CN109225092A - A kind of temperature control equipment for diborane reaction kettle - Google Patents
A kind of temperature control equipment for diborane reaction kettle Download PDFInfo
- Publication number
- CN109225092A CN109225092A CN201811144110.XA CN201811144110A CN109225092A CN 109225092 A CN109225092 A CN 109225092A CN 201811144110 A CN201811144110 A CN 201811144110A CN 109225092 A CN109225092 A CN 109225092A
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- groups
- bottom end
- pipe
- reaction kettle
- gauge
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 55
- 238000009434 installation Methods 0.000 claims abstract description 73
- 238000010438 heat treatment Methods 0.000 claims abstract description 70
- 239000007788 liquid Substances 0.000 claims abstract description 62
- 238000012546 transfer Methods 0.000 claims abstract description 54
- 239000002828 fuel tank Substances 0.000 claims abstract description 40
- 238000013016 damping Methods 0.000 claims abstract description 35
- 238000005192 partition Methods 0.000 claims abstract description 14
- 238000003825 pressing Methods 0.000 claims abstract description 13
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 22
- 238000005485 electric heating Methods 0.000 claims description 6
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 239000002937 thermal insulation foam Substances 0.000 claims description 5
- 238000004891 communication Methods 0.000 claims description 3
- 238000005538 encapsulation Methods 0.000 claims description 3
- 230000008676 import Effects 0.000 claims description 3
- 238000003780 insertion Methods 0.000 claims description 3
- 230000037431 insertion Effects 0.000 claims description 3
- 241000255777 Lepidoptera Species 0.000 claims description 2
- 238000002627 tracheal intubation Methods 0.000 abstract description 20
- 239000012535 impurity Substances 0.000 abstract description 17
- 238000000034 method Methods 0.000 abstract description 7
- 230000008569 process Effects 0.000 abstract description 6
- 238000004064 recycling Methods 0.000 abstract description 6
- 230000002159 abnormal effect Effects 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 description 7
- 239000002585 base Substances 0.000 description 6
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 4
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 229910052796 boron Inorganic materials 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- UORVGPXVDQYIDP-UHFFFAOYSA-N trihydridoboron Substances B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229910015900 BF3 Inorganic materials 0.000 description 2
- 229910000085 borane Inorganic materials 0.000 description 2
- 239000000872 buffer Substances 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 229910000102 alkali metal hydride Inorganic materials 0.000 description 1
- 150000008046 alkali metal hydrides Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- -1 boron Sodium hydride Chemical compound 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical compound Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 239000002019 doping agent Substances 0.000 description 1
- 239000002816 fuel additive Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 125000000962 organic group Chemical group 0.000 description 1
- 238000006053 organic reaction Methods 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/96—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor in which the filtering elements are moved between filtering operations; Particular measures for removing or replacing the filtering elements; Transport systems for filters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
- F04B53/00—Component parts, details or accessories not provided for in, or of interest apart from, groups F04B1/00 - F04B23/00 or F04B39/00 - F04B47/00
- F04B53/001—Noise damping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00092—Tubes
Abstract
The present invention relates to the technical fields that diborane production prepares auxiliary equipment, more particularly to a kind of temperature control equipment for diborane reaction kettle, it can the internal more impurity being mixed with removes during recycling to conduction oil, prevents the impurity inside conduction oil from generating abnormal sound with pipeline inner walls collisions such as outlet tube, heating coil and liquid back pipes in thermally conductive oil circulation process；And it can carry out damping to Heat-transfer Oil Pump, reduce the noise caused by overall operation in the Heat-transfer Oil Pump course of work；Including intubation, four groups of setting of casings, four groups of damping springs, four groups of screwed pipes, four groups of pressing plates and four groups of threaded rods on resilient cushion under resilient cushion on bottom plate, reaction kettle, heating coil, cabinet body, Heat-transfer Oil Pump, heat conduction fuel tank, heating tube, partition, liquid back pipe, outlet tube, left U-typed pipe, right U-typed pipe, screen pipe, filter core, mounting ring, upper mounting plate, platform sling, four groups of screw rods, four groups of nuts, four groups of support columns, lower installation board, four groups, four groups, four groups.
Description
Technical field
The present invention relates to the technical fields that diborane production prepares auxiliary equipment, anti-for diborane more particularly to one kind
Answer the temperature control equipment of kettle.
Background technique
It is well known that diborane is simplest borine, colourless liquid, chemical property is quite active, can spontaneous combustion, the combustion heat
It is very high, it is reacted with water and generates boric acid and hydrogen, the boron hydrohalogenic acid salt to become increasingly complex can be formed with alkali metal hydride, sent out with alkene
Raw addition reaction, and top-end hydrogen can be replaced by organic group or as electrophilic reducing agent, with sodium alanate and boron trifluoride or boron
Sodium hydride is reacted with boron trifluoride or calogreen to be produced, and for making pure boron or synthesizes other borines and boracic and nitrogen, phosphorus, arsenic
The raw material of the compound of key etc. is often made the dopant of organic reaction reducing agent, fuel additive and p-type semiconductor material, is used for
The temperature control equipment of diborane reaction kettle is that a kind of prepare to production carries out temperature raising control inside diborane reaction kettle, with
Convenient for better meeting the auxiliary device of combination reaction required temperature in diborane production preparation process, produces and make in diborane
It is widely used in a variety of applications in standby field；The existing temperature control equipment for diborane reaction kettle includes bottom plate, reaction
Kettle, heating coil, cabinet body, Heat-transfer Oil Pump, heat conduction fuel tank, heating tube, partition, liquid back pipe and outlet tube, a left side for reaction kettle bottom end
Front side, left rear side, forward right side and right lateral side are provided with supporting leg, and the bottom end of four groups of supporting legs respectively with bottom plate top right side region
Front left side, left rear side, the forward right side in domain are connected with right lateral side, and the bottom end of cabinet body is connect with the left side on bottom plate top, cabinet body it is interior
Portion is provided with working chamber, and the front end of cabinet body is provided with operation port, communicates inside operation port and working chamber, the top of heat conduction fuel tank
End is connect with the inner roof wall of working chamber, and the inner bottom wall of the bottom end of Heat-transfer Oil Pump and working chamber connects, and the left end of heating tube is set
It is equipped with mounting base, multiple groups electric heating block has been uniformly arranged on the outer wall of heating tube, the inside that partition is longitudinally mounted to working chamber is left
Side, and connection in the middle part of the right end of the left end of mounting base and partition, heat conduction fuel tank are internally provided with conduction oil, and heat conduction fuel tank
Bottom end on the right side of by being connected to the input terminal on the right side of heating tube top the first communicating pipe, control is provided on the first communicating pipe
Valve, and the output end on the left of heating tube bottom end is with the input terminal of Heat-transfer Oil Pump by being connected to the second communicating pipe, outlet tube it is defeated
Enter end to be connected to the output end of Heat-transfer Oil Pump, and the surrounding outer wall of reaction kettle, and outlet tube is arranged in heating coil coiling
Right part output end the right end inner wall of working chamber is passed through inside the working chamber and extend out to cabinet body right end is extraneous and heating coil
Input terminal connection on the downside of left part, the input terminal of liquid back pipe is connected to the output end on the upside of heating coil left part, and liquid back pipe
Output end be connected to from the upside of the right end outer wall that the right side of cabinet body passes through cabinet body with the right end of heat conduction fuel tank；It is existing to be used for second boron
Then the temperature control equipment of alkane reaction kettle opens control valve in use, conduction oil is injected into inside heat conduction fuel tank first, will
Conduction oil inside heat conduction fuel tank is delivered to inside heating tube from inside heat conduction fuel tank by the first communicating pipe, then by electric heating
Block and external power supply are connected, and make to be preheated inside heating tube, conduction oil is heated, while by Heat-transfer Oil Pump and external electrical
Source is connected, and opens Heat-transfer Oil Pump, the conduction oil after heating is delivered to inside heating coil from Heat-transfer Oil Pump by outlet tube, is made
Conduction oil after heating is in heating coil internal circulation, so that the heat transfer inside conduction oil is given to reaction kettle inside, for second
Borane gases prepare combination reaction and use, and the conduction oil after heat transmitting is gone successively to inside heat conduction fuel tank by liquid back pipe, continue
It is internally heated into heating tube, is recycled by Heat-transfer Oil Pump, reaction kettle inside continually and steadily heat；
It is found in the existing temperature control equipment use for diborane reaction kettle, conduction oil internal meeting during recycling
It is mixed with more impurity, cannot be removed in time, into inside Heat-transfer Oil Pump, is easy to damage Heat-transfer Oil Pump, while in conduction oil
The impurity in portion is then produced with easy in thermally conductive oil circulation process with pipeline inner walls collisions such as outlet tube, heating coil and liquid back pipes
Raw abnormal sound, causes its use reliability lower；And it cannot carry out damping to Heat-transfer Oil Pump, make in the Heat-transfer Oil Pump course of work
Cause overall operation noise larger, it is higher using limitation.
