CN109137604A - A kind of preparation method of essence coupling paper - Google Patents
A kind of preparation method of essence coupling paper Download PDFInfo
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- CN109137604A CN109137604A CN201811023019.2A CN201811023019A CN109137604A CN 109137604 A CN109137604 A CN 109137604A CN 201811023019 A CN201811023019 A CN 201811023019A CN 109137604 A CN109137604 A CN 109137604A
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F13/00—Making discontinuous sheets of paper, pulpboard or cardboard, or of wet web, for fibreboard production
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/10—Packing paper
Abstract
The invention belongs to pulp technology for making paper, are related to a kind of preparation method of essence coupling paper.Pre- paper pulp, 20~70g/m of solid content is made first with conventional techniques in the industry in the present invention3, according still further to the ratio of 60~95 parts of the pre- paper pulp of mass fraction, 0.5~10 part of coupling agent, 0.01~5 part of auxiliary agent, obtained after 0.5~4h of mechanical stirring and be coupled paper pulp in advance；Then 60~95 parts of paper pulp, fragrance or 0.5~8 part of aromatic of ratio are coupled in advance according to mass fraction, essence is obtained after 0.2~3h of mechanical stirring and is coupled paper pulp；Essence finally is made with conventional techniques in the industry and is coupled paper.Fragrance, aromatic are implanted into paper main structure by coupling mode by the present invention, with it is traditional fragrance, aromatic are coated on paper surface compared with, fragrance, aromatic attachment fastness through coupling implantation are stronger, and acidproof base strength significantly improves, and heated rear stack paper is not susceptible to be adhered；In addition, fragrance, the aromatic retention time in paper are longer, influenced by temperature or wetness smaller.
Description
Technical field
The invention belongs to pulp technology for making paper, are related to the preparation of paper more particularly to a kind of preparation of essence coupling paper
Method.
Background technique
As the papermaking technology of one of Ancient Times in China four inventions, indelible promotion is played for the progress of human civilization
Effect.Even to this day, although digitizing very fast development, paper still play in people's lives information transmitting, data storage and
The important function such as article packaging.Why paper can be used widely, and mainly have benefited from the raw material sources for making paper
It is wide in range, such as trees, forage are also or waste and old fishing net, theoretically for all articles rich in toughness fiber structure can use
In processing and make paper；Meanwhile manufacture craft is comparatively simple, is beaten after extracting fibre structure by boiling, paper pulp
Layer, squeezing, drying are copied again, finally obtain finished paper.In addition, people can improve according to needing to add corresponding auxiliary material or
Prominent characteristic in a certain respect, such as addition bleaching agent can enhance the whiteness of paper, add talcum powder, calcium carbonate fine powder for another example
The smoothness of paper surface then can be improved in end, the above SiO 2 powder of 500 mesh, for another example by asbestos and paper pulp mixing papermaking,
The fire resistance of paper significantly improves.
Certainly, the continuous proposition with people to new type of paper function, scientific workers make great efforts to lead to the development of the times
The means such as addition specific function auxiliary material or modified pulp fibers structure are crossed, performance is more prominent, function is more powerful to obtain
Paper.
In terms of food packaging industry, achievement acquired by paper and contribution are striking, previous scientific worker by
Paper surface coats the methods of essence, aromatic to improve paper to the affinity of people.However, this method does not obtain extensively
General application and market are approved.Since multiple-void structure, the painting containing essence or aromatic is presented in the paper surface after being squeezed, being dried
Material directly coats its surface and easily causes erosion of oozing, and damages to finish, the form and aspect etc. of paper, and passes through fluidized bed or Ultramicro-powder
Essence or aromatic are positioned directly in paper surface by last directly sprinkling etc. modes, but the poor, nonvolatile because of attachment fastness
The drawbacks such as the migration total amount of matter is higher and abandoned by people.
For this purpose, can be by the materials such as essence, aromatic and paper pulp homogeneous blend, and suitable coupling agent is introduced, by " building
Bridge " mode improves additive for the attachment fastness of paper.This very likely becomes the important breakthrough for preparing essence paper.
Summary of the invention
The purpose of the invention is to improve the additives such as essence, aromatic and paper main structure attachment fastness and chemistry
Stability discloses a kind of preparation method of essence coupling paper.
