CN109202199A - A kind of method of titanium welding pipe production titanium vacuum cup - Google Patents
A kind of method of titanium welding pipe production titanium vacuum cup Download PDFInfo
- Publication number
- CN109202199A CN109202199A CN201811343228.5A CN201811343228A CN109202199A CN 109202199 A CN109202199 A CN 109202199A CN 201811343228 A CN201811343228 A CN 201811343228A CN 109202199 A CN109202199 A CN 109202199A
- Authority
- CN
- China
- Prior art keywords
- titanium
- vacuum cup
- welding pipe
- shell
- inner casing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K1/00—Soldering, e.g. brazing, or unsoldering
- B23K1/008—Soldering within a furnace
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K1/00—Soldering, e.g. brazing, or unsoldering
- B23K1/0008—Soldering, e.g. brazing, or unsoldering specially adapted for particular articles or work
Abstract
The present invention provides a kind of methods of titanium welding pipe production titanium vacuum cup, make the shell of upper opening and the inner casing of upper opening respectively of titanium welding pipe, open up aspirating hole in outer casing bottom；Inner casing is placed in interior of shell, and shell and inner casing top are subjected to sealing welding of healing up；Extract the air in the interlayer that shell and inner casing are formed in vacuum drying oven out；Titanium vacuum cup first product is made in heat preservation after carrying out sealed with brazing sealing to aspirating hole with solder；To titanium vacuum cup first product polishing treatment, titanium vacuum cup finished product is formed.The titanium vacuum cup made by above method has many advantages, such as that light, at low cost, soaking time is long, yield rate improves.
Description
Technical field
The present invention relates to titanium insulation cup technology fields, and in particular to a kind of method of titanium welding pipe production titanium vacuum cup.
Background technique
For titanium as metal harmless to the human body, can now be implanted into human body safely becomes the advanced medical of human organ
Material, titanium can also become the material of production vacuum cup.Come across at present the titanium vacuum cup in all kinds of exhibitions be essentially titanium without
Slit-tube is made, but titanium seamless tubes yield is less, expensive, causes titanium vacuum cup production cost higher, it is difficult to produce in enormous quantities.
Moreover, typically, cup material is thinner, and soaking time is longer, titanium seamless tubes are thicker, protected using the titanium of titanium seamless tubes production
The heat insulation effect of warm cup is often bad.
Traditional technology maturation using stainless steel or titanium production vacuum cup, using one-to-two legal system cup, i.e., with one
The welded tube of kind specification produces vacuum cup inside and outside shell simultaneously.Vacuum cup shell using bulging method production (inside and outside shell gap is about
5.5mm), since stainless steel welded pipe plasticity is good (elongation percentage is up to 53%), the bulging requirement of glass shell can be met.But titanium welding pipe
The difference (elongation percentage is not less than 24%) of plasticity ratio stainless steel welded pipe, is difficult to realize the deformation requirements of cup shell or bulging often occurs
The case where spalling, causes yield rate low, is unable to stable mass production.
Meanwhile vacuum cup is in the production process, material used in general sealing aspirating hole is solid glass glue, this method
For metal and nonmetallic connection, metal and nonmetallic associativity is bad is easy to fall off causes vacuum cup gas leakage, to make to protect
The warm cup lost of life.
Such as, 103405104 A of Chinese invention patent CN authorized, a kind of vacuum cup and its manufacturing method of titanium,
Cup body is exactly made after bulging using the titanium tube of same specification, there is also the deformation requirements of cup shell difficult to realize or often
There is the case where bulging spalling, the problem of causing yield rate low, be unable to stable mass production.Meanwhile after evacuation, it uses
Solid glass glue is sealed sealing to through-hole (i.e. gas vent), and this method is metal and nonmetallic connection, metal and Fei Jin
The associativity of category is bad to be easy to fall off, and vacuum cup gas leakage is caused, to make the vacuum cup lost of life.
In view of this, it is necessary to titanium vacuum cup production method in the prior art be improved, to solve the above problems.
Summary of the invention
When it is an object of the invention to solve in the prior art using titanium seamless tubes production vacuum cup, titanium seamless tubes deformation is easy
Split, yield rate is low, is unable to the problem of stable mass production, provide a kind of side using titanium welding pipe production titanium vacuum cup
Method.
