CN109179849A - A kind of silicone industry sewage water treatment method - Google Patents
A kind of silicone industry sewage water treatment method Download PDFInfo
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- CN109179849A CN109179849A CN201811086596.6A CN201811086596A CN109179849A CN 109179849 A CN109179849 A CN 109179849A CN 201811086596 A CN201811086596 A CN 201811086596A CN 109179849 A CN109179849 A CN 109179849A
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- waste liquid
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/48—Treatment of water, waste water, or sewage with magnetic or electric fields
- C02F1/481—Treatment of water, waste water, or sewage with magnetic or electric fields using permanent magnets
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
- C02F1/06—Flash evaporation
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
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- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention belongs to technical field of organic silicon production, specifically a kind of silicone industry sewage water treatment method, this method uses recovery and processing system, and recovery and processing system includes top end socket, No.1 cylinder, two horn bodies and collet；It further include driving unit, No.1 pipe, No.1 spiral plate, No. two spiral plates and controller.Pass through the mutual cooperation between driving unit, No.1 spiral plate, No. two spiral plates and No.1 pipe, on the one hand, driving unit drives No. two spiral plates that organic silicon waste liquid is transported at No.1 spiral plate, No.1 spiral plate carries out organic silicon waste liquid adequately to stir stirring, so that high-boiling components adequately steam, to improve the evaporation efficiency of organic silicon waste liquid；On the other hand, inert gas is passed through into No.1 cylinder by No.1 pipe, the flash gas steamed is quickly exported from flashed vapour and is discharged by inert gas, to improve the evaporation efficiency of subsequent organic silicon waste liquid.
Description
Technical field
The invention belongs to technical field of organic silicon production, specifically a kind of silicone industry sewage water treatment method.
Background technique
Organic silicon waste liquid is generated waste in organic silicon monomer especially methyl chlorosilane monomer synthesis process,
Mainly by a large amount of high-boiling components and a small amount of fluidized bed take unreacted silicon powder out of, copper powder forms, high-boiling components refer to methylchlorosilane
70.3~50 DEG C of the boiling range generated in monomer synthesis process, it is high boiling based on silicon-silicon key, silicon-carbon-silicon key, silicon-oxygen-silicon
Point multi-silane mixture.If the exposure of this partial material is in air, it will burn or form strong acid mist or liquid, so if
Direct emission can cause environment seriously to pollute, it is necessary to carry out Harmless processing.
Currently, organic silicon monomer manufacturing enterprise is all by flashing the lower object of its mid-boiling point to the processing method of slurry
Matter recycling, waste residue direct hydrolysis, this processing method do not recycle high-boiling components a large amount of in slurry, cause efficient resource
A large amount of wastes.The present invention proposes a kind of silicone industry sewage water treatment method, and the method increase the recycling of high-boiling components in slag paddle
It utilizes, to improve the utilization rate of resource.
Occur a kind of technical solution of the patent about silicone industry sewage water treatment method, such as application number in the prior art
The processing method and its device of a kind of organosilicon slag slurry, including top are disclosed for 2008101953752 Chinese patent
End socket, cylindrical tube, up big and down small cone angle cylinder and solid discharge are constituted, and are gone out on the end socket of top equipped with material inlet and flashed vapour
Mouthful, flanged joint is used between top end socket and cylindrical tube, helical ribbon agitator and twin-screw be fixed on main shaft, cylindrical tube and
Heat-conducting medium outlet and heat-conducting medium entrance are respectively provided on cone angle cylinder.
The processing method and its device of a kind of organosilicon slag slurry of the technical solution, by blender to organosilicon slag paddle into
Row stirring, so that the high-boiling components in organic slag paddle steam.But blender cannot be in organic silicon waste liquid in the technical solution
High-boiling components are adequately stirred, prevent the high-boiling components in organic silicon waste liquid are from steaming completely, to influence organic silicon waste liquid
The evaporation effect of middle high-boiling components；Meanwhile the flash gas that high-boiling components stirring steams quickly cannot export discharge from flashed vapour, from
And influence the evaporation efficiency of subsequent high-boiling components；So that the technical solution is restricted.
Summary of the invention
In order to make up for the deficiencies of the prior art, a kind of silicone industry sewage water treatment method proposed by the present invention, this method
Using recovery and processing system, recovery and processing system passes through the phase between driving unit, No.1 spiral plate, No. two spiral plates and No.1 pipe
Mutually cooperation, on the one hand, driving unit drives No. two spiral plates that organic silicon waste liquid is transported at No.1 spiral plate, No.1 spiral plate
Stirring adequately is stirred to organic silicon waste liquid progress, so that high-boiling components adequately steam, to improve the steaming of organic silicon waste liquid
Send out efficiency；On the other hand, inert gas is passed through into No.1 cylinder by No.1 pipe, inert gas is fast by the flash gas steamed
The slave flashed vapour of speed exports discharge, to improve the evaporation efficiency of subsequent organic silicon waste liquid.