Technical solution
A kind of preparation method of essence coupling paper, includes the following steps:
A, pre- paper pulp is made with conventional techniques in the industry, wherein 20~70g/m of solid content of pre- paper pulp3, preferably 36g/m3；
B, according to the ratio of 60~95 parts of the pre- paper pulp of mass fraction, 0.5~10 part of coupling agent, 0.01~5 part of auxiliary agent, 10~
80 DEG C, 200~3000r/min mechanical stirring be uniformly mixed it, pre- coupling paper pulp is made after stirring 0.5~4h；
Wherein, preferably 50 DEG C, 3h is kept under 1000r/min mechanical stirring, preferably pre- pulp quality number is 80 parts；
The coupling agent can be silane coupling agent NXT, VP-Si-363, KH550, KH560 and KH570, be also possible to amino
Silane coupling agent KH-792 etc.；It is preferred that KH550, preferred mass number is 2.5 parts；
The auxiliary agent can be the powder in 50~1500 mesh numbers, such as SiO 2 powder, calcium carbonate powder；It is preferred that 500 mesh
SiO 2 powder, preferred mass number are 0.02 part；
C, 60~95 parts of paper pulp, fragrance or 0.5~8 part of aromatic of ratio are coupled in advance according to mass fraction, 5~60 DEG C,
50~2000r/min mechanical stirring is uniformly mixed it, and essence coupling paper pulp is made after stirring 0.2~3h,
Wherein, coupling paper pulp preferred mass number is 90 parts in advance；
Wherein, preferably 20 DEG C, 1000r/min mechanical stirring make its be uniformly mixed, stir 1.5h；
The fragrance can be glucose, fructose, sucrose, maltose, starch sugar, lactose stevioside, Radix Glycyrrhizae, glycyrrhizic acid two
Sodium, tripotassium glycyrrhetate and trisodium, saccharin, saccharin sodium, sodium cyclohexylsulfamate, L-aspartyl-L-phenylalanine methylester alitame,
Citric acid, tartaric acid, malic acid, fumaric acid, ascorbic acid, lactic acid, gluconic acid, phosphoric acid etc.；
The aromatic can be strawberry essential oil, Lavender, lemon, apple essential oil, Rosa Damascana, refined jasmine oil,
Cloud take aromatic, the careless aromatic of sea spirit, santal aromatic, chocolate aromatic, honeydew melon essential oil, grapefruit essential oil, saussurea involucrata essential oil,
Green tea essential oil, cherry essence, pine essential oil, beautiful osmanthus essential oil, honey peach essential oil, rosemary aromatic etc.；
The fragrance or aromatic preferred mass number are 0.7 part；
D, essence is made with conventional techniques in the industry and is coupled paper, defoaming, abatement pressure are concentrated after 0.5~2h of ultrasonic vibration
Phenomenon also makes material evenly laid out, demoulds after 60~200 DEG C, 0.5~6h surface drying and is coupled paper up to essence；It is preferred that ultrasound
Shake 1h, surface drying 3h at 120 DEG C.
Have the normal attribute of paper in traditional sense according to the essence coupling paper of above method preparation, such as writes, can
Fold, can cut out, simultaneously because introduce fragrance or aromatic in paper system, thus paper can also give out it is specific
Taste or smell so that the affinity that paper is certain to people.However fragrance or aromatic are big because of molecular structure and polarity
It is small different, it is difficult to be locked in paper structure, therefore the invention discloses coupling methods that specific coupling agent is blended with pre- paper pulp,
Pre- coupling paper pulp, nucleophilic group on coupling agent, such as double bond, three keys, cyano, amino, hydroxyl, ehter bond is prepared easily and in advance
Electron rich group forms more firm covalent bond in paper pulp, when the pre- coupling paper pulp introduces fragrance or aromatic, coupling agent
The electrophilic group of the upper other side, such as carbonyl, carboxyl, alkyl, acyl group, nitro can be bonded therewith, and will as " chain "
Fragrance or aromatic are firmly locked in paper system.
Technical step analysis of the invention:
(1) it is suitable for be coupled the pre- paper pulp being bonded firstly, obtaining, it can slurrying in several ways:
1. high pressure homogenization method slurrying: during high-pressure homogeneous, the release of pressure energy and high-speed motion crush pulping raw material,
Particle size can be adjusted by pressure energy size, length of time.Control pre- paper pulp solid content in a certain range.
2. acid-hydrolysis method slurrying: it is more mature that the legal system prepares sizing process, adaptable to plurality of raw materials, as needlebush,
Cotton and crudefiber crop epidermis etc..Control pre- paper pulp solid content in a certain range.
3. enzymatic isolation method slurrying: the method working condition is mild, and specificity is strong, and reagent enzyme used and cellulase be can
Regenerated resources, therefore it is of great significance to social sustainable development, prediction enzymatic isolation method will become the hot spot of future studies, but
There is also the drawbacks such as enzyme-deactivating, by-product be more simultaneously, it has to draw attention.Pre- paper pulp solid content is controlled in a certain range
It is interior.
It is worth noting that since its technique is mature already and openly, thus the application be not directed to slurrying application protection and
It is briefly described herein only for production procedure integrality.
