CN109260347A - A kind of rhizoma cyperi saponins compound separating and extracting process - Google Patents
A kind of rhizoma cyperi saponins compound separating and extracting process Download PDFInfo
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- CN109260347A CN109260347A CN201811246456.0A CN201811246456A CN109260347A CN 109260347 A CN109260347 A CN 109260347A CN 201811246456 A CN201811246456 A CN 201811246456A CN 109260347 A CN109260347 A CN 109260347A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/89—Cyperaceae (Sedge family)
- A61K36/8905—Cyperus (flatsedge)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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Abstract
The invention belongs to technical field of biological extraction, a kind of rhizoma cyperi saponins compound separating and extracting process is disclosed, the rhizoma cyperi saponins compound separation and Extraction system includes: weight detecting module, temperature detecting module, pressure detection module, main control module, crushes module, sterilization module, concentration module, stirring module, irradiation modules, fault detection module, display module.The present invention can reach 99% or more by the Detection accuracy of temperature detecting module measuring targets, error is almost can be controlled within 1%, adjust automatically temperature test point automatically generates temperature curve report, the abnormality of examined object is carried out efficiently and precise positioning, while improving extraction quality；Meanwhile fault detection module avoids dangerous generation, improves safety by may be implemented to find potential risk in time to the detection of dynamic circuit incipient fault in the case where not influencing system normal operation.
Description
Technical field
The invention belongs to technical field of biological extraction more particularly to a kind of rhizoma cyperi saponins compound separating and extracting process.
Background technique
Saponin(e is the compound that structure is more complicated in glycoside.They are widely present in plant, many kinds of, composition
It is complicated.It is very active to the research of saponin(e in the world, enter a new climax eighties.Not only some complicated soaps
The structure of glycosides is confirmed, and correct for certain mistakes in previous Structural Identification, their system researches it is many it is important in
Saponin(e in herbal medicine.Saponin(e is made of sapogenin and sugar.Composition saponin(e sugar common are glucose, galactolipin, rhamnose, Ah
Draw uncle's sugar, xylose, glucuronic acid and galacturonic acid etc..Aglycon is that the saponin(e of spirostane class (C-27 steroidal compounds) claims
For steroid saponin, it is primarily present in Dioscoreaceae, Liliaceae and Scrophulariaceae etc..Carboxyl is free of in molecule, is in neutrality.Avenacoside D
It is common steroid saponin with Dioscin.Aglycon is that the saponin(e of triterpenes is known as triterpenoid saponin, is primarily present in Araliaceae, beans
Section, Polygalaceae and Curcurbitaceae etc., kind of analogy steroid saponin is more, is distributed also more extensive.Most of triterpenoid saponin is few in acidity
Number is in neutrality.Saponin(e connects the difference of sugar chain number according to aglycon, can be divided into monodesmosidic saponin, bisdesmoside and three sugar chain soaps
Glycosides.On the sugar chain of some saponin(es, other groups are also connected with by ester bond.However, existing rhizoma cyperi saponins compound separation mentions
During taking, temperature data detection inaccuracy influences the quality extracted；Meanwhile separation and Extraction relevant device control circuit cannot
Equipment fault is detected in time, safety is low.
In conclusion problem of the existing technology is: during existing rhizoma cyperi saponins compound separation and Extraction, temperature
Data Detection inaccuracy, influences the quality extracted；Meanwhile separation and Extraction relevant device control circuit cannot be in time to equipment fault
It is detected, safety is low.
Summary of the invention
In view of the problems of the existing technology, the present invention provides a kind of rhizoma cyperi saponins compound separating and extracting process.
The invention is realized in this way a kind of rhizoma cyperi saponins compound separation and Extraction system includes:
Weight detecting module, pressure detection module, main control module, crushes module, is sterilization module, dense temperature detecting module
Contracting module, stirring module, irradiation modules, fault detection module, display module.
