, tank body, feed inlet, discharge port and gas outlet, feed inlet and gas outlet are provided on the cover, pass through flanged joint between the cover and tank body, the tank base is provided with discharge port, is provided with controller on the outside of the tank body；The motor is mounted in mounting bracket, and the motor output shaft is connect with shaft；It is fixedly connected in shaft in the middle part of the support rod, is connected on support rod at the top of support frame as described above, the shaft bottom is connected No.1 cylinder, and the telescopic rod of No.1 cylinder passes through support frame and is connected to stirring module；Processing unit used in the present invention moves back and forth up and down the intracorporal organosilicon slag slurry of agitator tank while driving stirring module rotation by No.1 cylinder, so that the stirring of organosilicon slag slurry is abundant, the evaporation efficiency for improving device, realizes being effectively treated for organosilicon slag slurry.
Description
Technical field
The invention belongs to technical field of organic silicon production, specifically a kind of organosilicon slag slurry processing method.
Background technique
Organosilicon slag slurry is generated waste in organic silicon monomer especially methyl chlorosilane monomer synthesis process,
Mainly by a large amount of high-boiling components and a small amount of fluidized bed take unreacted silicon powder out of, copper powder forms, high-boiling components refer to methylchlorosilane
70.3~250 DEG C of the boiling range generated in monomer synthesis process, the height based on silicon-silicon key, silicon-carbon-silicon key, silicon-oxygen-silicon
Boiling point multi-silane mixture.If the exposure of this partial material is in air, it will burn or form strong acid mist or liquid, therefore such as
Fruit direct emission can cause environment seriously to pollute, it is necessary to carry out Harmless processing.Currently, processing of the manufacturing enterprise to slurry
Method is to be recycled high-boiling components therein by separating mostly, and the slurry after separating high-boiling components, which is directly discharged into water, to be hydrolyzed.Because of slag
Contain part high-boiling components in slurry, a large amount of acid mists hydrolyzed to form are easy excessive, cause the pollution to environment.
Also occur the technical solution of some organosilicon slag slurries processing in the prior art, such as application No. is
2008101953752 Chinese patent discloses the processing method and its device of a kind of organosilicon slag slurry, which will have
After the preheating of machine silicon slurry, it is passed through taper evaporator, steams high-boiling components by stirring, condensation is collected to storage tank, residual residue row
Out.The invention also discloses a kind of taper evaporators.Organosilicon slag slurry processing method of the invention overcomes big in the prior art
The irretrievable disadvantage of high-boiling components is measured, is as far as possible steamed high-boiling components in the case where guaranteeing that slurry is not agglomerated seriously, the rate of recovery
>=80%, the high-boiling components of recycling are cracked to obtain methyl chlorosilane monomer, and evaporation is residue obtained to be recycled well, no
Environmental protection and safety problem are addressed only, and saves slurry processing cost；But only by helical screw agitator in the technical solution, not
It is able to achieve being sufficiently stirred for organosilicon slag slurry, and the heat insulation effect of device is not directed to, treatment effeciency needs to be further increased.
For above situation, the invention proposes a kind of organosilicon slag slurry processing method, dress is handled used in this method
It sets and moves back and forth up and down the intracorporal organosilicon slag slurry of agitator tank while driving stirring module rotation by No.1 cylinder, to make
The stirring for obtaining organosilicon slag slurry is abundant, improves the evaporation efficiency of device, realizes being effectively treated and avoiding pollution for organosilicon slag slurry
Environment.
Summary of the invention
In order to make up for the deficiencies of the prior art, a kind of organosilicon slag slurry processing method proposed by the present invention, the master of this method
The environmental pollution for being to avoid in organosilicon slag slurry treatment process of syllabus.Processing unit used in this method passes through will be organic
Silicon slurry preheating after imported into tank body by feed inlet, controller control heat block heated, electric motor starting, motor driven
Shaft rotation, so that No.1 rotational cylinder is driven, so that stirring module rotates the intracorporal organosilicon slag slurry of agitator tank, when shaft turns
While dynamic, support rod is rotated with it, and drives support frame rotation, so that rotation leaf rotation, the protrusion rotation rotated on leaf is squeezed
Air bag, the gas in air bag are imported by conduit in the air cavity of No.1 cylinder, so that No.1 cylinder drives agitation module rotation
It back and forth moves up and down simultaneously, so that stirring organosilicon slag slurry, and then improves the working efficiency of device.
