CN109164520A - A kind of preparation method of reflectorized material - Google Patents
A kind of preparation method of reflectorized material Download PDFInfo
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- CN109164520A CN109164520A CN201811017010.0A CN201811017010A CN109164520A CN 109164520 A CN109164520 A CN 109164520A CN 201811017010 A CN201811017010 A CN 201811017010A CN 109164520 A CN109164520 A CN 109164520A
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- mixture
- drying
- preparation
- reflectorized material
- calcining
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/12—Reflex reflectors
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- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
Abstract
The invention discloses a kind of preparation methods of reflectorized material, the specific steps are as follows: S1: stirring, S2: S3: calcining crushes, S4: secondary agitation, S5: drying, S6: grinding, S7: deposit.The present invention is using simple, convenient method prepares reflectorized material, by calcining, it is freezing together raw material, it is convenient that it is crushed, pass through secondary agitation, the material of anti-oxidant, anticorrosion and waterproof is added in mixture, increases mixture by the service life, passes through drying, mixture can be made to be condensed into solid, facilitate last grinding, the light for becoming mixture increases reflective effect, the present invention is by becoming powdered for mixture, convenient for storage, it is corrosion-resistant that the present invention can be such that reflectorized material increases, and the time used is longer, it is easy to operate, it is convenient.
Description
Technical field
The present invention relates to reflectorized material preparation technical field, specially a kind of preparation method of reflectorized material.
Background technique
Reflectorized material, also referred to as reflecting material, emitting retroreflective material, be widely used in traffic sign and marked, protuberant guide post,
The different kinds of roads traffic safety facilities such as profile mark, cone, anti-collision barrel and License Plate, clothing shoes and hats, fire-fighting, railway,
Water transport, mining area etc. can be divided into traffic sign reflectorized material, roadmarking reflectorized material, protuberant guide post, delineator, clothing with instead
Luminescent material etc., traditional preparation method are all overlong times, and the reflectorized material prepared is ineffective, are not grown using the time,
So it is proposed that a kind of preparation method of reflectorized material, to solve the above problems.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of reflectorized material, mentioned above in the background art to solve
Problem.
To achieve the above object, the invention provides the following technical scheme: a kind of preparation method of reflectorized material, specific steps
It is as follows:
S1, stirring: according to a certain percentage by raw material, being added in agitator tank and be stirred, and the revolving speed of agitator tank is set as
Antioxidant and preservative are added during stirring, adds moisture content according to the actual situation, is mixed by 500-600r/min
Expect A；
S2, calcining: calcining mixture A, and the temperature setting of calcining is 50 DEG C -70 DEG C, and calcination time is set as 30min,
In calcination process, every 10min, observation calcining situation finally obtains solid A；
S3, crushing: being put into pulverizer for solid A and crush, and the degree of crushing is graininess；
S4, secondary agitation: the raw material in S3 being added in reaction kettle, while thickener is added, and the temperature setting of reaction kettle is
20 DEG C -25 DEG C, the revolving speed of stirring is set as 300-400r/min, after uniform stirring, obtains mixture B；
S5, drying: the mixture B in S4 is placed into drying box drying, the time of drying is set as 20min, the temperature of drying room
25 DEG C are set as, solid B is obtained；
S6, grinding: grinding solid B, and degree of grinding is powdered；
S7, deposit: the material in S6 being packed into dry aluminum bucket and closed, and aluminum bucket is placed on dry, shady and cool, ventilation
Place.
Preferably, the antioxidant in the S1 selects tea polyphenols, tocopherol, butylated hydroxy anisole, dibutyl hydroxy
One of toluene is a variety of.
Preferably, preservative in the S1 select sodium benzoate, nitrohydrochloric acid, nitrite, sulfur dioxide, one of
Or a variety of methods.
Preferably, the thickener in the S4 is selected methylcellulose, carboxymethyl cellulose, polyanion cellulose, is gathered
One of vinyl alcohol, polyethylene wax or a variety of methods.
Preferably, the interval time of S2 to the S3 is set as 30min and the interval time of S5 to S6 is set as 10min.