(2) secondly, the preparation of coupling paper pulp in advance:
Appropriate pre- paper pulp is taken to be blended with coupling agent, auxiliary agent, certain temperature condition mechanical stirring is uniformly mixed it, and control is certain to be turned
Speed obtains the higher pre- coupling paper pulp of concentration after mixing evenly.
Take the appropriate above-mentioned higher pre- coupling paper pulp of concentration to be blended with a certain amount of pre- paper pulp, mechanical stirring temperature, revolving speed and
Time with it is constant, certain density pre- coupling paper pulp can be obtained.
Coupling agent can be silane coupling agent NXT, VP-Si-363, KH550, KH560 and KH570, be also possible to amino
Silane coupling agent KH-792 etc.；Auxiliary agent can be SiO 2 powder, calcium carbonate powder etc..Pre- coupling paper pulp each component according to
Mass fraction can be with are as follows:
Pre- paper pulp: 60~95 parts；
Coupling agent: 0.5~10 part；
Auxiliary agent: 0.01~5 part.
(3) again, the preparation of essence coupling paper pulp:
Pre- coupling paper pulp described in appropriate (2) is taken to be blended with fragrance or aromatic, certain temperature condition mechanical stirring makes it
It is uniformly mixed, controls revolving speed, obtain the higher essence coupling paper pulp of concentration after mixing evenly.
The higher essence coupling paper pulp of appropriate above-mentioned concentration is taken to be blended with a certain amount of pre- coupling paper pulp, mechanical stirring temperature,
Revolving speed and time with it is constant, certain density pre- coupling paper pulp can be obtained.
The essence can be glucose, fructose, sucrose, maltose, starch sugar, lactose stevioside, Radix Glycyrrhizae, glycyrrhizic acid two
Sodium, tripotassium glycyrrhetate and trisodium, saccharin, saccharin sodium, sodium cyclohexylsulfamate, L-aspartyl-L-phenylalanine methylester alitame,
Citric acid, tartaric acid, malic acid, fumaric acid, ascorbic acid, lactic acid, gluconic acid, phosphoric acid etc.；
The aromatic can be strawberry essential oil, Lavender, lemon, apple essential oil, Rosa Damascana, refined jasmine oil,
Cloud take aromatic, the careless aromatic of sea spirit, santal aromatic, chocolate aromatic, honeydew melon essential oil, grapefruit essential oil, saussurea involucrata essential oil,
Green tea essential oil, cherry essence, pine essential oil, beautiful osmanthus essential oil, honey peach essential oil, rosemary aromatic etc..
It is not difficult to find out that being whether coupled the preparation of slurrying described in (2) in advance, also or essence described in (3) is coupled paper pulp
Preparation, all use stepwise dilution method.It may insure that material is uniformly mixed, not to be related to other dispersion solvents etc. excellent using the method
Point.
Essence is coupled paper pulp each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 60~95 parts；
Fragrance or aromatic: 0.5~8 part.
(4) finally, the preparation of finished product essence coupling paper:
Appropriate (3) described essence coupling paper pulp is taken to be placed in the mold of specific paper making equipment, ultrasonic vibration defoams after a certain period of time,
Cut down pressure concentration phenomenon, also makes material evenly laid out.It is demoulded after certain temperature, certain time surface drying and both obtains finished product essence idol
Join paper.
It is worth noting that since paper pulp papermaking technique is mature already and openly, thus the application is not directed to the step Shen
Please technical protection and be briefly described herein only for production procedure integrality.