Summary of the invention
In order to solve the above technical problems, the present invention, which provides one kind, internal during recycling to conduction oil can be mixed with
More impurity removed in time, prevent impurity from entering inside Heat-transfer Oil Pump, prevent from damaging Heat-transfer Oil Pump, while preventing from leading
Impurity inside hot oil is collided with easy in thermally conductive oil circulation process with pipeline inner walls such as outlet tube, heating coil and liquid back pipes
Abnormal sound is generated, use reliability is improved；And damping can be carried out to Heat-transfer Oil Pump, it reduces in the Heat-transfer Oil Pump course of work to entirety
Noise caused by operation reduces the temperature control equipment for diborane reaction kettle for using limitation.
A kind of temperature control equipment for diborane reaction kettle of the invention, including bottom plate, reaction kettle, heating coil,
Cabinet body, Heat-transfer Oil Pump, heat conduction fuel tank, heating tube, partition, liquid back pipe and outlet tube, the front left side of reaction kettle bottom end, left rear side,
Forward right side and right lateral side are provided with supporting leg, and the bottom end of four groups of supporting legs respectively with the front left side of bottom plate top right area,
Left rear side, forward right side are connected with right lateral side, and the bottom end of cabinet body is connect with the left side on bottom plate top, and cabinet body is internally provided with work
Chamber, and the front end of cabinet body is provided with operation port, communicates inside operation port and working chamber, the top of heat conduction fuel tank and working chamber
Inner roof wall connection, and the inner bottom wall of the bottom end of Heat-transfer Oil Pump and working chamber connects, and the left end of heating tube is provided with mounting base, adds
Multiple groups electric heating block is uniformly arranged on the outer wall of heat pipe, partition is longitudinally mounted to the inside left of working chamber, and mounting base
Left end and partition right end in the middle part of connect, heat conduction fuel tank is internally provided with conduction oil, and logical on the right side of the bottom end of heat conduction fuel tank
It is connected to after the first communicating pipe with the input terminal on the right side of heating tube top, control valve, and heating tube is provided on the first communicating pipe
Output end on the left of bottom end with the input terminal of Heat-transfer Oil Pump by being connected to the second communicating pipe, the input terminal and Heat-transfer Oil Pump of outlet tube
Output end connection, and heating coil coiling is arranged in the surrounding outer wall of reaction kettle, and the right part output end of outlet tube from
The right end inner wall of working chamber is passed through inside working chamber and the right end external world for extending out to cabinet body and the input on the downside of heating coil left part
End connection, the input terminal of liquid back pipe is connected to the output end on the upside of heating coil left part, and the output end of liquid back pipe is from cabinet body
Right side pass through and be connected on the upside of the right end outer wall of cabinet body with the right end of heat conduction fuel tank；Including left U-typed pipe, right U-typed pipe, filtering
Pipe, filter core, mounting ring, upper mounting plate, platform sling, four groups of screw rods and four groups of nuts, the liquid back pipe are set as left liquid back pipe and the right side
Liquid back pipe, and the left part output end of the left liquid back pipe is connected to the right end of the heat conduction fuel tank, and the right liquid back pipe
Right part input terminal be connected to the output end of the heating coil left upper portion, the left U-typed pipe and right U-typed pipe are respectively provided with
Between the left liquid back pipe and right liquid back pipe, the left end of left U-typed pipe is connected to the right part input terminal of left liquid back pipe, and institute
The right end for stating right U-typed pipe is connected to the left part output end of the right liquid back pipe, the top of the upper mounting plate and the work
The right side of intracavitary roof connects, the top of four groups of screw rods respectively with the front left side of the upper mounting plate bottom end, left rear side, the right side
Front side is connected with right lateral side, and front left side, left rear side, forward right side and the right lateral side of platform sling bottom end are provided with connecting rod, and institute
The bottom end for stating four groups of connecting rods is connect with front left side, left rear side, forward right side and the right lateral side on the screen pipe top respectively, described
Front left side, left rear side, forward right side and the right lateral side on platform sling top are provided with perforative installation through-hole up and down, and described four groups
The bottom end of screw rod is each passed through inside four groups of installation through-holes from the top of platform sling and extend out to the bottom end of platform sling, four groups of spiral shells
The other spiral shell encapsulation of mother stock is located at the outside of four groups of screw rods, and bottom end of the top of four groups of nuts with the platform sling is adjacent to,
The screen pipe is internally provided with filter chamber, and the left and right side of screen pipe bottom end is respectively arranged with export and import,
The right end and outlet of the left U-typed pipe, and the left end of the right U-typed pipe and inlet communication, the mounting ring are vertical
To being mounted on inside the right side of the filter chamber, and the circumferential inner wall of the circumferential inner wall of the mounting ring and the filter chamber is solid
Fixed connection, the right end of the left end self installation ring of the filter core pass through mounting ring inner wall and extend out to the left end external world of mounting ring, filter
It is communicated inside the right part output end of core and the filter chamber；It further include four groups of support columns, lower installation board, resilient cushion, four on four groups
The lower resilient cushion of group, intubation, four groups of setting of casings, four groups of damping springs, four groups of screwed pipes, four groups of pressing plates and four groups of screw threads on four groups
Bar, the bottom end of the Heat-transfer Oil Pump are provided with pedestal, and four groups of support columns top respectively with the lower installation board bottom end
Front left side, left rear side, forward right side connected with right lateral side, the pedestal be arranged in lower installation by top, four groups of supports
The bottom end of column is connect with front left side, left rear side, forward right side and the right lateral side of the working chamber inner bottom wall right area respectively, described
The top of resilient cushion is connect with front left side, left rear side, forward right side and the right lateral side of the lower installation board bottom end respectively on four groups, and
And under described four groups resilient cushion bottom end front left side, left rear side, the forward right side with the working chamber inner bottom wall right area respectively
It connecting with right lateral side, resilient cushion is respectively positioned on the inside of four groups of support columns under resilient cushion and four groups on described four groups, and described four groups
The top of upper intubation is connect with the bottom end of resilient cushion on described four groups respectively, and four groups of cased bottom ends are respectively with described four
The top of the lower resilient cushion of group connects, and the bottom end being intubated on described four groups is can be slidably inserted into respectively to four groups of cased tops
Portion, the bottom end of four groups of damping springs are connect with described four groups cased bottom end inner walls respectively, and are inserted on described four groups
It is provided with regulating tank on the top inner wall of pipe, ball bearing, four groups of screw threads are provided with inside four groups of regulating tanks
The top of pipe is inserted and fixed respectively inside installation to four groups of ball bearings, and the top of four groups of threaded rods is inserted into respectively and spiral shell
It is filled to the bottom inner portion of four groups of screwed pipes, the top of four groups of pressing plates is connect with the bottom end of four groups of threaded rods respectively, and