The technical solution adopted by the present invention to solve the technical problems is: a kind of organosilicon slag slurry processing method, this method
Steps are as follows:
S1: organosilicon slag slurry is imported in processing unit, carries out heating evaporation, after the high-boiling components vaporization in organosilicon slag slurry
It exports in condenser from the gas outlet of processing unit, is collected into holding vessel after condensation, remaining solid slag is from discharge port
It excludes；
S2: the solid slag in S1 being passed into hydrolytic decomposition pot, is hydrolyzed, and buck is housed in the hydrolytic decomposition pot,
Solid slag is passed through in hydrolytic decomposition pot to react with buck, generates organosilicon slag slurry hydrolysate and hydrogen chloride gas, the hydrogen chloride of generation
Gas is reacted with buck generates water；Hydrogen chloride gas have corrosivity, be directly discharged into air and will cause pollution, by with alkali
Water, which sufficiently reacts, to be avoided hydrogen chloride gas and is vented directly in air, and environment is polluted；
S3: using grid plate by S2 in hydrolytic decomposition pot organosilicon slag slurry hydrolysate and water separate, by water it is cooling after
It is passed into condenser by pipeline as cooling water；
S4: the water in S3 in condenser is passed into processing unit by pipeline, processing unit is cleaned；
Wherein, the processing unit includes cover, tank body, feed inlet, discharge port and gas outlet, is provided on the cover
Feed inlet and gas outlet, by flanged joint between the cover and tank body, the tank body is tapered, the tank base setting
There is discharge port, is provided with controller on the outside of the tank body；It further include motor, shaft, mounting bracket, support rod, support frame, gas
Capsule, No.1 cylinder, stirring module and support column, the tank body outer layer are provided with mud layer, the mud layer be used for tank body into
Row heat-insulation and heat-preservation；The motor is mounted in mounting bracket, controller control motor rotation, the motor output shaft with turn
Axis connection；The mounting bracket bottom is fixedly mounted on cover, is slidably fitted with support rod in the mounting bracket；The branch
It is fixedly connected in shaft, is connected on support rod at the top of support frame as described above, support frame as described above is cylindrical tube, institute in the middle part of strut
It states support frame bottom and is circumferentially provided with one group of rotation leaf, a protrusion is equipped on the rotation leaf, is set on the cover inner wall
There is one group of air bag, air bag can be expressed to when the protrusion is with rotation leaf rotation；The air bag is connected to the air cavity of No.1 cylinder；
The shaft bottom is connected No.1 cylinder, and the No.1 cylinder is located inside support frame and the telescopic rod of No.1 cylinder passes through
Support frame bottom is connected to stirring module；The stirring module is used for the intracorporal organosilicon slag slurry of agitator tank；
Wherein, the stirring module includes turntable, gear and screw rod, and the turntable is circumferentially uniformly distributed, and there are four sliding slots, described
Screw rod is slidably fitted in sliding slot, the screw rod is connected in sliding slot by spring；It is equipped at the top and bottom of the turntable
The gear being meshed with screw rod, times of a height of reference addendum of the tooth of the gear, is equipped between adjacent gear on the turntable and leads to
Slot is mounted on paddle in the through slot；It is fixedly installed with heat block at the top and bottom of the turntable middle position, it is described
Heat block heating is controlled by the controller, and the telescopic rod bottom end of the No.1 cylinder passes through heat block and support column is connected, the branch
Inner cavity is equipped with inside dagger, the inner cavity is connected to the cavity that screw rod and sliding slot are formed, and passes through ball-screw in the support column
Pair is connected to connecting rod, and the connecting rod bottom end is connected fan.In use, being passed into after organosilicon slag slurry is preheated from feed inlet
In tank body, controller controls motor and heat block starting, and tank body temperature gradually rises, and motor drives shaft rotation, rotates band
The connected No.1 rotational cylinder in dynamic bottom, No.1 rotational cylinder drive telescopic rod rotation, so that stirring module rotates with it,
The organosilicon slag slurry entered in stirring module agitator tank body when dropping on turntable, has when organosilicon slag slurry is passed into tank body
Machine silicon slurry is pounded on the paddle fallen on turntable in through slot, and paddle can be with rotation be generated, to preferably stir organic
Silicon slurry, so that evaporation efficiency improves；Shaft drives connected support rod rotation simultaneously, and support rod drives connected support frame to turn
Dynamic, support frame drives rotation leaf to rotate, the air bag on the periodical extruding cover inner wall of the protrusion that top is equipped with when rotating leaf rotation,
It is imported by tracheae in the air cavity of No.1 cylinder after gas in air bag is compressed, the pressure increase in No.1 cylinder air cavity,
To push the telescopic rod of No.1 cylinder to move back and forth up and down, so that stirring module is driven up and down reciprocatingly to stir organosilicon slag slurry,
So that organosilicon slag slurry stirring is more uniform, to improve the working efficiency of device；When stirring module moves back and forth up and down,
Middle screw rod, which synchronizes, to be moved up and down, and since tank body is tapered, is reciprocatingly slided in sliding slot when screw rod moves back and forth up and down on turntable,
It is rotated to push with screw rod meshed gears, so that gear positive and negative rotation, since the tooth height of gear is higher, when gear turns
It is dynamic more preferable to the mixing effect of organosilicon slag slurry, to further improve the working efficiency of device；Wherein heat block is directly right
Turntable heating, improves heating efficiency；Simultaneously when turntable moves back and forth up and down, screw rod reciprocatingly slides in sliding slot, works as screw rod
It up moves while when toward sliding slot internal slide, is passed into the inner cavity of support column after the gas in air cavity is compressed by tracheae
Interior, the pressure of the inner cavity of support column increases, so that the fan of bottom be pushed to rotate clockwise；When screw rod moves down, while
When sliding outward under the action of spring, negative pressure is formed in the air cavity in sliding slot, so that gas intracavitary in support column passes through tracheae
It is drawn into air cavity, while connecting rod is up moved, fan is driven to rotate counterclockwise；Clockwise and anticlockwise with fan
Rotation, thus the preferably intracorporal organosilicon slag slurry of agitator tank, and then improve the working efficiency of device.