Part chemical reagent title that the present invention uses, manufacturer are as follows: Compton Co., Ltd of the U.S. NXT(), VP-
Compton Co., Ltd of the U.S. Si-363(), KH-550(goldschmidt chemical corporation), KH-792(goldschmidt chemical corporation), KH560(Degussa it is public
Department) and KH570(goldschmidt chemical corporation), SiO 2 powder (Jiangyin Guang Yuan Ultramicro-powder Co., Ltd), calcium carbonate powder (Jiangyin
Guang Yuan Ultramicro-powder Co., Ltd), saccharin sodium (Changzhou Bai Yundu Chemical Co., Ltd.), L-aspartyl-L-phenylalanine methylester alitame
(the happy safe food in Henan is limited for (Henan Le Tai Food Co., Ltd), citric acid (Changzhou Bai Yundu Chemical Co., Ltd.), malic acid
Company), fumaric acid (Changzhou Bai Yundu Chemical Co., Ltd.), lactic acid (Changzhou Bai Yundu Chemical Co., Ltd.), gluconic acid
(Changzhou Bai Yundu Chemical Co., Ltd.), strawberry essential oil (Changzhou Bai Yundu Chemical Co., Ltd.), Lavender (are transported in Changzhou hundred
Cross Chemical Co., Ltd.), lemon (Changzhou Bai Yundu Chemical Co., Ltd.), (Changzhou Bai Yundu chemical industry is limited for apple essential oil
Company), Rosa Damascana (Xi'an good harvest Biotechnology Co., Ltd), refined jasmine oil (the limited public affairs of Xi'an good harvest biotechnology
Department), cloud take aromatic (Henan Le Tai Food Co., Ltd), the careless aromatic (Changzhou Bai Yundu Chemical Co., Ltd.) of sea spirit,
Santal aromatic (Henan Le Tai Food Co., Ltd), chocolate aromatic (Henan Le Tai Food Co., Ltd), honeydew melon essential oil
(Henan Le Tai Food Co., Ltd), grapefruit essential oil (Xi'an good harvest Biotechnology Co., Ltd), saussurea involucrata essential oil (Xi'an great Feng
Receive Biotechnology Co., Ltd), green tea essential oil (Henan Le Tai Food Co., Ltd), (the happy safe food in Henan is limited for pine essential oil
Company), beautiful osmanthus essential oil (Xi'an good harvest Biotechnology Co., Ltd), (Xi'an good harvest biotechnology has rosemary aromatic
Limit company).
Beneficial effect
The present invention creatively by fragrance, aromatic etc. by coupling mode be implanted into paper main structure, with it is traditional will be fragrant
Smart agent, aromatic are coated on paper surface and compare, and fragrance, the aromatic attachment fastness for being coupled implantation are stronger, while acid and alkali-resistance
Intensity significantly improves, and heated rear stack paper is not susceptible to be adhered；In addition, fragrance, aromatic on paper retention time compared with
It is long, it is influenced by temperature or wetness smaller.
Specific embodiment
The present invention is described in detail combined with specific embodiments below, and following embodiment will be helpful to the technology of this field
Personnel further understand the present invention, but the invention is not limited in any way.It should be pointed out that those skilled in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Protect scope.
Embodiment 1
(1) firstly, preparing pre- paper pulp, solid content 36g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 50 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring,
3h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 80 parts；
KH550:2.5 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 0.02 part.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 20 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring
It is even, 1.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 90 parts；
Saccharin sodium: 0.7 part.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1h, cut down pressure concentration phenomenon, also make material evenly laid out.It is demoulded after 120 DEG C, 3h surface drying and both obtains finished product
Essence is coupled paper.
Embodiment 2
(1) firstly, preparing pre- paper pulp, solid content 20g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 200r/min mechanical stirring, stirs
Mix 0.5h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 60 parts；
KH550:0.5 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 0.01 part.
(3) again, essence coupling paper pulp is prepared, it is uniformly mixed under 5 DEG C of temperature-controlled conditions, 50r/min mechanical stirring, stirs
Mix 0.2h, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 60 parts；
Saccharin sodium: 0.5 part.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.5h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 60 DEG C, 0.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 3
(1) firstly, preparing pre- paper pulp, solid content 70g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 80 DEG C of temperature-controlled conditions, 3000r/min mechanical stirring,
4h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 95 parts；
KH550:10 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 5 parts.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 60 DEG C of temperature-controlled conditions, 2000r/min mechanical stirring
It is even, 3h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 95 parts；
Saccharin sodium: 8 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 2h, cut down pressure concentration phenomenon, also make material evenly laid out.It is demoulded after 200 DEG C, 6h surface drying and both obtains finished product
Essence is coupled paper.
Embodiment 4
(1) firstly, preparing pre- paper pulp, solid content 55g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 500r/min mechanical stirring, stirs
Mix 1h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 75 parts；
VP-Si-363:4 parts of coupling agent；
500 calcium carbonate powder of auxiliary agent: 0.02 part.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 10 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring
It is even, 0.25h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 85 parts；
Rosa Damascana: 7 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.6h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 150 DEG C, 1.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 5
(1) firstly, preparing pre- paper pulp, solid content 55g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 70 DEG C of temperature-controlled conditions, 400r/min mechanical stirring, stirs
Mix 4h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 66 parts；
NXT:4 parts of coupling agent；
150 mesh SiO 2 powder of auxiliary agent: 5 parts.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 15 DEG C of temperature-controlled conditions, 1500r/min mechanical stirring
It is even, 1h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 65 parts；
Lemon: 5.5 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.2h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 110 DEG C, 3h surface drying both at
Product essence is coupled paper.