Weight detecting module, connect with main control module, for passing through weighing apparatus Detection and Extraction raw material weight data；
Temperature detecting module is connect with main control module, when for by temperature sensor Detection and Extraction saponins compound
Temperature data；
Pressure detection module, connect with main control module, when for by pressure transducer Detection and Extraction saponins compound
Pressure data；
Main control module, with weight detecting module, temperature detecting module, pressure detection module, crush module, sterilization module,
Module, stirring module, irradiation modules, fault detection module, display module connection is concentrated, it is each for being controlled by single-chip microcontroller
A module works normally；
Module is crushed, is connect with main control module, for being crushed by pulverizer control model；
Sterilization module is connect with main control module, for by ultraviolet radiator to carrying out illumination-based disinfection after crushing；
Module is concentrated, is connect with main control module, for that will be maintained using deionized water as solvent by vacuum decker
Under 0.1 atmospheric pressure state, 75 DEG C are taken ethanol-water to extract 1 hour, and the filtrate of collection is concentrated in vacuo to filtrate volume
One third；
Module is stirred, connect with main control module, for being stirred alcohol and concentrate by blender, is collected by filtration
Filtrate and precipitating；
Irradiation modules are connect with main control module, and for being dried in vacuo precipitating by 80 DEG C by heater, filtrate is used
It depressurizes rotary evaporation and removes ethyl alcohol, low temperature drying obtains rhizoma cyperi saponins compound；
Fault detection module, connect with main control module, for being believed by circuit signal collector detection circuit failure
Breath；
Display module is connect with main control module, for being believed by the weight, temperature, pressure data of display display detection
Breath.
A kind of rhizoma cyperi saponins compound separating and extracting process the following steps are included:
Step 1 utilizes weighing apparatus Detection and Extraction raw material weight data by weight detecting module；Pass through temperature detection mould
Block utilizes temperature data when temperature sensor Detection and Extraction saponins compound；Pressure sensing is utilized by pressure detection module
Pressure data when device Detection and Extraction saponins compound；
Step 2, main control module scheduling are crushed module and are crushed using pulverizer control model；It is utilized by sterilization module ultraviolet
Line lamp is to carrying out illumination-based disinfection after crushing；
Step 3 will maintain 0.1 atmosphere using deionized water as solvent using vacuum decker by concentration module
Under pressure condition, 75 DEG C take ethanol-water extract 1 hour, the filtrate of collection, be concentrated in vacuo to filtrate volume three/
One；
Alcohol and concentrate are stirred by stirring module using blender, filtrate are collected by filtration and sinks by step 4
It forms sediment；
Precipitating is dried in vacuo by step 5 by irradiation modules using heater by 80 DEG C, and filtrate is using decompression rotation
Evaporative removal ethyl alcohol, low temperature drying obtain rhizoma cyperi saponins compound；
Step 6 utilizes circuit signal collector detection circuit fault message by fault detection module；By aobvious
Show module using weight, the temperature, pressure data information of display display detection.
Further, the temperature detecting module detection method is as follows:
(1) temperature information of object under test in detection platform is obtained in the first preset time；
(2) temperature information for the object under test that will acquire is compared with preset temperature threshold；
(3) according to the step (2) comparison as a result, when the partial region temperature of the object under test is higher than described preset
When temperature threshold, the region that will be above the object under test of the preset temperature threshold is set as the temperature of the object under test
Abnormal area further carries out temperature detection to the temperature anomaly region；
(4) temperature information in the temperature anomaly region of the object under test is obtained in the second preset time, and generates temperature
Degree report curve；
(5) curve is reported according to the temperature, maintenance processing is carried out to the temperature anomaly region of the object under test, handle
Execute step (2) again after the completion.
Further, before the step (1) further include:
Detect and whether place the object under test in the detection platform, when detect be placed with the object under test when,
Control the object under test enters operating mode.
Further, the step (3) includes:
When the partial region temperature of the object under test is higher than the preset temperature threshold, the institute of object under test described in root
Temperature anomaly region is stated, control adjusts the height and corresponding azimuth information of the detection platform；
According to the height of the detection platform adjusted and corresponding azimuth information to the temperature anomaly region into
The carry out temperature detection of one step.
Further, the step (4) includes:
Include at least one test point in the temperature anomaly region of the object under test, is set as abnormality detection point；
Trip temperature detection is clicked through each described abnormality detection, and the time at equal intervals in second preset time
Obtain corresponding temperature information；
According to the temperature information of the acquisition, the corresponding temperature report is generated each described abnormality detection point
Accuse curve.