And the bottom end of four groups of pressing plates is connect with the top of four groups of damping springs respectively.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes four groups of holddown springs and support
Plate, the top of four groups of holddown springs front left side, left rear side, forward right side and the right lateral side with the upper mounting plate bottom end respectively
Connection, four groups of holddown springs are respectively positioned on the inside of four groups of screw rods, and the bottom end of four groups of holddown springs respectively with the branch
Front left side, left rear side, the forward right side on fagging top are connected with right lateral side, and the bottom end of support plate and the top of the platform sling are adjacent to.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes left snap-gauge, right snap-gauge, two groups of left sides
Wing bolt and two groups of right wing bolts, the front left side and left rear side on the pedestal top are provided with left installation jack, and
The forward right side and right lateral side on the pedestal top are provided with right installation jack, the forward right side and right lateral side of the left snap-gauge bottom end
It is provided with left plug, and the front left side of the right snap-gauge bottom end and left rear side are provided with right plug, the lower installation board
The front left side and left rear side on top are provided with left-hand thread hole, and the forward right side and right lateral side on the lower installation board top are provided with
Right-hand thread hole, the bottom end of two groups of left wing bolts are each passed through front left side inside left snap-gauge and left rear side and extend out to a left side
The bottom end of snap-gauge is extraneous, and the bottom end of two groups of left wing bolts is inserted into respectively and spiral shell is filled to inside two groups of left-hand thread holes, and
The bottom end of two groups of left plugs is inserted into respectively inside two groups of left installation jacks, the top of the bottom end of left snap-gauge and the pedestal
Left side is adjacent to, and the bottom end of two groups of right wing bolts is each passed through forward right side inside right snap-gauge and right lateral side and extend out to the right side
The bottom end of snap-gauge is extraneous, and the bottom end of two groups of right wing bolts is inserted into respectively and spiral shell is filled to inside two groups of right-hand thread holes, and
The bottom end of two groups of right plugs is inserted into respectively inside two groups of right installation jacks, the top of the bottom end of right snap-gauge and the pedestal
Right side is adjacent to.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes two groups of left support springs and two groups
Right support spring, the outside for being respectively sleeved at two groups of left wing bolts of two groups of left support springs, and two groups are left
The bottom end of support spring is connect with the front left side on the lower installation board top and left rear side respectively, the top of two groups of left support springs
It is connect respectively with the front left side of the left snap-gauge bottom end and left rear side, two groups of right support springs are respectively sleeved at described two
The outside of the right wing bolt of group, and the bottom end of two groups of right support springs respectively with the forward right side on the lower installation board top and the right side
Rear side connection, the top of two groups of right support springs is connect with the forward right side of the right snap-gauge bottom end and right lateral side respectively.
A kind of temperature control equipment for diborane reaction kettle of the invention, further include mounting disc, the first bolt of multiple groups,
Stop collar, round door and the second bolt of multiple groups, the mounting disc are fixedly set in the external right side of the filter core, and install
The left end of disk and the right end of the mounting ring are adjacent to, and circumference is provided with the installation bolt hole of multiple groups first, peace in mounting disc
The right end circumference of dress ring is provided with multiple groups first and installs threaded hole, and the left end of first bolt of multiple groups is each passed through multiple groups first
Installation bolt hole is inserted into respectively and spiral shell is filled to multiple groups first and installs inside threaded hole, and the right end of the screen pipe is provided with operation
Mouthful, and communicated inside operation port and the filter chamber, the stop collar is fixedly set in the external right side of the screen pipe, and
And the right end circumference of stop collar is provided with multiple groups second and installs threaded hole, circumference is provided with the peace of multiple groups second on the circle door
Bolt hole is filled, the left end of second bolt of multiple groups is each passed through inside the installation bolt hole of multiple groups second insertion and spiral shell respectively
Multiple groups second are filled to install inside threaded hole.
A kind of temperature control equipment for diborane reaction kettle of the invention, further includes collet, the collet is set in
The outside of the heating coil, and heat insulation foam has been filled in the gap between collet and heating coil.
A kind of temperature control equipment for diborane reaction kettle of the invention, further includes oil level indicator, and the oil level indicator connects
It is logical to be mounted on the left of the front end of the heat conduction fuel tank on outer wall.
A kind of temperature control equipment for diborane reaction kettle of the invention, further includes handle, the left end of the handle
It is connect with the right end of the round door.
It compared with prior art the invention has the benefit that can be by the filter core inside screen pipe to liquid back pipe inside
Conduction oil be filtered, be delivered to inside left U-typed pipe after filtering by filter chamber and be fed back to conduction oil by left liquid back pipe
Inside case, it can be arranged by the U-typed of left U-typed pipe and right U-typed pipe, delay the conduction oil inside liquid back pipe
Punching, so as to reduce impact of the conduction oil inside liquid back pipe to filter core, while can reduce the speed of conduction oil, make filter core
Impurity inside conduction oil can sufficiently be filtered, the spiral shell assembly between four groups of screw rods respectively of four groups of nuts can be passed through
Close, screen pipe facilitated to carry out hanging assembly and disassembly, so as to conduction oil during recycling it is internal be mixed with it is more miscellaneous
Matter is removed in time, prevents impurity from entering inside Heat-transfer Oil Pump, prevents from damaging Heat-transfer Oil Pump, while preventing inside conduction oil
Impurity different with the pipeline inner walls collision generation such as outlet tube, heating coil and liquid back pipe with being easy in thermally conductive oil circulation process
It rings, improves use reliability；And it can be mitigated respectively by resilient cushion on four groups on four groups between intubation and lower installation board
Vibration, mitigates the vibration between four groups of setting of casings and working chamber inner bottom wall by resilient cushion under four groups respectively, can pass through four groups
Upper intubation with being slidably matched inside setting of casing, makes to carry out moving up and down inside intubation and four groups of setting of casings on four groups respectively
Make, while can be supported respectively between intubation under intubation on four groups and four groups by the retractility of four groups of damping springs,
So as to so that four groups of damping springs up and down action to Heat-transfer Oil Pump carry out damping, can be by rotating four groups of screw threads respectively
Pipe, rotates four groups of screwed pipes inside four groups of ball bearings respectively, so as to by four groups of threaded rods respectively with four
Spiral shell between group screwed pipe, which assembles, to be closed, and four groups of threaded rods is allow to carry out precession and back-out inside four groups of screwed pipes respectively, from
And can push four groups of pressing plates that the decrement of four groups of damping springs is adjusted respectively respectively by four groups of threaded rods, so as to
To facilitate according to actual field environment, the damping effect of four groups of damping springs is adjusted, so as to realize to conduction oil
Pump carries out damping, reduces the noise caused by overall operation in the Heat-transfer Oil Pump course of work, reduces and uses limitation.
