CN109248641B - Hydrolysis reaction tank for chemical production - Google Patents

Hydrolysis reaction tank for chemical production Download PDF

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Publication number
CN109248641B
CN109248641B CN201811207176.9A CN201811207176A CN109248641B CN 109248641 B CN109248641 B CN 109248641B CN 201811207176 A CN201811207176 A CN 201811207176A CN 109248641 B CN109248641 B CN 109248641B
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China
Prior art keywords
liquid
block
pipeline
fixed
reaction
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CN201811207176.9A
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CN109248641A (en
Inventor
方文星
陈同翔
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ALLCHEMY Co.,Ltd.
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Allchemy Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/02Cleaning pipes or tubes or systems of pipes or tubes
    • B08B9/027Cleaning the internal surfaces; Removal of blockages
    • B08B9/04Cleaning the internal surfaces; Removal of blockages using cleaning devices introduced into and moved along the pipes
    • B08B9/043Cleaning the internal surfaces; Removal of blockages using cleaning devices introduced into and moved along the pipes moved by externally powered mechanical linkage, e.g. pushed or drawn through the pipes
    • B08B9/0436Cleaning the internal surfaces; Removal of blockages using cleaning devices introduced into and moved along the pipes moved by externally powered mechanical linkage, e.g. pushed or drawn through the pipes provided with mechanical cleaning tools, e.g. scrapers, with or without additional fluid jets

Abstract

The invention relates to the field of reaction tanks, in particular to a hydrolysis reaction tank for chemical production, which comprises a support, a circulating mechanism, a reaction mechanism, a water injection mechanism, a stirring mechanism, a fixing mechanism, a liquid injection mechanism, a cleaning mechanism and a limiting mechanism, wherein the circulating mechanism is arranged on the support; the cleaning mechanism is matched with the pipeline for use, so that residual stains on the side wall of the pipeline are brushed back and forth by using the hairbrush, and the stains on the side wall of the processing pipeline are washed, so that the next reaction is facilitated, the liquid of the next reaction is not polluted by the residual stains on the side wall of the pipeline, and the next reaction is not facilitated to be carried out; through wiper mechanism cooperation stop gear's use, utilize the baffle to block the bottom of pipeline to make gliding brush and slider do not return from the bottom landing of spliced pole on the spliced pole, thereby be convenient for wiper mechanism washs the inner wall of pipeline.

Description

Hydrolysis reaction tank for chemical production
Technical Field
The invention relates to the field of reaction tanks, in particular to a hydrolysis reaction tank for chemical production.
Background
The reaction tank, chemical reaction vessel and physical reaction vessel are divided into pressure vessel and normal pressure vessel. The reaction tank has various varieties and has the characteristics of advanced process, stable quality, stable transmission, convenient operation and the like. The device is widely applied to industries such as petroleum, chemical industry, food, medicine, pesticide, scientific research and the like, and is reaction equipment for completing chemical processes such as polymerization, condensation, vulcanization, alkylation, hydrogenation and the like and performing a plurality of processes of organic dyes and intermediates.
When hydrolysis reaction uses the retort, add the pipeline at the transfusion mouth, make the bottom that liquid got into the retort, can not splash, but when wasing, because the stirring structure can only stir the water in the reation kettle inner wall, nevertheless can wash through pouring into the clear water to intraductal liquid washing, it remains on the inner wall of pipeline to get off to have the chemical for a long time to can make the liquid through this pipeline contaminated, thereby be unfavorable for the reaction. In view of the above, the invention provides a hydrolysis reaction tank for chemical production, which has the following characteristics:
(1) according to the hydrolysis reaction tank for chemical production, the cleaning mechanism is matched with the pipeline for use, so that residual stains on the side wall of the pipeline are brushed back and forth by the hairbrush, and the stains on the side wall of the processing pipeline are washed, so that next reaction can be carried out favorably, liquid of the next reaction is not polluted by the residual stains on the side wall of the pipeline, and the next reaction is not favorably carried out.
(2) According to the hydrolysis reaction tank for chemical production, the cleaning mechanism is matched with the limiting mechanism, and the baffle is used for blocking the bottom end of the pipeline, so that the brush and the sliding block sliding on the connecting column cannot slide back from the bottom end of the connecting column, and the cleaning mechanism is convenient to clean the inner wall of the pipeline.