Further, the fault detection module detection method is as follows:
Step 1, dynamic circuit be driving and Acquisition Circuit power supply operational process in, periodically stop dynamic circuit it is defeated
Enter signal；
After step 2, dynamic circuit input signal disappear, safety relay disconnects driving and Acquisition Circuit power supply, using peace
The large bulk capacitance of all relay rear end is continuously driving and Acquisition Circuit power supply；
The capacitance of capacitor is needed according to power-off time, driving and Acquisition Circuit power, driving and Acquisition Circuit allowable pressure drop
Range computation obtains；
Select the calculation formula of capacitor as follows:
C is the large bulk capacitance of safety relay selection；U is the operating voltage of driving and Acquisition Circuit；I is driving and adopts
The operating current of collector；T is power-off time；
Step 3, safety relay disconnected in the period of driving and Acquisition Circuit power supply, controller back production safety relay
Contacts status situation of change obtains current relay status；
Step 4, controller judge the safety relay in dynamic circuit according to the dynamic circuit state after collected power-off
Whether device function is normal, if it is, Restoration dynamics circuit input signal, dynamic circuit continues as driving and Acquisition Circuit supplies
Electricity；Otherwise safety relay dysfunction records malfunction, and alert；
Step 5, when next detection cycle arrive when, repeat the above steps.
Further, the periodicity refers to the last dynamic circuit input signal that stops to this time stopping dynamic circuit
Time interval between input signal, is set according to the actual situation；
The dynamic circuit input signal refers to the reverse phase square-wave signal of one group 0 degree He 180 degree；When this group of signal not
Meet 0 degree and 180 degree phase relation or any of them all the way signal output disappear can all cause dynamic circuit stop be
Driving and Acquisition Circuit power supply.
Advantages of the present invention and good effect are as follows: the present invention passes through the Detection accuracy of temperature detecting module measuring targets
99% or more can be reached, error is almost can be controlled within 1%, and entire test process can be automatically processed intelligently, therefore is improved
Testing efficiency and reduction test error, realize real time temperature monitoring, adjust automatically temperature test point, automatically generate temperature curve report
It accuses, the abnormality of examined object is carried out efficiently and precise positioning, while improving extraction quality；Meanwhile fault
Detection module by do not influence system operate normally in the case where, the detection to dynamic circuit incipient fault may be implemented, and
Shi Faxian potential risk avoids dangerous generation, improves safety.
Detailed description of the invention
Fig. 1 is that the present invention implements the rhizoma cyperi saponins compound separating and extracting process flow chart provided.
Fig. 2 is that the present invention implements the rhizoma cyperi saponins compound separation and Extraction system structure diagram provided.
In Fig. 2: 1, weight detecting module；2, temperature detecting module；3, pressure detection module；4, main control module；5, it crushes
Module；6, sterilization module；7, module is concentrated；8, module is stirred；9, irradiation modules；10, fault detection module；11, it shows
Module.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
With reference to the accompanying drawing and specific embodiment is further described application principle of the invention.
As shown in Figure 1, a kind of rhizoma cyperi saponins compound separating and extracting process provided by the invention the following steps are included:
Step S101 utilizes weighing apparatus Detection and Extraction raw material weight data by weight detecting module；Pass through temperature detection
Module utilizes temperature data when temperature sensor Detection and Extraction saponins compound；It is passed by pressure detection module using pressure
Pressure data when sensor Detection and Extraction saponins compound；
Step S102, main control module scheduling are crushed module and are crushed using pulverizer control model；Purple is utilized by sterilization module
Outside line lamp is to carrying out illumination-based disinfection after crushing；
Step S103 will be maintained 0.1 big by concentration module using vacuum decker using deionized water as solvent
Under atmospheric pressure state, 75 DEG C take ethanol-water extract 1 hour, the filtrate of collection, be concentrated in vacuo to filtrate volume three/
One；
Alcohol and concentrate are stirred by stirring module using blender by step S104, be collected by filtration filtrate and
Precipitating；
Precipitating is dried in vacuo by step S105 by irradiation modules using heater by 80 DEG C, and filtrate is using decompression rotation
Turn evaporative removal ethyl alcohol, low temperature drying obtains rhizoma cyperi saponins compound；
Step S106 utilizes circuit signal collector detection circuit fault message by fault detection module；Pass through
Weight, the temperature, pressure data information that display module is detected using display display.
As shown in Fig. 2, rhizoma cyperi saponins compound separation and Extraction system provided by the invention include: weight detecting module 1,
Temperature detecting module 2, main control module 4, crushes module 5, sterilization module 6, concentration module 7, stirring module at pressure detection module 3
8, irradiation modules 9, fault detection module 10, display module 11.