Embodiment 6
(1) firstly, preparing pre- paper pulp, solid content 45g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 60 DEG C of temperature-controlled conditions, 400r/min mechanical stirring, stirs
Mix 1.5h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 78 parts；
VP-Si-363:2.2 parts of coupling agent；
120 mesh calcium carbonate powder of auxiliary agent: 2.4 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 100r/min mechanical stirring,
2.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 67 parts；
Rosa Damascana: 4.2 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.8h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 80 DEG C, 4.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 7
(1) firstly, preparing pre- paper pulp, solid content 65g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 70 DEG C of temperature-controlled conditions, 600r/min mechanical stirring, stirs
Mix 2.5h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 80 parts；
KH550:3.3 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 0.02 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 800r/min mechanical stirring,
2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 78 parts；
Chocolate aromatic: 0.6 part.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.2h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 80 DEG C, 5.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 8
(1) firstly, preparing pre- paper pulp, solid content 40g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 55 DEG C of temperature-controlled conditions, 800r/min mechanical stirring, stirs
Mix 3.5h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 69 parts；
KH560:9.7 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 0.03 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 35 DEG C of temperature-controlled conditions, 900r/min mechanical stirring,
1.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 65 parts；
Beautiful osmanthus essential oil: 5.5 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.8h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 140 DEG C, 1h surface drying both at
Product essence is coupled paper.
Embodiment 9
(1) firstly, preparing pre- paper pulp, solid content 70g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 2500r/min mechanical stirring,
4h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 68 parts；
KH570:9.7 parts of coupling agent；
800 mesh SiO 2 powder of auxiliary agent: 3.4 parts.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 60 DEG C of temperature-controlled conditions, 1800r/min mechanical stirring
It is even, 0.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 80 parts；
Pine essential oil: 2 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.6h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 120 DEG C, 3.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 10
(1) firstly, preparing pre- paper pulp, solid content 40g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring,
4h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 80 parts；
KH-550:4.4 parts of coupling agent；
150 mesh SiO 2 powder of auxiliary agent: 2 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 55 DEG C of temperature-controlled conditions, 700r/min mechanical stirring,
1.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 70 parts；
Refined jasmine oil: 3 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.2h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 100 DEG C, 2.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 11
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 55 DEG C of temperature-controlled conditions, 900r/min mechanical stirring, stirs
Mix 2h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 77 parts；
KH-792:5 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 0.04 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 12 DEG C of temperature-controlled conditions, 600r/min mechanical stirring,
1.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 77 parts；
Green tea essential oil: 6 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.2h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 80 DEG C, 2h surface drying both at
Product essence is coupled paper.
Embodiment 12
(1) firstly, preparing pre- paper pulp, solid content 65g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 1500r/min mechanical stirring,
4h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 67 parts；
KH-792:2 parts of coupling agent；
500 mesh calcium carbonate powder of auxiliary agent: 4 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 18 DEG C of temperature-controlled conditions, 300r/min mechanical stirring,
2.8h is stirred, each component can be with according to mass fraction are as follows:
Malic acid: 7.9 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.8h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 120 DEG C, 5h surface drying both at
Product essence is coupled paper.
Embodiment 13
(1) firstly, preparing pre- paper pulp, solid content 38g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 35 DEG C of temperature-controlled conditions, 400r/min mechanical stirring, stirs
Mix 0.5h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 67 parts；
VP-Si-363:5.6 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 4.6 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 25 DEG C of temperature-controlled conditions, 200r/min mechanical stirring,
1.6h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 77 parts；
L-aspartyl-L-phenylalanine methylester alitame: 7 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.8h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 150 DEG C, 4h surface drying both at
Product essence is coupled paper.
Embodiment 14
(1) firstly, preparing pre- paper pulp, solid content 60g/m3.
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 70 DEG C of temperature-controlled conditions, 770r/min mechanical stirring, stirs
Mix 4h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 65 parts；
KH570:3 parts of coupling agent；
800 mesh SiO 2 powder of auxiliary agent: 0.05 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 100r/min mechanical stirring,
0.4h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 70 parts；
Honeydew melon essential oil: 5.9 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.9h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 180 DEG C, 0.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 15
(1) firstly, preparing pre- paper pulp, solid content 42g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 1200r/min mechanical stirring,
2.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 68 parts；
KH-792:5 parts of coupling agent；
80 mesh SiO 2 powder of auxiliary agent: 5 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 800r/min mechanical stirring,
1.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 78 parts；
Santal aromatic: 2 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 170 DEG C, 0.5h surface drying both at
Product essence is coupled paper.