(3) According to the hydrolysis reaction tank for chemical production, the fixing plate of the fixing mechanism is matched with the clamping block of the cleaning mechanism, so that the connecting column is favorably fixed in the pipeline, and the connecting column is prevented from falling off from the pipeline in the process of pulling the circular ring to drive the sliding block and the hairbrush.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a hydrolysis reaction tank for chemical production, which is used by matching a cleaning mechanism with a pipeline, so that residual stains on the side wall of the pipeline are brushed back and forth by using a brush, and the stains on the side wall of the processing pipeline are washed, thereby being beneficial to the next reaction, ensuring that the liquid of the next reaction is not polluted by the residual stains on the side wall of the pipeline, and being not beneficial to the next reaction; the cleaning mechanism is matched with the limiting mechanism, and the bottom end of the pipeline is blocked by the baffle plate, so that the brush and the sliding block sliding on the connecting column cannot slide back from the bottom end of the connecting column, and the cleaning mechanism is convenient to clean the inner wall of the pipeline; the fixing plate that includes through fixed establishment cooperates the use of the fixture block that wiper mechanism includes to be favorable to the spliced pole fixed in the pipeline, thereby prevent to stimulate the in-process that the ring drove slider and brush, thereby prevent that the spliced pole from droing from the pipeline.
The technical scheme adopted by the invention for solving the technical problems is as follows: the utility model provides a hydrolysis reaction tank for chemical production, includes support, circulation mechanism, reaction mechanism, water injection mechanism, rabbling mechanism, fixed establishment, annotates liquid mechanism, wiper mechanism and stop gear, the top fixed mounting of support has and is used for through circulation heat and cold liquid in order to accelerate the reaction circulation mechanism, the inside fixed mounting of circulation mechanism has the reaction mechanism that is used for the hydrolysis reaction, the top fixed mounting of reaction mechanism has the water injection mechanism that is used for the water injection, the top fixed mounting of reaction mechanism has the rabbling mechanism that is used for stirring to accelerate the reaction, the top fixed mounting of reaction mechanism has the liquid mechanism of annotating that is used for pouring into the reaction liquid, the lateral wall fixed mounting of rabbling mechanism has the fixed establishment that is used for fixed wiper mechanism, the lateral wall fixed connection of circulation mechanism fixed establishment, the liquid injection mechanism is characterized in that the fixing mechanism is suspended with a cleaning mechanism used for cleaning the liquid injection mechanism, the cleaning mechanism is connected with the liquid injection mechanism in a sliding mode, and the cleaning mechanism is connected with a limiting mechanism used for limiting the cleaning mechanism to slide down from the liquid injection mechanism.
Specifically, circulation mechanism includes feed liquor pipe, drain pipe, outer jar and flowing back lid, the bottom mounting of outer jar is in the top of support, the feed liquor pipe is fixed in outer jar, the drain pipe is fixed in outer jar deviates from one side of feed liquor pipe, flowing back lid fixed mounting in the bottom of outer jar.
Specifically, reaction mechanism includes inner tank, stopper and handle, the inner tank is fixed in the inside of outer jar, the stopper block is connected the bottom of inner tank, the bottom fixed mounting of stopper has the handle, the inner tank and be equipped with the cavity of circulating liquid storage between the outer jar, the length of handle is less than the bottom of stopper extremely the distance of flowing back lid.
Specifically, the water injection mechanism includes tube cap and ascending pipe, the ascending pipe install in the top of inner tank, the tube cap with threaded connection between the ascending pipe.
Specifically, annotate liquid mechanism and include lid and pipeline, pipeline fixed mounting in the inner tank, the lid with through threaded connection between the pipeline, the bottom slope of pipeline sets up.
Specifically, rabbling mechanism includes motor, set casing, connecting block, fixed block, stock and flabellum, the bottom fixed connection of set casing the top of inner tank, the top fixed mounting of set casing has the motor, the motor has cup jointed the connecting block, the connecting block deviates from the one end of motor has cup jointed the stock, fixed block fixed mounting in the top of inner tank, the stock runs through the fixed block gets into the inside of inner tank, the stock deviates from the one end of motor is cup jointed the flabellum, the fixed block with the connecting block is located the inside of set casing.
