CN109137519A - A method of promoting non-woven fabrics anti-pollution characteristic - Google Patents
A method of promoting non-woven fabrics anti-pollution characteristic Download PDFInfo
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- CN109137519A CN109137519A CN201810961152.6A CN201810961152A CN109137519A CN 109137519 A CN109137519 A CN 109137519A CN 201810961152 A CN201810961152 A CN 201810961152A CN 109137519 A CN109137519 A CN 109137519A
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- woven fabrics
- pollution characteristic
- fouling coatings
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
- D06M15/277—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof containing fluorine
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/34—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxygen, ozone or ozonides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
- D06M13/148—Polyalcohols, e.g. glycerol or glucose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/01—Stain or soil resistance
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention discloses a kind of method for promoting non-woven fabrics anti-pollution characteristic, including following operating procedure: (1) will prepare after molding nonwoven surface cleans up, surface oxidation treatment is carried out using ozone, then it puts it into soak, after immersion treatment 3-4 hours, it takes out and cleans surface, modification nonwoven cloth is made；(2) waterborne anti-fouling coatings are sprayed on modification nonwoven cloth surface again, put it into baking oven later, after drying and processing, finished product.A kind of method promoting non-woven fabrics anti-pollution characteristic provided by the invention, easy to operate, environmentally protective, non-woven fabrics obtained, anti-pollution characteristic is excellent, and grease stain and grieshoch are not easy to deposit on its surface, greatly extends its service life.
Description
Technical field
The invention belongs to non-woven fabrics preparation technical fields, and in particular to a method of promote non-woven fabrics anti-pollution characteristic.
Background technique
Non-woven fabrics is a kind of non-woven cloth, it is that fiber is directly passed through gas using high polymer slice, staple fiber or long filament
Then spun lacing is passed through in stream or mechanical networking, needle thorn or hot rolling are reinforced, the non-woven cloth finally formed by final finishing.Tool
There is soft, ventilative and planar structure tencel product, advantage is not generate Soft flocks, it is tough, durable, silky soft,
It is one kind of reinforcing material, and there are also the feelings of cotton to compare with cotton goods, the sack of non-woven fabrics is easily formed, Er Qiezao
Valence is cheap.But non-woven fabrics obtained in the prior art, anti-pollution characteristic is poor, causes its service life shorter.
Summary of the invention
In order to solve the above technical problem, the present invention provides a kind of methods for promoting non-woven fabrics anti-pollution characteristic.
The present invention is achieved by the following technical solutions.
A method of promoting non-woven fabrics anti-pollution characteristic, including following operating procedure:
(1) it will prepare after molding nonwoven surface cleans up, surface oxidation treatment carried out using ozone, is then put it into
In soak, after immersion treatment 3-4 hours, takes out and clean surface, modification nonwoven cloth is made, wherein soak is by following parts by weight
Component be made: 17-22 parts of sodium borohydride, 9-13 parts of sodium phytate, pentanediol 10-15 parts of season, 200-250 parts of water；
(2) waterborne anti-fouling coatings are sprayed on modification nonwoven cloth surface again, put it into baking oven later, after drying and processing, is made
Finished product, wherein waterborne anti-fouling coatings are made of the component of following parts by weight: 25-30 parts of allyl acrylate, acrylic acid glycerin ether
10-15 parts of ester, 18-22 parts of acrylic acid octafluoro pentyl ester, 0.1-0.3 parts of initiator, 3-6 parts of Dimethicone, triethanolamine oil
1-3 parts of acid esters, 40-50 parts of deionized water.
Specifically, in above-mentioned steps (1), when ozone treatment, the concentration of ozone is 80-90ppm, and the time of ozone treatment is
20-30min。
Specifically, in above-mentioned steps (2), waterborne anti-fouling coatings are made of following methods: by Dimethicone, three second
Hydramine oleate is added into deionized water, and after being mixed evenly, emulsification system is made, is then added thereto: acrylic acid
Allyl ester, acrylic acid glycerol ether-ether, acrylic acid octafluoro pentyl ester, after being mixed evenly, under nitrogen protection, are heated to
85-90 DEG C, initiator is then added thereto, after isothermal holding 3-4 hours, waterborne anti-fouling coatings are made.
Specifically, the initiator is methyl ethyl ketone peroxide, any one in cyclohexanone peroxide.