Detailed description of the invention
Fig. 1 is structural schematic diagram of the invention；
Fig. 2 is the partial enlargement structural representation at A of the present invention；
Fig. 3 is the partial enlargement structural representation at B of the present invention；
Fig. 4 is the partial enlargement structural representation at C of the present invention；
Fig. 5 is the partial enlargement structural representation at D of the present invention；
It is attached marked in the figure: 1, bottom plate；2, reaction kettle；3, heating coil；4, cabinet body；5, Heat-transfer Oil Pump；6, heat conduction fuel tank；7,
Heating tube；8, partition；9, liquid back pipe；10, outlet tube；11, left U-typed pipe；12, screen pipe；13, filter core；14, mounting ring；15,
Upper mounting plate；16, platform sling；17, screw rod；18, nut；19, support column；20, lower installation board；21, upper resilient cushion；22, upper intubation；
23, setting of casing；24, damping spring；25, screwed pipe；26, pressing plate；27, threaded rod；28, holddown spring；29, left snap-gauge；30, left
Wing bolt；31, left support spring；32, mounting disc；33, the first bolt；34, stop collar；35, round door；36, the second spiral shell
Bolt；37, collet；38, oil level indicator；39, handle；40, support plate.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiments of the present invention will be described in further detail.Implement below
Example is not intended to limit the scope of the invention for illustrating the present invention.
As shown in Figures 1 to 5, a kind of temperature control equipment for diborane reaction kettle of the invention, including bottom plate 1,
Reaction kettle 2, heating coil 3, cabinet body 4, Heat-transfer Oil Pump 5, heat conduction fuel tank 6, heating tube 7, partition 8, liquid back pipe 9 and outlet tube 10,
Front left side, left rear side, forward right side and the right lateral side of 2 bottom end of reaction kettle are provided with supporting leg, and the bottom end difference of four groups of supporting legs
It is connect with front left side, left rear side, forward right side and the right lateral side of 1 top right area of bottom plate, the bottom end and 1 top of bottom plate of cabinet body 4
Left side connection, cabinet body 4 is internally provided with working chamber, and the front end of cabinet body 4 is provided with operation port, operation port and working chamber
Inside communicates, and the inner roof wall of the top of heat conduction fuel tank 6 and working chamber connects, and the bottom end of Heat-transfer Oil Pump 5 and working chamber is interior
Bottom wall connection, the left end of heating tube 7 is provided with mounting base, multiple groups electric heating block, partition has been uniformly arranged on the outer wall of heating tube 7
8 are longitudinally mounted to the inside left of working chamber, and connect in the middle part of the left end of mounting base and the right end of partition 8, in heat conduction fuel tank 6
Portion is provided with conduction oil, and passes through the input terminal on the right side of the first communicating pipe and 7 top of heating tube on the right side of the bottom end of heat conduction fuel tank 6
Connection, is provided with control valve on the first communicating pipe, and the output end on the left of 7 bottom end of heating tube by the second communicating pipe with it is thermally conductive
The input terminal of oil pump 5 is connected to, and the input terminal of outlet tube 10 is connected to the output end of Heat-transfer Oil Pump 5, and the coiling of heating coil 3 is set
The surrounding outer wall in reaction kettle 2 is set, and the right part output end of outlet tube 10 is passed through from inside working chamber in the right end of working chamber
The wall and right end external world for extending out to cabinet body 4 is connected to the input terminal on the downside of 3 left part of heating coil, the input terminal of liquid back pipe 9 with plus
Output end connection on the upside of 3 left part of hot coil, and the output end of liquid back pipe 9 is from outside the right end that the right side of cabinet body 4 passes through cabinet body 4
It is connected on the upside of wall with the right end of heat conduction fuel tank 6；Including left U-typed pipe 11, right U-typed pipe, screen pipe 12, filter core 13, mounting ring
14, upper mounting plate 15,16, four groups of screw rods 17 of platform sling and four groups of nuts 18, liquid back pipe 9 are set as left liquid back pipe 9 and right liquid back pipe
9, and the left part output end of left liquid back pipe 9 is connected to the right end of heat conduction fuel tank 6, and the right part input terminal of right liquid back pipe 9 with
The output end of 3 left upper portion of heating coil is connected to, and left U-typed pipe 11 and right U-typed pipe are arranged at left liquid back pipe 9 and right time liquid
Between pipe 9, the left end of left U-typed pipe 11 is connected to the right part input terminal of left liquid back pipe 9, and the right end of right U-typed pipe and the right side
The left part output end of liquid back pipe 9 is connected to, and the top of upper mounting plate 15 is connect with the right side of working chamber inner roof wall, four groups of screw rods 17
Top is connect with front left side, left rear side, forward right side and the right lateral side of 15 bottom end of upper mounting plate respectively, 16 bottom end of platform sling it is left front
Side, left rear side, forward right side and right lateral side are provided with connecting rod, and the bottom end of four groups of connecting rods respectively with 12 top of screen pipe
Front left side, left rear side, forward right side connected with right lateral side, the front left side on 16 top of platform sling, left rear side, forward right side and right lateral side are equal
It is provided with perforative installation through-hole up and down, and the bottom end of four groups of screw rods 17 is each passed through four groups of installations from the top of platform sling 16
Inside through-hole and it extend out to the bottom end of platform sling 16, spiral shell encapsulation is located at the outsides of four groups of screw rods 17, and four to four groups of nuts 18 respectively
Bottom end of the top of group nut 18 with platform sling 16 is adjacent to, and screen pipe 12 is internally provided with filter chamber, and 12 bottom of screen pipe
The left and right side at end is respectively arranged with export and import, the right end and outlet of left U-typed pipe 11, and right U-typed pipe
Left end and inlet communication, mounting ring 14 be longitudinally mounted to inside the right side of filter chamber, and the circumferential inner wall of mounting ring 14 with
The circumferential inner wall of filter chamber is fixedly connected, and the right end of the left end self installation ring 14 of filter core 13 passes through 14 inner wall of mounting ring and extend out to
The left end of mounting ring 14 is extraneous, communicates inside the right part output end and filter chamber of filter core 13；It further include four groups of support columns 19, lower peace
Resilient cushion under 21, four groups of resilient cushion on 20, four groups of loading board, be intubated on four groups 22, four groups of setting of casings, 23, four groups of damping springs 24,
Four groups of screwed pipes, 25, four groups of pressing plates 26 and four groups of threaded rods 27, the bottom end of Heat-transfer Oil Pump 5 are provided with pedestal, and four groups of branch
The top of dagger 19 is connect with front left side, left rear side, forward right side and the right lateral side of 20 bottom end of lower installation board respectively, and pedestal setting exists
It is lower that the top pressed is installed, the bottom end of four groups of support columns 19 respectively with the front left side of working chamber inner bottom wall right area, left rear side, the right side
Front side is connected with right lateral side, and the top of resilient cushion 21 is respectively and before the front left side of 20 bottom end of lower installation board, left rear side, the right side on four groups
Side is connected with right lateral side, and under four groups resilient cushion bottom end respectively with the front left side of working chamber inner bottom wall right area, left back
Side, forward right side are connected with right lateral side, and resilient cushion is respectively positioned on four groups of support columns, 19 inside under resilient cushion 21 and four groups on four groups, and four groups
It is upper intubation 22 top connect respectively with the bottom end of resilient cushion 21 on four groups, and the bottom end of four groups of setting of casings 23 respectively with four groups
The top of lower resilient cushion connects, and the bottom end of intubation 22 is can be slidably inserted into respectively inside the top to four groups of setting of casings 23 on four groups,
The bottom end of four groups of damping springs 24 is connect with the bottom end inner wall of four groups of setting of casings 23 respectively, and on four groups in the top of intubation 22
It is provided with regulating tank on wall, ball bearing is provided with inside four groups of regulating tanks, the top of four groups of screwed pipes 25 is inserted into respectively