Specifically, fixed establishment includes fixed plate and solid fixed ring, the fixed plate is fixed in the lateral wall of set casing, gu fixed ring is fixed in the lateral wall of outer jar, the fixed plate with same one side is located to the pipeline.
Specifically, wiper mechanism includes handle, ring, fixture block, spring, spliced pole, steel wire, slider and brush, the fixture block is connected draw-in groove on the fixed plate, the bottom fixed connection of fixture block the spliced pole, spliced pole suit and sliding connection the slider, slider bottom fixed connection the brush, the one end fixed connection of spring the slider, the other end fixed connection of spring the bottom of fixture block, the spring runs through the spliced pole, the one end of steel wire is fixed in the slider, the other end of steel wire runs through fixture block and fixed winding in on the ring, the steel wire is equipped with two, two the steel wire symmetry sets up, the top fixed connection of ring has the semicircle annular handle, solid fixed ring cup joints the spliced pole.
Specifically, stop gear includes cylinder, rope and dog, the rope runs through the fixture block and the spliced pole, the one end fixed connection of rope the cylinder twine in on the cylinder, the rope block in draw-in groove on the cylinder, the other end fixed connection of rope the dog, the length of dog is greater than the diameter of pipeline, the width of dog is less than the diameter of pipeline, the cylinder is located the fixture block deviates from the one end of spliced pole, the dog is located the spliced pole deviates from the one end of fixture block.
The invention has the beneficial effects that:
(1) according to the hydrolysis reaction tank for chemical production, the cleaning mechanism is matched with the pipeline for use, so that residual stains on the side wall of the pipeline are brushed back and forth by the hairbrush, and the stains on the side wall of the processing pipeline are washed, so that next reaction can be carried out favorably, liquid of the next reaction is not polluted by the residual stains on the side wall of the pipeline, and the next reaction is not favorably carried out.
(2) According to the hydrolysis reaction tank for chemical production, the cleaning mechanism is matched with the limiting mechanism, and the baffle is used for blocking the bottom end of the pipeline, so that the brush and the sliding block sliding on the connecting column cannot slide back from the bottom end of the connecting column, and the cleaning mechanism is convenient to clean the inner wall of the pipeline.
(3) According to the hydrolysis reaction tank for chemical production, the fixing plate of the fixing mechanism is matched with the clamping block of the cleaning mechanism, so that the connecting column is favorably fixed in the pipeline, and the connecting column is prevented from falling off from the pipeline in the process of pulling the circular ring to drive the sliding block and the hairbrush.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a schematic structural diagram of a hydrolysis reactor for chemical production according to a preferred embodiment of the present invention;
FIG. 2 is a schematic cross-sectional view of the agitation mechanism shown in FIG. 1;
FIG. 3 is an enlarged view of portion A of FIG. 1;
fig. 4 is an enlarged schematic view of a portion B shown in fig. 1.
In the figure: 1. the device comprises a support, 2, a circulating mechanism, 21, a liquid inlet pipe, 22, a liquid outlet pipe, 23, an outer tank, 24, a liquid draining cover, 3, a reaction mechanism, 31, an inner tank, 32, a plug, 33, a handle, 4, a water injection mechanism, 41, a pipe cover, 42, an injection pipe, 5, a stirring mechanism, 51, a motor, 52, a fixed shell, 53, a connecting block, 54, a fixed block, 55, a long rod, 56, fan blades, 6, a fixing mechanism, 61, a fixed plate, 62, a fixed ring, 7, a liquid injection mechanism, 71, a cover, 72, a pipeline, 8, a cleaning mechanism, 81, a handle, 82, a ring, 83, a clamping block, 84, a spring, 85, a connecting column 85, 86, a steel wire, 87, a sliding block, 88, a brush, 9, a limiting mechanism, 91, a roller, 92, a rope, 93.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
As shown in fig. 1-4, the hydrolysis reaction tank for chemical production according to the present invention includes a support 1, a circulation mechanism 2, a reaction mechanism 3, a water injection mechanism 4, a stirring mechanism 5, a fixing mechanism 6, a liquid injection mechanism 7, a cleaning mechanism 8, and a limiting mechanism 9, wherein the circulation mechanism 2 for accelerating a reaction by circulating hot and cold liquids is fixedly installed at the top end of the support 1, the reaction mechanism 3 for hydrolysis reaction is fixedly installed inside the circulation mechanism 2, the water injection mechanism 4 for water injection is fixedly installed at the top end of the reaction mechanism 3, the stirring mechanism 5 for stirring and accelerating a reaction is fixedly installed at the top end of the reaction mechanism 3, the liquid injection mechanism 7 for injecting a reaction liquid is fixedly installed at the top end of the reaction mechanism 3, the fixing mechanism 6 for fixing the cleaning mechanism 8 is fixedly installed at the side wall of the stirring mechanism 5, the lateral wall fixed connection of circulation mechanism 2 fixed establishment 6, it is used for the washing to hang on the fixed establishment 6 annotate liquid mechanism 7 wiper mechanism 8, 8 sliding connection of wiper mechanism annotate liquid mechanism 7, 8 sliding connection of wiper mechanism have and are used for the restriction wiper mechanism 8 follows it makes 7 in the liquid mechanism 7 landing to annotate the stop gear 9.