Realize that the technical solution of goal of the invention is as follows: a kind of method of titanium welding pipe production titanium vacuum cup, comprising the following steps:
Step 1: making the shell of upper opening, the inner casing of upper opening of titanium welding pipe respectively, opens up pumping in outer casing bottom
Hole；The caliber for making the titanium welding pipe of shell is greater than the caliber for making the titanium welding pipe of inner casing.
Step 2: being placed in interior of shell for inner casing, then will heal up after shell upper and the contraction distortion of inner casing top, will
It heals up sealing welding, and titanium body of vacuum cup is made in the roll threading at sealing.
Step 3: titanium body of vacuum cup is put into vacuum drying oven, then the air in the interlayer that shell and inner casing are formed from
It is extracted out in aspirating hole.
Step 4: in a vacuum furnace, sealed with brazing sealing is carried out to aspirating hole with solder, and keep the temperature in a vacuum furnace, made
The solder for sealing the thawing of aspirating hole solidifies completely is made titanium vacuum cup first product.
Step 5: to the titanium vacuum cup first product polishing treatment in step 4, titanium vacuum cup finished product is formed.
In the preferred embodiment of the method for titanium welding pipe production titanium vacuum cup of the invention, titanium welding pipe thickness of pipe wall is 0.3 ~
1.0mm。
In the preferred embodiment of the method for titanium welding pipe production titanium vacuum cup of the invention, shell is made in step 1
The caliber of titanium welding pipe is greater than 5.0 ~ 6.0mm of caliber of the titanium welding pipe of production inner casing.
In the preferred embodiment of the method for titanium welding pipe production titanium vacuum cup of the invention, in step 3, on shell
Portion's contraction distortion is 15.0% ~ 20.0%.
In the preferred embodiment of the method for titanium welding pipe production titanium vacuum cup of the invention, the solder in step 4 is
Hard metal solder or nonmetallic glass solder.Preferably, hard metal solder is yellow gold, and the fusing point of hard solder is generally greater than
450 DEG C, therefore according to the influence of the factors such as solder, weld interval, welding quality, using when hard solder to welding temperature parameter into
Row research and screening, brazing temperature is preferably 450 ~ 550 DEG C.
In the preferred embodiment of the method for titanium welding pipe production titanium vacuum cup of the invention, in vacuum drying oven in step 4
4 ~ 6h of middle heat preservation solidifies the solder for the thawing for sealing aspirating hole completely.
Welding side in the preferred embodiment of the method for titanium welding pipe production titanium vacuum cup of the invention, in step 2
Method is laser welding.
Compared with prior art, the invention has the advantage that:
1. the wall of titanium welding pipe is relatively thin, and manufacture craft is simple using the titanium vacuum cup of titanium welding pipe production, titanium heat preservation is greatly reduced
The cost of cup is low, thus further such that titanium vacuum cup Rapid Popularization on the market.
2. the titanium vacuum cup made of the titanium welding pipe of different size, has broken the production method of original one-to-two, has kept away
Exempt from the production process because the bulging difficulty of titanium tube is big or bulging failure, to improve titanium vacuum cup yield rate.
Specific embodiment
Invention is described in detail below by each embodiment, but it should be stated that, these embodiments are not
Limitation of the present invention, those of ordinary skill in the art are according to these embodiments in made function, method or structure
Equivalent transformation or substitution, all belong to the scope of protection of the present invention within.
In addition, term " first ", " second ", " third " etc. are used for description purposes only, it is not understood to indicate or imply
Relative importance or the quantity for implicitly indicating indicated technical characteristic.The feature of " first ", " second " etc. is defined as a result,
It can explicitly or implicitly include one or more of the features.In the description of the invention, unless otherwise indicated,
The meaning of " plurality " is two or more.
Term " installation ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, be also possible to removable
Connection is unloaded, or is integrally connected；It can be mechanical connection, be also possible to be electrically connected；It can be directly connected, it can also be in
Between medium be indirectly connected, can be the connection inside two elements.For the ordinary skill in the art, can pass through
Concrete condition understands concrete meaning of the above-mentioned term in the invention.
Embodiment 1:
In the present embodiment, a kind of method of titanium welding pipe production titanium vacuum cup, comprising the following steps:
Step 1: making the shell of upper opening, the inner casing of upper opening of titanium welding pipe respectively, opens up pumping in outer casing bottom
Hole；Wherein, make the titanium welding pipe of shell caliber be greater than production inner casing titanium welding pipe caliber 5.0mm, select production shell and
The titanium welding pipe thickness of pipe wall of inner casing is 0.3mm.