The technical solution adopted by the present invention to solve the technical problems is: a kind of silicone industry sewage of the present invention
Processing method, method includes the following steps:
S1: mounting permanent magnet and condenser, permanent magnet are mounted at material inlet in recovery and processing system, are passed through
Permanent magnet adsorbs the iron substance in organosilicon slag paddle, and condenser is mounted on flash distillation gas outlet, and condenser is used for
Flash gas is condensed；High temperature heat conductive oil is added into collet by organosilicon synthesizer simultaneously, conduction oil be used for
Recovery and processing system provides heat, so that the high-boiling components in organosilicon slag paddle are adequately evaporated, to improve organosilicon
The evaporation efficiency of slag paddle；
S2: the collet in S1 is connected to the organosilicon synthesizer in S1, on the one hand, so that the conduction oil of collet
Temperature reduces, and conduction oil may return in organosilicon synthesizer and directly use；On the other hand, recovery and processing system body can be made
Interior slurry temperature increases, and is conducive to high-boiling components evaporation, achievees the purpose that heat-source Cycles utilize；
S3: the high temperature sludge paddle in organic silicon monomer synthesis of detergent tower reboiler is sent from the material inlet in S1 by pumping
Enter into recovery and processing system, high-boiling components are steamed；
S4: being condensed the flash gas steamed in S3 by the condenser in S1 and is sent to storage tank storage；
Wherein, recovery and processing system is used in S1, recovery and processing system includes top end socket, No.1 cylinder, two horn bodies
And collet；It further include driving unit, No.1 pipe, No.1 spiral plate, No. two spiral plates and controller；The controller is fixedly mounted
The outside of end socket on top, controller is for controlling recovery and processing system automatic operating；The No.1 cylinder be cylindrical tube, one
It is exported on the side wall of horn body equipped with heat-conducting medium, No.1 cylinder one end is connected to two horn bodies, and the No.1 cylinder other end passes through
Flange is connect with top end socket；The top end socket is equipped with material inlet and flashed vapour exports, and the quantity of flashed vapour outlet is
Two；The bottom of the two horns body is equipped with solid discharge, and heat-conducting medium entrance is housed on the side wall of two horn bodies；The collet
Be set on the outer ring of No.1 cylinder and two horn bodies, setting collet avoid No.1 cylinder and the intracorporal temperature of two horns it is excessively high and
Harm is generated to staff, to improve the practicability of recovery and processing system；The driving unit is located in No.1 cylinder
Portion, driving unit is for driving No.1 spiral plate to be stirred organic silicon waste liquid；The No.1 spiral plate is useless for organosilicon
The stirring of liquid, No.1 spiral plate are connected on driving unit, and No.1 spiral plate is equipped with one group of No.1 hole, and No.1 hole is arranged, makes
It obtains No.1 spiral plate to be stirred in evaporation organic silicon waste liquid, organic silicon waste liquid need not be carried out along the hand of spiral of spiral plate
Stirring, increases the mobile route of organic silicon waste liquid, so that organic silicon waste liquid progress repeatedly stirs stirring, to improve organic
The evaporation efficiency of silicon waste liquid；No. two spiral plates are used for the conveying of organic silicon scrap, and No. two spiral plates are connected in driving unit
On；The No.1 pipe is located on driving unit, and No.1 pipe is used to convey inert gas to No.1 cylinder, by being passed through indifferent gas
Body, on the one hand, inert gas reduces the purity of residue in organic silicon waste liquid, avoids exploding since purity is excessively high, from
And improve the safety of recovery and processing system；On the other hand, inert gas, the air pressure liter of No.1 cylinder body bottom are continually fed into
Height, inert gas quickly push flash gas to export away from flashed vapour, to improve the evaporation effect of subsequent organic silicon waste liquid
Rate；Wherein,
The driving unit includes driving motor, No.1 axis and No. two axis；The driving motor is fixedly mounted by pillar
At the top of the end socket of top；No.1 axis one end is connected by bearing and driving motor output shaft, the No.1 axis other end by from
Clutch is connected with No. two axis, and No.1 axle position is equipped with air inlet in top end socket lateral ends, offers one number service inside No.1 axis
Road is equipped with gas outlet positioned at the No.1 axis outer ring of No.1 cylinder；The No.1 pipe is located at No.1 channel, and No.1 pipe one end is solid
It is scheduled on No.1 channel, and No.1 pipe one end is connected to gas outlet, the No.1 pipe other end is for arc surface and vacantly in No.1 channel
On, and the No.1 pipe other end is connected to gas outlet；No.1 region is formed between the No.1 axis inner wall and No.1 pipe outer wall；It is described go out
Two sides are equipped with sealing ring to port up and down；The sealing ring is for being sealed No.1 region, so that being input into from No.1 pipe lazy
Property gas be transported to No.1 inner barrel from gas outlet, be connected inside sealing ring outer wall and No.1 axis, sealing ring inner wall and one
Number pipe outer wall is connected；No. two axis are far from No.1 axis one end vacantly above solid discharge.Exist in organic silicon waste liquid a large amount of
High-boiling components and a small amount of fluidized bed take unreacted substance out of, this material exposure in air, can burn or formed strong acid object and
Liquid causes damages to environment, so nuisanceless disposal must be carried out；The processing dress of organic silicon waste liquid exists in the prior art
It sets, existing processing unit Shortcomings, on the one hand, blender cannot adequately stir the high-boiling components in organic silicon waste liquid
It mixes, prevent the high-boiling components in organic silicon waste liquid are from steaming completely, to influence the evaporation effect of high-boiling components in organic silicon waste liquid；
On the other hand, the flash gas that high-boiling components stirring steams, which cannot be exported quickly from flashed vapour, to be discharged, to influence subsequent high boiling
The evaporation efficiency of object；Driving unit, No.1 spiral plate, No. two spiral plates and No.1 pipe is arranged in the present invention, passes through driving unit, one
Mutual cooperation number between spiral plate, No. two spiral plates and No.1 pipe, on the one hand, driving unit drives No. two spiral plates by organosilicon
Waste liquid is transported at No.1 spiral plate, and No.1 spiral plate adequately stirs stirring to organic silicon waste liquid progress, so that high-boiling components fill
That divides steams, to improve the evaporation efficiency of organic silicon waste liquid；On the other hand, it is passed through by No.1 pipe into No.1 cylinder lazy
Property gas, the flash gas steamed is quickly exported from flashed vapour and is discharged by inert gas, so that it is useless to improve subsequent organosilicon
The evaporation efficiency of liquid.
Organic silicon waste liquid is transported to from two horn bodies from material inlet, while heat-conducting medium being sent from heat-conducting medium entrance
Enter into two horn bodies；At this point, driving driving motor, opens clutch, driving motor drives No.1 spiral plate and No. two spirals
Plate rotation, passes through the rotation of No. two spiral plates, on the one hand, will be located at the organic silicon waste liquid at two horn bodies along No. two spiral plates
Hand of helix, organic silicon waste liquid is sent at No.1 spiral plate；On the other hand, No. two spiral plates of rotation have agglomeration
Machine silicon is crushed, and the organosilicon of agglomeration is avoided to influence the evaporation effect of organic silicon waste liquid；No.1 spiral shell is sent in organic silicon waste liquid
After rotating plate, clutch is closed, No. two spiral plates stop operating, so that No. two spiral plates stop conveying organosilicon to No.1 spiral plate
Waste liquid；And it is delivered to the organic silicon waste liquid of No.1 spiral plate, under the action of No.1 spiral plate, organic silicon waste liquid carries out sufficient
Stirring is stirred, so that the high-boiling components in organic silicon waste liquid evaporate flash gas；At this point, inert gas is transported to from air inlet
In No.1 pipe, the two sides due to being located at gas outlet are sealed by sealing ring, and the gas in No.1 pipe can only convey from gas outlet
Into No.1 cylinder, under the action of inert gas, inert gas quickly pushes flash gas to export from flashed vapour and is discharged, thus
Improve subsequent organic silicon waste liquid steams efficiency；Residue after evaporation is discharged from solid discharge.