Specifically, the circulating mechanism 2 comprises a liquid inlet pipe 21, a liquid outlet pipe 22, an outer tank 23 and a liquid discharge cover 24, wherein the bottom end of the outer tank 23 is fixed at the top end of the support 1, the liquid inlet pipe 21 is fixed at the outer tank 23, the liquid outlet pipe 22 is fixed at one side of the outer tank 23, which is far away from the liquid inlet pipe 21, and the liquid discharge cover 24 is fixedly installed at the bottom end of the outer tank 23; thereby facilitating the addition of heated and cooled liquid from the liquid inlet pipe 21 into the outer tank 23 and then the discharge through the liquid outlet pipe 22, thereby facilitating the acceleration of the hydrolysis reaction in the reaction mechanism 3, and the liquid discharge cover 24 facilitates the discharge of the entire liquid in the outer tank 23.
Specifically, the reaction mechanism 3 comprises an inner tank 31, a plug 32 and a handle 33, the inner tank 31 is fixed inside the outer tank 23, the plug 32 is connected with the bottom end of the inner tank 31 in a clamping manner, the handle 33 is fixedly installed at the bottom end of the plug 32, a cavity for storing circulating liquid is arranged between the inner tank 31 and the outer tank 23, and the length of the handle 33 is smaller than the distance from the bottom end of the plug 32 to the liquid discharge cover 24; when the reaction kettle is used, water and a reflecting object are respectively filled into the inner tank 31 through the water filling mechanism 4 and the liquid filling mechanism 7, so that a reaction is carried out in the inner tank 31, the handle 33 on the plug 32 facilitates the use of the plug 32, and a user can conveniently install and remove the plug 32.
Specifically, the water injection mechanism 4 comprises a pipe cover 41 and an injection pipe 42, the injection pipe 42 is installed at the top end of the inner tank 31, and the pipe cover 41 is in threaded connection with the injection pipe 42; the water in the hydrolysis reaction is injected through the injection pipe 42, and the pipe cover 41 facilitates the device to prevent dust from entering the inner vessel 31 when not in use.
Specifically, the liquid injection mechanism 7 comprises a cover 71 and a pipeline 72, the pipeline 72 is fixedly mounted on the inner tank 31, the cover 71 is connected with the pipeline 72 through threads, and the bottom end of the pipeline 72 is obliquely arranged; the substance which is subjected to hydrolysis reaction with water is put into the inner tank 31 through the pipeline 72, and the pipeline 72 is attached to the side wall of the inner tank 31, so that the substance which is subjected to hydrolysis reaction enters the water along the side wall of the inner tank 31, the splashing of the liquid is prevented, and the intensity of the hydrolysis reaction can be effectively reduced.