Weight detecting module 1 is connect with main control module 4, for passing through the weight data of weighing apparatus Detection and Extraction raw material；
Temperature detecting module 2 is connect with main control module 4, for passing through temperature sensor Detection and Extraction saponins compound
When temperature data；
Pressure detection module 3 is connect with main control module 4, for passing through pressure transducer Detection and Extraction saponins compound
When pressure data；
Main control module 4, with weight detecting module 1, temperature detecting module 2, pressure detection module 3, crushing module 5, disinfection
Module 6, concentration module 7, stirring module 8, irradiation modules 9, fault detection module 10, display module 11 connect, for leading to
Single-chip microcontroller control modules are crossed to work normally；
Module 5 is crushed, is connect with main control module 4, for being crushed by pulverizer control model；
Sterilization module 6 is connect with main control module 4, for by ultraviolet radiator to carrying out illumination-based disinfection after crushing；
Module 7 is concentrated, is connect with main control module 4, for that will be maintained using deionized water as solvent by vacuum decker
Under 0.1 atmospheric pressure state, 75 DEG C are taken ethanol-water to extract 1 hour, and the filtrate of collection is concentrated in vacuo to filtrate body
Long-pending one third；
Module 8 is stirred, is connect with main control module 4, for being stirred alcohol and concentrate by blender, filtering is received
Collect filtrate and precipitating；
Irradiation modules 9 are connect with main control module 4, for being adopted precipitating by 80 DEG C of vacuum drying filtrates by heater
Ethyl alcohol is removed with decompression rotary evaporation, low temperature drying obtains rhizoma cyperi saponins compound；
Fault detection module 10 is connect with main control module 4, for passing through circuit signal collector detection circuit failure
Information；
Display module 11 is connect with main control module 4, for weight, the temperature, pressure data by display display detection
Information.
2 detection method of temperature detecting module provided by the invention is as follows:
(1) temperature information of object under test in detection platform is obtained in the first preset time；
(2) temperature information for the object under test that will acquire is compared with preset temperature threshold；
(3) according to the step (2) comparison as a result, when the partial region temperature of the object under test is higher than described preset
When temperature threshold, the region that will be above the object under test of the preset temperature threshold is set as the temperature of the object under test
Abnormal area further carries out temperature detection to the temperature anomaly region；
(4) temperature information in the temperature anomaly region of the object under test is obtained in the second preset time, and generates temperature
Degree report curve；
(5) curve is reported according to the temperature, maintenance processing is carried out to the temperature anomaly region of the object under test, handle
Execute step (2) again after the completion.
Before step (1) provided by the invention further include:
Detect and whether place the object under test in the detection platform, when detect be placed with the object under test when,
Control the object under test enters operating mode.
Step (3) provided by the invention includes:
When the partial region temperature of the object under test is higher than the preset temperature threshold, the institute of object under test described in root
Temperature anomaly region is stated, control adjusts the height and corresponding azimuth information of the detection platform；
According to the height of the detection platform adjusted and corresponding azimuth information to the temperature anomaly region into
The carry out temperature detection of one step.
Step (4) provided by the invention includes:
Include at least one test point in the temperature anomaly region of the object under test, is set as abnormality detection point；
Trip temperature detection is clicked through each described abnormality detection, and the time at equal intervals in second preset time
Obtain corresponding temperature information；
According to the temperature information of the acquisition, the corresponding temperature report is generated each described abnormality detection point
Accuse curve.
10 detection method of fault detection module provided by the invention is as follows:
Step 1, dynamic circuit be driving and Acquisition Circuit power supply operational process in, periodically stop dynamic circuit it is defeated
Enter signal；
After step 2, dynamic circuit input signal disappear, safety relay disconnects driving and Acquisition Circuit power supply, using peace
The large bulk capacitance of all relay rear end is continuously driving and Acquisition Circuit power supply；
The capacitance of capacitor is needed according to power-off time, driving and Acquisition Circuit power, driving and Acquisition Circuit allowable pressure drop
Range computation obtains；
Select the calculation formula of capacitor as follows:
C is the large bulk capacitance of safety relay selection；U is the operating voltage of driving and Acquisition Circuit；I is driving and adopts
The operating current of collector；T is power-off time；
Step 3, safety relay disconnected in the period of driving and Acquisition Circuit power supply, controller back production safety relay
Contacts status situation of change obtains current relay status；
Step 4, controller judge the safety relay in dynamic circuit according to the dynamic circuit state after collected power-off
Whether device function is normal, if it is, Restoration dynamics circuit input signal, dynamic circuit continues as driving and Acquisition Circuit supplies
Electricity；Otherwise safety relay dysfunction records malfunction, and alert；
Step 5, when next detection cycle arrive when, repeat the above steps.
