CN109208329A - A kind of cotton gauze with good absorbency - Google Patents
A kind of cotton gauze with good absorbency Download PDFInfo
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- CN109208329A CN109208329A CN201811067120.8A CN201811067120A CN109208329A CN 109208329 A CN109208329 A CN 109208329A CN 201811067120 A CN201811067120 A CN 201811067120A CN 109208329 A CN109208329 A CN 109208329A
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- cotton gauze
- good absorbency
- cotton
- gauze
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Abstract
The invention discloses a kind of cotton gauzes with good absorbency, be related to textile material technical field, will treated that cotton yarn is arranged in closed reactor by cation-modified, addition processing medium, then processing pressure is boosted to, 10-12min is handled, is subsequently released stress again with constant rate of speed, then insulated and stirred 40-45min under the conditions of being not higher than 43 DEG C of temperature again, then it is filtered, it is cleaned using deionized water to neutrality, drying to constant weight;The present invention provides a kind of cotton gauzes with good absorbency, and the present invention can not only improve the absorbent of cotton gauze by the processing to cotton gauze, while can also improve the mechanical property of cotton gauze to a certain extent.
Description
Technical field
The invention belongs to textile material technical fields, and in particular to a kind of cotton gauze with good absorbency.
Background technique
Gauze is a kind of cotton goods that longitude and latitude is sparse.Belong to textile raw material, dry goods, feature be it is sparse, have apparent grid.
Gauze is widely used, and can be applied to medicinal dressing, stype, mask, mosquito net, bamboo curtain splint summer sleeping mat etc. multiple fields,
With the development of economy and the acceleration of aging of population process, China are increasing to the demand of medical material.Medical dressing
It is the important component of medical material.In medical dressing, traditional medical absorbent cotton gauze relies on its cheap, source
Extensively, the advantages that the processing is simple is widely applied.However, medical absorbent cotton gauze used at present is because of its absorbent
It is limited, the sepage of the surface of a wound cannot be effectively absorbed, causes wound healing slower;In addition, medical absorbent cotton gauze is in use
It needs to frequently replace, which increase the workloads of medical worker.It is main at present for the absorbent for improving medical absorbent cotton gauze
Using chemical modification methods such as grafting, etherificate, oxidations.In Graft Method, reaction is difficult to effectively control, and side reaction is more, preparation
Higher cost.Using etherification method handle medical absorbent cotton gauze when, the byproducts of reaction such as salinity are more, cause preparation cost compared with
It is high;In addition, medical absorbent cotton gauze absorbs liquid by the hydrogen bond action between hydroxyl and hydrone, the physics to liquid is only played
Suction-operated.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of cotton gauze with good absorbency is provided.
The present invention is achieved by the following technical solutions:
A kind of cotton gauze with good absorbency, will treated that cotton yarn is arranged in closed reactor by cation-modified
Interior, then addition processing medium is boosted to processing pressure, handles 10-12min, subsequently released stress again with constant rate of speed, so
Insulated and stirred 40-45min under the conditions of being not higher than 43 DEG C of temperature again afterwards, is then filtered, using deionized water clean to
Neutrality, drying to constant weight.
Further, it is described by cation-modified treated cotton gauze the preparation method comprises the following steps: by cotton gauze and 2,3- ring
Oxygen propyl group trimethyl ammonia chloride ammonium salt solution impregnates 40min, is then filtered again in the case where temperature is 45 DEG C, then uses quality again
Score is 80% alcohol solution dipping 10min, then is filtered, and drying to constant weight.
Further, the cotton gauze and 2,3- epoxypropyltrimethylchloride chloride solution mixing mass ratio is 1:8, described
2,3- epoxypropyltrimethylchloride chloride solution concentration is 0.28mol/L.
Further, its tissue of the cotton gauze is plain weave, and filling yarn density is 26.3tex, and weft density is respectively
105,104/(10 cm).
Further, the processing medium is made of following component by weight: alkyl trimethyl ammonium salt 1.5-1.9,
SODIUM PERCARBONATE 3.6-3.8, dimethyl ring body siloxanes 0.02-0.04, sodium metasilicate 2.4-2.6, deionized water 50-55.
Further, the processing pressure is 0.55-0.57MPa.
Further, the constant rate of speed releases stress to discharge processing pressure to normal pressure with 0.1MPa/s constant rate.
Further, the temperature condition for being not higher than 43 DEG C is specially 41-43 DEG C.
Further, the speed of agitator is 250r/min.
The utility model has the advantages that the present invention provides a kind of cotton gauze with good absorbency, the present invention passes through to cotton gauze
Processing, can not only improve the absorbent of cotton gauze, while can also improve the mechanical property of cotton gauze to a certain extent, lead to
It crosses and cation-modified processing is carried out to cotton gauze, can effectively enhance the mechanical property of cotton gauze, while can effectively exist
A certain amount of active group of cotton gauze surface grafting handles in medium that finite element can be into when by handling media processes
One step is modified processing to cotton gauze surface fiber, so that hydroxyl more on cotton yarn measuring fiber is oxidized to carboxyl, because
The absorbent of this cotton gauze is improved, while the capillary fiber structure in cotton gauze obtains firm effect, capillary wicking effect
It should enhance, by handling shape between medium energy and cotton gauze cellulose in the case where certain pressure is handled and under the processing of subsequent release
At a large amount of hydrogen bond, the hydrogen bond network between cellulosic molecule is reconstructed, so as to effectively improve the mechanical property of cotton gauze, place
During a certain amount of dimethyl ring body siloxanes is handled herein in reason medium, using silicon oxygen (Si-O) key as the macromolecular knot of main chain
Structure, directly grafting are connected to cotton gauze fiber surface, to further improve the mechanical property of cotton gauze.