Specifically, the stirring mechanism 5 includes a motor 51, a fixed shell 52, a connecting block 53, a fixed block 54, a long rod 55 and fan blades 56, the bottom end of the fixed shell 52 is fixedly connected to the top end of the inner tank 31, the top end of the fixed shell 52 is fixedly provided with the motor 51, the motor 51 is sleeved with the connecting block 53, one end of the connecting block 53 away from the motor 51 is sleeved with the long rod 55, the fixed block 54 is fixedly installed at the top end of the inner tank 31, the long rod 55 penetrates through the fixed block 54 and enters the inner tank 31, one end of the long rod 55 away from the motor 51 is sleeved with the fan blades 56, and the fixed block 54 and the connecting block 53 are arranged inside the fixed shell 52; during the use, the switch on, motor 51 begins to rotate to the drive cup joints in connecting block 53 stock 55 rotates, flabellum 56 stirs the raw materials of hydrolysis reaction, thereby the mixture of the raw materials of being convenient for, thereby quickening the hydrolysis reaction, the fixed block 54 is right stock 55's position is fixed, and prevents stock 55 with the friction between the inner tank 31.
Specifically, the fixing mechanism 6 includes a fixing plate 61 and a fixing ring 62, the fixing plate 61 is fixed on the side wall of the fixing shell 52, the fixing ring 62 is fixed on the side wall of the outer tank 23, and the fixing plate 61 and the pipeline 72 are arranged on the same side; therefore, the fixing plate 61 is used for clamping the cleaning mechanism 8, so that the position of the cleaning mechanism 8 is convenient to fix, the position of the cleaning mechanism 8 is prevented from being displaced when the cleaning mechanism 8 is used, and the fixing ring 62 is used for accommodating the cleaning mechanism 8 when the cleaning mechanism 8 is not used, so that the cleaning mechanism 8 is convenient to store.
Specifically, the cleaning mechanism 8 includes a handle 81, a ring 82, a latch 83, a spring 84, a connection post 85, a steel wire 86, a slider 87 and a brush 88, the latch 83 is connected to a slot on the fixing plate 61 in a clamping manner, the bottom end of the latch 83 is fixedly connected to the connection post 85, the connection post 85 is sleeved and slidably connected to the slider 87, the bottom end of the slider 87 is fixedly connected to the brush 88, one end of the spring 84 is fixedly connected to the slider 87, the other end of the spring 84 is fixedly connected to the bottom end of the latch 83, the spring 84 penetrates through the connection post 85, one end of the steel wire 86 is fixed to the slider 87, the other end of the steel wire 86 penetrates through the latch 83 and is fixedly wound on the ring 82, two steel wires 86 are symmetrically arranged, the top end of the ring 82 is fixedly connected to the handle 81 having a semicircular shape, the fixing ring 62 is sleeved with the connecting column 85; when the handle 81 is released, the spring 84 is released, so that the sliding block 87 and the brush 88 move to the position away from the fixture block 83, and the handle 81 is pulled back and forth and released, so that the brush 88 brushes the inner wall of the pipe 72, and the inner wall of the pipe 72 is cleaned back and forth, and the inside of the pipe 72 is cleaned, and the handle 33 facilitates the pulling of the ring 82.
Specifically, the limiting mechanism 9 includes a roller 91, a rope 92 and a stopper 93, the rope 92 penetrates through the fixture block 83 and the connecting post 85, one end of the rope 92 is fixedly connected to the roller 91 and wound on the roller 91, the rope 92 is clamped in a clamping groove on the roller 91, the other end of the rope 92 is fixedly connected to the stopper 93, the length of the stopper 93 is greater than the diameter of the duct 72, the width of the stopper 93 is smaller than the diameter of the duct 72, the roller 91 is arranged at one end of the fixture block 83 away from the connecting post 85, and the stopper 93 is arranged at one end of the connecting post 85 away from the fixture block 83; in use, the stopper 93 is vertically placed in the inlet of the duct 72, the connecting column 85 is used for sending the stopper 93 to the other end of the duct 72, then the rope 92 is pulled to transversely place the stopper 93 so as to stop the stopper 93 at the bottom end of the duct 72, then the redundant rope 92 is wound in the roller 91 and the rope 92 is clamped in the clamping groove on the roller 91, then the handle 81 is pulled, so that the position of the connecting column 85 is prevented from moving, and the sliding block 87 and the brush 88 are prevented from being separated from the connecting column 85.