Preferably, the screw rod is fixed with elastic piece close to inner tank wall one end, and the elastic piece is arc-shaped, elastic piece
For striking off the solid residue in inner tank wall.In use, screw rod is connected the elastic piece of arc close to inner tank wall one end, when
When turntable moves back and forth up and down under the action of the telescopic rod of No.1 cylinder, screw rod synchronization back and forth moves in the inner tank wall of taper
It is dynamic, on the one hand the elastic piece of arc be driven back and forth to strike off the solid slag attached on inner wall, it on the other hand can be avoided silk
Bar is directly contacted with inner tank wall, improves the service life of screw rod.
Preferably, sealing ring is equipped between the flange, the sealing ring is closed between tank body and cover for improving
Property.In use, sealing ring is arranged between the flanges, the leakproofness of device can be improved, so that the intracorporal temperature of tank is not easy
It is lost, and then increases the utilization rate of the energy and the evaporation efficiency of device.
Preferably, elastic balloon layer is provided in the inner tank wall, the elastic balloon layer passes through in through-hole and tank body
Portion is connected to, and unidirectional filter membrane is provided in the inner tank wall on the inside of the elastic balloon layer, the unidirectional filter membrane is for preventing
The organosilicon slag slurry of tank interior is flowed into elastic balloon layer.In use, by the way that elastic balloon layer is arranged in inner tank wall,
When turntable moves back and forth up and down under the action of the telescopic rod of No.1 cylinder, screw rod is synchronous reciprocal in the inner tank wall of taper
It is mobile, to squeeze elastic balloon layer, on the one hand makes the gas in elastic balloon layer be injected to tank interior by through-hole, make
In tank body pressure increase, realize the stirring to organosilicon slag slurry, can be on the other hand the direct of screw rod and inner tank wall
Contact provides buffering, improves the service life of device；The unidirectional filter membrane of setting avoids the organosilicon of tank interior simultaneously
Slurry is flowed into elastic balloon layer.
Preferably, the inner tank wall on the inside of elastic balloon layer is made of aluminum alloy materials.In use, aluminum alloy materials system
At inner tank wall good heat conductivity so that when heat block in tank body to heating, temperature is promoted fast, and then improves dress
The evaporation efficiency set.
Preferably, setting one group of deflector hole in interval on the turntable.In use, the deflector hole being arranged on turntable, when organic
When silicon slurry is dropped on turntable from feed inlet, deflector hole whipping organosilicon slag slurry when rotation, thus to organosilicon slag slurry into
The first stirring of row, to improve the working efficiency of device.
Beneficial effects of the present invention are as follows:
1. a kind of organosilicon slag slurry processing method of the present invention, processing unit used in this method is by will be organic
Silicon slurry preheating after imported into tank body by feed inlet, controller control heat block heated, electric motor starting, motor driven
Shaft rotation, so that No.1 rotational cylinder is driven, so that stirring module rotates the intracorporal organosilicon slag slurry of agitator tank, when shaft turns
While dynamic, support rod is rotated with it, and drives support frame rotation, so that rotation leaf rotation, the protrusion rotation rotated on leaf is squeezed
Air bag, the gas in air bag are imported by conduit in the air cavity of No.1 cylinder, so that No.1 cylinder drives agitation module rotation
It back and forth moves up and down simultaneously, so that stirring organosilicon slag slurry, and then improves the working efficiency of device.
2. a kind of organosilicon slag slurry processing method of the present invention, processing unit used in this method passes through in screw rod
Close to the elastic piece of inner tank wall one end setting arc, when turntable moves back and forth up and down under the action of the telescopic rod of No.1 cylinder
When, screw rod synchronization moves back and forth in the inner tank wall of taper, on the one hand the elastic piece of arc be driven back and forth to strike off inner wall
On the solid slag that attaches, on the other hand can be avoided screw rod and directly contacted with inner tank wall, improve the service life of screw rod.