Specific embodiment
Embodiment 1
A kind of cotton gauze with good absorbency, will treated that cotton yarn is arranged in closed reactor by cation-modified
Interior, then addition processing medium is boosted to processing pressure, handles 10min, subsequently released stress again with constant rate of speed, then
Insulated and stirred 40min under the conditions of being not higher than 43 DEG C of temperature again, is then filtered, is cleaned using deionized water to neutrality,
Drying to constant weight.
Further, it is described by cation-modified treated cotton gauze the preparation method comprises the following steps: by cotton gauze and 2,3- ring
Oxygen propyl group trimethyl ammonia chloride ammonium salt solution impregnates 40min, is then filtered again in the case where temperature is 45 DEG C, then uses quality again
Score is 80% alcohol solution dipping 10min, then is filtered, and drying to constant weight.
Further, the cotton gauze and 2,3- epoxypropyltrimethylchloride chloride solution mixing mass ratio is 1:8, described
2,3- epoxypropyltrimethylchloride chloride solution concentration is 0.28mol/L.
Further, its tissue of the cotton gauze is plain weave, and filling yarn density is 26.3tex, and weft density is respectively
105,104/(10 cm).
Further, the processing medium is made of following component by weight: alkyl trimethyl ammonium salt 1.5 crosses carbon
Sour sodium 3.6, dimethyl ring body siloxanes 0.02, sodium metasilicate 2.4, deionized water 50.
Further, the processing pressure is 0.55MPa.
Further, the constant rate of speed releases stress to discharge processing pressure to normal pressure with 0.1MPa/s constant rate.
Further, the temperature condition for being not higher than 43 DEG C is specially 41 DEG C.
Further, the speed of agitator is 250r/min.
Embodiment 2
A kind of cotton gauze with good absorbency, will treated that cotton yarn is arranged in closed reactor by cation-modified
Interior, then addition processing medium is boosted to processing pressure, handles 12min, subsequently released stress again with constant rate of speed, then
Insulated and stirred 45min under the conditions of being not higher than 43 DEG C of temperature again, is then filtered, is cleaned using deionized water to neutrality,
Drying to constant weight.
Further, it is described by cation-modified treated cotton gauze the preparation method comprises the following steps: by cotton gauze and 2,3- ring
Oxygen propyl group trimethyl ammonia chloride ammonium salt solution impregnates 40min, is then filtered again in the case where temperature is 45 DEG C, then uses quality again
Score is 80% alcohol solution dipping 10min, then is filtered, and drying to constant weight.
Further, the cotton gauze and 2,3- epoxypropyltrimethylchloride chloride solution mixing mass ratio is 1:8, described
2,3- epoxypropyltrimethylchloride chloride solution concentration is 0.28mol/L.
Further, its tissue of the cotton gauze is plain weave, and filling yarn density is 26.3tex, and weft density is respectively
105,104/(10 cm).
Further, the processing medium is made of following component by weight: alkyl trimethyl ammonium salt 1.9 crosses carbon
Sour sodium 3.8, dimethyl ring body siloxanes 0.04, sodium metasilicate 2.6, deionized water 55.
Further, the processing pressure is 0.57MPa.
Further, the constant rate of speed releases stress to discharge processing pressure to normal pressure with 0.1MPa/s constant rate.
Further, the temperature condition for being not higher than 43 DEG C is specially 43 DEG C.
Further, the speed of agitator is 250r/min.
Embodiment 3
A kind of cotton gauze with good absorbency, will treated that cotton yarn is arranged in closed reactor by cation-modified
Interior, then addition processing medium is boosted to processing pressure, handles 11min, subsequently released stress again with constant rate of speed, then
Insulated and stirred 42min under the conditions of being not higher than 43 DEG C of temperature again, is then filtered, is cleaned using deionized water to neutrality,
Drying to constant weight.
Further, it is described by cation-modified treated cotton gauze the preparation method comprises the following steps: by cotton gauze and 2,3- ring
Oxygen propyl group trimethyl ammonia chloride ammonium salt solution impregnates 40min, is then filtered again in the case where temperature is 45 DEG C, then uses quality again
Score is 80% alcohol solution dipping 10min, then is filtered, and drying to constant weight.
Further, the cotton gauze and 2,3- epoxypropyltrimethylchloride chloride solution mixing mass ratio is 1:8, described
2,3- epoxypropyltrimethylchloride chloride solution concentration is 0.28mol/L.
Further, its tissue of the cotton gauze is plain weave, and filling yarn density is 26.3tex, and weft density is respectively
105,104/(10 cm).
