CN109135626A - One kind exempting from roasting and exempts to shine quick-drying fireworks reel glue - Google Patents
One kind exempting from roasting and exempts to shine quick-drying fireworks reel glue Download PDFInfo
- Publication number
- CN109135626A CN109135626A CN201811000692.4A CN201811000692A CN109135626A CN 109135626 A CN109135626 A CN 109135626A CN 201811000692 A CN201811000692 A CN 201811000692A CN 109135626 A CN109135626 A CN 109135626A
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- CN
- China
- Prior art keywords
- weight
- parts
- dosage
- glue
- drying
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J129/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Adhesives based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Adhesives based on derivatives of such polymers
- C09J129/14—Homopolymers or copolymers of acetals or ketals obtained by polymerisation of unsaturated acetals or ketals or by after-treatment of polymers of unsaturated alcohols
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
Abstract
Exempt from roasting the invention discloses one kind to exempt to shine quick-drying fireworks reel glue.Feature is: by following component and weight fraction ratio processing preparation, 132 parts by weight of polyvinyl alcohol；400 parts by weight of formalin；28 parts by weight of urea；8 parts by weight of hydrochloric acid；7 parts by weight of ammonium carbonate；Sodium hydroxide q.s.；1000 parts by weight of water；The outer plus moisture-proof volatilization glue 10-20 parts by weight in above-mentioned component.Above-mentioned component is made through stock mixing, immersion, stirring, heat temperature raising neutralization, heat preservation, impurity elimination, has reel drying time short, production short time limit, and the good advantage of fluency is processed in no three wastes dip dyeing.
Description
Technical field
Exempt from roasting the present invention relates to one kind to exempt to shine quick-drying fireworks reel glue.
Background technique
In the prior art, it after firworks string gun barrel roll-forming, requires to use or be put in storage storage by drying or drying
It is standby stand-by, the main reason is that the moisture content in traditional glue is more, it is necessary to dry or dry and be attached in the glue of paper tube surface layer
Moisture, not so certain intensity is not achieved in chart drum, and the paper tube not being completely dried also influence its storage deposit, especially
To the meeting moldy metamorphism of fireworks finished product made of not dry powder charge, product quality and firework display effect are seriously affected, manufacturing enterprise is caused to pass through
Ji loss.And since chart drum needs fire or electricity to dry in rainy weather, making chart drum, the production cost increases, produces sometimes
Enterprise influences the normal production of firework product because paper tube is dried not in time.For this purpose, being badly in need of seeking a kind of cigarette that can exempt from roasting and exempt to shine
Steamed twisted roll cylinder glue.
Summary of the invention
The purpose of the present invention is the conventional formulation technology used in the fireworks reel glue in the prior art there are aiming at the problem that, mention
One kind exempts from roasting and exempts to shine quick-drying fireworks reel glue out, and it is absolutely dry which can reach nature in a short time, long-time storage
It will not go mouldy and soften rotten effect.
The purpose of the present invention can be realized by following technical solution:
One kind exempting from roasting and exempts to shine quick-drying fireworks reel glue, is characterized in that: it is by following component and weight fraction ratio processing system
It is standby, it may be assumed that
Polyvinyl alcohol: dosage is 132 parts by weight；
Formalin: dosage is 400 parts by weight；
Urea: dosage is 28 parts by weight；
Hydrochloric acid: dosage is 8 parts by weight；
Ammonium carbonate: dosage is 7 parts by weight；
Sodium hydroxide: appropriate；
Water: dosage is 1000 parts by weight；
The outer plus moisture-proof volatilization glue in above-mentioned component: 10-20 parts by weight.
Specifically include following process steps:
1. stocking up, weighs and be equipped with by the raw material weight number of above-mentioned component；
2. impregnating, the formalin that polyvinyl alcohol content is 36% is impregnated at normal temperature；
3. stirring addition component, is sufficiently stirred at normal temperatures and pressures and is slowly added to the salt acid constituents that content is 10%；
4. heat temperature raising neutralization reaction, it is to be mixed uniformly after mixed solution heating water heating, when fluid temperature rises to 80-100
DEG C continue to be slow added into suitable sodium hydroxide neutralization reaction under stirring, to approach neutral liquid；
5. adding component heat preservation, content is added after the addition component of above-mentioned steps heat temperature raising and neutralization reaction all dissolves
For 98% urea, continues to stir and keep the temperature 20-40min;
6. adding ammonium carbonate tune pH value 7, continue insulated and stirred 2h；
7. decontamination discharges, after insulated and stirred 2h, when discharging, removes insoluble impurity, obtains quick-drying fireworks reel of the invention
Glue finished product.
Product of the present invention produces three-waste free pollution, and properties of product are stablized, and prepares that equipment is simple, and energy consumption is small, at low cost, meets
Environmentally friendly production requirement.
It follows that the present invention has the special feature that is with beneficial effect:
1, exempt to shine quick-drying fireworks reel glue rolling for fireworks paper tube using roasting of exempting from of the invention, fluency is good, water content
It is low, can be dry in the short time in natural temperature, the fireworks chart drum production cycle is shortened, ensure that manufacturing enterprise prepares
The needs of firework product；
2, reel glue stability of the invention is good, non-toxic and tasteless, three-waste free pollution in production, due in component China and foreign countries added with anti-
Tide volatilization glue, accelerates the evaporation of moisture in glue, while in turn ensuring the fireworks paper tube rolled not moisture-sensitive, paper tube intensity
Height, medicament component used meet environmental requirement, and paper tube and the firework product pot life being processed into are long, will not be because producing caused by glue
Product Deformation And Metamorphism.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
One kind of the invention exempts from roasting and exempts to shine quick-drying fireworks reel glue, is liquid glue-like, its main feature is that: it is by with the following group
Part and weight fraction ratio processing preparation, it may be assumed that
Polyvinyl alcohol: dosage is 132 parts by weight；
Formalin: dosage is 400 parts by weight；
Urea: dosage is 28 parts by weight；
Hydrochloric acid: dosage is 8 parts by weight；
Ammonium carbonate: dosage is 7 parts by weight；
Sodium hydroxide: appropriate；
Water: dosage is 1000 parts by weight；
The outer plus moisture-proof volatilization glue in above-mentioned component: 10-20 parts by weight.