And be fixedly installed to inside four groups of ball bearings, the top of four groups of threaded rods 27 is inserted into respectively and spiral shell is filled to four groups of screwed pipes 25
Bottom inner portion, the top of four groups of pressing plates 26 are connect with the bottom end of four groups of threaded rods 27 respectively, and the bottom end of four groups of pressing plates 26 point
It is not connect with the top of four groups of damping springs 24；The conduction oil inside liquid back pipe can be carried out by the filter core inside screen pipe
Filtering is delivered to inside left U-typed pipe by filter chamber after filtering and is fed back to inside heat conduction fuel tank by left liquid back pipe, Ke Yitong
The U-typed setting for crossing left U-typed pipe and right U-typed pipe, buffers the conduction oil inside liquid back pipe, so as to subtract
Impact of the conduction oil to filter core inside few liquid back pipe, while the speed of conduction oil can be reduced, allow filter core by conduction oil
Internal impurity is sufficiently filtered, and can be closed by spiral shell assembly of four groups of nuts respectively between four groups of screw rods, be facilitated filtering
Pipe carries out hanging assembly and disassembly, so as to which to conduction oil, the internal more impurity being mixed with is gone in time during recycling
It removes, prevents impurity from entering inside Heat-transfer Oil Pump, prevent from damaging Heat-transfer Oil Pump, while preventing impurity inside conduction oil with leading
It is easy to generate abnormal sound with the collision of the pipeline inner walls such as outlet tube, heating coil and liquid back pipe during hot-oil circulation, improving use can
By property；And the vibration on four groups between intubation and lower installation board can be mitigated respectively by resilient cushion on four groups, pass through four groups
Lower resilient cushion mitigates the vibration between four groups of setting of casings and working chamber inner bottom wall respectively, can be by being intubated respectively under on four groups
Inside pipe casing is slidably matched, and makes to be moved up and down inside intubation and four groups of setting of casings on four groups, while can pass through
The retractility of four groups of damping springs is supported, so as to so that four groups respectively between intubation under intubation on four groups and four groups
The up and down action of damping spring carries out damping to Heat-transfer Oil Pump, can make four groups of screwed pipes by rotating four groups of screwed pipes respectively
It is rotated inside four groups of ball bearings respectively, so as to pass through four groups of threaded rods spiral shell between four groups of screwed pipes respectively
Assembly is closed, and so that four groups of threaded rods is carried out precession and back-out inside four groups of screwed pipes respectively, so as to pass through four groups of spiral shells
Rasp bar pushes four groups of pressing plates that the decrement of four groups of damping springs is adjusted respectively respectively, so as to facilitate according to practical existing
Field environment, is adjusted the damping effect of four groups of damping springs, carries out damping to Heat-transfer Oil Pump so as to realize, reduction is led
The noise caused by overall operation in the hot oil pump course of work reduces and uses limitation.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes four groups of holddown springs 28 and support
Plate 40, the top of four groups of holddown springs 28 connect with the front left side of 15 bottom end of upper mounting plate, left rear side, forward right side and right lateral side respectively
Connect, four groups of holddown springs 28 are respectively positioned on the inside of four groups of screw rods 17, and the bottom end of four groups of holddown springs 28 respectively with support plate
Front left side, left rear side, the forward right side on 40 tops are connected with right lateral side, and the bottom end of support plate 40 and the top of platform sling 16 are adjacent to；It can
Hold out against support plate to the top of screen pipe with the elastic force by four groups of holddown springs, so as to so that support plate cooperation four
Group nut carries out stretching to platform sling and fixes, and the shaking between platform sling and four groups of screw rods is reduced, so as to improve the steady of screen pipe
It is qualitative, improve use reliability.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes left snap-gauge 29, right snap-gauge, two groups
Left wing bolt 30 and two groups of right wing bolts, the front left side and left rear side on pedestal top are provided with left installation jack, and
The forward right side and right lateral side on pedestal top are provided with right installation jack, and the forward right side and right lateral side of left 29 bottom end of snap-gauge are respectively provided with
There is left plug, and the front left side of right snap-gauge bottom end and left rear side are provided with right plug, the front left side on 20 top of lower installation board
Left-hand thread hole is provided with left rear side, the forward right side and right lateral side on 20 top of lower installation board are provided with right-hand thread hole, and two groups
The bottom end of left wing bolt 30 is each passed through front left side inside left snap-gauge 29 and left rear side and the bottom end for extending out to left snap-gauge 29
The external world, and the bottom end of two groups of left wing bolts 30 is inserted into respectively and spiral shell is filled to inside two groups of left-hand thread holes, and two groups of left sides are inserted
The bottom end of head is inserted into respectively inside two groups of left installation jacks, and the bottom end of left snap-gauge 29 and the top left hand of pedestal are adjacent to, and two groups
The bottom end of right wing bolt be each passed through forward right side inside right snap-gauge and right lateral side and extend out to right snap-gauge bottom end it is extraneous, and
And the bottom end of two groups of right wing bolts is inserted into respectively and spiral shell is filled to inside two groups of right-hand thread holes, and the bottom end of two groups of right plugs point
It is not inserted into inside two groups of right installation jacks, is adjacent on the right side of the bottom end of right snap-gauge and the top of pedestal；It can be by separately down
Rotate two groups of left wing bolts and two groups of right wing bolts, make left snap-gauge and right snap-gauge by Heat-transfer Oil Pump pedestal and lower installation
Plate is clamped so far, and can be passed through simultaneously by the cooperation between two groups of left installation jacks respectively of two groups of left plugs
The cooperation between two groups of right installation jacks respectively of two groups of right plugs, prevents that laterally opposed shifting occurs between pedestal and lower installation board
It is dynamic, so as to improve the mounting stability of Heat-transfer Oil Pump, while two groups of left wing bolts and two groups of left-hand thread holes can be passed through
Between spiral shell assemble and close, while by two groups of right wing bolts distinguishing the spiral shell between two groups of right-hand thread holes and assemble and closing, facilitate thermally conductive
Oil pump is dismantled, and practicability is improved.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes two groups of left support springs 31 and two
Group right support spring, the outside for being respectively sleeved at two groups of left wing bolts 30 of two groups of left support springs 31, and two groups of left branch
The bottom end of support spring 31 is connect with the front left side on 20 top of lower installation board and left rear side respectively, the top of two groups of left support springs 31
It is connect respectively with the front left side of left 29 bottom end of snap-gauge and left rear side, two groups of right support springs are respectively sleeved at two groups of right butterfly spiral shells
The outside of bolt, and the bottom end of two groups of right support springs is connect with the forward right side on 20 top of lower installation board and right lateral side respectively, two
The top of group right support spring is connect with the forward right side of right snap-gauge bottom end and right lateral side respectively；Heat-transfer Oil Pump dismantled
Cheng Zhong, when two groups of left wing bolts of rotation and when two groups of right wing bolts upwards respectively, can by two groups of left support springs and
The elastic force of two groups of right support springs is respectively supported left snap-gauge and right snap-gauge, make left snap-gauge and right snap-gauge respectively by
On thrust, facilitate left snap-gauge and right snap-gauge to be lifted up, to facilitate two groups of left plugs and two groups of right plugs respectively from two groups
It is extracted upwards inside group installation jack and two groups of right installation jacks, saves manpower, improve practicability.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes mounting disc 32, the first spiral shell of multiple groups