Further, the processing medium is made of following component by weight: alkyl trimethyl ammonium salt 1.6 crosses carbon
Sour sodium 3.7, dimethyl ring body siloxanes 0.03, sodium metasilicate 2.5, deionized water 52.
Further, the processing pressure is 0.56MPa.
Further, the constant rate of speed releases stress to discharge processing pressure to normal pressure with 0.1MPa/s constant rate.
Further, the temperature condition for being not higher than 43 DEG C is specially 42 DEG C.
Further, the speed of agitator is 250r/min.
Comparative example 1: SODIUM PERCARBONATE will not be added in processing medium by being only that with the difference of embodiment 1.
Comparative example 2: dimethyl ring body siloxanes will not be added in processing medium by being only that with the difference of embodiment 1.
Comparative example 3: it is only that cotton gauze with the difference of embodiment 1 without cation-modified processing.
Control group: untreated flax fiber.
Absorbent test
Referring to the hygroscopic method of surface of a wound dressing is commonly tested in the world, absorbent survey is carried out using moisture absorption weighing method
Concrete operation step: examination firstly, cutting out the embodiment and comparative example cotton gauze sample of 5cm × 5cm, accurately weighs up its drying
Quality;Then, sample is put into imbibition in 100mL deionized water, is taken out after 30min, it is natural, flatly after vertical hanging 30s
Its quality is weighed up at once.Calculate the imbibition rate of sample:
Q=(W1-W0)/W 0
In formula:
The imbibition rate of Q --- sample, g/g;
W0 --- samples dried quality, g;
W1 --- the quality after sample imbibition, g.;
Table 1
The absorbent of cotton gauze prepared by the present invention is greatly improved as can be seen from Table 1.
Mechanics Performance Testing
Referring to professional standard YY 0331-2006 " degreasing cotton gauze, the performance requirement of the blended gauze of absorbent cotton viscose and test
Method ", Mechanics Performance Testing is carried out using electronic fabric strength tester, sample warp, broadwise are tested respectively, 50 mm of specimen width,
200 mm of clamp distance, 100 mm/min of tensile speed;
Table 2
As can be seen from Table 2, the present invention treated cotton gauze has good mechanical property.
Claims (9)
1. a kind of cotton gauze with good absorbency, which is characterized in that will be by cation-modified treated cotton yarn arrangement
In in closed reactor, then addition processing medium boosts to processing pressure, 10-12min is handled, subsequently again with constant speed
Rate releases stress, then insulated and stirred 40-45min under the conditions of being not higher than 43 DEG C of temperature again, is then filtered, using going
Ionized water is cleaned to neutrality, and drying to constant weight.
2. a kind of cotton gauze with good absorbency as described in claim 1, which is characterized in that described to change by cation
Property treated cotton gauze the preparation method comprises the following steps: in temperature being 45 DEG C by cotton gauze and 2,3- epoxypropyltrimethylchloride chloride solution
Under, 40min is impregnated, is then filtered again, then uses mass fraction for 80% alcohol solution dipping 10min again, then carries out
Filtering, drying to constant weight.
3. a kind of cotton gauze with good absorbency as claimed in claim 2, which is characterized in that the cotton gauze and 2,3-
Epoxypropyltrimethylchloride chloride solution mixing mass ratio is 1:8,2, the 3- epoxypropyltrimethylchloride chloride solution concentration
For 0.28mol/L.
4. a kind of cotton gauze with good absorbency as claimed in claim 1 or 2, which is characterized in that the cotton gauze its
Tissue is plain weave, and filling yarn density is 26.3tex, weft density is respectively 105,104/(10 cm).
5. a kind of cotton gauze with good absorbency as described in claim 1, which is characterized in that the processing medium is by weight
Amount part meter is made of following component: alkyl trimethyl ammonium salt 1.5-1.9, SODIUM PERCARBONATE 3.6-3.8, dimethyl ring body siloxanes
0.02-0.04, sodium metasilicate 2.4-2.6, deionized water 50-55.
6. a kind of cotton gauze with good absorbency as described in claim 1, which is characterized in that the processing pressure is
0.55-0.57MPa。
7. a kind of cotton gauze with good absorbency as described in claim 1, which is characterized in that the constant rate of speed release
Pressure is that processing pressure is discharged with 0.1MPa/s constant rate to normal pressure.
8. a kind of cotton gauze with good absorbency as described in claim 1, which is characterized in that described to be not higher than 43 DEG C
Temperature condition is specially 41-43 DEG C.
9. a kind of cotton gauze with good absorbency as described in claim 1, which is characterized in that the speed of agitator is
250r/min。
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CN201811067120.8A CN109208329A (en) | 2018-09-13 | 2018-09-13 | A kind of cotton gauze with good absorbency |
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CN201811067120.8A CN109208329A (en) | 2018-09-13 | 2018-09-13 | A kind of cotton gauze with good absorbency |
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CN107412843A (en) * | 2016-05-23 | 2017-12-01 | 华东理工大学 | A kind of starch base micropore hemostatic material with anti-microbial property and its preparation method and application |
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2018
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