Step 2: inner casing is placed in interior of shell, then will be closed after shell upper and inner casing top contraction distortion 20%
Mouthful, the sealing welding that will heal up (welding method is preferably method for laser welding), and at sealing roll threading (including internal screw thread,
External screw thread, internal screw thread and external screw thread) titanium body of vacuum cup is made.
Step 3: titanium body of vacuum cup is put into vacuum drying oven, then the air in the interlayer that shell and inner casing are formed from
It is extracted out in aspirating hole.
Step 4: in a vacuum furnace, carrying out sealed with brazing sealing to aspirating hole with solder, and heat preservation 4 is small in a vacuum furnace
When, it solidifies the solder for the thawing for sealing aspirating hole completely and titanium vacuum cup first product is made.
Step 5: to the titanium vacuum cup first product polishing treatment in step 4, titanium vacuum cup finished product is formed.
The titanium vacuum cup made by above method, after test, soaking time is greater than 10 hours, and yield rate improves 5.0%.
Embodiment 2:
In the present embodiment, a kind of method of titanium welding pipe production titanium vacuum cup, comprising the following steps:
Step 1: making the shell of upper opening, the inner casing of upper opening of titanium welding pipe respectively, opens up pumping in outer casing bottom
Hole；Wherein, make the titanium welding pipe of shell caliber be greater than production inner casing titanium welding pipe caliber 6.0mm, select production shell and
The titanium welding pipe thickness of pipe wall of inner casing is 0.6mm.
Step 2: inner casing is placed in interior of shell, then will be closed after shell upper and inner casing top contraction distortion 15%
Mouthful, the sealing welding that will heal up (welding method is preferably method for laser welding), and at sealing roll threading (including internal screw thread,
External screw thread, internal screw thread and external screw thread) titanium body of vacuum cup is made.
Step 3: titanium body of vacuum cup is put into vacuum drying oven, then the air in the interlayer that shell and inner casing are formed from
It is extracted out in aspirating hole.
Step 4: in a vacuum furnace, carrying out sealed with brazing sealing to aspirating hole with solder, and heat preservation 6 is small in a vacuum furnace
When, it solidifies the solder for the thawing for sealing aspirating hole completely and titanium vacuum cup first product is made.
Step 5: to the titanium vacuum cup first product polishing treatment in step 4, titanium vacuum cup finished product is formed.
The titanium vacuum cup made by above method, after test, soaking time is greater than 8 hours, and yield rate improves 7.5%.
Embodiment 3:
In the present embodiment, a kind of method of titanium welding pipe production titanium vacuum cup, comprising the following steps:
Step 1: making the shell of upper opening, the inner casing of upper opening of titanium welding pipe respectively, opens up pumping in outer casing bottom
Hole；Wherein, make the titanium welding pipe of shell caliber be greater than production inner casing titanium welding pipe caliber 5.6mm, select production shell and
The titanium welding pipe thickness of pipe wall of inner casing is 0.55mm.
Step 2: inner casing is placed in interior of shell, then will be closed after shell upper and inner casing top contraction distortion 17.0%
Mouthful, the sealing welding that will heal up (welding method is preferably method for laser welding), and at sealing roll threading (including internal screw thread,
External screw thread, internal screw thread and external screw thread) titanium body of vacuum cup is made.
Step 3: titanium body of vacuum cup is put into vacuum drying oven, then the air in the interlayer that shell and inner casing are formed from
It is extracted out in aspirating hole.
Step 4: in a vacuum furnace, sealed with brazing sealing is carried out to aspirating hole with solder, and keep the temperature 5.5 in a vacuum furnace
Hour, it solidifies the solder for the thawing for sealing aspirating hole completely and titanium vacuum cup first product is made.
Step 5: to the titanium vacuum cup first product polishing treatment in step 4, titanium vacuum cup finished product is formed.
The titanium vacuum cup made by above method, after test, soaking time is greater than 8.5 hours, and yield rate improves 5.3%.