Periodicity provided by the invention refers to the last dynamic circuit input signal that stops to this time stopping dynamic circuit
Time interval between input signal, is set according to the actual situation；
The dynamic circuit input signal refers to the reverse phase square-wave signal of one group 0 degree He 180 degree；When this group of signal not
Meet 0 degree and 180 degree phase relation or any of them all the way signal output disappear can all cause dynamic circuit stop be
Driving and Acquisition Circuit power supply.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (8)
1. a kind of rhizoma cyperi saponins compound separating and extracting process, which is characterized in that the rhizoma cyperi saponins compound separation mentions
The method is taken to include:
Step 1 utilizes the weight data of weighing apparatus Detection and Extraction raw material by weight detecting module；Pass through temperature detecting module
Temperature data when using temperature sensor Detection and Extraction saponins compound；Pressure transducer is utilized by pressure detection module
Pressure data when Detection and Extraction saponins compound；
Step 2, main control module scheduling are crushed module and are crushed using pulverizer control model；Ultraviolet radiator is utilized by sterilization module
To carrying out illumination-based disinfection after crushing；
Step 3 will maintain 0.1 atmospheric pressure shape using deionized water as solvent using vacuum decker by concentration module
Under state, 75 DEG C are taken ethanol-water to extract 1 hour, and the filtrate of collection is concentrated in vacuo to the one third of filtrate volume；
Alcohol and concentrate are stirred by stirring module using blender by step 4, and chlorogenic acid is complete after standing 1 hour
Filtrate and precipitating is collected by filtration in precipitating；
Precipitating is dried in vacuo by step 5 by irradiation modules using heater by 80 DEG C, and filtrate is using decompression rotary evaporation
Ethyl alcohol is removed, low temperature drying obtains rhizoma cyperi saponins compound；
Step 6 utilizes circuit signal collector detection circuit fault message by fault detection module；By showing mould
Weight, the temperature, pressure data information that block is detected using display display.
2. rhizoma cyperi saponins compound separating and extracting process as described in claim 1, which is characterized in that the temperature detection mould
Block detection method is as follows:
(1) temperature information of object under test in detection platform is obtained in the first preset time；
(2) temperature information for the object under test that will acquire is compared with preset temperature threshold；
(3) according to the step (2) comparison as a result, the partial region temperature when the object under test is higher than the preset temperature
When threshold value, the region that will be above the object under test of the preset temperature threshold is set as the temperature anomaly of the object under test
Region further carries out temperature detection to the temperature anomaly region；
(4) temperature information in the temperature anomaly region of the object under test is obtained in the second preset time, and generates temperature report
Accuse curve；
(5) curve is reported according to the temperature, maintenance processing is carried out to the temperature anomaly region of the object under test, processing is completed
Execute step (2) again afterwards.
3. rhizoma cyperi saponins compound separating and extracting process as claimed in claim 2, which is characterized in that the step (1) it
Before further include:
Detect and whether place the object under test in the detection platform, when detect be placed with the object under test when, control
The object under test enters operating mode.
4. rhizoma cyperi saponins compound separating and extracting process as claimed in claim 2, which is characterized in that step (3) packet
It includes:
When the partial region temperature of the object under test is higher than the preset temperature threshold, the temperature of object under test described in root
Abnormal area is spent, control adjusts the height and corresponding azimuth information of the detection platform；
It is further to the temperature anomaly region according to the height of the detection platform adjusted and corresponding azimuth information
Carry out temperature detection.
5. rhizoma cyperi saponins compound separating and extracting process as claimed in claim 2, which is characterized in that step (4) packet
It includes:
Include at least one test point in the temperature anomaly region of the object under test, is set as abnormality detection point；
Trip temperature detection, and the acquisition of time at equal intervals in second preset time are clicked through each described abnormality detection
Corresponding temperature information；
According to the temperature information of the acquisition, it is bent that the corresponding temperature report is generated each described abnormality detection point
Line.