Specifically include following process steps:
1. stocking up, weighs and be equipped with by the raw material weight number of above-mentioned component；
2. impregnating, the formalin that polyvinyl alcohol content is 36% is impregnated at normal temperature；
3. stirring addition component, is sufficiently stirred at normal temperatures and pressures and is slowly added to the salt acid constituents that content is 10%；
4. heat temperature raising neutralization reaction, it is to be mixed uniformly after mixed solution heating water heating, when fluid temperature rises to 80-100
DEG C continue to be slow added into suitable sodium hydroxide neutralization reaction under stirring, to approach neutral liquid；
5. adding component heat preservation, content is added after the addition component of above-mentioned steps heat temperature raising and neutralization reaction all dissolves
For 98% urea, continues to stir and keep the temperature 20-40min;
6. adding ammonium carbonate tune pH value 7, continue insulated and stirred 2h；
7. decontamination discharges, after insulated and stirred 2h, when discharging, removes insoluble impurity, obtains quick-drying fireworks reel of the invention
Glue finished product.
But above embodiment described in the invention is merely illustrative of the technical solution of the present invention and should not be understood as pair
The present invention imposes any restrictions.Those skilled in the art should understand that there is the present invention well known multiple material to substitute/replace
Change, without departing from essential meaning of the invention under the premise of, should all cover within the protection scope of the present invention.
Claims (1)
- Exempt to shine quick-drying fireworks reel glue 1. one kind exempts from roasting, it is characterised in that: it is by following component and weight fraction ratio processing system It is standby, it may be assumed thatPolyvinyl alcohol: dosage is 132 parts by weight；Formalin: dosage is 400 parts by weight；Urea: dosage is 28 parts by weight；Hydrochloric acid: dosage is 8 parts by weight；Ammonium carbonate: dosage is 7 parts by weight；Sodium hydroxide: appropriate；Water: dosage is 1000 parts by weight；The outer plus moisture-proof volatilization glue in above-mentioned component: 10-20 parts by weight；Specifically include following process steps:1. stocking up, weighs and be equipped with by the raw material weight number of above-mentioned component；2. impregnating, the formalin that polyvinyl alcohol content is 36% is impregnated at normal temperature；3. stirring addition component, is sufficiently stirred at normal temperatures and pressures and is slowly added to the salt acid constituents that content is 10%；4. heat temperature raising neutralization reaction, it is to be mixed uniformly after mixed solution heating water heating, when fluid temperature rises to 80-100 DEG C continue to be slow added into suitable sodium hydroxide neutralization reaction under stirring, to approach neutral liquid；5. adding component heat preservation, content is added after the addition component of above-mentioned steps heat temperature raising and neutralization reaction all dissolves For 98% urea, continues to stir and keep the temperature 20-40min；6. adding ammonium carbonate tune pH value 7, continue insulated and stirred 2h；7. decontamination discharges, after insulated and stirred 2h, when discharging, removes insoluble impurity, obtains quick-drying fireworks reel of the invention Glue finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811000692.4A CN109135626A (en) | 2018-08-30 | 2018-08-30 | One kind exempting from roasting and exempts to shine quick-drying fireworks reel glue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811000692.4A CN109135626A (en) | 2018-08-30 | 2018-08-30 | One kind exempting from roasting and exempts to shine quick-drying fireworks reel glue |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109135626A true CN109135626A (en) | 2019-01-04 |
Family
ID=64829169
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811000692.4A Withdrawn CN109135626A (en) | 2018-08-30 | 2018-08-30 | One kind exempting from roasting and exempts to shine quick-drying fireworks reel glue |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109135626A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006075392A1 (en) * | 2005-01-14 | 2006-07-20 | Mitsui Chemicals, Inc. | Polyvinyl acetal resin varnish, gelling agent, nonaqueous electrolyte and electrochemical element |
| CN101037578A (en) * | 2007-04-30 | 2007-09-19 | 湖南神力实业有限公司 | Nano mildew-proof quick-drying white emulsion and preparation method thereof |
| CN106281131A (en) * | 2016-08-25 | 2017-01-04 | 强新正品（苏州）环保材料科技有限公司 | A kind of glue |
| CN107353850A (en) * | 2017-06-14 | 2017-11-17 | 安徽友捷包装材料有限公司 | A kind of polyvinyl formal adhesive and its processing method |
-
2018
- 2018-08-30 CN CN201811000692.4A patent/CN109135626A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006075392A1 (en) * | 2005-01-14 | 2006-07-20 | Mitsui Chemicals, Inc. | Polyvinyl acetal resin varnish, gelling agent, nonaqueous electrolyte and electrochemical element |
| CN101037578A (en) * | 2007-04-30 | 2007-09-19 | 湖南神力实业有限公司 | Nano mildew-proof quick-drying white emulsion and preparation method thereof |
| CN106281131A (en) * | 2016-08-25 | 2017-01-04 | 强新正品（苏州）环保材料科技有限公司 | A kind of glue |
| CN107353850A (en) * | 2017-06-14 | 2017-11-17 | 安徽友捷包装材料有限公司 | A kind of polyvinyl formal adhesive and its processing method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190104 |
|
| WW01 | Invention patent application withdrawn after publication |