Preferably, the outer ring of the No.1 axis is equipped with drainage unit；The drainage unit is used for flashed vapour from No.1
Cylinder is drawn, and drainage unit includes transition plates, swivel becket and No. two pipes；The swivel becket is rotatably installed in the outer ring of No.1 axis
On；Described No. two pipe one end and flashed vapour outlet, No. two pipe other ends are connected to by swivel becket with No.1 axis；The transition
Plate is located at the lower section of No. two pipes, and transition plates is connected on the outer ring of No.1 axis, and transition plates on the outer ring of No.1 axis at circumference
Distribution, transition plates, at being uniformly distributed, offer No. two regions in the side of No.1 axis inside transition plates, transition plates is equipped with No. two
Hole；No. two holes are uniformly distributed in transition plates side, and No. two holes, No. two regions and No.1 region are interconnected.The prior art
Middle inert gas pushes flash gas from flashed vapour outlet discharge process, and flash gas is always in No.1 cylinder, flashed vapour
Body influences the evaporation of subsequent organic silicon waste liquid, to influence the evaporation efficiency of flash gas；The present invention passes through setting drainage unit,
By drainage unit flash gas is followed the prescribed course discharge, flash gas is avoided to steam generation to organic silicon waste liquid
It influences, so that improve organic silicon waste liquid steams efficiency.
Inert gas is transported in No.1 pipe from air inlet, since sealing ring acts on, inert gas is conveyed from gas outlet
To at two horn bodies, under inert gas effect, inert gas pushes flash gas to enter No. two regions from No. two holes, due to
It is sealed at No.1 region by sealing ring, the flash gas in No. two regions cannot be re-introduced into No.1 cylinder from gas outlet
In, the flash gas in No. two regions, which can only be exported by No. two pipes from flashed vapour, to be discharged, so that it is useless to improve subsequent organosilicon
Liquid steams efficiency.
Preferably, No. two axis are equipped with scroll plate；The scroll plate is used to organic silicon waste liquid being sent to No.1 spiral shell
At rotating plate, scroll plate is rotatably installed on the outer ring of No. two axis.It is transported to by No. two spiral plates organic at No.1 spiral plate
Silicon waste liquid is easily clumped together, to influence stirring of the No.1 spiral plate to organic silicon waste liquid；The present invention is vortexed by setting
Plate, so that organic silicon waste liquid tiles outward, avoids organic silicon waste liquid from flocking together by scroll plate, so that No.1 spiral plate
Stirring adequately is stirred to organic silicon waste liquid progress, so that improve organic silicon waste liquid steams efficiency and effect.
Preferably, the scroll plate adjacent turn wall is equipped with pilot unit；The pilot unit is for organic silicon waste liquid
One-way movement, pilot unit include No.1 plate and No. two plates；The cross sectional shape of the No.1 plate is concave, No.1 plate one end
It is contacted with No. two plates, the No.1 plate other end is hinged on vortex wooden partition, and hinged place is equipped with torsional spring；The cross sectional shape of No. two plates
For " b " font, No. two plates are hinged on vortex wooden partition far from No.1 plate one end, and hinged place is equipped with torsional spring, No. two plate " b " fonts one
End is rotated in No.1 plate concave one end, and No. two plate " b " font one end are located at the lower end surface of No.1 plate concave.It is existing
In technology, when organic silicon waste liquid does not stir completion completely, organic silicon waste liquid is just fallen to from scroll plate at two horn bodies, thus
No.1 spiral plate is influenced to the stirring efficiency of organic silicon waste liquid；The present invention is organic by pilot unit by setting pilot unit
Silicon waste liquid can only one-way transmission, be transferred to scroll plate upper end from scroll plate lower end, No.1 spiral plate fills organic silicon waste liquid
That divides stirs stirring, to improve the evaporation efficiency of organic silicon waste liquid.
It is transported at scroll plate in organic silicon waste liquid, on the one hand, organic silicon waste liquid is outside along the swirl direction of scroll plate
Tiling, so that No.1 spiral plate adequately stirs stirring to organic silicon waste liquid progress, to improve steaming for organic silicon waste liquid
Efficiency；On the other hand, organic silicon waste liquid along scroll plate swirl direction in rotating, organic silicon waste liquid No. two plates of extruding, and No. two
Plate is squeezed and rotates, and when No. two plates turn to the upper surface of No.1 plate concave, No. two plates are blocked stopping
Rotation.
Preferably, the No.1 plate is equipped with No.1 magnet, and No. two plates are equipped with No. two magnet；The No.1 magnet and two
It attracts each other between number magnet, the mutual cooperation between No.1 magnet and No. two magnet is for stablizing turning for No.1 plate and No. two plates
It is dynamic.The present invention is arranged No.1 magnet and No. two magnet and avoids No.1 plate by the mutual cooperation between No.1 magnet and No. two magnet
With No. two plates in rotation, the residue after evaporation is fallen in the running clearance of No.1 plate and No. two plates, so that No.1 plate and two
Number plate is not capable of resetting, and influences the conveying of organic silicon waste liquid, to improve the evaporation efficiency of organic silicon waste liquid.
Preferably, No. two axis are equipped with No. three magnet；No. three magnet is connected on the outer ring of No. two axis, and three
Number magnet is installed along No. two axial symmetry；The two horns body sidewall is equipped with No.1 slot；The No.1 slot is equipped with No. four magnet；
Described No. four magnet one end are connected on No.1 slot, and No. four magnet other ends attract each other with No. three magnet.The present invention is by setting
No. three magnet and No. four magnet are set, by the mutual cooperation between No. three magnet and No. four magnet, balance the stress of No. two axis two sides,
It avoids No. two axis from shaking in rotation, influences the conveying of organic silicon waste liquid, to improve the conveying effect of organic silicon waste liquid
Rate.