Specifically, in above-mentioned steps (2), the fountain height 450-500g/m of waterborne anti-fouling coatings2。
From the above technical scheme, it can be seen that the beneficial effects of the present invention are:
A kind of method promoting non-woven fabrics anti-pollution characteristic provided by the invention, easy to operate, environmentally protective, non-woven fabrics obtained,
Anti-pollution characteristic is excellent, and grease stain and grieshoch are not easy to deposit on its surface, greatly extends its service life.Wherein, of the invention
After carrying out oxidation processes to non-woven fabrics using ozone, a large amount of peroxy-radical of Surface Creation, then made by the modified of soak
With can effectively promote waterborne anti-fouling coatings in the adhesion strength on its surface, simultaneously in a large amount of activity hydroxy of its Surface Creation
The uniformity of distribution of the waterborne anti-fouling coatings on its surface can also be promoted and unfold effect, can further promote the antifouling of non-woven fabrics
Performance can effectively enhance the reduction effect of sodium borohydride, facilitate boron hydrogen after wherein sodium phytate and season pentanediol act synergistically
The peroxy-radical for changing sodium and nonwoven surface is effectively combined；Waterborne anti-fouling coatings in step (2) can be in nonwoven after dry
The lower film layer of cloth Surface Creation surface energy, can effectively reduce grease stain and grieshoch in the adhesion strength on its surface, while itself and nothing
The activity hydroxy combination fastness on woven fabric surface is high, will not influence the original mechanical property of non-woven fabrics and pliability.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person carries out according to conventional conditions or manufacturer's recommended conditions.Reagents or instruments used without specified manufacturer is
The conventional products that can be obtained by commercially available purchase.
Embodiment 1
A method of promoting non-woven fabrics anti-pollution characteristic, including following operating procedure:
(1) it will prepare after molding nonwoven surface cleans up, surface oxidation treatment carried out using ozone, is then put it into
In soak, after immersion treatment 3 hours, takes out and clean surface, modification nonwoven cloth is made, wherein soak is by following parts by weight
Component is made: 17 parts of sodium borohydride, 9 parts of sodium phytate, 10 parts of season pentanediol, 200 parts of water；
(2) waterborne anti-fouling coatings are sprayed on modification nonwoven cloth surface again, put it into baking oven later, after drying and processing, is made
Finished product, wherein waterborne anti-fouling coatings are made of the component of following parts by weight: 25 parts of allyl acrylate, acrylic acid glycerol ether-ether 10
Part, 18 parts of acrylic acid octafluoro pentyl ester, 0.1 part of initiator, 3 parts of Dimethicone, 1 part of Emulphor FM, deionized water
40 parts.
Specifically, in above-mentioned steps (1), when ozone treatment, the concentration of ozone is 80ppm, and the time of ozone treatment is
20min。
Specifically, in above-mentioned steps (2), waterborne anti-fouling coatings are made of following methods: by Dimethicone, three second
Hydramine oleate is added into deionized water, and after being mixed evenly, emulsification system is made, is then added thereto: acrylic acid
Allyl ester, acrylic acid glycerol ether-ether, acrylic acid octafluoro pentyl ester, after being mixed evenly, under nitrogen protection, are heated to 85
DEG C, initiator is then added thereto, after isothermal holding 3 hours, waterborne anti-fouling coatings are made.
Specifically, the initiator is methyl ethyl ketone peroxide.
Specifically, in above-mentioned steps (2), the fountain height 450g/m of waterborne anti-fouling coatings2。
Embodiment 2
A method of promoting non-woven fabrics anti-pollution characteristic, including following operating procedure:
(1) it will prepare after molding nonwoven surface cleans up, surface oxidation treatment carried out using ozone, is then put it into
In soak, after immersion treatment 3.5 hours, takes out and clean surface, modification nonwoven cloth is made, wherein soak is by following parts by weight
Component be made: 20 parts of sodium borohydride, 11 parts of sodium phytate, 13 parts of season pentanediol, 230 parts of water；
(2) waterborne anti-fouling coatings are sprayed on modification nonwoven cloth surface again, put it into baking oven later, after drying and processing, is made
Finished product, wherein waterborne anti-fouling coatings are made of the component of following parts by weight: 28 parts of allyl acrylate, acrylic acid glycerol ether-ether 13
Part, 20 parts of acrylic acid octafluoro pentyl ester, 0.2 part of initiator, 5 parts of Dimethicone, 2 parts of Emulphor FM, deionized water
45 parts.