Bolt 33, stop collar 34, round door 35 and the second bolt of multiple groups 36, mounting disc 32 are fixedly set in the external right side of filter core 13,
And the left end of mounting disc 32 and the right end of mounting ring 14 are adjacent to, and circumference is provided with the installation spiral shell of multiple groups first in mounting disc 32
Bolt throughhole, the right end circumference of mounting ring 14 are provided with multiple groups first and install threaded hole, and the left end of the first bolt of multiple groups 33 is worn respectively
Cross multiple groups first install bolt hole be inserted into respectively and spiral shell be filled to multiple groups first installation threaded hole inside, the right end of screen pipe 12 is set
It is equipped with operation port, and is communicated inside operation port and filter chamber, stop collar 34 is fixedly set in the external right side of screen pipe 12, and
And the right end circumference of stop collar 34 is provided with multiple groups second and installs threaded hole, circumference is provided with the peace of multiple groups second on round door 35
Bolt hole is filled, the left end of the second bolt of multiple groups 36 is each passed through inside the installation bolt hole of multiple groups second insertion and spiral shell dress respectively
It is installed inside threaded hole to multiple groups second；The spiral shell that can be installed between threaded hole with two group first respectively by the first bolt of multiple groups
Assembly is closed, and filter core is made to be easy for installation and removal, while can install threaded hole with multiple groups second respectively by the second bolt of multiple groups
Between spiral shell assemble close, facilitate round door to be mounted and dismounted, so as to so that filter core can be installed from operation port
And disassembly, convenient cleaning and replacement to filter core improve practicability.
A kind of temperature control equipment for diborane reaction kettle of the invention, further includes collet 37, and collet 37 is set in
The outside of heating coil 3, and heat insulation foam has been filled in the gap between collet 37 and heating coil 3；Folder can be passed through
Set and heat insulation foam reduce the heat loss of heating coil, improve the use reliability of heating coil.
A kind of temperature control equipment for diborane reaction kettle of the invention, further includes oil level indicator 38, and oil level indicator 38 connects
It is logical to be mounted on the left of the front end of heat conduction fuel tank 6 on outer wall；Operator can be facilitated to observe heat conduction fuel tank in time by oil level indicator
Internal oil level situation reduces and uses limitation.
A kind of temperature control equipment for diborane reaction kettle of the invention further includes handle 39, the left end of handle 39
It is connect with the right end of round door 35；Can conveniently be taken round door by handle, improve practicability.
A kind of temperature control equipment for diborane reaction kettle of the invention at work first infuses conduction oil
Enter to heat conduction fuel tank, then open control valve, the conduction oil inside heat conduction fuel tank is passed through first from inside heat conduction fuel tank
Communicating pipe is delivered to inside heating tube, then connects electric heating block and external power supply, makes to be preheated inside heating tube, will lead
Hot oil is heated, while Heat-transfer Oil Pump and external power supply being connected, and opens Heat-transfer Oil Pump, by the conduction oil after heating from thermally conductive
Oil pump is delivered to inside heating coil by outlet tube, and the conduction oil after making heating is in heating coil internal circulation, to will lead
Heat transfer inside hot oil gives reaction kettle inside, uses for diborane gas preparation combination reaction, the conduction oil after heat transmitting
It is gone successively to inside heat conduction fuel tank by liquid back pipe, goes successively to heating tube and be internally heated, followed by Heat-transfer Oil Pump
Ring continually and steadily heats reaction kettle inside, is carried out by the filter core inside screen pipe to the conduction oil inside liquid back pipe
Filtering is delivered to inside left U-typed pipe by filter chamber after filtering and is fed back to inside heat conduction fuel tank by left liquid back pipe, Ke Yitong
The U-typed setting for crossing left U-typed pipe and right U-typed pipe, buffers the conduction oil inside liquid back pipe, so as to subtract
Impact of the conduction oil to filter core inside few liquid back pipe, while the speed of conduction oil can be reduced, allow filter core by conduction oil
Internal impurity is sufficiently filtered, and can be closed by spiral shell assembly of four groups of nuts respectively between four groups of screw rods, be made screen pipe
It carries out hanging assembly and disassembly, so as to which to conduction oil, the internal more impurity being mixed with is gone in time during recycling
It removes, while the impurity inside conduction oil being prevented to be easy and outlet tube, heating coil and liquid back pipe in thermally conductive oil circulation process
Equal pipeline inner walls collision generates abnormal sound, and can be mitigated respectively by resilient cushion on four groups on four groups intubation and lower installation board it
Between vibration, the vibration between four groups of setting of casings and working chamber inner bottom wall is mitigated by resilient cushion under four groups respectively, can be passed through
It is intubated on four groups respectively with being slidably matched inside setting of casing, makes to carry out up and down inside intubation and four groups of setting of casings on four groups
Movement, while can be propped up respectively between intubation under intubation on four groups and four groups by the retractility of four groups of damping springs
Support, so as to so that four groups of damping springs up and down action to Heat-transfer Oil Pump carry out damping, can be by rotating four groups of spiral shells respectively
Line pipe rotates four groups of screwed pipes inside four groups of ball bearings respectively, so as to by four groups of threaded rods respectively with
Spiral shell between four groups of screwed pipes, which assembles, to be closed, and four groups of threaded rods is allow to carry out precession and back-out inside four groups of screwed pipes respectively,
So as to push four groups of pressing plates that the decrement of four groups of damping springs is adjusted respectively respectively by four groups of threaded rods, thus
It can make that the damping effect of four groups of damping springs is adjusted according to actual field environment, so as to realize to conduction oil
Pump carries out damping, reduces the noise caused by overall operation in the Heat-transfer Oil Pump course of work, passes through the elastic force of four groups of holddown springs
Hold out against support plate to the top of screen pipe, so as to so that support plate cooperates four groups of nuts solid to platform sling progress stretching
It is fixed, the shaking between platform sling and four groups of screw rods is reduced, by rotating two groups of left wing bolts and two groups of right butterfly spiral shells separately down
Bolt is clamped left snap-gauge and right snap-gauge so far the pedestal in Heat-transfer Oil Pump with lower installation board, and can pass through two groups
Left plug respectively two groups it is left installation jacks between cooperations, while by two groups of right plugs respectively with two groups of right installation jacks it
Between cooperation, prevent that laterally opposed movement occurs between pedestal and lower installation board, it is steady so as to the installation that improves Heat-transfer Oil Pump
It is qualitative, while can be assembled and be closed by the spiral shell between two groups of left wing bolts and two groups of left-hand thread holes, while pass through two groups of right butterflies
Shape bolt distinguishes the spiral shell between two groups of right-hand thread holes and assembles conjunction, carries out in disassembly process to Heat-transfer Oil Pump, when rotation upwards respectively
When turning two groups of left wing bolts and two groups of right wing bolts, the bullet of two groups of left support springs and two groups of right support springs can be passed through
Power is respectively supported left snap-gauge and right snap-gauge, makes left snap-gauge and right snap-gauge respectively by upward thrust, make left snap-gauge and
Right snap-gauge is lifted up, so that two groups of left plugs and two groups of right plugs be made to insert respectively from two groups of group installation jacks and two groups of right installations
It is extracted upwards inside hole, is assembled and closed by the spiral shell that the first bolt of multiple groups is installed between threaded hole with two group first respectively, make filter core
Make to mount and dismount, while the spiral shell between threaded hole can be installed with multiple groups second respectively by the second bolt of multiple groups and assemble conjunction,