Embodiment 16
(1) firstly, preparing pre- paper pulp, solid content 38g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 1800r/min mechanical stirring,
1.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 66 parts；
KH570:2 parts of coupling agent；
120 mesh SiO 2 powder of auxiliary agent: 0.2 part.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 10 DEG C of temperature-controlled conditions, 1800r/min mechanical stirring
It is even, 2.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 78 parts；
Radix Glycyrrhizae: 4.4 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.6h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 190 DEG C, 0.8h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 17
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 40 DEG C of temperature-controlled conditions, 2500r/min mechanical stirring,
2h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 76 parts；
VP-Si-363:6 parts of coupling agent；
150 mesh calcium carbonate powder of auxiliary agent: 0.6 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 15 DEG C of temperature-controlled conditions, 100r/min mechanical stirring,
2.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 83 parts；
Honeydew melon essential oil: 5.9 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.5h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 130 DEG C, 6h surface drying both at
Product essence is coupled paper.
Embodiment 18
(1) firstly, preparing pre- paper pulp, solid content 43g/m3。
(2) it secondly, preparation is pre- to be coupled paper pulp, is uniformly mixed it under 60 DEG C of temperature-controlled conditions, 450r/min mechanical stirring, stirs
Mix 1.2h, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 61 parts；
KH-792:5.3 parts of coupling agent；
50 mesh SiO 2 powder of auxiliary agent: 3.2 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 400r/min mechanical stirring,
2.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 84 parts；
Green tea essential oil: 4 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.5h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 140 DEG C, 1.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 19
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 40 DEG C of temperature-controlled conditions, 2800r/min mechanical stirring,
3.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 68 parts；
KH550:5.3 parts of coupling agent；
1500 mesh SiO 2 powder of auxiliary agent: 0.02 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 45 DEG C of temperature-controlled conditions, 800r/min mechanical stirring,
2.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 89 parts；
Saccharin sodium: 3.4 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.5h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 60 DEG C, 6h surface drying both at
Product essence is coupled paper.
Embodiment 20
(1) firstly, preparing pre- paper pulp, solid content 36g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 60 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring,
3h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 77 parts；
KH-792:0.8 parts of coupling agent；
50 mesh calcium carbonate powder of auxiliary agent: 0.9 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 800r/min mechanical stirring,
1.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 67 parts；
Santal aromatic: 6 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.5h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 190 DEG C, 1h surface drying both at
Product essence is coupled paper.
Embodiment 21
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 60 DEG C of temperature-controlled conditions, 2200r/min mechanical stirring,
0.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 80 parts；
NXT:9 parts of coupling agent；
50 mesh calcium carbonate powder of auxiliary agent: 0.04 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 12 DEG C of temperature-controlled conditions, 90r/min mechanical stirring,
2.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 78 parts；
Hai Lingcao aromatic: 2 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.2h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 160 DEG C, 5h surface drying both at
Product essence is coupled paper.
Embodiment 22
(1) firstly, preparing pre- paper pulp, solid content 48g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring,
0.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 66 parts；
KH560:7 parts of coupling agent；
1500 mesh calcium carbonate powder of auxiliary agent: 0.9 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 100r/min mechanical stirring,
0.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 66 parts；
Pine essential oil: 3 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.5h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 80 DEG C, 6h surface drying both at
Product essence is coupled paper.
Embodiment 23
(1) firstly, preparing pre- paper pulp, solid content 38g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 80 DEG C of temperature-controlled conditions, 2200r/min mechanical stirring,
0.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 88 parts；
KH560:9 parts of coupling agent；
1500 mesh calcium carbonate powder of auxiliary agent: 4 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 200r/min mechanical stirring,
1.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 66 parts；
Green tea essential oil: 6 parts.
Wherein, coupling paper pulp preferred mass number is 90 parts in advance；
(4) finished paper, ultrasound shake are prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City)
Defoaming, abatement pressure concentration phenomenon, also make material evenly laid out after dynamic 1.2h.It is demoulded after 90 DEG C, 0.5h surface drying and both obtains finished product
Essence is coupled paper.
Embodiment 24
(1) firstly, preparing pre- paper pulp, solid content 55g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 1400r/min mechanical stirring,
2.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 66 parts；
KH-792:4 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 1 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 55 DEG C of temperature-controlled conditions, 80r/min mechanical stirring,
1.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 88 parts；
Grapefruit essential oil: 4 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.5h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 100 DEG C, 4h surface drying both at
Product essence is coupled paper.
Embodiment 25
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 65 DEG C of temperature-controlled conditions, 2400r/min mechanical stirring,
3.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 66 parts；
NXT:0.6 parts of coupling agent；
800 mesh SiO 2 powder of auxiliary agent: 0.02 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 30 DEG C of temperature-controlled conditions, 500r/min mechanical stirring,
2.0h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 66 parts；
L-aspartyl-L-phenylalanine methylester alitame: 0.8 part.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.5h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 90 DEG C, 0.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 26
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 75 DEG C of temperature-controlled conditions, 1500r/min mechanical stirring,
0.5h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 70 parts；
KH-550:6 parts of coupling agent；
500 mesh SiO 2 powder of auxiliary agent: 0.04 part.