3. a kind of organosilicon slag slurry processing method of the present invention, processing unit used in this method passes through in flange
Between sealing ring is set, can be improved the leakproofness of device, so that the intracorporal temperature of tank not easily runs off, and then increase the energy
Utilization rate and device evaporation efficiency；Tank body by the way that elastic balloon layer is arranged in inner tank wall, on the inside of elastic balloon layer
Inner wall is made of aluminum alloy materials, and when turntable moves back and forth up and down under the action of the telescopic rod of No.1 cylinder, screw rod is same
Step moves back and forth in the inner tank wall of taper, to squeeze elastic balloon layer, on the one hand makes the gas in elastic balloon layer
It is injected to tank interior by through-hole, so that pressure increases in tank body, realizes the stirring to organosilicon slag slurry, another aspect energy
Buffering enough is provided with directly contacting for inner tank wall for screw rod, improves the service life of device；The unidirectional filtering of setting simultaneously
The organosilicon slag slurry that film avoids tank interior is flowed into elastic balloon layer.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is the flow chart of method of the invention；
Fig. 2 is the structural schematic diagram of processing unit used in the present invention；
Fig. 3 is the cross-sectional view in Fig. 2 at A-A；
In figure: cover 1, tank body 2, feed inlet 3, discharge port 4, gas outlet 5, flange 6, motor 7, shaft 8, mounting bracket 9,
Support rod 91, support frame 92, air bag 93, rotation leaf 94, protrusion 95, No.1 cylinder 10, stirring module 11, turntable 111, gear
112, screw rod 113, paddle 114, support column 12, heat block 13, fan 14, elastic piece 15, sealing ring 16, elastic balloon layer
17, deflector hole 18.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As shown in Figure 1 to Figure 3, a kind of organosilicon slag slurry processing method of the present invention, the method steps are as follows:
S1: organosilicon slag slurry is imported in processing unit, carries out heating evaporation, after the high-boiling components vaporization in organosilicon slag slurry
It exports in condenser from the gas outlet of processing unit, is collected into holding vessel after condensation, remaining solid slag is from discharge port
It excludes；
S2: the solid slag in S1 being passed into hydrolytic decomposition pot, is hydrolyzed, and buck is housed in the hydrolytic decomposition pot,
Solid slag is passed through in hydrolytic decomposition pot to react with buck, generates organosilicon slag slurry hydrolysate and hydrogen chloride gas, the hydrogen chloride of generation
Gas is reacted with buck generates water；Hydrogen chloride gas have corrosivity, be directly discharged into air and will cause pollution, by with alkali
Water, which sufficiently reacts, to be avoided hydrogen chloride gas and is vented directly in air, and environment is polluted；
S3: using grid plate by S2 in hydrolytic decomposition pot organosilicon slag slurry hydrolysate and water separate, by water it is cooling after
It is passed into condenser by pipeline as cooling water；
S4: the water in S3 in condenser is passed into processing unit by pipeline, processing unit is cleaned；
Wherein, the processing unit includes cover 1, tank body 2, feed inlet 3, discharge port 4 and gas outlet 5, on the cover 1
It is provided with feed inlet 3 and gas outlet 5, is connected between the cover 1 and tank body 2 by flange 6, the tank body 2 is tapered, described
2 bottom of tank body is provided with discharge port 4, is provided with controller on the outside of the tank body 2；Further include motor 7, shaft 8, mounting bracket 9,
Support rod 91, support frame 92, air bag 93, No.1 cylinder 10, stirring module 11 and support column 12,2 outer layer of tank body are provided with
Mud layer, the mud layer is for being thermally shielded heat preservation to tank body 2；The motor 7 is mounted in mounting bracket 9, the control
Device controls motor 7 and rotates, and 7 output shaft of motor is connect with shaft 8；9 bottom of mounting bracket is fixedly mounted on cover 1
On, support rod 91 is slidably fitted in the mounting bracket 9；It is fixedly connected in shaft 8 in the middle part of the support rod 91, the branch
It is connected at the top of support 92 on support rod 91, support frame as described above 92 is cylindrical tube, and 92 bottom of support frame as described above is circumferentially provided with
One group of rotation leaf 94, a protrusion 95 is equipped on the rotation leaf 94, and 1 inner wall of cover is equipped with one group of air bag 93, institute
Air bag 93 can be expressed to by stating when protrusion 95 is rotated with rotation leaf 94；The air bag 93 is connected to the air cavity of No.1 cylinder 10；Institute
8 bottom of shaft is stated to be connected No.1 cylinder 10, the No.1 cylinder 10 be located inside support frame 92 and No.1 cylinder 10 it is flexible
Bar passes through 92 bottom of support frame and is connected to stirring module 11；The stirring module 11 is used to stir the organosilicon slag slurry in tank body 2；
Wherein, the stirring module 11 includes turntable 111, gear 112 and screw rod 113, and the turntable 111 is circumferential to be evenly equipped with
Four sliding slots are slidably fitted with screw rod 113 in the sliding slot, and the screw rod 113 is connected in sliding slot by spring；Described turn
It is equipped with the gear 112 being meshed with screw rod 113 at the top and bottom of disk 111, the 3 of a height of reference addendum of tooth of the gear 112
Times, through slot is equipped on the turntable 111 between adjacent gear 112, is mounted on paddle 114 in the through slot；The turntable
Heat block 13 is fixedly installed at the top and bottom of 111 middle positions, the heating of heat block 13 is controlled by the controller, and described one
The telescopic rod bottom end of number cylinder 10 passes through heat block 13 and support column 12 is connected, and inner cavity is equipped with inside the support column 12, described
Inner cavity is connected to the cavity that screw rod 113 and sliding slot are formed, and is connected to connecting rod by ball screw assembly, in the support column 12, described