When in use, heated and cooled liquid is added into the outer tank 23 fixed on the support 1 from the liquid inlet pipe 21, then is discharged through the liquid outlet pipe 22, the pipe cover 41 is opened, water is injected into the inner tank 31 from the injection pipe 42, the cover 71 is opened, a substance to be hydrolyzed is injected from the pipeline 72, the power is switched on, the motor 51 arranged on the fixed shell 52 starts to rotate, so as to drive the long rod 55 sleeved on the connecting block 53 to rotate, the long rod 55 is further fixed by the fixed block 54, so that the fan blades 56 fixed on the long rod 55 rotate, so as to stir the water in the inner tank 31 and the substance to be hydrolyzed, so as to accelerate the hydrolysis reaction of the substance, when the reaction is complete, the liquid in the liquid inlet pipe 21 is stopped, when the liquid in the liquid outlet pipe 22 is complete, then the liquid discharge cover 24 is opened, then the liquid in the outer tank 23 is completely discharged, then the handle 33 is pinched, the plug 32 is opened, then the liquid in the inner tank 31 is discharged from the inner tank 31, the liquid is collected, after the liquid is discharged, the plug 32 is covered in the inner tank 31, the liquid discharge cover 24 is installed in the outer tank 23, then clear water is injected from the injection pipe 42 and the pipeline 72, the motor 51 installed on the fixed shell 52 starts to rotate, so as to drive the long rod 55 sleeved on the connecting block 53 to rotate, the long rod 55 is further fixed by the fixed block 54, so that the fan blades 56 fixed on the long rod 55 rotate, the clear water in the inner tank 31 is stirred, so as to clean the inner wall of the inner tank 31, the liquid in the next reaction is prevented from being polluted due to the residue on the inner wall of the inner tank 31 in the next reaction, but the liquid in the pipeline 72 is in a standing state and cannot be influenced by the stirring of the fan blades 56, then the long rod 55 on the connecting block 53 is taken out, the stop block 93 is placed in the inlet of the pipeline 72, the connecting post 85 is used for sending the stopper 93 to the other end of the pipeline 72, then the rope 92 is pulled to transversely place the stopper 93 so as to stop the stopper 93 at the bottom end of the pipeline 72, then the redundant rope 92 is wound in the roller 91 and the rope 92 is clamped in the clamping groove on the roller 91, the clamping block 83 is clamped on the fixing plate 61, then the handle 81 is pulled, the steel wire 86 connected on the ring 82 connected with the handle 81 drives the sliding block 87 and the brush 88 to slide on the connecting post 85, and the spring 84 is compressed, so that the brush 88 brushes the inner wall of the pipeline 72, when the handle 81 is loosened, the spring 84 is loosened, the sliding block 87 and the brush 88 move to the position away from the clamping block 83, the handle 81 is pulled back and forth and loosened, the brush 88 brushes the inner wall of the pipeline 72 back and forth, so as to clean the inside of the pipeline 72 and prevent the residue of the last reaction, affecting the liquid of the next reaction.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the embodiments and descriptions given above are only illustrative of the principles of the present invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which fall within the scope of the claims. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (1)

1. The utility model provides a hydrolysis reaction jar for chemical production which characterized in that: including support (1), circulation mechanism (2), reaction mechanism (3), water injection mechanism (4), rabbling mechanism (5), fixed establishment (6), annotate liquid mechanism (7), wiper mechanism (8) and stop gear (9), the top fixed mounting of support (1) has and is used for through circulation heat and cold liquid in order to accelerate the reaction circulation mechanism (2), the inside fixed mounting of circulation mechanism (2) has and is used for hydrolysis reaction mechanism (3), the top fixed mounting of reaction mechanism (3) has and is used for the water injection mechanism (4), the top fixed mounting of reaction mechanism (3) has and is used for stirring to accelerate the reaction rabbling mechanism (5), the top fixed mounting of reaction mechanism (3) has and is used for injecting into reaction liquid annotate liquid mechanism (7), the lateral wall fixed mounting of rabbling mechanism (5) has and is used for fixed wiper mechanism (8) fixed establishment (6) ) The side wall of the circulating mechanism (2) is fixedly connected with the fixing mechanism (6), the cleaning mechanism (8) used for cleaning the liquid injection mechanism (7) is hung on the fixing mechanism (6), the cleaning mechanism (8) is connected with the liquid injection mechanism (7) in a sliding manner, and the cleaning mechanism (8) is connected with the limiting mechanism (9) used for limiting the cleaning mechanism (8) to slide from the liquid injection mechanism (7) in a sliding manner;
