CN109231960A - The method of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls - Google Patents
The method of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls Download PDFInfo
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- CN109231960A CN109231960A CN201811202498.4A CN201811202498A CN109231960A CN 109231960 A CN109231960 A CN 109231960A CN 201811202498 A CN201811202498 A CN 201811202498A CN 109231960 A CN109231960 A CN 109231960A
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- Prior art keywords
- waste
- hours
- ceramic balls
- raw material
- water treatment
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Structural Engineering (AREA)
- Materials Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- Hydrology & Water Resources (AREA)
- Water Supply & Treatment (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
A kind of method that the present invention discloses waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls, the following steps are included: 1) after waste ceramic filler being placed in 200-250 DEG C of high-temperature water vapor and heating 2-4 hours, it is stirred 8-10 hours in 80-100 DEG C of water, filtering removal liquid dries solid, obtains primary raw materials；2) primary raw materials is placed in tunnel oven, is warming up to 1200-1320 DEG C with 50-80 DEG C per hour of heating rate, keeps the temperature 1-2 hours, activation raw material is obtained after cooling；The present invention is at low cost, is suitble to environmentally friendly recycling and reusing waste ceramic filler.
Description
Technical field
The present invention relates to a kind of methods that waste ceramic filler regenerates preparation use in waste water treatment Ceramic Balls.
Background technique
Ceramic packing is using be easy to causeing the waste of resource after discarded and to the destruction of environment, but since ceramic packing adsorbs
Organic matter, new uncontrollable atmosphere pollution can be brought by directlying adopt pyrogenic attack, therefore be developed environmental friendly regenerated using useless
The method for abandoning ceramic packing has important practical significance.
Summary of the invention
The technical problem to be solved by the present invention is to the shortcomings that overcoming the above prior art: provide a kind of at low cost, suitable
The method of environmentally friendly recycling and reusing waste ceramic filler preparation use in waste water treatment Ceramic Balls.
Technical solution of the invention is as follows: a kind of side of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls
Method, comprising the following steps:
1) waste ceramic filler is placed in 200-250 DEG C of high-temperature water vapor after heating 2-4 hours, in 80-100 DEG C of water
Stirring 8-10 hours, filtering removal liquid dry solid, obtain primary raw materials；
2) primary raw materials is placed in tunnel oven, is warming up to 1200-1320 DEG C with 50-80 DEG C per hour of heating rate, heat preservation
1-2 hours, activation raw material is obtained after cooling；
3) taking the activation raw material and kaolin, carboxymethyl cellulose mixed grinding to average grain diameter is 3-10 microns, is then made
The Ceramic Balls green compact that average grain diameter is 8-20mm are made in grain；
4) the Ceramic Balls green compact are placed in kiln, are warming up to 1320 DEG C -1350 with 50 DEG C -80 DEG C per hour of heating rate
DEG C, 3-8 hours are kept the temperature, up to use in waste water treatment Ceramic Balls after cooling.
In step 3), the proportion of each raw material is as follows in parts by weight: raw material 50-70 parts of activation；Kaolin 20-30
Part；5-12 parts of carboxymethyl cellulose.
The beneficial effects of the present invention are: since waste ceramic filler contains foreign organic matter, the present invention is by waste ceramic filler
Boiling stirring is added after high temperature steam treatment, filters out and is dried after large amount of organic, is activated, then in conjunction with other components
Prepare wastewater purification Ceramic Balls, not only economize on resources, preserve the ecological environment, and greatly reduce production cost with
And extend Ceramic Balls raw material sources.Industrial waste is set to obtain recycling and high value added utilization, it is with good economic efficiency
And social benefit.
Specific embodiment
The present invention is described in further details with specific embodiment below, but the present invention is not only limited in detail below in fact
Apply example.