Beneficial effects of the present invention are as follows:
1. a kind of silicone industry sewage water treatment method of the present invention, this method uses recovery and processing system, recycling
Processing system passes through the mutual cooperation between driving unit, No.1 spiral plate, No. two spiral plates and No.1 pipe, on the one hand, driving is single
Organic silicon waste liquid is transported at No.1 spiral plate by member No. two spiral plates of driving, and No.1 spiral plate carries out organic silicon waste liquid abundant
Stir stirring so that high-boiling components adequately steam, to improve the evaporation efficiency of organic silicon waste liquid；On the other hand, pass through
No.1 pipe is passed through inert gas into No.1 cylinder, and inert gas by the flash gas steamed, quickly arrange by middle flashed vapour outlet
Out, to improve the evaporation efficiency of subsequent organic silicon waste liquid.
2. a kind of silicone industry sewage water treatment method of the present invention, this method uses recovery and processing system, recycling
Processing system makes flash gas follow the prescribed course discharge by setting drainage unit, by drainage unit, avoids flashing
Gas has an impact steaming for organic silicon waste liquid, so that improve organic silicon waste liquid steams efficiency.
3. a kind of silicone industry sewage water treatment method of the present invention, this method uses recovery and processing system, recycling
Processing system, so that organic silicon waste liquid tiles outward, avoids organic silicon waste liquid from being gathered in by setting scroll plate by scroll plate
Together, so that No.1 spiral plate adequately stirs stirring to organic silicon waste liquid progress, to improve steaming for organic silicon waste liquid
Efficiency and effect.
4. a kind of silicone industry sewage water treatment method of the present invention, this method uses recovery and processing system, recycling
Processing system is by setting pilot unit, by pilot unit, organic silicon waste liquid can only one-way transmission, transmitted from scroll plate lower end
To scroll plate upper end, No.1 spiral plate adequately stirs stirring to organic silicon waste liquid progress, to improve organic silicon waste liquid
Evaporation efficiency.
5. a kind of silicone industry sewage water treatment method of the present invention, this method uses recovery and processing system, recycling
Processing system passes through the mutual cooperation between No. three magnet and No. four magnet, balance two by No. three magnet of setting and No. four magnet
The stress of number axis two sides, avoids No. two axis from shaking in rotation, influences the conveying of organic silicon waste liquid, to improve organic
The transfer efficiency of silicon waste liquid.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is process flow chart of the invention；
Fig. 2 is the main view of recovery and processing system；
Fig. 3 is the partial enlarged view in Fig. 2 at A；
Fig. 4 is the cross-sectional view of B-B in Fig. 2；
Fig. 5 is the cross-sectional view of C-C in Fig. 4；
Fig. 6 is the partial enlarged view in Fig. 5 at D；
In figure: top end socket 1, collet 11, material inlet 12, flashed vapour outlet 13, No.1 cylinder 2, heat-conducting medium outlet
21, flange 22, two horn bodies 3, solid discharge 31, heat-conducting medium entrance 32, No.1 slot 33, driving unit 4, driving motor 41,
No.1 axis 42, air inlet 421, No.1 channel 422, gas outlet 423, No.1 region 424, sealing ring 425, No. two axis 43, clutch
Device 44, the magnet 46, four of scroll plate 45, three magnet 47, No.1 pipe 5, No.1 spiral plate 6, the spiral plate 7 of No.1 hole 61, two,
Drainage unit 8, the region 811, two of transition plates 81, two hole 812, swivel becket 82, No. two pipes 83, pilot unit 9, No.1 plates
91,93, No. two No. two plates 92, No.1 magnet magnet 94.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As shown in Figures 1 to 6, a kind of silicone industry sewage water treatment method of the present invention, this method includes following
Step:
S1: mounting permanent magnet and condenser, permanent magnet are mounted at material inlet in recovery and processing system, are passed through
Permanent magnet adsorbs the iron substance in organosilicon slag paddle, and condenser is mounted on flash distillation gas outlet, and condenser is used for
Flash gas is condensed；High temperature heat conductive oil is added into collet by organosilicon synthesizer simultaneously, conduction oil be used for
Recovery and processing system provides heat, so that the high-boiling components in organosilicon slag paddle are adequately evaporated, to improve organosilicon
The evaporation efficiency of slag paddle；
S2: the collet in S1 is connected to the organosilicon synthesizer in S1, on the one hand, so that the conduction oil of collet
Temperature reduces, and conduction oil may return in organosilicon synthesizer and directly use；On the other hand, recovery and processing system body can be made
Interior slurry temperature increases, and is conducive to high-boiling components evaporation, achievees the purpose that heat-source Cycles utilize；
S3: the high temperature sludge paddle in organic silicon monomer synthesis of detergent tower reboiler is sent from the material inlet in S1 by pumping
Enter into recovery and processing system, high-boiling components are steamed；
S4: being condensed the flash gas steamed in S3 by the condenser in S1 and is sent to storage tank storage；
Wherein, recovery and processing system is used in S1, recovery and processing system includes top end socket 1, No.1 cylinder 2, two horns
Body 3 and collet 11；It further include driving unit 4, No.1 pipe 5, No.1 spiral plate 6, No. two spiral plates 7 and controllers；The control
Device is fixedly mounted on the outside of top end socket, and controller is for controlling recovery and processing system automatic operating；The No.1 cylinder 2 is
Cylindrical tube, equipped with heat-conducting medium outlet 21 on the side wall of No.1 cylinder 2,2 one end of No.1 cylinder is connected to two horn bodies 3, and one
2 other end of horn body is connect by flange 22 with top end socket 1；The top end socket 1 is equipped with material inlet 12 and flashed vapour
Outlet 13, the quantity of flashed vapour outlet 13 are two；The bottom of the two horns body 3 is equipped with solid discharge 31, two horn bodies 3
Heat-conducting medium entrance 32 is housed on side wall；The collet 11 is set on the outer ring of No.1 cylinder 2 and two horn bodies 3, setting folder
Set 11 avoids the temperature in No.1 cylinder 2 and two horn bodies 3 excessively high and generates harm to staff, to improve at recycling