the circulating mechanism (2) comprises a liquid inlet pipe (21), a liquid outlet pipe (22), an outer tank (23) and a liquid discharge cover (24), the bottom end of the outer tank (23) is fixed to the top end of the support (1), the liquid inlet pipe (21) is fixed to the outer tank (23), the liquid outlet pipe (22) is fixed to one side, away from the liquid inlet pipe (21), of the outer tank (23), and the liquid discharge cover (24) is fixedly mounted at the bottom end of the outer tank (23);
the reaction mechanism (3) comprises an inner tank (31), a plug (32) and a handle (33), the inner tank (31) is fixed inside the outer tank (23), the plug (32) is connected with the bottom end of the inner tank (31) in a clamping mode, the handle (33) is fixedly installed at the bottom end of the plug (32), a cavity for storing circulating liquid is formed between the inner tank (31) and the outer tank (23), and the length of the handle (33) is smaller than the distance from the bottom end of the plug (32) to the liquid drainage cover (24);
the water injection mechanism (4) comprises a pipe cover (41) and an injection pipe (42), the injection pipe (42) is installed at the top end of the inner tank (31), and the pipe cover (41) is in threaded connection with the injection pipe (42);
the liquid injection mechanism (7) comprises a cover (71) and a pipeline (72), the pipeline (72) is fixedly arranged on the inner tank (31), the cover (71) is connected with the pipeline (72) through threads, and the bottom end of the pipeline (72) is obliquely arranged;
the stirring mechanism (5) comprises a motor (51), a fixed shell (52), a connecting block (53), a fixed block (54), a long rod (55) and fan blades (56), the bottom end of the fixed shell (52) is fixedly connected with the top end of the inner tank (31), the top end of the fixed shell (52) is fixedly provided with the motor (51), the motor (51) is sleeved with the connecting block (53), one end of the connecting block (53) departing from the motor (51) is sleeved with the long rod (55), the fixing block (54) is fixedly arranged at the top end of the inner tank (31), the long rod (55) penetrates through the fixing block (54) to enter the inner tank (31), one end of the long rod (55) departing from the motor (51) is sleeved with the fan blade (56), the fixing block (54) and the connecting block (53) are arranged inside the fixing shell (52);
the fixing mechanism (6) comprises a fixing plate (61) and a fixing ring (62), the fixing plate (61) is fixed on the side wall of the fixing shell (52), the fixing ring (62) is fixed on the side wall of the outer tank (23), and the fixing plate (61) and the pipeline (72) are arranged on the same side;
the cleaning mechanism (8) comprises a handle (81), a ring (82), a clamping block (83), a spring (84), a connecting column (85), a steel wire (86), a sliding block (87) and a brush (88), the clamping block (83) is clamped and connected with a clamping groove in the fixing plate (61), the bottom end of the clamping block (83) is fixedly connected with the connecting column (85), the connecting column (85) is sleeved and slidably connected with the sliding block (87), the bottom end of the sliding block (87) is fixedly connected with the brush (88), one end of the spring (84) is fixedly connected with the sliding block (87), the other end of the spring (84) is fixedly connected with the bottom end of the clamping block (83), the spring (84) penetrates through the connecting column (85), one end of the steel wire (86) is fixed on the sliding block (87), the other end of the steel wire (86) penetrates through the clamping block (83) and is fixedly wound on the ring (82, the number of the steel wires (86) is two, the two steel wires (86) are symmetrically arranged, the top end of the circular ring (82) is fixedly connected with a semicircular handle (81), and the fixing ring (62) is sleeved with the connecting column (85);
the limiting mechanism (9) comprises a roller (91), a rope (92) and a stop block (93), the rope (92) penetrates through the clamping block (83) and the connecting column (85), one end of the rope (92) is fixedly connected with the roller (91) and wound on the roller (91), the rope (92) is clamped in a clamping groove in the roller (91), the other end of the rope (92) is fixedly connected with the stop block (93), the length of the stop block (93) is larger than the diameter of the pipeline (72), the width of the stop block (93) is smaller than the diameter of the pipeline (72), the roller (91) is arranged at one end, deviating from the connecting column (85), of the clamping block (83), and the stop block (93) is arranged at one end, deviating from the clamping block (83), of the connecting column (85);