Embodiment 1
1) waste ceramic filler is placed in 250 DEG C of high-temperature water vapor and is heated 4 hours, waste ceramic filler can be specifically placed in
It is passed through high-temperature vapor heat treatment in drum sieve, is stirred 8 hours in 80 DEG C of water, filtering removal liquid dries solid,
Obtain primary raw materials；
2) primary raw materials is placed in tunnel oven, is warming up to 1320 DEG C with 60 DEG C per hour of heating rate, keeps the temperature 2 hours, it is cold
But activation raw material is obtained afterwards；
3) taking the activation raw material and kaolin, carboxymethyl cellulose mixed grinding to average grain diameter is 10 microns, is then granulated
The Ceramic Balls green compact that average grain diameter is 8mm are made；The proportion of each raw material is as follows in parts by weight: 70 parts of raw material of activation；It is high
20 parts of ridge soil；10 parts of carboxymethyl cellulose.
4) the Ceramic Balls green compact are placed in kiln, are warming up to 1320 DEG C with 50 DEG C per hour of heating rate, heat preservation 8
Hour, up to use in waste water treatment Ceramic Balls after cooling.
Embodiment 2
1) waste ceramic filler is placed in 220 DEG C of high-temperature water vapor and is heated 4 hours, stirred 8 hours in 100 DEG C of water,
Filtering removal liquid dries solid, obtains primary raw materials；
2) primary raw materials is placed in tunnel oven, is warming up to 1320 DEG C with 60 DEG C per hour of heating rate, keeps the temperature 2 hours, it is cold
But activation raw material is obtained afterwards；
3) taking the activation raw material and kaolin, carboxymethyl cellulose mixed grinding to average grain diameter is 10 microns, is then granulated
The Ceramic Balls green compact that average grain diameter is 8mm are made；The proportion of each raw material is as follows in parts by weight: 70 parts of raw material of activation；It is high
20 parts of ridge soil；10 parts of carboxymethyl cellulose.
4) the Ceramic Balls green compact are placed in kiln, are warming up to 1320 DEG C with 50 DEG C per hour of heating rate, heat preservation 8
Hour, up to use in waste water treatment Ceramic Balls after cooling.
Embodiment 3
1) waste ceramic filler is placed in 230 DEG C of high-temperature water vapor and is heated 4 hours, stirred 8 hours in 90 DEG C of water, mistake
It filters off and is dried except liquid, by solid, obtain primary raw materials；
2) primary raw materials is placed in tunnel oven, is warming up to 1320 DEG C with 60 DEG C per hour of heating rate, keeps the temperature 2 hours, it is cold
But activation raw material is obtained afterwards；
3) taking the activation raw material and kaolin, carboxymethyl cellulose mixed grinding to average grain diameter is 10 microns, is then granulated
The Ceramic Balls green compact that average grain diameter is 8mm are made；The proportion of each raw material is as follows in parts by weight: 58 parts of raw material of activation；It is high
30 parts of ridge soil；12 parts of carboxymethyl cellulose.
4) the Ceramic Balls green compact are placed in kiln, are warming up to 1320 DEG C with 50 DEG C per hour of heating rate, heat preservation 8
Hour, up to use in waste water treatment Ceramic Balls after cooling.
The above is only feature implementation examples of the invention, are not limited in any way to the scope of the present invention.It is all to use together
The technical solution formed Deng exchange or equivalence replacement, all falls within rights protection scope of the present invention.
Claims (2)
1. a kind of method of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls, it is characterised in that: the following steps are included:
1) waste ceramic filler is placed in 200-250 DEG C of high-temperature water vapor after heating 2-4 hours, in 80-100 DEG C of water
Stirring 8-10 hours, filtering removal liquid dry solid, obtain primary raw materials；
2) primary raw materials is placed in tunnel oven, is warming up to 1200-1320 DEG C with 50-80 DEG C per hour of heating rate, heat preservation
1-2 hours, activation raw material is obtained after cooling；
3) taking the activation raw material and kaolin, carboxymethyl cellulose mixed grinding to average grain diameter is 3-10 microns, is then made
The Ceramic Balls green compact that average grain diameter is 8-20mm are made in grain；
4) the Ceramic Balls green compact are placed in kiln, are warming up to 1320 DEG C -1350 with 50 DEG C -80 DEG C per hour of heating rate
DEG C, 3-8 hours are kept the temperature, up to use in waste water treatment Ceramic Balls after cooling.