(3) again, essence coupling paper pulp is prepared, keeps its mixing equal under 40 DEG C of temperature-controlled conditions, 1500r/min mechanical stirring
It is even, 2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 71 parts；
Lavender: 0.9 part.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.51h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 180 DEG C, 4h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 27
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 75 DEG C of temperature-controlled conditions, 2100r/min mechanical stirring,
3.6h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 67 parts；
KH570:5.9 parts of coupling agent；
1000 mesh SiO 2 powder of auxiliary agent: 4.3 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 400r/min mechanical stirring,
1.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 67 parts；
Fumaric acid: 5.9 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1h, cut down pressure concentration phenomenon, also make material evenly laid out.It is demoulded after 190 DEG C, 6h surface drying and both obtains finished product
Essence is coupled paper.
Embodiment 28
(1) firstly, preparing pre- paper pulp, solid content 54g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 35 DEG C of temperature-controlled conditions, 1800r/min mechanical stirring,
4h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 93 parts；
VP-Si-363:0.7 parts of coupling agent；
100 mesh SiO 2 powder of auxiliary agent: 0.09 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 10 DEG C of temperature-controlled conditions, 500r/min mechanical stirring,
2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 80 parts；
Gluconic acid: 5 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.9h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 200 DEG C, 0.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 29
(1) firstly, preparing pre- paper pulp, solid content 56g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 45 DEG C of temperature-controlled conditions, 1000r/min mechanical stirring,
2h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 70 parts；
KH-792:4 parts of coupling agent；
800 mesh SiO 2 powder of auxiliary agent: 3 parts.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 20 DEG C of temperature-controlled conditions, 440r/min mechanical stirring,
1.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 68 parts；
Sodium cyclohexylsulfamate: 7 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 1.5h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 120 DEG C, 0.5h surface drying and both obtained
Finished product essence is coupled paper.
Embodiment 30
(1) firstly, preparing pre- paper pulp, solid content 22g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 35 DEG C of temperature-controlled conditions, 1200r/min mechanical stirring,
2h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 80 parts；
KH-550:9 parts of coupling agent；
900 mesh SiO 2 powder of auxiliary agent: 0.09 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 35 DEG C of temperature-controlled conditions, 100r/min mechanical stirring,
1.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 70 parts；
L-aspartyl-L-phenylalanine methylester alitame: 0.51 part.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.5h, cut down pressure concentration phenomenon, also make material evenly laid out.Demoulded after 200 DEG C, 6h surface drying both at
Product essence is coupled paper.
Embodiment 31
(1) firstly, preparing pre- paper pulp, solid content 66g/m3。
(2) secondly, preparation is pre- to be coupled paper pulp, it is uniformly mixed it under 50 DEG C of temperature-controlled conditions, 1500r/min mechanical stirring,
0.8h is stirred, each component can be with according to mass fraction are as follows:
Pre- paper pulp: 70 parts；
KH-792:0.9 parts of coupling agent；
80 mesh calcium carbonate powder of auxiliary agent: 0.04 part.
(3) again, essence coupling paper pulp is prepared, is uniformly mixed it under 55 DEG C of temperature-controlled conditions, 800r/min mechanical stirring,
2.2h is stirred, each component can be with according to mass fraction are as follows:
Pre- coupling paper pulp: 77 parts；
Saccharin: 6 parts.
(4) finished paper is prepared using professional paper making equipment (787-4600 type paper machine, Yong Hui machinery plant of Qinyang City), surpassed
It defoamed after acoustic vibration 0.5h, cut down pressure concentration phenomenon, also make material evenly laid out.It demoulds after 200 DEG C, 0.5h surface drying and both obtained
Finished product essence is coupled paper.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent structure or equivalent flow shift made by bright specification is applied directly or indirectly in other relevant technical fields,
Similarly it is included within the scope of the present invention.