when in use, heated and cooled liquid is added into an outer tank (23) fixed on a support (1) from a liquid inlet pipe (21), then the liquid is discharged through a liquid outlet pipe (22), a pipe cover (41) is opened, water is injected into an inner tank (31) from an injection pipe (42), a cover (71) is opened, a substance needing hydrolysis is injected from a pipeline (72), a power supply is switched on, a motor (51) arranged on a fixed shell (52) starts to rotate so as to drive a long rod (55) sleeved on a connecting block (53) to rotate, the long rod (55) is further fixed by a fixed block (54), so that a fan blade (56) fixed on the long rod (55) rotates, the water in the inner tank (31) and the substance needing hydrolysis are stirred, the hydrolysis reaction of the substance is accelerated, when the reaction is complete, the liquid in the liquid inlet pipe (21) is stopped, and when the liquid in the liquid outlet pipe (22) is completely discharged, then the liquid discharge cover (24) is opened, then the liquid in the outer tank (23) is completely discharged, then the handle (33) is pinched, the plug (32) is opened, then the liquid in the inner tank (31) is discharged, the liquid is collected, after the liquid is discharged, the plug (32) is covered in the inner tank (31), the liquid discharge cover (24) is installed in the outer tank (23), then clear water is injected from the injection pipe (42) and the pipeline (72), the motor (51) installed on the fixed shell (52) starts to rotate, so that the long rod (55) sleeved on the connecting block (53) is driven to rotate, the fixed block (54) further fixes the long rod (55), so that the fan blades (56) fixed on the long rod (55) rotate, the clear water in the inner tank (31) is stirred, so that the inner wall of the inner tank (31) is cleaned, and the next reaction is prevented because of the residue on the inner wall of the inner tank (31), the liquid in the next reaction is polluted, but the liquid in the pipeline (72) is in a standing state and cannot be influenced by stirring of the fan blades (56), then the long rod (55) on the connecting block (53) is taken out, the block (93) is vertically placed in the inlet of the pipeline (72), the block (93) is sent to the other end of the pipeline (72) by utilizing the connecting column (85), then the rope (92) is pulled to transversely place the block (93) so as to block the block (93) at the bottom end of the pipeline (72), then the redundant rope (92) is wound in the roller (91) and the rope (92) is clamped in the clamping groove on the roller (91), the clamping block (83) is clamped on the fixing plate (61), then the handle (81) is pulled, the steel wire (86) connected on the circular ring (82) connected with the handle (81) drives the sliding block (87) and the brush (88) to slide on the connecting column (85), and the spring (84) is compressed, so that the brush (88) brushes the inner wall of the pipeline (72), when the handle (81) is released, the spring (84) is released, the sliding block (87) and the brush (88) move to the position away from the clamping block (83), the handle (81) is pulled back and forth and released, and the brush (88) brushes the inner wall of the pipeline (72) back and forth, so that the interior of the pipeline (72) is cleaned, and the liquid of the next reaction is prevented from being influenced by the residue of the object of the previous reaction.
CN201811207176.9A 2018-10-17 2018-10-17 Hydrolysis reaction tank for chemical production Active CN109248641B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2512349A (en) * 2013-03-27 2014-10-01 Airnesco Group Ltd Expandable tool for cleaning pipes
CN206794301U (en) * 2017-05-19 2017-12-26 重庆市九龙坡职业教育中心 A kind of teat glass cleaning device
CN207446894U (en) * 2017-10-16 2018-06-05 广东森濠建设有限公司 A kind of novel steel tube processes maintenance device

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN205379884U (en) * 2016-01-06 2016-07-13 哈尔滨合佳制药有限公司 Hydrolyzing tank
CN207418916U (en) * 2017-10-30 2018-05-29 宁夏中晶半导体材料有限公司 A kind of cleaning plant that pipeline is evacuated for czochralski crystal growing furnace

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2512349A (en) * 2013-03-27 2014-10-01 Airnesco Group Ltd Expandable tool for cleaning pipes
CN206794301U (en) * 2017-05-19 2017-12-26 重庆市九龙坡职业教育中心 A kind of teat glass cleaning device
CN207446894U (en) * 2017-10-16 2018-06-05 广东森濠建设有限公司 A kind of novel steel tube processes maintenance device

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