The practicability of reason system；The driving unit 4 is located inside No.1 cylinder 2, and driving unit 4 is for driving No.1 spiral plate 6 right
Organic silicon waste liquid is stirred；The No.1 spiral plate 6 is used for the stirring of organic silicon waste liquid, and No.1 spiral plate 6 is connected in driving
On unit 4, No.1 spiral plate 6 is equipped with one group of No.1 hole 61, and No.1 hole 61 is arranged, so that No.1 spiral plate 6 is useless to organosilicon
Liquid is stirred in evaporation, and organic silicon waste liquid need not be stirred along the hand of spiral of spiral plate, increases organic silicon waste liquid
Mobile route so that organic silicon waste liquid progress repeatedly stir stirring, to improve the evaporation efficiency of organic silicon waste liquid；It is described
No. two spiral plates 7 are used for the conveying of organic silicon scrap, and No. two spiral plates 7 are connected on driving unit 4；The No.1 pipe 5 is located at
On driving unit 4, No.1 pipe 5 is used to convey inert gas to No.1 cylinder 2, by being passed through inert gas, on the one hand, indifferent gas
Body reduces the purity of residue in organic silicon waste liquid, avoids exploding since purity is excessively high, to improve recovery processing
The safety of system；On the other hand, it is continually fed into inert gas, the air pressure of 2 bottom of No.1 cylinder increases, and inert gas quickly pushes away
Dynamic flash gas is gone out from flashed vapour outlet 13, to improve the evaporation efficiency of subsequent organic silicon waste liquid；Wherein,
The driving unit 4 includes driving motor 41, No.1 axis 42 and No. two axis 43；The driving motor 41 passes through pillar
It is fixedly mounted on 1 top of top end socket；Described 42 one end of No.1 axis passes through bearing and 41 output shaft fixed connection of driving motor, No.1 axis
42 other ends are connected by clutch 44 and No. two axis 43, and No.1 axis 42 is located at 1 lateral ends of top end socket equipped with air inlet
421, No.1 channel 422 is offered inside No.1 axis 42, is equipped with gas outlet 423 positioned at 42 outer ring of No.1 axis of No.1 cylinder 2；
The No.1 pipe 5 is located at No.1 channel 422, and 5 one end of No.1 pipe is fixed on No.1 channel 422, and 5 one end of No.1 pipe with go out
Port 423 is connected to, and 5 other end of No.1 pipe is arc surface and vacantly on No.1 channel 422, and 5 other end of No.1 pipe and outlet
Mouth 423 is connected to；No.1 region 424 is formed between 42 inner wall of No.1 axis and 5 outer wall of No.1 pipe；The gas outlet about 423 two
Side is equipped with sealing ring 425；The sealing ring 425 is for being sealed No.1 region 424, so that being input into from No.1 pipe 5 lazy
Property gas be transported to inside No.1 cylinder 2 from gas outlet 423, be connected inside 425 outer wall of sealing ring and No.1 axis 42, sealing ring
425 inner walls and 5 outer wall of No.1 pipe are connected；No. two axis 43 are far from 42 one end of No.1 axis vacantly above solid discharge 31.Have
There are a large amount of high-boiling components and a small amount of fluidized bed to take unreacted substance out of in machine silicon waste liquid, this material exposes meeting in air
Burning forms strong acid object and liquid, causes damages to environment, so nuisanceless disposal must be carried out；It has existed in the prior art
The processing unit of machine silicon waste liquid, existing processing unit Shortcomings, on the one hand, blender cannot be to high boiling in organic silicon waste liquid
Object is adequately stirred, prevent the high-boiling components in organic silicon waste liquid are from steaming completely, to influence high in organic silicon waste liquid
Boil the evaporation effect of object；On the other hand, the flash gas that high-boiling components stirring steams cannot quickly be discharged from flashed vapour outlet 13,
To influence the evaporation efficiency of subsequent high-boiling components；6, No. two driving unit 4, No.1 spiral plate spiral plates 7 and one is arranged in the present invention
Number pipe 5, passes through driving unit 4, No.1 spiral plate 6, two mutual cooperations between spiral plate 7 and No.1 pipe 5, on the one hand, driving
Unit 4 drive No. two spiral plates 7 organic silicon waste liquid is transported at No.1 spiral plate 6, No.1 spiral plate 6 to organic silicon waste liquid into
Row adequately stirs stirring, so that high-boiling components adequately steam, to improve the evaporation efficiency of organic silicon waste liquid；Another party
Face is passed through inert gas into No.1 cylinder 2 by No.1 pipe 5, and inert gas is by the flash gas steamed quickly from flash distillation
13 discharge of gas outlet, to improve the evaporation efficiency of subsequent organic silicon waste liquid.
Organic silicon waste liquid is transported to from two horn bodies 3 from material inlet 12, while heat-conducting medium being entered from heat-conducting medium
Mouth 32 is sent in two horn bodies 3；At this point, driving driving motor 41, opens clutch 44, driving motor 41 drives No.1 spiral
Plate 6 and No. two spiral plates 7 rotate, and pass through the rotation of No. two spiral plates 7, on the one hand, the organosilicon being located at two horn bodies 3 gives up
Along the hand of helix of No. two spiral plates 7, organic silicon waste liquid is sent at No.1 spiral plate 6 liquid；On the other hand, the two of rotation
The organosilicons of numbers 7 pairs of spiral plate agglomerations are crushed, and the organosilicon of agglomeration is avoided to influence the evaporation effect of organic silicon waste liquid；Having
After machine silicon waste liquid is sent to No.1 spiral plate 6, clutch 44 is closed, No. two spiral plates 7 stop operating, so that No. two spiral plates 7 stop
Only organic silicon waste liquid is conveyed to No.1 spiral plate 6；And it is delivered to the organic silicon waste liquid of No.1 spiral plate 6, in No.1 spiral plate 6
Under effect, organic silicon waste liquid progress adequately stirs stirring, so that the high-boiling components in organic silicon waste liquid evaporate flash gas；This
When, inert gas is transported in No.1 pipe 5 from air inlet 421, the two sides due to being located at gas outlet 423 pass through sealing ring 425
It seals, the gas in No.1 pipe 5 can only be delivered in No.1 cylinder 2 from gas outlet 423, lazy under the action of inert gas
Property gas quickly push flash gas from 13 discharge of flashed vapour outlet, so that improve subsequent organic silicon waste liquid steams efficiency；
Residue after evaporation is discharged from solid discharge 31.