Claims (10)
1. a kind of preparation method of essence coupling paper, which comprises the steps of:
A, pre- paper pulp is made with conventional techniques in the industry, wherein 20~70g/m of solid content of the pre- paper pulp3, preferably 36g/
m3；
B, according to the ratio of 60~95 parts of the pre- paper pulp of mass fraction, 0.5~10 part of coupling agent, 0.01~5 part of auxiliary agent, 10~
80 DEG C, 200~3000r/min mechanical stirring be uniformly mixed it, pre- coupling paper pulp is made after stirring 0.5~4h；
Wherein, the coupling agent is silane coupling agent NXT, VP-Si-363, KH550, KH560 or KH570；
The auxiliary agent is the powder in 50~1500 mesh numbers；
C, 60~95 parts of paper pulp, fragrance or 0.5~8 part of aromatic of ratio are coupled in advance according to mass fraction, 5~60 DEG C,
50~2000r/min mechanical stirring is uniformly mixed it, and essence coupling paper pulp is made after stirring 0.2~3h,
Wherein,
The fragrance is glucose, fructose, sucrose, maltose, starch sugar, lactose stevioside, Radix Glycyrrhizae, disodium glycyrrhizinate, sweet
Oxalic acid tripotassium and trisodium, saccharin, saccharin sodium, sodium cyclohexylsulfamate, L-aspartyl-L-phenylalanine methylester alitame, lemon
Acid, tartaric acid, malic acid, fumaric acid, ascorbic acid, lactic acid, gluconic acid, phosphoric acid etc.；
The aromatic is strawberry essential oil, Lavender, lemon, apple essential oil, Rosa Damascana, refined jasmine oil, cloud
By aromatic, sea spirit careless aromatic, santal aromatic, chocolate aromatic, honeydew melon essential oil, grapefruit essential oil, saussurea involucrata essential oil, green tea
Essential oil, cherry essence, pine essential oil, beautiful osmanthus essential oil, honey peach essential oil, rosemary aromatic etc.；
D, essence is made with conventional techniques in the industry and is coupled paper, defoaming, abatement pressure are concentrated after 0.5~2h of ultrasonic vibration
Phenomenon also makes material evenly laid out, demoulds after 60~200 DEG C, 0.5~6h surface drying to obtain the final product.
2. the preparation method of essence coupling paper according to claim 1, it is characterised in that: pre- paper pulp consolidates described in step A
Content is 36g/m3。
3. the preparation method of essence coupling paper according to claim 1, it is characterised in that: according to mass parts described in step B
The ratio of pre- 80 parts of the paper pulp of number, 2.5 parts of coupling agent, 0.02 part of auxiliary agent keeps its mixing equal in 50 DEG C, 1000r/min mechanical stirring
It is even, pre- coupling paper pulp is made after stirring 3h.
4. the preparation method of essence coupling paper according to claim 1, it is characterised in that: coupling agent described in step B is ammonia
Base silane class coupling agent KH-792.
5. the preparation method of essence coupling paper according to claim 1, it is characterised in that: coupling agent described in step B is silicon
Alkanes coupling agent KH550.
6. the preparation method of essence coupling paper according to claim 1, it is characterised in that: auxiliary agent described in step B is dioxy
SiClx powder, calcium carbonate powder etc..
7. the preparation method of essence coupling paper according to claim 1, it is characterised in that: auxiliary agent described in step B is 500 mesh
SiO 2 powder.
8. the preparation method of essence coupling paper according to claim 1, it is characterised in that: according to mass parts described in step C
Pre- 90 parts of the paper pulp of coupling of number, fragrance or 0.7 part of aromatic of ratio keep its mixing equal in 20 DEG C, 1000r/min mechanical stirring
It is even, essence coupling paper pulp is made after stirring 1.5h.
9. the preparation method of essence coupling paper according to claim 1, it is characterised in that: with usual in the industry described in step D
Technological means is made essence and is coupled paper, and defoaming, abatement pressure concentration phenomenon, also make material evenly laid out after ultrasonic vibration 1h,
It is demoulded after 120 DEG C, 3h surface drying to obtain the final product.
10. essence made from -9 any claim the methods is coupled paper according to claim 1.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110578266A (en) * | 2019-09-04 | 2019-12-17 | 泰中特种纸有限公司 | Special paper with low hygroexpansivity and high recovery and preparation method thereof |
| CN111721737A (en) * | 2020-06-15 | 2020-09-29 | 上海应用技术大学 | Characterization method for researching interaction mechanism of slow-release essence nanoparticles and paper |
| CN114713076A (en) * | 2022-05-06 | 2022-07-08 | 日照华泰纸业有限公司 | Paper pulp mediation device |
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| CN87106213A (en) * | 1986-09-09 | 1988-03-23 | 纳幕尔杜邦公司 | Fill composition and the application in wood fiber paper is made thereof |
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| CN105350389A (en) * | 2015-11-04 | 2016-02-24 | 铜陵三佳变压器有限责任公司 | Multi-purpose insulation paper for transformers |
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| CN110578266A (en) * | 2019-09-04 | 2019-12-17 | 泰中特种纸有限公司 | Special paper with low hygroexpansivity and high recovery and preparation method thereof |
| CN111721737A (en) * | 2020-06-15 | 2020-09-29 | 上海应用技术大学 | Characterization method for researching interaction mechanism of slow-release essence nanoparticles and paper |
| CN114713076A (en) * | 2022-05-06 | 2022-07-08 | 日照华泰纸业有限公司 | Paper pulp mediation device |
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