The series of detailed descriptions listed above only for feasible embodiment of the invention specifically
Protection scope bright, that they are not intended to limit the invention, it is all without departing from equivalent implementations made by technical spirit of the present invention
Or change should all be included in the protection scope of the present invention.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (8)
1. a kind of method of titanium welding pipe production titanium vacuum cup, it is characterised in that: the following steps are included:
1) shell of upper opening, the inner casing of upper opening are made respectively of titanium welding pipe, opens up aspirating hole in outer casing bottom；Production
The caliber of the titanium welding pipe of the shell is greater than the caliber for making the titanium welding pipe of the inner casing；
2) inner casing is placed in interior of shell, then will healed up after shell upper and the contraction distortion of inner casing top, will heal up sealing
Welding, and titanium body of vacuum cup is made in the roll threading at sealing；
3) titanium body of vacuum cup is put into vacuum drying oven, then the air in interlayer that shell is formed with inner casing is taken out from aspirating hole
Out；
4) sealed with brazing sealing in a vacuum furnace, is carried out to aspirating hole with solder, and is kept the temperature in a vacuum furnace, makes to seal aspirating hole
The solder of thawing solidify titanium vacuum cup first product is made completely；
5) to the titanium vacuum cup first product polishing treatment in step 4), titanium vacuum cup finished product is formed.
2. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 1, it is characterised in that: titanium welding pipe thickness of pipe wall
For 0.3 ~ 1.0mm.
3. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 2, it is characterised in that: in the step 1)
The caliber for making the titanium welding pipe of shell is greater than the 5.0 ~ 6.0mm of caliber for making the titanium welding pipe of inner casing.
4. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 1, it is characterised in that: the step 3)
In, shell upper contraction distortion is 15.0% ~ 20.0%.
5. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 1, it is characterised in that: in the step 4)
Solder be hard metal solder or nonmetallic glass solder.
6. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 5, it is characterised in that: the hard metal pricker
Material is yellow gold.
7. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 1, it is characterised in that: in the step 4)
4 ~ 6h is kept the temperature in a vacuum furnace, solidifies the solder for the thawing for sealing aspirating hole completely.
8. a kind of method of titanium welding pipe production titanium vacuum cup according to claim 1, it is characterised in that: in the step 2
Welding method be laser welding.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811343228.5A CN109202199A (en) | 2018-11-13 | 2018-11-13 | A kind of method of titanium welding pipe production titanium vacuum cup |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811343228.5A CN109202199A (en) | 2018-11-13 | 2018-11-13 | A kind of method of titanium welding pipe production titanium vacuum cup |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109202199A true CN109202199A (en) | 2019-01-15 |
Family
ID=64996434
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811343228.5A Pending CN109202199A (en) | 2018-11-13 | 2018-11-13 | A kind of method of titanium welding pipe production titanium vacuum cup |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109202199A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114310058A (en) * | 2022-01-20 | 2022-04-12 | 浙江安胜科技股份有限公司 | Welding process based on automatic shrinkage integrated welding fixture |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04114614A (en) * | 1990-09-05 | 1992-04-15 | Odashima Kibutsu Seisakusho:Kk | Manufacture of metallic vacuum heat-insulating double vacuum bottle |
| CN1166438A (en) * | 1997-05-27 | 1997-12-03 | 元济敦 | Manufacture of cylinder for vacuum heat-insulating container |
| JPH11221667A (en) * | 1997-12-03 | 1999-08-17 | Nippon Sanso Kk | Manufacture of metallic vacuum double container |
| CN1231874A (en) * | 1998-02-18 | 1999-10-20 | 日本酸素株式会社 | Metal vessel and fabrication method for the same |
| CN1640351A (en) * | 2004-01-12 | 2005-07-20 | 陈安涛 | Processing method for communicating internal-external wall pipes for two-layer stainless steel wacuum thermal insulating container |