Connecting rod bottom end is connected fan 14.In use, being passed into tank body 2 from feed inlet 3, controller after organosilicon slag slurry is preheated
It controls motor 7 and heat block 13 starts, temperature gradually rises in tank body 2, and motor 7 drives shaft 8 to rotate, and rotation drives bottom solid
No.1 cylinder 10 even rotates, and the rotation of No.1 cylinder 10 drives telescopic rod rotation, so that stirring module 11 rotates with it, stirs
It mixes module 11 and stirs the organosilicon slag slurry entered in tank body 2, when organosilicon slag slurry is passed into tank body 2, drop on turntable 111
When, organosilicon slag slurry, which is pounded, to be fallen on the paddle 114 on turntable 111 in through slot, and paddle 114 can be rotated with generating, thus
Preferably stirring organosilicon slag slurry, so that evaporation efficiency improves；Shaft 8 drives connected support rod 91 to rotate simultaneously, support rod
91 drive connected support frame 92 to rotate, and support frame 92 drives rotation leaf 94 to rotate, and top is equipped with convex when rotation leaf 94 rotates
The 95 periodical air bags 93 squeezed on 1 inner wall of cover are played, No.1 gas is imported by tracheae after the gas in air bag 93 is compressed
In in the air cavity of cylinder 10, the pressure in 10 air cavity of No.1 cylinder increases, to push the telescopic rod of No.1 cylinder 10 up and down reciprocatingly
It is mobile, so that stirring module 11 is driven up and down reciprocatingly to stir organosilicon slag slurry, so that organosilicon slag slurry stirring is more uniform, thus
Improve the working efficiency of device；When stirring module 11 moves back and forth up and down, wherein screw rod 113, which synchronizes, is moved up and down, due to tank
Body 2 is tapered, reciprocatingly slides in the sliding slot on turntable 111 when screw rod 113 moves back and forth up and down, to push and screw rod 113
Meshed gears 112 rotates, so that 112 positive and negative rotation of gear, since the tooth height of gear 112 is higher, when gear 112 rotates
It is more preferable to the mixing effect of organosilicon slag slurry, to further improve the working efficiency of device；Wherein heat block 13 is directly right
Turntable 111 heats, and improves heating efficiency；Simultaneously when turntable 111 moves back and forth up and down, screw rod 113 is back and forth slided in sliding slot
It is dynamic, when screw rod 113 up moves while when toward sliding slot internal slide, branch is passed by tracheae after the gas in air cavity is compressed
Interior intracavitary, the pressure increase of the inner cavity of support column 12, so that the fan 14 of bottom be pushed to rotate clockwise of dagger 12；Work as screw rod
113 move down, while when sliding outward under the action of the spring, negative pressure are formed in air cavity, so that intracavitary in support column 12
Gas is drawn into the air cavity in sliding slot by tracheae, while connecting rod is up moved, and fan 14 is driven to rotate counterclockwise；With
The rotation clockwise and anticlockwise of fan 14, to preferably stir the organosilicon slag slurry in tank body 2, and then improve device
Working efficiency.
As one such embodiment, the screw rod 113 is fixed with elastic piece 15 close to 2 inner wall one end of tank body,
The elastic piece 15 is arc-shaped, and elastic piece 15 is used to strike off the solid residue on 2 inner wall of tank body.In use, screw rod 113 is close to tank
2 inner wall one end of body is connected the elastic piece 15 of arc, when turntable 111 under the action of the telescopic rod of No.1 cylinder 10 up and down reciprocatingly
When mobile, the synchronization of screw rod 113 moves back and forth on 2 inner wall of tank body of taper, on the one hand drive the elastic piece 15 of arc past
The solid slag attached on inner wall is struck off again, screw rod 113 is on the other hand can be avoided and directly contacts with 2 inner wall of tank body, improves silk
The service life of bar 113.
As one such embodiment, sealing ring 16 is equipped between the flange 6, the sealing ring 16 is for improving
Airtightness between tank body 2 and cover 1.In use, sealing ring 16 is arranged between flange 6, the leakproofness of device can be improved,
So that the temperature in tank body 2 not easily runs off, and then increase the utilization rate of the energy and the evaporation efficiency of device.
As one such embodiment, elastic balloon layer 17, the elastic balloon are provided on 2 inner wall of tank body
Layer 17 is provided with unidirectional filtering on 2 inner wall of tank body of 17 inside of elastic balloon layer by being connected to inside through-hole and tank body 2
Film, the unidirectional filter membrane is for preventing the organosilicon slag slurry inside tank body 2 from being flowed into elastic balloon layer 17.In use, logical
Cross on 2 inner wall of tank body setting elastic balloon layer 17, when turntable 111 under the action of the telescopic rod of No.1 cylinder 10 up and down reciprocatingly
When mobile, the synchronization of screw rod 113 moves back and forth on 2 inner wall of tank body of taper, to squeeze elastic balloon layer 17, on the one hand makes
Gas in elastic balloon layer 17 is injected to inside tank body 2 by through-hole, so that pressure increases in tank body 2, is realized to organic
On the other hand the stirring of silicon slurry can provide buffering with directly contacting for 2 inner wall of tank body for screw rod 113, improve device
Service life；The unidirectional filter membrane of setting avoids the organosilicon slag slurry inside tank body 2 and is flowed into elastic balloon layer 17 simultaneously.
As one such embodiment, 2 inner wall of tank body of 17 inside of elastic balloon layer uses aluminum alloy materials
It is made.In use, 2 inner wall good heat conductivity of tank body made of aluminum alloy materials, so that heat block 13 in tank body 2 to carrying out
When heating, temperature promotes evaporation efficiency that is fast, and then improving device.
As one such embodiment, setting one group of deflector hole 18 in interval on the turntable 111.In use, turntable
The deflector hole 18 being arranged on 111, when organosilicon slag slurry drops on turntable 111 from feed inlet 3, the deflector hole 18 when rotation is got rid of
Dynamic organosilicon slag slurry, to be stirred for the first time to organosilicon slag slurry, to improve the working efficiency of device.