Mount and dismount round door, so as to make to filter core so that filter core can be mounted and dismounted from operation port
Cleaning and replacement are reduced the heat loss of heating coil by collet and heat insulation foam, see operator in time by oil level indicator
The oil level situation inside heat conduction fuel tank is examined, round door of taking is made by handle.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, several improvements and modifications, these improvements and modifications can also be made
Also it should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of temperature control equipment for diborane reaction kettle, including bottom plate (1), reaction kettle (2), heating coil (3), cabinet
Body (4), Heat-transfer Oil Pump (5), heat conduction fuel tank (6), heating tube (7), partition (8), liquid back pipe (9) and outlet tube (10), reaction kettle
(2) front left side, left rear side, forward right side and right lateral side of bottom end are provided with supporting leg, and the bottom end of four groups of supporting legs respectively with bottom
Front left side, left rear side, the forward right side of plate (1) top right area are connected with right lateral side, and the bottom end and bottom plate (1) of cabinet body (4) are pushed up
The left side at end connects, and cabinet body (4) is internally provided with working chamber, and the front end of cabinet body (4) is provided with operation port, operation port with
Communicated inside working chamber, the inner roof wall of the top of heat conduction fuel tank (6) and working chamber connects, and the bottom end of Heat-transfer Oil Pump (5) with
The inner bottom wall of working chamber connects, and the left end of heating tube (7) is provided with mounting base, has been uniformly arranged on the outer wall of heating tube (7) more
Group electric heating block, partition (8) are longitudinally mounted to the inside left of working chamber, and the right end of the left end of mounting base and partition (8)
Middle part connection, heat conduction fuel tank (6) is internally provided with conduction oil, and passes through for the first communicating pipe on the right side of the bottom end of heat conduction fuel tank (6)
It is connected to the input terminal on the right side of heating tube (7) top, control valve is provided on the first communicating pipe, and heating tube (7) bottom end is left
The output end of side with the input terminal of Heat-transfer Oil Pump (5) by being connected to the second communicating pipe, the input terminal and conduction oil of outlet tube (10)
The output end connection of (5) is pumped, and the surrounding outer wall in reaction kettle (2), and outlet tube (10) is arranged in heating coil (3) coiling
Right part output end the right end inner wall of working chamber is passed through inside the working chamber and extend out to cabinet body (4) right end is extraneous and heating dish
The input terminal connection on the downside of (3) left part is managed, the input terminal of liquid back pipe (9) is connected to the output end on the upside of heating coil (3) left part,
And the output end of liquid back pipe (9) passes through the right end outer wall upside and heat conduction fuel tank (6) of cabinet body (4) from the right side of cabinet body (4)
Right end connection；It is characterised in that it includes left U-typed pipe (11), right U-typed pipe, screen pipe (12), filter core (13), mounting ring
(14), upper mounting plate (15), platform sling (16), four groups of screw rods (17) and four groups of nuts (18), the liquid back pipe (9) are set as left and return
Liquid pipe (9) and right liquid back pipe (9), and the left part output end of the left liquid back pipe (9) and the right end of the heat conduction fuel tank (6) connect
It is logical, and the right part input terminal of the right liquid back pipe (9) is connected to the output end of the heating coil (3) left upper portion, it is described
Left U-typed pipe (11) and right U-typed pipe are arranged between the left liquid back pipe (9) and right liquid back pipe (9), left U-typed pipe
(11) left end is connected to the right part input terminal of left liquid back pipe (9), and the right end of the right U-typed pipe and the right liquid back pipe
(9) left part output end connection, the top of the upper mounting plate (15) are connect with the right side of the working chamber inner roof wall, and described four
The top of group screw rod (17) is connect with the front left side, left rear side, forward right side and right lateral side of the upper mounting plate (15) bottom end respectively,
The front left side, left rear side, forward right side and right lateral side of platform sling (16) bottom end are provided with connecting rod, and four groups of connecting rods
Bottom end is connect with front left side, left rear side, forward right side and the right lateral side on the screen pipe (12) top respectively, platform sling (16) top
Front left side, left rear side, forward right side and the right lateral side at end are provided with perforative installation through-hole, and four groups of screw rods up and down
(17) bottom end is each passed through inside four groups of installation through-holes from the top of platform sling (16) and extend out to the bottom end of platform sling (16), institute
Stating four groups of nuts (18), spiral shell encapsulation is located at the outsides of four groups of screw rods (17) respectively, and the top of four groups of nuts (18) with
The bottom end of the platform sling (16) is adjacent to, and the screen pipe (12) is internally provided with filter chamber, and screen pipe (12) bottom end
Left and right side is respectively arranged with export and import, the right end and outlet of the left U-typed pipe (11), and the right side
The left end of U-typed pipe and inlet communication, the mounting ring (14) are longitudinally mounted to inside the right side of the filter chamber, and described
The circumferential inner wall of mounting ring (14) is fixedly connected with the circumferential inner wall of the filter chamber, the left end self installation ring of the filter core (13)
(14) right end passes through mounting ring (14) inner wall and extend out to the left end external world of mounting ring (14), the right part output end of filter core (13)
It is communicated with inside the filter chamber；It further include four groups of support columns (19), lower installation board (20), resilient cushion (21), four groups on four groups
Lower resilient cushion is intubated (22), four groups of setting of casings (23), four groups of damping springs (24), four groups of screwed pipes (25), four groups of pressures on four groups
Plate (26) and four groups of threaded rods (27), the bottom end of the Heat-transfer Oil Pump (5) are provided with pedestal, and four groups of support columns (19)
Top is connect with the front left side, left rear side, forward right side and right lateral side of the lower installation board (20) bottom end respectively, the pedestal setting
On the lower top installed and pressed, the bottom end of four groups of support columns (19) is left front with the working chamber inner bottom wall right area respectively
Side, left rear side, forward right side are connected with right lateral side, on described four groups the top of resilient cushion (21) respectively with the lower installation board (20)
Front left side, left rear side, the forward right side of bottom end are connected with right lateral side, and under described four groups resilient cushion bottom end respectively with the work
Front left side, left rear side, the forward right side for making intracavitary bottom wall right area are connected with right lateral side, resilient cushion (21) and four on described four groups
The lower resilient cushion of group is respectively positioned on the inside of four groups of support columns (19), be intubated on described four groups the top of (22) respectively with described four groups
The bottom end of upper resilient cushion (21) connects, and the bottom end of four groups of setting of casings (23) respectively with described four groups under the top of resilient cushion connect
It connecing, the bottom end that (22) are intubated on described four groups is can be slidably inserted into respectively inside the top to four groups of setting of casings (23), and described four groups
The bottom end of damping spring (24) is connect with the bottom end inner wall of four groups of setting of casings (23) respectively, and is intubated on described four groups
(22) it is provided with regulating tank on top inner wall, ball bearing, four groups of spiral shells are provided with inside four groups of regulating tanks
The top of line pipe (25) is inserted and fixed respectively inside installation to four groups of ball bearings, the top point of four groups of threaded rods (27)
Not Cha Ru and spiral shell be filled to the bottom inner portions of four groups of screwed pipes (25), the top of four groups of pressing plates (26) respectively with four groups of spiral shells
The bottom end of rasp bar (27) connects, and the bottom end of four groups of pressing plates (26) top with four groups of damping springs (24) respectively
Connection.