| US20110162761A1 (en) * | 2008-09-22 | 2011-07-07 | Seven Seven Co., Ltd. | Method for producing a vacuum-insulated double container |
| CN106881564A (en) * | 2017-01-09 | 2017-06-23 | 洛阳双瑞精铸钛业有限公司 | A kind of method that utilization thin-walled major diameter titanium welding pipe produces titanium matter cup/kettle |
| CN108127045A (en) * | 2017-12-26 | 2018-06-08 | 湖南湘投金天新材料有限公司 | The expanding die and expanding method of thermal insulation cup titanium welding pipe |
-
2018
- 2018-11-13 CN CN201811343228.5A patent/CN109202199A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04114614A (en) * | 1990-09-05 | 1992-04-15 | Odashima Kibutsu Seisakusho:Kk | Manufacture of metallic vacuum heat-insulating double vacuum bottle |
| CN1166438A (en) * | 1997-05-27 | 1997-12-03 | 元济敦 | Manufacture of cylinder for vacuum heat-insulating container |
| JPH11221667A (en) * | 1997-12-03 | 1999-08-17 | Nippon Sanso Kk | Manufacture of metallic vacuum double container |
| CN1231874A (en) * | 1998-02-18 | 1999-10-20 | 日本酸素株式会社 | Metal vessel and fabrication method for the same |
| CN1640351A (en) * | 2004-01-12 | 2005-07-20 | 陈安涛 | Processing method for communicating internal-external wall pipes for two-layer stainless steel wacuum thermal insulating container |
| US20110162761A1 (en) * | 2008-09-22 | 2011-07-07 | Seven Seven Co., Ltd. | Method for producing a vacuum-insulated double container |
| CN106881564A (en) * | 2017-01-09 | 2017-06-23 | 洛阳双瑞精铸钛业有限公司 | A kind of method that utilization thin-walled major diameter titanium welding pipe produces titanium matter cup/kettle |
| CN108127045A (en) * | 2017-12-26 | 2018-06-08 | 湖南湘投金天新材料有限公司 | The expanding die and expanding method of thermal insulation cup titanium welding pipe |
Non-Patent Citations (1)
| Title |
|---|
| 文华里: "《轻冶工业实用技术知识手册》", 30 June 2001, 东北大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114310058A (en) * | 2022-01-20 | 2022-04-12 | 浙江安胜科技股份有限公司 | Welding process based on automatic shrinkage integrated welding fixture |
| CN114310058B (en) * | 2022-01-20 | 2024-03-01 | 浙江安胜科技股份有限公司 | Welding process based on automatic shrinkage integrated welding fixture |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR920009830B1 (en) | Vacuum-insulated, double walled metal structure and method for its production | |
| ES2705060T3 (en) | Nuclear fuel pods, manufacturing process and uses against oxidation / hydration | |
| US4856174A (en) | Method of making a stainless steel vacuum bottle with a silver mirrored surface | |
| CN109465601A (en) | A kind of method of titanium seamless tubes production titanium vacuum cup | |
| CN109202199A (en) | A kind of method of titanium welding pipe production titanium vacuum cup | |
| JP7453302B2 (en) | Glass/metal feedthrough | |
| WO2014022109A1 (en) | Vacuum insulated glass (vig) window unit including hybrid getter and method of making same | |
| TW201530852A (en) | Method of manufacturing prismatic type battery case | |
| US20140223842A1 (en) | Integrated lower-plate glass and manufacturing method of vacuum multi-layer glass including same | |
| CN104150109A (en) | Vacuum sealing method of heat preservation vessel | |
| CN109171389A (en) | A kind of titanium vacuum cup and preparation method thereof | |
| CN101145484B (en) | T2-T1 standard hot electrode fluorescence lamp production method | |
| WO2022147861A1 (en) | Manufacturing method for vapor chamber, vapor chamber and middle frame vapor chamber | |
| CN108556290A (en) | Injection mold water route blocks and appearance treatment process | |
| CN104227258B (en) | A kind of encapsulating method of cesium beam tube caesium bubble | |
| EA025801B1 (en) | Glazing panel comprising glass sheets linked together via spacers and method for production thereof | |
| CN105973489A (en) | Low-surface-adhesion liquid metal and application of low-surface-adhesion liquid metal in thermometer | |
| CN108611230A (en) | a kind of brewing method of rice wine | |
| US20200040645A1 (en) | Vacuum Insulated Glazing Unit | |
| JP2001250504A (en) | High-pressure discharge lamp | |
| US6518701B1 (en) | Mercury capsule for use in a fluorescent lamp | |
| CN107881354B (en) | Preparation method of nickel-platinum alloy | |
| CN109907130A (en) | A kind of black tea fermentation device | |
| CN110349751A (en) | A kind of fuse heat setting process method | |
| CN218891011U (en) | Alloy wire preparation facilities |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190115 |
|
| RJ01 | Rejection of invention patent application after publication |