As one embodiment of the present invention, the outer ring of the No.1 axis 42 is equipped with drainage unit 8；The drainage is single
For member 8 for drawing flashed vapour from No.1 cylinder 2, drainage unit 8 includes transition plates 81, swivel becket 82 and No. two pipes 83；It is described
Swivel becket 82 is rotatably installed on the outer ring of No.1 axis 42；83 one end of No. two pipes is connected to flashed vapour outlet 13, No. two pipes
83 other ends are connected to by swivel becket 82 with No.1 axis 42；The transition plates 81 is located at the lower section of No. two pipes 83, and transition plates 81 is solid
Be connected on the outer ring of No.1 axis 42, and transition plates 81 on the outer ring of No.1 axis 42 at circle distribution, transition plates 81 is in No.1 axis
42 side offers No. two regions 811 at being uniformly distributed inside transition plates 81, transition plates 81 is equipped with No. two holes 812；It is described
No. two holes 812 are uniformly distributed in 81 side of transition plates, and No. two regions 811 of hole 812, two and No.1 region 424 are interconnected.It is existing
There is inert gas in technology that flash gas is pushed to export in 13 discharge processes from flashed vapour, flash gas is always in No.1 cylinder 2
In, flash gas influences the evaporation of subsequent organic silicon waste liquid, to influence the evaporation efficiency of flash gas；The present invention passes through setting
Drainage unit 8 makes flash gas follow the prescribed course discharge by drainage unit 8, avoids flash gas useless to organosilicon
Steaming for liquid has an impact, so that improve organic silicon waste liquid steams efficiency.
Inert gas is transported in No.1 pipe 5 from air inlet 421, since sealing ring 425 acts on, inert gas is from outlet
Mouth 423 is transported at two horn bodies 3, and under inert gas effect, inert gas pushes flash gas to enter from No. two holes 812
No. two regions 811 are sealed due to passing through sealing ring 425 at No.1 region 424, and the flash gas in No. two regions 811 cannot be from
Gas outlet 423 is re-introduced into No.1 cylinder 2, and the flash gas in No. two regions 811 can only be by No. two pipes 83 from flash distillation
13 discharge of gas outlet, so that improve subsequent organic silicon waste liquid steams efficiency.
As one embodiment of the present invention, No. two axis 43 are equipped with scroll plate 45；The scroll plate 45 is used for
Organic silicon waste liquid is sent at No.1 spiral plate 6, scroll plate 45 is rotatably installed on the outer ring of No. two axis 43.Pass through No. two spiral shells
The organic silicon waste liquid that rotating plate 7 is transported at No.1 spiral plate 6 is easily clumped together, to influence No.1 spiral plate 6 to organic
The stirring of silicon waste liquid；The present invention, so that organic silicon waste liquid tiles outward, is avoided by the way that scroll plate 45 is arranged by scroll plate 45
Organic silicon waste liquid flocks together, so that No.1 spiral plate 6 adequately stirs stirring to organic silicon waste liquid progress, to improve
Organic silicon waste liquid steams efficiency and effect.
As one embodiment of the present invention, the 45 adjacent turn wall of scroll plate is equipped with pilot unit 9；The guiding
Unit 9 is used for the one-way movement of organic silicon waste liquid, and pilot unit 9 includes No.1 plate 91 and No. two plates 92；The No.1 plate 91
Cross sectional shape is concave, and 91 one end of No.1 plate is contacted with No. two plates 92, and 91 other end of No.1 plate is hinged on 45 wall of scroll plate
On, hinged place is equipped with torsional spring；The cross sectional shape of No. two plates 92 is " b " font, and No. two plates 92 are cut with scissors far from 91 one end of No.1 plate
It connects on 45 wall of scroll plate, hinged place is equipped with torsional spring, and No. two " b " font one end of plate 92 turn in 91 concave one end of No.1 plate
It is dynamic, and No. two " b " font one end of plate 92 are located at the lower end surface of 91 concave of No.1 plate.In the prior art, organic silicon waste liquid is not
When stirring is completed completely, organic silicon waste liquid is just fallen to from scroll plate 45 at two horn bodies 3, to influence No.1 spiral plate 6
To the stirring efficiency of organic silicon waste liquid；The present invention is by setting pilot unit 9, and by pilot unit 9, organic silicon waste liquid can only be single
To transmission, it is transferred to 45 upper end of scroll plate from 45 lower end of scroll plate, No.1 spiral plate 6 adequately stirs organic silicon waste liquid
Stirring, to improve the evaporation efficiency of organic silicon waste liquid.
It is transported at scroll plate 45 in organic silicon waste liquid, on the one hand, swirl direction of the organic silicon waste liquid along scroll plate 45
Tiling outward, so that No.1 spiral plate 6 adequately stirs stirring to organic silicon waste liquid progress, to improve organic silicon waste liquid
Steam efficiency；On the other hand, for organic silicon waste liquid in the rotation of 45 swirl direction of scroll plate, organic silicon waste liquid squeezes No. two plates
92, No. two plates 92 are squeezed and rotate, when No. two plates 92 turn to the upper surface of 91 concave of No.1 plate, No. two
Plate 92, which is blocked, to stop operating.
As one embodiment of the present invention, the No.1 plate 91 is equipped with No.1 magnet 93, and No. two plates 92 are equipped with
No. two magnet 94；It attracts each other between the No.1 magnet 93 and No. two magnet 94, between No.1 magnet 93 and No. two magnet 94
The rotation to cooperate for stablizing No.1 plate 91 and No. two plates 92.No.1 magnet 93 and No. two magnet 94 are arranged in the present invention, lead to
The mutual cooperation between No.1 magnet 93 and No. two magnet 94 is crossed, avoids No.1 plate 91 and No. two plates 92 in rotation, after evaporation
Residue is fallen in the running clearance of No.1 plate 91 and No. two plates 92, so that No.1 plate 91 and No. two plates 92 are not capable of resetting, and shadow
The conveying for ringing organic silicon waste liquid, to improve the evaporation efficiency of organic silicon waste liquid.
As one embodiment of the present invention, No. two axis 43 are equipped with No. three magnet 46；No. three magnet 46
It is connected on the outer ring of No. two axis 43, and No. three magnet 46 are symmetrically installed along No. two axis 43；Two horns body, 3 side wall is equipped with
No.1 slot 33；The No.1 slot 33 is equipped with No. four magnet 47；47 one end of No. four magnet is connected on No.1 slot 33, and No. four
47 other end of magnet attracts each other with No. three magnet 46.The present invention passes through three by No. three magnet 46 of setting and No. four magnet 47
Mutual cooperation number between magnet 46 and No. four magnet 47, balances the stress of No. two 43 two sides of axis, avoids No. two axis 43 in rotation
It shakes, influences the conveying of organic silicon waste liquid, to improve the transfer efficiency of organic silicon waste liquid.
In use, organic silicon waste liquid is transported to from two horn bodies 3 from material inlet 12, while by heat-conducting medium from thermally conductive
Medium inlet 32 is sent in two horn bodies 3；At this point, driving driving motor 41, opens clutch 44, driving motor 41 drives one
Number spiral plate 6 and No. two spiral plates 7 rotate, and pass through the rotation of No. two spiral plates 7, on the one hand, will be located at having at two horn bodies 3
Along the hand of helix of No. two spiral plates 7, organic silicon waste liquid is transported at scroll plate 45, made by spiral plate machine silicon waste liquid
With so that organic silicon waste liquid is transported at No.1 spiral plate 6 as what swirl direction tiled outward；On the other hand, No. two of rotation
The organosilicon of 7 pairs of spiral plate agglomerations is crushed, and the organosilicon of agglomeration is avoided to influence the evaporation effect of organic silicon waste liquid；Organic
After silicon waste liquid is sent to No.1 spiral plate 6, clutch 44 is closed, No. two spiral plates 7 stop operating, so that No. two spiral plates 7 stop
Organic silicon waste liquid is conveyed to No.1 spiral plate 6；And it is delivered to the organic silicon waste liquid of No.1 spiral plate 6, in the work of No.1 spiral plate 6
Under, organic silicon waste liquid progress adequately stirs stirring, so that the high-boiling components in organic silicon waste liquid steam flash gas；At this point,
Inert gas is transported in No.1 pipe 5 from air inlet 421, since the two sides for being located at gas outlet 423 are close by sealing ring 425
It sealing, the gas in No.1 pipe 5 can only be delivered in No.1 cylinder 2 from gas outlet 423, under the action of inert gas, inertia
Gas push flash gas enters No. two regions 811 from No. two holes 812, due to 425 sealing function of sealing ring, No. two regions
Flash gas in 811 can only be by No. two pipes 83 from 13 discharge of flashed vapour outlet, to improve subsequent organic silicon waste liquid
Steam efficiency；Residue after evaporation is discharged from solid discharge 31.
Above-mentioned front, back, left, right, up, down is mark according to personage's observation visual angle on the basis of Fig. 2 in Figure of description
Standard, device surface are defined as a left side on the left of observer to before being defined as on one side of observer, and so on.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", "front", "rear",
The orientation or positional relationship of the instructions such as "left", "right", "vertical", "horizontal", "top", "bottom" "inner", "outside" is based on attached drawing institute
The orientation or positional relationship shown, is merely for convenience of description of the present invention and simplification of the description, rather than the dress of indication or suggestion meaning
It sets or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as protecting the present invention
The limitation of range.
Finally it is noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations.To the greatest extent
Present invention has been described in detail with reference to the aforementioned embodiments for pipe, those skilled in the art should understand that: it is still
It is possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is equally replaced
It changes；And these are modified or replaceed, the essence for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution
Mind and range.Every other embodiment obtained by those of ordinary skill in the art without making creative efforts,
It shall fall within the protection scope of the present invention.
Claims (6)
1. a kind of silicone industry sewage water treatment method, it is characterised in that: method includes the following steps:
S1: mounting permanent magnet and condenser, permanent magnet are mounted at material inlet in recovery and processing system, condenser peace
Mounted in flash distillation gas outlet；High temperature heat conductive oil is added into collet by organosilicon synthesizer simultaneously；
S2: the collet in S1 is connected to the organosilicon synthesizer in S1；
S3: the high temperature sludge paddle in organic silicon monomer synthesis of detergent tower reboiler is sent to from the material inlet in S1 by pumping
In recovery and processing system, high-boiling components are steamed；
S4: being condensed the flash gas steamed in S3 by the condenser in S1 and is sent to storage tank storage；
Wherein, recovery and processing system is used in S1, recovery and processing system includes top end socket (1), No.1 cylinder (2), two horns
Body (3) and collet (11)；It further include driving unit (4), No.1 pipe (5), No.1 spiral plate (6), No. two spiral plates (7) and control
Device；The controller is fixedly mounted on the outside of top end socket (1), and controller is for controlling recovery and processing system automatic operating；
The No.1 cylinder (2) is cylindrical tube, and heat-conducting medium outlet (21), No.1 cylinder (2) are housed on the side wall of No.1 cylinder (2)
One end is connected to two horn bodies (3), and No.1 cylinder (2) other end is connect by flange (22) with top end socket (1)；The top
End socket (1) is equipped with material inlet (12) and flashed vapour outlet (13), and the quantity that flashed vapour exports (13) is two；Described No. two
The bottom of cylinder (3) is equipped with solid discharge (31), and heat-conducting medium entrance (32) are housed on the side wall of two horn bodies (3)；The folder
Set (11) is set on No.1 cylinder (2) and the outer ring of two horn bodies (3)；The driving unit (4) is located in No.1 cylinder (2)
Portion, driving unit (4) is for driving No.1 spiral plate (6) to be stirred organic silicon waste liquid；The No.1 spiral plate (6) is used for
The stirring of organic silicon waste liquid, No.1 spiral plate (6) are connected on driving unit (4), and No.1 spiral plate (6) is equipped with one group of No.1
Hole (61)；No. two spiral plates (7) are used for the conveying of organic silicon scrap, and No. two spiral plates (7) are connected in driving unit (4)
On；The No.1 pipe (5) is located on driving unit (4), and No.1 pipe (5) is used to convey inert gas to No.1 cylinder (2)；Its
In,
The driving unit (4) includes driving motor (41), No.1 axis (42) and No. two axis (43)；The driving motor (41) is logical
Pillar is crossed to be fixedly mounted at the top of top end socket (1)；Described No.1 axis (42) one end is exported by bearing and driving motor (41)
Axis is connected, and No.1 axis (42) other end is connected by clutch (44) and No. two axis (43), and No.1 axis (42) is located at top end socket
(1) lateral ends are equipped with air inlet (421), offer No.1 channel (422) inside No.1 axis (42), are located at No.1 cylinder (2)
No.1 axis (42) outer ring be equipped with gas outlet (423)；The No.1 pipe (5) is located at No.1 channel (422), No.1 pipe (5)
One end is fixed on No.1 channel (422), and No.1 pipe (5) one end is connected to gas outlet (423), and No.1 pipe (5) other end is
Arc surface and vacantly on No.1 channel (422), and No.1 pipe (5) other end is connected to gas outlet (423)；The No.1 axis
(42) No.1 region (424) are formed between inner wall and No.1 pipe (5) outer wall；Two sides are equipped with sealing ring to the gas outlet (423) up and down
(425)；The sealing ring (425) is for being sealed No.1 region (424), so that the indifferent gas being input into from No.1 pipe (5)
Body is transported to No.1 cylinder (2) inside from gas outlet (423), is connected inside sealing ring (425) outer wall and No.1 axis (42), close
Seal (425) inner wall and No.1 pipe (5) outer wall are connected；No. two axis (43) vacantly go out in residue far from No.1 axis (42) one end
Above mouth (31).