6. rhizoma cyperi saponins compound separating and extracting process as described in claim 1, which is characterized in that the fault inspection
It is as follows to survey module detection method:
Step 1, dynamic circuit be driving and Acquisition Circuit power supply operational process in, periodically stop dynamic circuit input letter
Number；
Step 2, dynamic circuit input signal disappear after, safety relay disconnect driving and Acquisition Circuit power supply, using safety after
The large bulk capacitance of electric appliance rear end is continuously driving and Acquisition Circuit power supply；
The capacitance of capacitor is needed according to power-off time, driving and Acquisition Circuit power, driving and Acquisition Circuit allowable pressure drop range
It is calculated；
Select the calculation formula of capacitor as follows:
C is the large bulk capacitance of safety relay selection；U is the operating voltage of driving and Acquisition Circuit；I is driving and acquisition electricity
The operating current on road；T is power-off time；
Step 3, safety relay disconnected in the period of driving and Acquisition Circuit power supply, controller back production safety relay contact
State change situation obtains current relay status；
Step 4, controller judge the safety relay function in dynamic circuit according to the dynamic circuit state after collected power-off
Can whether normal, if it is, Restoration dynamics circuit input signal, dynamic circuit continues as driving and Acquisition Circuit power supply；It is no
Then safety relay dysfunction records malfunction, and alert；
Step 5, when next detection cycle arrive when, repeat the above steps.
7. rhizoma cyperi saponins compound separating and extracting process as claimed in claim 6, which is characterized in that the periodicity is
Refer to the last dynamic circuit input signal that stops to the time interval this time stopped between dynamic circuit input signal, according to reality
Border situation is set；
The dynamic circuit input signal refers to the reverse phase square-wave signal of one group 0 degree He 180 degree；When this group of signal is unsatisfactory for
Signal output disappears and can all cause dynamic circuit to stop for driving the phase relation or any of them of 0 degree and 180 degree all the way
It powers with Acquisition Circuit.
8. a kind of rhizoma cyperi saponins compound separation for implementing rhizoma cyperi saponins compound separating and extracting process described in claim 1
Extraction system, which is characterized in that the rhizoma cyperi saponins compound separation and Extraction system includes:
Weight detecting module, pressure detection module, main control module, crushes module, sterilization module, enrichment mode at temperature detecting module
Block, stirring module, irradiation modules, fault detection module, display module.
Weight detecting module, connect with main control module, for passing through the weight data of weighing apparatus Detection and Extraction raw material；
Temperature detecting module is connect with main control module, for passing through temperature when temperature sensor Detection and Extraction saponins compound
Degree evidence；
Pressure detection module, connect with main control module, for passing through pressure when pressure transducer Detection and Extraction saponins compound
Strong data；
Main control module, with weight detecting module, temperature detecting module, pressure detection module, crushing module, sterilization module, concentration
Module, stirring module, irradiation modules, fault detection module, display module connection, for controlling each mould by single-chip microcontroller
Block works normally；
Module is crushed, is connect with main control module, for being crushed by pulverizer control model；
Sterilization module is connect with main control module, for by ultraviolet radiator to carrying out illumination-based disinfection after crushing；
Module is concentrated, is connect with main control module, deionized water maintains under 0.1 atmospheric pressure state as solvent, and 75 DEG C are taken
Ethanol-water extracts 1 hour, and the filtrate of collection is concentrated in vacuo to the one third of filtrate volume；
Module is stirred, is connect with main control module, for being stirred alcohol and concentrate by blender, filtrate is collected by filtration
And precipitating；
Irradiation modules are connect with main control module, and for being dried in vacuo precipitating by 80 DEG C by heater, filtrate is using decompression
Rotary evaporation removes ethyl alcohol, and low temperature drying obtains rhizoma cyperi saponins compound；
Fault detection module, connect with main control module, for passing through circuit signal collector detection circuit fault message；
Display module is connect with main control module, for weight, the temperature, pressure data information by display display detection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811246456.0A CN109260347A (en) | 2018-10-25 | 2018-10-25 | A kind of rhizoma cyperi saponins compound separating and extracting process |
Applications Claiming Priority (1)
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| CN103860622A (en) * | 2012-12-07 | 2014-06-18 | 廉吉芳 | Method for extracting saponin compounds from honeysuckle |
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| CN103860622A (en) * | 2012-12-07 | 2014-06-18 | 廉吉芳 | Method for extracting saponin compounds from honeysuckle |
| CN108226747A (en) * | 2017-11-30 | 2018-06-29 | 北京康拓科技有限公司 | A kind of dynamic circuit failure on-line detecting method |
| CN108375426A (en) * | 2018-03-27 | 2018-08-07 | 四川斐讯信息技术有限公司 | A kind of temperature checking method and system |
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Application publication date: 20190125 |