In use, being passed into tank body 2 after organosilicon slag slurry is preheated from feed inlet 3, controller controls motor 7 and adds
Heat block 13 starts, and temperature gradually rises in tank body 2, and motor 7 drives shaft 8 to rotate, the No.1 cylinder that rotation drives bottom connected
10 rotations, the rotation of No.1 cylinder 10 drive telescopic rod rotation, so that stirring module 11 rotates with it, stirring module 11 is rotated
The organosilicon slag slurry entered in tank body 2 is stirred, it is organic when organosilicon slag slurry is passed into tank body 2, is dropped on turntable 111
Silicon slurry, which is pounded, to be fallen on the paddle 114 on turntable 111 in through slot, and paddle 114 can be with rotation be generated, to preferably stir
Organosilicon slag slurry is mixed, so that evaporation efficiency improves；Shaft 8 drives connected support rod 91 to rotate simultaneously, and support rod 91 drives phase
Support frame 92 even rotates, and support frame 92 drives rotation leaf 94 to rotate, 95 period of protrusion that top is equipped with when rotation leaf 94 rotates
Property squeeze air bag 93 on 1 inner wall of cover, the gas of No.1 cylinder 10 is imported into after the gas in air bag 93 is compressed by tracheae
In intracavitary, the pressure in 10 air cavity of No.1 cylinder increases, so that the telescopic rod of No.1 cylinder 10 is pushed to move back and forth up and down, thus
Stirring module 11 is driven up and down reciprocatingly to stir organosilicon slag slurry, so that organosilicon slag slurry stirring is more uniform, to improve device
Working efficiency；When stirring module 11 moves back and forth up and down, wherein screw rod 113, which synchronizes, is moved up and down, since tank body 2 is in cone
Shape reciprocatingly slides in the sliding slot on turntable 111 when screw rod 113 moves back and forth up and down, to push the tooth engaged with screw rod 113
112 rotation of wheel, so that 112 positive and negative rotation of gear, since the tooth height of gear 112 is higher, when gear 112 is rotated to organosilicon
The mixing effect of slurry is more preferable, to further improve the working efficiency of device；Wherein heat block 13 directly adds turntable 111
Heat improves heating efficiency；Simultaneously when turntable 111 moves back and forth up and down, screw rod 113 reciprocatingly slides in sliding slot, works as screw rod
113 up move while when toward sliding slot internal slide, are passed into support column 12 by tracheae after the gas in air cavity is compressed
Interior intracavitary, the pressure of the inner cavity of support column 12 increases, so that the fan 14 of bottom be pushed to rotate clockwise；When screw rod 113 down
When moving, while sliding outward under the action of the spring, negative pressure is formed in the air cavity in sliding slot, so that intracavitary in support column 12
Gas is drawn into air cavity by tracheae, while connecting rod is up moved, and fan 14 is driven to rotate counterclockwise；With fan 14
Rotation clockwise and anticlockwise, thus preferably stir tank body 2 in organosilicon slag slurry, and then improve device work effect
Rate；By the way that the elastic piece 15 of arc is arranged close to 2 inner wall one end of tank body in screw rod 113, when the stretching in No.1 cylinder 10 of turntable 111
When moving back and forth up and down under the action of contracting bar, the synchronization of screw rod 113 moves back and forth on 2 inner wall of tank body of taper, thus on the one hand
Drive arc elastic piece 15 back and forth strike off the solid slag attached on inner wall, on the other hand can be avoided screw rod 113 directly with
The contact of 2 inner wall of tank body, improves the service life of screw rod 113；Simultaneously by the way that sealing ring 16 is arranged between flange 6, can be improved
The leakproofness of device so that the temperature in tank body 2 not easily runs off, and then increases the utilization rate of the energy and the evaporation effect of device
Rate；By the way that elastic balloon layer 17 is arranged on 2 inner wall of tank body, 2 inner wall of tank body of 17 inside of elastic balloon layer uses aluminium alloy material
Material is made, and when turntable 111 moves back and forth up and down under the action of the telescopic rod of No.1 cylinder 10, screw rod 113 is synchronous in taper
2 inner wall of tank body on move back and forth, to squeeze elastic balloon layer 17, pass through the gas in elastic balloon layer 17
Through-hole is injected to inside tank body 2, so that pressure increases in tank body 2, is realized the stirring to organosilicon slag slurry, on the other hand can
Buffering is provided with directly contacting for 2 inner wall of tank body for screw rod 113, improves the service life of device；The unidirectional mistake of setting simultaneously
The organosilicon slag slurry that filter membrane avoids inside tank body 2 is flowed into elastic balloon layer 17.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", "front", "rear",
The orientation or positional relationship of the instructions such as "left", "right", "vertical", "horizontal", "top", "bottom" "inner", "outside" is based on attached drawing institute
The orientation or positional relationship shown, is merely for convenience of description of the present invention and simplification of the description, rather than the dress of indication or suggestion meaning
It sets or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as protecting the present invention
The limitation of range.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the above embodiments and description only describe originals of the invention
Reason, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes and improvements
It all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appended claims and its equivalent circle
It is fixed.