Compared with prior art, the beneficial effects of the present invention are: the present invention is using simply, convenient method prepares reflective material
Material is freezing together raw material by calcining, convenient to crush to it, by secondary agitation, be added in mixture it is anti-oxidant,
The material of anticorrosion and waterproof increases mixture by the service life, by drying, mixture can be made to be condensed into solid, convenient last
Grinding, the light for becoming mixture increases reflective effect, and the present invention is by becoming powdered for mixture, convenient for storage,
It is corrosion-resistant that the present invention can be such that reflectorized material increases, and the time used is longer, easy to operate, convenient.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
A kind of preparation method of reflectorized material, the specific steps are as follows:
S1, stirring: according to a certain percentage by raw material, being added in agitator tank and be stirred, and the revolving speed of agitator tank is set as
Antioxidant and preservative are added during stirring, adds moisture content according to the actual situation, is mixed by 500-600r/min
Expect A；
S2, calcining: calcining mixture A, and the temperature setting of calcining is 50 DEG C -70 DEG C, and calcination time is set as 30min,
In calcination process, every 10min, observation calcining situation finally obtains solid A；
S3, crushing: being put into pulverizer for solid A and crush, and the degree of crushing is graininess；
S4, secondary agitation: the raw material in S3 being added in reaction kettle, while thickener is added, and the temperature setting of reaction kettle is
20 DEG C -25 DEG C, the revolving speed of stirring is set as 300-400r/min, after uniform stirring, obtains mixture B；
S5, drying: the mixture B in S4 is placed into drying box drying, the time of drying is set as 20min, the temperature of drying room
25 DEG C are set as, solid B is obtained；
S6, grinding: grinding solid B, and degree of grinding is powdered；
S7, deposit: the material in S6 being packed into dry aluminum bucket and closed, and aluminum bucket is placed on dry, shady and cool, ventilation
Place.
Specifically, the antioxidant in the S1 selects tea polyphenols, tocopherol, butylated hydroxy anisole, dibutyl hydroxy
One of toluene is a variety of.
Specifically, preservative in the S1 select sodium benzoate, nitrohydrochloric acid, nitrite, sulfur dioxide, one of
Or a variety of methods.
Specifically, the thickener in the S4 is selected methylcellulose, carboxymethyl cellulose, polyanion cellulose, is gathered
One of vinyl alcohol, polyethylene wax or a variety of methods.
Specifically, the interval time of S2 to the S3 is set as 30min and the interval time of S5 to S6 is set as 10min.
For the present invention using simply, convenient method prepares reflectorized material, by calcining, is freezing together raw material, convenient
It is crushed, by secondary agitation, the material of anti-oxidant, anticorrosion and waterproof is added in mixture, increases mixture by the longevity
Life can make mixture be condensed into solid, facilitate last grinding by drying, and the light for becoming mixture increases reflective
Effect, the present invention is by becoming powdered for mixture, and convenient for storage, the present invention adds thickener during the preparation process, can be with
Reflectorized material device keeps adhesiveness stronger on reflective fabric, easy to operate, convenient.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of preparation method of reflectorized material, which is characterized in that specific step is as follows:
S1, stirring: according to a certain percentage by raw material, being added in agitator tank and be stirred, and the revolving speed of agitator tank is set as
Antioxidant and preservative are added during stirring, adds moisture content according to the actual situation, is mixed by 500-600r/min
Expect A；
S2, calcining: calcining mixture A, and the temperature setting of calcining is 50 DEG C -70 DEG C, and calcination time is set as 30min,
In calcination process, every 10min, observation calcining situation finally obtains solid A；
S3, crushing: being put into pulverizer for solid A and crush, and the degree of crushing is graininess；
S4, secondary agitation: the raw material in S3 being added in reaction kettle, while thickener is added, and the temperature setting of reaction kettle is
20 DEG C -25 DEG C, the revolving speed of stirring is set as 300-400r/min, after uniform stirring, obtains mixture B；
S5, drying: the mixture B in S4 is placed into drying box drying, the time of drying is set as 20min, the temperature of drying room
25 DEG C are set as, solid B is obtained；
S6, grinding: grinding solid B, and degree of grinding is powdered；
S7, deposit: the material in S6 being packed into dry aluminum bucket and closed, and aluminum bucket is placed on dry, shady and cool, ventilation
Place.
2. a kind of preparation method of reflectorized material according to claim 1, it is characterised in that: the antioxidant in the S1
Select one of tea polyphenols, tocopherol, butylated hydroxy anisole, dibutyl hydroxy toluene or a variety of.
3. a kind of preparation method of reflectorized material according to claim 1, it is characterised in that: the preservative choosing in the S1
With sodium benzoate, nitrohydrochloric acid, nitrite, sulfur dioxide, one of or a variety of methods.
4. a kind of preparation method of reflectorized material according to claim 1, it is characterised in that: the thickener choosing in the S4
With one of methylcellulose, carboxymethyl cellulose, polyanion cellulose, polyvinyl alcohol, polyethylene wax or a variety of methods.
5. a kind of preparation method of reflectorized material according to claim 1, it is characterised in that: when the interval of S2 to the S3
Between be set as 30min and the interval time of S5 to S6 is set as 10min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811017010.0A CN109164520A (en) | 2018-09-03 | 2018-09-03 | A kind of preparation method of reflectorized material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811017010.0A CN109164520A (en) | 2018-09-03 | 2018-09-03 | A kind of preparation method of reflectorized material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109164520A true CN109164520A (en) | 2019-01-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811017010.0A Pending CN109164520A (en) | 2018-09-03 | 2018-09-03 | A kind of preparation method of reflectorized material |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110261952A (en) * | 2019-08-02 | 2019-09-20 | 广州希恩朋克光电产品股份有限公司 | A kind of light guide plate and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4218260A (en) * | 1976-11-19 | 1980-08-19 | Institut Fur Privatwirtschaft Gschwend & Stadler | Reflective concrete body, process for the manufacture and utilization of the same |
| CN103964676A (en) * | 2014-05-06 | 2014-08-06 | 湖州远光路标涂料有限公司 | All-weather high-refraction reflective micro-crystal ceramic bead |
| CN104926125A (en) * | 2015-07-01 | 2015-09-23 | 合肥鼎亮光学科技有限公司 | Glass microspheres for acrylic resin type reflective film and preparation method thereof |
| CN106221201A (en) * | 2016-08-30 | 2016-12-14 | 国网山东省电力公司日照供电公司 | A kind of protection of electric power facility reflectorized material and preparation method thereof |
| CN107955542A (en) * | 2017-12-01 | 2018-04-24 | 合肥华福土工合成材料有限公司 | A kind of high-brightness reflective material and preparation method thereof |
-
2018
- 2018-09-03 CN CN201811017010.0A patent/CN109164520A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4218260A (en) * | 1976-11-19 | 1980-08-19 | Institut Fur Privatwirtschaft Gschwend & Stadler | Reflective concrete body, process for the manufacture and utilization of the same |
| CN103964676A (en) * | 2014-05-06 | 2014-08-06 | 湖州远光路标涂料有限公司 | All-weather high-refraction reflective micro-crystal ceramic bead |
| CN104926125A (en) * | 2015-07-01 | 2015-09-23 | 合肥鼎亮光学科技有限公司 | Glass microspheres for acrylic resin type reflective film and preparation method thereof |
| CN106221201A (en) * | 2016-08-30 | 2016-12-14 | 国网山东省电力公司日照供电公司 | A kind of protection of electric power facility reflectorized material and preparation method thereof |
| CN107955542A (en) * | 2017-12-01 | 2018-04-24 | 合肥华福土工合成材料有限公司 | A kind of high-brightness reflective material and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110261952A (en) * | 2019-08-02 | 2019-09-20 | 广州希恩朋克光电产品股份有限公司 | A kind of light guide plate and preparation method thereof |
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Application publication date: 20190108 |