2. the method for waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls according to claim 1, feature exist
In: in step 3), the proportion of each raw material is as follows in parts by weight: raw material 50-70 parts of activation；20-30 parts of kaolin；Carboxylic first
5-12 parts of base cellulose.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811202498.4A CN109231960A (en) | 2018-10-16 | 2018-10-16 | The method of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811202498.4A CN109231960A (en) | 2018-10-16 | 2018-10-16 | The method of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls |
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| Publication Number | Publication Date |
|---|---|
| CN109231960A true CN109231960A (en) | 2019-01-18 |
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|---|---|---|---|
| CN201811202498.4A Pending CN109231960A (en) | 2018-10-16 | 2018-10-16 | The method of waste ceramic filler regeneration preparation use in waste water treatment Ceramic Balls |
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Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4334026A (en) * | 1980-01-18 | 1982-06-08 | Institute Of Gas Technology | Hybrid bio-thermal liquefaction |
| JPH01254294A (en) * | 1988-04-05 | 1989-10-11 | Onoda Cement Co Ltd | Treatment of living waste water |
| CN1511630A (en) * | 2002-12-30 | 2004-07-14 | 北京华本光催化技术有限公司 | Method for preparing porous ceramics supported high activity nano titanium dioxide |
| CN1174935C (en) * | 2001-03-30 | 2004-11-10 | 广东佛陶集团金刚新材料有限公司 | Polished brick waste mud ceramiste and its preparing method |
| CN1644550A (en) * | 2004-12-15 | 2005-07-27 | 袁景华 | Polymer aluminium silicate cement and production thereof |
| CN102099448A (en) * | 2008-07-18 | 2011-06-15 | 法国圣戈班玻璃厂 | Industrial device manufacturing its own fuel |
| CN102557712A (en) * | 2011-12-26 | 2012-07-11 | 大连工业大学 | Method for manufacturing water permeable brick by using sugar filter mud |
| CN102688881A (en) * | 2011-03-24 | 2012-09-26 | 上海万帝环境技术有限公司 | Urban kitchen waste recycling utilization and harmless treatment technology |
| CN105060743A (en) * | 2015-08-24 | 2015-11-18 | 盐城工学院 | Cement material prepared from waste tile powder |
| CN105060754A (en) * | 2015-08-24 | 2015-11-18 | 盐城工学院 | Waste ceramic tile powder cement admixture |
-
2018
- 2018-10-16 CN CN201811202498.4A patent/CN109231960A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4334026A (en) * | 1980-01-18 | 1982-06-08 | Institute Of Gas Technology | Hybrid bio-thermal liquefaction |
| JPH01254294A (en) * | 1988-04-05 | 1989-10-11 | Onoda Cement Co Ltd | Treatment of living waste water |
| CN1174935C (en) * | 2001-03-30 | 2004-11-10 | 广东佛陶集团金刚新材料有限公司 | Polished brick waste mud ceramiste and its preparing method |
| CN1511630A (en) * | 2002-12-30 | 2004-07-14 | 北京华本光催化技术有限公司 | Method for preparing porous ceramics supported high activity nano titanium dioxide |
| CN1644550A (en) * | 2004-12-15 | 2005-07-27 | 袁景华 | Polymer aluminium silicate cement and production thereof |
| CN102099448A (en) * | 2008-07-18 | 2011-06-15 | 法国圣戈班玻璃厂 | Industrial device manufacturing its own fuel |
| CN102688881A (en) * | 2011-03-24 | 2012-09-26 | 上海万帝环境技术有限公司 | Urban kitchen waste recycling utilization and harmless treatment technology |
| CN102557712A (en) * | 2011-12-26 | 2012-07-11 | 大连工业大学 | Method for manufacturing water permeable brick by using sugar filter mud |
| CN105060743A (en) * | 2015-08-24 | 2015-11-18 | 盐城工学院 | Cement material prepared from waste tile powder |
| CN105060754A (en) * | 2015-08-24 | 2015-11-18 | 盐城工学院 | Waste ceramic tile powder cement admixture |
Non-Patent Citations (3)
| Title |
|---|
| 冯聪: "几种金属氧化物纤维的制备及其性能研究", 《中国博士学位论文全文数据库 工程科技Ⅰ辑》 * |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190118 |
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| RJ01 | Rejection of invention patent application after publication |