2. a kind of temperature control equipment for diborane reaction kettle as described in claim 1, which is characterized in that further include four
Group holddown spring (28) and support plate (40), the top of four groups of holddown springs (28) respectively with the upper mounting plate (15) bottom
Front left side, left rear side, the forward right side at end are connected with right lateral side, and four groups of holddown springs (28) are respectively positioned on four groups of screw rods (17)
Inside, and the bottom end of four groups of holddown springs (28) front left side, left rear side, the forward right side with the support plate (40) top respectively
It is connected with right lateral side, the bottom end of support plate (40) and the top of the platform sling (16) are adjacent to.
3. a kind of temperature control equipment for diborane reaction kettle as claimed in claim 2, which is characterized in that further include a left side
Snap-gauge (29), right snap-gauge, two groups of left wing bolts (30) and two groups of right wing bolts, the front left side on the pedestal top and left back
Side is provided with left installation jack, and the forward right side on the pedestal top and right lateral side are provided with right installation jack, described
The forward right side and right lateral side of left snap-gauge (29) bottom end are provided with left plug, and the front left side of the right snap-gauge bottom end and left back
Side is provided with right plug, and the front left side and left rear side on lower installation board (20) top are provided with left-hand thread hole, under described
The forward right side and right lateral side on mounting plate (20) top are provided with right-hand thread hole, the bottom end point of two groups of left wing bolts (30)
Not Chuan Guo the internal front left side of left snap-gauge (29) and left rear side and extend out to left snap-gauge (29) bottom end it is extraneous, and two groups of left butterflies
The bottom end of shape bolt (30) is inserted into respectively and spiral shell is filled to inside two groups of left-hand thread holes, and the bottom end difference of two groups of left plugs
It is inserted into inside two groups of left installation jacks, the bottom end of left snap-gauge (29) and the top left hand of the pedestal are adjacent to, and described two groups right
The bottom end of wing bolt be each passed through forward right side inside right snap-gauge and right lateral side and extend out to right snap-gauge bottom end it is extraneous, and
The bottom end of two groups of right wing bolts is inserted into respectively and spiral shell is filled to inside two groups of right-hand thread holes, and the bottom end of two groups of right plugs
It is inserted into inside two groups of right installation jacks, is adjacent on the right side of the bottom end of right snap-gauge and the top of the pedestal respectively.
4. a kind of temperature control equipment for diborane reaction kettle as claimed in claim 3, which is characterized in that further include two
Group left support spring (31) and two groups of right support springs, two groups of left support springs (31) are respectively sleeved at two groups of left sides
The outside of wing bolt (30), and the bottom end of two groups of left support springs (31) left side with the lower installation board (20) top respectively
Front side is connected with left rear side, the top of two groups of left support springs (31) respectively with the front left side of left snap-gauge (29) bottom end and a left side
Rear side connection, the outside for being respectively sleeved at two groups of right wing bolts of two groups of right support springs, and two groups of right branch
The bottom end of support spring is connect with the forward right side on the lower installation board (20) top and right lateral side respectively, the top of two groups of right support springs
End is connect with the forward right side of the right snap-gauge bottom end and right lateral side respectively.
5. a kind of temperature control equipment for diborane reaction kettle as claimed in claim 4, which is characterized in that further include peace
Sabot (32), the first bolt of multiple groups (33), stop collar (34), round door (35) and the second bolt of multiple groups (36), the installation
Disk (32) is fixedly set in the external right side of the filter core (13), and the left end of mounting disc (32) and the mounting ring (14)
Right end is adjacent to, and circumference is provided with the installation bolt hole of multiple groups first, the right end circumference of mounting ring (14) in mounting disc (32)
It is provided with multiple groups first and threaded hole is installed, it is logical that the left end of first bolt of multiple groups (33) is each passed through the installation bolt of multiple groups first
Hole is inserted into respectively and spiral shell is filled to multiple groups first and installs inside threaded hole, and the right end of the screen pipe (12) is provided with operation port, and
And communicated inside operation port and the filter chamber, the stop collar (34) is fixedly set in the external right of the screen pipe (12)
Side, and the right end circumference of stop collar (34) is provided with multiple groups second and installs threaded hole, and circumference is set on the circle door (35)
It is equipped with multiple groups second and bolt hole is installed, it is logical that the left end of second bolt of multiple groups (36) is each passed through the installation bolt of multiple groups second
Insertion and spiral shell are filled to inside the installation threaded hole of multiple groups second respectively inside hole.
6. a kind of temperature control equipment for diborane reaction kettle as claimed in claim 5, which is characterized in that further include folder
It covers (37), the collet (37) is set in the outside of the heating coil (3), and between collet (37) and heating coil (3)
Gap in be filled with heat insulation foam.
7. a kind of temperature control equipment for diborane reaction kettle as claimed in claim 6, which is characterized in that further include oil
Position meter (38), oil level indicator (38) connection are mounted on the left of the front end of the heat conduction fuel tank (6) on outer wall.
8. a kind of temperature control equipment for diborane reaction kettle as claimed in claim 7, which is characterized in that further include handle
Hand (39), the left end of the handle (39) are connect with the right end of the round door (35).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811144110.XA CN109225092A (en) | 2018-09-27 | 2018-09-27 | A kind of temperature control equipment for diborane reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811144110.XA CN109225092A (en) | 2018-09-27 | 2018-09-27 | A kind of temperature control equipment for diborane reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109225092A true CN109225092A (en) | 2019-01-18 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811144110.XA Pending CN109225092A (en) | 2018-09-27 | 2018-09-27 | A kind of temperature control equipment for diborane reaction kettle |
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| Country | Link |
|---|---|
| CN (1) | CN109225092A (en) |
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Application publication date: 20190118 |