Claims (6)
1. a kind of organosilicon slag slurry processing method, which is characterized in that the method steps are as follows:
S1: organosilicon slag slurry is imported in processing unit, carries out heating evaporation, after the high-boiling components vaporization in organosilicon slag slurry from
The gas outlet of reason device exports in condenser, is collected into holding vessel after condensation, remaining solid slag is excluded from discharge port；
S2: the solid slag in S1 being passed into hydrolytic decomposition pot, is hydrolyzed, and buck, solid are housed in the hydrolytic decomposition pot
Waste residue is passed through in hydrolytic decomposition pot to react with buck, generates organosilicon slag slurry hydrolysate and hydrogen chloride gas, the hydrogen chloride gas of generation
It is reacted with buck and generates water；
S3: using grid plate by S2 in hydrolytic decomposition pot organosilicon slag slurry hydrolysate and water separate, will water it is cooling after pass through
Pipeline is passed into condenser as cooling water；
S4: the water in S3 in condenser is passed into processing unit by pipeline, processing unit is cleaned；
Wherein, the processing unit includes cover (1), tank body (2), feed inlet (3), discharge port (4) and gas outlet (5), described
It is provided with feed inlet (3) and gas outlet (5) on cover (1), is connected between the cover (1) and tank body (2) by flange (6),
The tank body (2) is tapered, and tank body (2) bottom is provided with discharge port (4), is provided with controller on the outside of the tank body (2)；
It further include motor (7), shaft (8), mounting bracket (9), support rod (91), support frame (92), air bag (93), No.1 cylinder
(10), module (11) and support column 12 are stirred, tank body (2) outer layer is provided with mud layer, and the mud layer is used for tank body
(2) it is thermally shielded heat preservation；The motor (7) is mounted on mounting bracket (9), controller control motor (7) rotation, described
Motor (7) output shaft is connect with shaft (8)；Mounting bracket (9) bottom is fixedly mounted on cover (1), the installation branch
Support rod (91) are slidably fitted in frame (9)；It is fixedly connected on shaft (8) in the middle part of the support rod (91), support frame as described above
(92) top is connected on support rod (91), and support frame as described above (92) is cylindrical tube, and support frame as described above (92) bottom is circumferentially set
It is equipped with one group of rotation leaf (94), a protrusion (95) is equipped on the rotation leaf (94), cover (1) inner wall is equipped with one
Group air bag (93) can be expressed to air bag (93) when the protrusion (95) is with rotation leaf (94) rotation；The air bag (93) and one
The air cavity connection of number cylinder (10)；Shaft (8) bottom is connected No.1 cylinder (10), and the No.1 cylinder (10) is located at branch
The telescopic rod of support (92) inside and No.1 cylinder (10) passes through support frame (92) bottom and is connected to stirring module (11)；It is described
Stirring module (11) is used to stir the organosilicon slag slurry in tank body (2)；
Wherein, the stirring module (11) includes turntable (111), gear (112) and screw rod (113), and the turntable (111) is circumferential
It is uniformly distributed there are four sliding slot, be slidably fitted with screw rod (113) in the sliding slot, the screw rod (113) is connected to cunning by spring
In slot；The gear (112) being meshed with screw rod (113), the gear (112) are equipped at the top and bottom of the turntable (111)
High 3 times of a height of full-height tooth gear teeth of tooth, through slot is equipped on the turntable (111) between adjacent gear (112), in the through slot
It is mounted on paddle (114)；The top and bottom in turntable (111) middle position are fixedly installed with heat block (13),
Heat block (13) heating is controlled by the controller, and the telescopic rod bottom end of the No.1 cylinder (10) passes through heat block (13) and branch
Dagger (12) is connected, and inner cavity is equipped with inside the support column (12), and the cavity that the inner cavity and screw rod (113) and sliding slot are formed connects
It is logical, connecting rod is connected to by ball screw assembly, in the support column (12), the connecting rod bottom end is connected fan (14).
2. a kind of organosilicon slag slurry processing method according to claim 1, it is characterised in that: the screw rod (113) is close
Tank body (2) inner wall one end is fixed with elastic piece (15), and the elastic piece (15) is arc-shaped, and elastic piece (15) is for striking off tank body
(2) solid residue on inner wall.
3. a kind of organosilicon slag slurry processing method according to claim 1, it is characterised in that: set between the flange (6)
Have sealing ring (16), sealing ring (16) is used to improve the airtightness between tank body (2) and cover (1).
4. a kind of organosilicon slag slurry processing method according to claim 1, it is characterised in that: on tank body (2) inner wall
It is provided with elastic balloon layer (17), the elastic balloon layer (17) inside through-hole and tank body (2) by being connected to, the elastic balloon
Unidirectional filter membrane is provided on tank body (2) inner wall on the inside of layer (17), unidirectional filter membrane is used to prevent tank body (2) internal organic
Silicon slurry is flowed into elastic balloon layer (17).
5. a kind of organosilicon slag slurry processing method according to claim 4, it is characterised in that: the elastic balloon layer (17)
Tank body (2) inner wall of inside is made of aluminum alloy materials.