Specifically, in above-mentioned steps (1), when ozone treatment, the concentration of ozone is 85ppm, and the time of ozone treatment is
25min。
Specifically, in above-mentioned steps (2), waterborne anti-fouling coatings are made of following methods: by Dimethicone, three second
Hydramine oleate is added into deionized water, and after being mixed evenly, emulsification system is made, is then added thereto: acrylic acid
Allyl ester, acrylic acid glycerol ether-ether, acrylic acid octafluoro pentyl ester, after being mixed evenly, under nitrogen protection, are heated to 88
DEG C, initiator is then added thereto, after isothermal holding 3.5 hours, waterborne anti-fouling coatings are made.
Specifically, the initiator is cyclohexanone peroxide.
Specifically, in above-mentioned steps (2), the fountain height 480g/m of waterborne anti-fouling coatings2。
Embodiment 3
A method of promoting non-woven fabrics anti-pollution characteristic, including following operating procedure:
(1) it will prepare after molding nonwoven surface cleans up, surface oxidation treatment carried out using ozone, is then put it into
In soak, after immersion treatment 4 hours, takes out and clean surface, modification nonwoven cloth is made, wherein soak is by following parts by weight
Component is made: 22 parts of sodium borohydride, 13 parts of sodium phytate, 15 parts of season pentanediol, 250 parts of water；
(2) waterborne anti-fouling coatings are sprayed on modification nonwoven cloth surface again, put it into baking oven later, after drying and processing, is made
Finished product, wherein waterborne anti-fouling coatings are made of the component of following parts by weight: 30 parts of allyl acrylate, acrylic acid glycerol ether-ether 15
Part, 22 parts of acrylic acid octafluoro pentyl ester, 0.3 part of initiator, 6 parts of Dimethicone, 3 parts of Emulphor FM, deionized water
50 parts.
Specifically, in above-mentioned steps (1), when ozone treatment, the concentration of ozone is 90ppm, and the time of ozone treatment is
30min。
Specifically, in above-mentioned steps (2), waterborne anti-fouling coatings are made of following methods: by Dimethicone, three second
Hydramine oleate is added into deionized water, and after being mixed evenly, emulsification system is made, is then added thereto: acrylic acid
Allyl ester, acrylic acid glycerol ether-ether, acrylic acid octafluoro pentyl ester, after being mixed evenly, under nitrogen protection, are heated to 90
DEG C, initiator is then added thereto, after isothermal holding 4 hours, waterborne anti-fouling coatings are made.
Specifically, the initiator is cyclohexanone peroxide.
Specifically, in above-mentioned steps (2), the fountain height 500g/m of waterborne anti-fouling coatings2。
Comparative example 1
Non-woven fabrics is handled without the mode of step (1), remaining operating procedure is identical with embodiment 1.
Respectively with the non-woven fabrics of each embodiment and comparative example, water contact angle and the vegetable oil contact on its surface are then tested
Angle, test result are as shown in table 1:
1 non-woven fabrics resistant measure of merit of table
As shown in Table 1, non-woven fabrics made from the present embodiment, water contact angle and oily contact angle are larger, and surface can be low, and anti-fouling effect is aobvious
It writes.
Although illustrate and describing the present invention with specific embodiment, it will be appreciated that without departing substantially from of the invention
Many other change and modification can be made in the case where spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (5)
1. a kind of method for promoting non-woven fabrics anti-pollution characteristic, which is characterized in that including following operating procedure:
(1) it will prepare after molding nonwoven surface cleans up, surface oxidation treatment carried out using ozone, is then put it into
In soak, after immersion treatment 3-4 hours, takes out and clean surface, modification nonwoven cloth is made, wherein soak is by following parts by weight
Component be made: 17-22 parts of sodium borohydride, 9-13 parts of sodium phytate, pentanediol 10-15 parts of season, 200-250 parts of water；
(2) waterborne anti-fouling coatings are sprayed on modification nonwoven cloth surface again, put it into baking oven later, after drying and processing, is made
Finished product, wherein waterborne anti-fouling coatings are made of the component of following parts by weight: 25-30 parts of allyl acrylate, acrylic acid glycerin ether
10-15 parts of ester, 18-22 parts of acrylic acid octafluoro pentyl ester, 0.1-0.3 parts of initiator, 3-6 parts of Dimethicone, triethanolamine oil
1-3 parts of acid esters, 40-50 parts of deionized water.
2. a kind of method for promoting non-woven fabrics anti-pollution characteristic according to claim 1, which is characterized in that above-mentioned steps (1)
In, when ozone treatment, the concentration of ozone is 80-90ppm, and the time of ozone treatment is 20-30min.
3. a kind of method for promoting non-woven fabrics anti-pollution characteristic according to claim 1, which is characterized in that above-mentioned steps (2)
In, waterborne anti-fouling coatings are made of following methods: Dimethicone, Emulphor FM are added to deionized water
In, after being mixed evenly, emulsification system is made, is then added thereto: allyl acrylate, acrylic acid glycerol ether-ether, third
Olefin(e) acid octafluoro pentyl ester after being mixed evenly, under nitrogen protection, is heated to 85-90 DEG C, is then added and causes thereto
After isothermal holding 3-4 hours, waterborne anti-fouling coatings are made in agent.
4. a kind of method for promoting non-woven fabrics anti-pollution characteristic according to claim 1 or 3, which is characterized in that the initiation
Agent is methyl ethyl ketone peroxide, any one in cyclohexanone peroxide.
5. a kind of method for promoting non-woven fabrics anti-pollution characteristic according to claim 1, which is characterized in that above-mentioned steps (2)
In, the fountain height 450-500g/m of waterborne anti-fouling coatings2。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810961152.6A CN109137519A (en) | 2018-08-22 | 2018-08-22 | A method of promoting non-woven fabrics anti-pollution characteristic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810961152.6A CN109137519A (en) | 2018-08-22 | 2018-08-22 | A method of promoting non-woven fabrics anti-pollution characteristic |
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| Publication Number | Publication Date |
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| CN109137519A true CN109137519A (en) | 2019-01-04 |
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ID=64790808
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| Application Number | Title | Priority Date | Filing Date |
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| CN201810961152.6A Pending CN109137519A (en) | 2018-08-22 | 2018-08-22 | A method of promoting non-woven fabrics anti-pollution characteristic |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113026374A (en) * | 2021-03-04 | 2021-06-25 | 杭州新福华无纺布有限公司 | Dirt-resistant non-woven fabric and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039957A (en) * | 1988-07-30 | 1990-02-28 | 袁介琪 | The antistaling agent that contains the food of animal protein |
| CN1055556A (en) * | 1990-03-31 | 1991-10-23 | 雷学军 | The production technique of sodium phytate, phytic acid zinc |
| CN1865364A (en) * | 2006-06-22 | 2006-11-22 | 华东理工大学 | Pigment carbon black neutral pen ink and its preparation method |
| CN101390553A (en) * | 2008-10-15 | 2009-03-25 | 福建南海食品有限公司 | Debitterized honey pomelo tea and production method thereof |
| CN108004770A (en) * | 2017-12-12 | 2018-05-08 | 马鞍山市鑫程纳米新材料科技有限公司 | A kind of preparation method filtered with resistant non-woven fabrics |
-
2018
- 2018-08-22 CN CN201810961152.6A patent/CN109137519A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039957A (en) * | 1988-07-30 | 1990-02-28 | 袁介琪 | The antistaling agent that contains the food of animal protein |
| CN1055556A (en) * | 1990-03-31 | 1991-10-23 | 雷学军 | The production technique of sodium phytate, phytic acid zinc |
| CN1865364A (en) * | 2006-06-22 | 2006-11-22 | 华东理工大学 | Pigment carbon black neutral pen ink and its preparation method |
| CN101390553A (en) * | 2008-10-15 | 2009-03-25 | 福建南海食品有限公司 | Debitterized honey pomelo tea and production method thereof |
| CN108004770A (en) * | 2017-12-12 | 2018-05-08 | 马鞍山市鑫程纳米新材料科技有限公司 | A kind of preparation method filtered with resistant non-woven fabrics |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113026374A (en) * | 2021-03-04 | 2021-06-25 | 杭州新福华无纺布有限公司 | Dirt-resistant non-woven fabric and preparation method thereof |
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Application publication date: 20190104 |