2. a kind of silicone industry sewage water treatment method according to claim 1, it is characterised in that: the No.1 axis (42)
Outer ring be equipped with drainage unit (8)；The drainage unit (8) is used to draw flashed vapour from No.1 cylinder (2), drainage unit
It (8) include transition plates (81), swivel becket (82) and No. two pipes (83)；The swivel becket (82) is rotatably installed in No.1 axis (42)
On outer ring；Described No. two pipe (83) one end are connected to flashed vapour outlet (13), and No. two pipe (83) other ends pass through swivel becket (82)
It is connected to No.1 axis (42)；The transition plates (81) is located at the lower section of No. two pipes (83), and transition plates (81) is connected in No.1 axis
(42) on outer ring, and transition plates (81) on the outer ring of No.1 axis (42) at circle distribution, transition plates (81) is in No.1 axis
(42) side offers No. two regions (811) at being uniformly distributed inside transition plates (81), transition plates (81) is equipped with No. two holes
(812)；No. two holes (812) are uniformly distributed in transition plates (81) side, No. two holes (812), No. two regions (811) and No.1
Region (424) is interconnected.
3. a kind of silicone industry sewage water treatment method according to claim 1, it is characterised in that: No. two axis (43)
It is equipped with scroll plate (45)；The scroll plate (45) is for organic silicon waste liquid to be sent at No.1 spiral plate (6), scroll plate
(45) it is rotatably installed on the outer ring of No. two axis (43).
4. a kind of silicone industry sewage water treatment method according to claim 3, it is characterised in that: the scroll plate (45)
Adjacent turn wall is equipped with pilot unit (9)；The pilot unit (9) is used for the one-way movement of organic silicon waste liquid, pilot unit (9)
Including No.1 plate (91) and No. two plates (92)；The cross sectional shape of the No.1 plate (91) is concave, No.1 plate (91) one end
It is contacted with No. two plates (92), No.1 plate (91) other end is hinged on scroll plate (45) wall, and hinged place is equipped with torsional spring；Described No. two
The cross sectional shape of plate (92) is " b " font, and No. two plates (92) are hinged on scroll plate (45) wall far from No.1 plate (91) one end, is cut with scissors
It meets place and is equipped with torsional spring, No. two plate (92) " b " font one end are rotated in No.1 plate (91) concave one end.
5. a kind of silicone industry sewage water treatment method according to claim 4, it is characterised in that: the No.1 plate (91)
It is equipped with No.1 magnet (93), No. two plates (92) are equipped with No. two magnet (94)；The No.1 magnet (93) and No. two magnet
(94) it attracts each other between.
6. a kind of silicone industry sewage water treatment method according to claim 3, it is characterised in that: No. two axis (43)
It is equipped with No. three magnet (46)；No. three magnet (46) is connected on the outer ring of No. two axis (43), and No. three magnet (46) edges
No. two axis (43) are symmetrically installed；Two horns body (3) side wall is equipped with No.1 slot (33)；The No.1 slot (33) is equipped with four
Number magnet (47)；Described No. four magnet (47) one end is connected on No.1 slot (33), No. four magnet (47) other ends and No. three magnetic
Iron (46) attracts each other.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811086596.6A CN109179849B (en) | 2018-09-18 | 2018-09-18 | Organic silicon industrial sewage treatment method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811086596.6A CN109179849B (en) | 2018-09-18 | 2018-09-18 | Organic silicon industrial sewage treatment method |
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| CN109179849B CN109179849B (en) | 2021-12-21 |
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| Application Number | Title | Priority Date | Filing Date |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113478712A (en) * | 2021-08-06 | 2021-10-08 | 抚州市天和硅业有限责任公司 | Organosilicon sediment thick liquid processing apparatus |
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| CN107501315A (en) * | 2017-09-01 | 2017-12-22 | 合盛硅业股份有限公司 | A kind of method and apparatus of effectively processing organic silicon slurry slag |
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| CN2483392Y (en) * | 2001-06-20 | 2002-03-27 | 王玉忠 | Gas generator |
| CN101386626A (en) * | 2008-10-31 | 2009-03-18 | 江苏宏达新材料股份有限公司 | Organosilicon slag slurry treatment method and apparatus thereof |
| CN105037414A (en) * | 2015-07-29 | 2015-11-11 | 湖北兴瑞化工有限公司 | Method and device for recovering efficient high-boiling substance from organic silicon residue slurry |
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Effective date of registration: 20211130 Address after: 518000 5th floor, building a, KEGU Science Park, No. 336-338, Baotian 1st Road, fenghuanggang community, Xixiang street, Bao'an District, Shenzhen City, Guangdong Province Applicant after: SHENZHEN RUISAI ENVIRONMENTAL PROTECTION TECHNOLOGY Co.,Ltd. Address before: 211189 Southeast University, No.2, Southeast University Road, Jiangning District, Nanjing City, Jiangsu Province Applicant before: LAN Feng |
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