6. a kind of organosilicon slag slurry processing method according to claim 1, it is characterised in that: between on the turntable (111)
Every one group of deflector hole (18) of setting.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811121262.8A CN109260815A (en) | 2018-09-26 | 2018-09-26 | A kind of organosilicon slag slurry processing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811121262.8A CN109260815A (en) | 2018-09-26 | 2018-09-26 | A kind of organosilicon slag slurry processing method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109260815A true CN109260815A (en) | 2019-01-25 |
Family
ID=65198929
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811121262.8A Pending CN109260815A (en) | 2018-09-26 | 2018-09-26 | A kind of organosilicon slag slurry processing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109260815A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111545153A (en) * | 2020-05-11 | 2020-08-18 | 蒋克钟 | Simple and easy fast reactor is used in chemistry experiment room |
| CN113478712A (en) * | 2021-08-06 | 2021-10-08 | 抚州市天和硅业有限责任公司 | Organosilicon sediment thick liquid processing apparatus |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU633846A1 (en) * | 1977-05-03 | 1978-11-25 | Государственный Научно-Исследовательский Институт Кварцевого Стекла | Charge for making refractory articles |
| CN101386626A (en) * | 2008-10-31 | 2009-03-18 | 江苏宏达新材料股份有限公司 | Organosilicon slag slurry treatment method and apparatus thereof |
| CN103537247A (en) * | 2012-07-17 | 2014-01-29 | 上海氟聚化学产品有限公司 | Organic silicon scrap treatment device |
| CN103553051A (en) * | 2013-10-29 | 2014-02-05 | 泸州北方化学工业有限公司 | Method for separating solids from liquid of dregs in production process of organic silicon |
| CN105037414A (en) * | 2015-07-29 | 2015-11-11 | 湖北兴瑞化工有限公司 | Method and device for recovering efficient high-boiling substance from organic silicon residue slurry |
| CN106220666A (en) * | 2016-07-18 | 2016-12-14 | 聊城市鲁西化工工程设计有限责任公司 | The processing system of a kind of organic silicon slurry slag and processing method |
| CN106492725A (en) * | 2016-11-18 | 2017-03-15 | 广西大学 | A kind of chemical industry stirred-tank reactor of achievable high-low-position treatment effect |
-
2018
- 2018-09-26 CN CN201811121262.8A patent/CN109260815A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU633846A1 (en) * | 1977-05-03 | 1978-11-25 | Государственный Научно-Исследовательский Институт Кварцевого Стекла | Charge for making refractory articles |
| CN101386626A (en) * | 2008-10-31 | 2009-03-18 | 江苏宏达新材料股份有限公司 | Organosilicon slag slurry treatment method and apparatus thereof |
| CN103537247A (en) * | 2012-07-17 | 2014-01-29 | 上海氟聚化学产品有限公司 | Organic silicon scrap treatment device |
| CN103553051A (en) * | 2013-10-29 | 2014-02-05 | 泸州北方化学工业有限公司 | Method for separating solids from liquid of dregs in production process of organic silicon |
| CN105037414A (en) * | 2015-07-29 | 2015-11-11 | 湖北兴瑞化工有限公司 | Method and device for recovering efficient high-boiling substance from organic silicon residue slurry |
| CN106220666A (en) * | 2016-07-18 | 2016-12-14 | 聊城市鲁西化工工程设计有限责任公司 | The processing system of a kind of organic silicon slurry slag and processing method |
| CN106492725A (en) * | 2016-11-18 | 2017-03-15 | 广西大学 | A kind of chemical industry stirred-tank reactor of achievable high-low-position treatment effect |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111545153A (en) * | 2020-05-11 | 2020-08-18 | 蒋克钟 | Simple and easy fast reactor is used in chemistry experiment room |
| CN113478712A (en) * | 2021-08-06 | 2021-10-08 | 抚州市天和硅业有限责任公司 | Organosilicon sediment thick liquid processing apparatus |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109260815A (en) | A kind of organosilicon slag slurry processing method | |
| CN103591780B (en) | The main drying of the continuous drying system of slurry or powder | |
| CN109157852A (en) | A kind of organosilicon slag slurry processing unit | |
| CN208975806U (en) | A kind of stirring apparatus for reaction kettle with elevating hopper | |
| CN212328259U (en) | Nontoxic apparatus for producing for phosphite | |
| CN210057736U (en) | Cable insulation blendor dust collector of resources are saved | |
| CN110772830B (en) | Cold crystallizer for chemical production | |
| CN210496376U (en) | Reaction device for producing water-based paint | |
| CN209828986U (en) | Toluene diamine liquid phase processing apparatus | |
| CN219502714U (en) | Reaction kettle for boehmite | |
| CN218502060U (en) | Tea saponin type shampoo making devices | |
| CN217614377U (en) | A raw materials mixing apparatus for cleaner production | |
| CN114485190B (en) | Continuous calcination device for processing pearlescent material with high production efficiency | |
| CN211384928U (en) | 5-methyl-1 production preparation medicament dropwise add device | |
| CN211659904U (en) | Based on solution freeze concentration raw material mixing jar for system | |
| CN209836096U (en) | Improved VCM production equipment | |
| CN110407425A (en) | A kind of environmentally protective coal slime drying and upgrading equipment | |
| CN212092251U (en) | Novel condensation reaction kettle | |
| CN220609141U (en) | Continuous mixing device for acetonitrile rectification | |
| CN220846012U (en) | Spice concentration equipment | |
| CN218012684U (en) | Reation kettle of hydroxyethyl urea production and processing usefulness | |
| CN218686421U (en) | Distillation kettle heat preservation heating structure | |
| CN110586006A (en) | Reaction kettle with novel stirring device | |
| CN214808527U (en) | Heating device for be used for diethyl phosphite to refine | |
| CN217856139U (en) | Reaction unit is used in poly aluminium chloride production |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |