CN109126680A - A kind of soluble soybean polysaccharide continuous extraction reactor - Google Patents
A kind of soluble soybean polysaccharide continuous extraction reactor Download PDFInfo
- Publication number
- CN109126680A CN109126680A CN201810695693.9A CN201810695693A CN109126680A CN 109126680 A CN109126680 A CN 109126680A CN 201810695693 A CN201810695693 A CN 201810695693A CN 109126680 A CN109126680 A CN 109126680A
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- Prior art keywords
- reaction tube
- plug flow
- flow reaction
- spiral plate
- end cap
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0253—Fluidised bed of solid materials
- B01D11/0257—Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Sustainable Development (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
The invention discloses a kind of soluble soybean polysaccharide continuous extraction reactors, including plug flow reaction tube, the spiral plate that the piston flow reactor end cap of plug flow reaction tube upper and lower ends is set and is arranged in inside plug flow reaction tube, spiral plate middle position inside the plug flow reaction tube is fixedly welded with spiral plate jackshaft, the present invention changes traditional reaction kettle extraction process, realize that serialization biology extracts, for industrialization, serialization biology extracts, the present invention realizes large-scale industrial production, eliminate the technological parameter difference between batch processed, realize automation control, reduce manual control bring uncertain factor, the spiral plate that the present invention uses has guide functions, realize traditional plug flow reaction purpose, it eliminates and is detained caused by current difference (center flow velocity is maximum) radially again, caused by back-mixing etc. React unbalanced.
Description
Technical field
The present invention relates to soluble soybean polysaccharide continuous extraction reactor technical field, specially a kind of soluble soybean is more
Sugared continuous extraction reactor.
Background technique
Soluble soybean polysaccharide continuously extracts the extraction that biology is realized often through traditional reaction kettle, reactor, tradition
Reaction kettle inconvenience realize serialization biology extract, for industrialization, serialization biology extract;
There is anti-caused by delay, back-mixing caused by current difference (center flow velocity is maximum) radially etc. for traditional reactor
It answers unbalanced;
Connection structure is unstable between traditional inside reactor and end construction, is easy to interfere with each other, inconvenience dismounting, and use is not square
Just.
Summary of the invention
The purpose of the present invention is to provide a kind of soluble soybean polysaccharide continuous extraction reactors, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the invention provides the following technical scheme: a kind of soluble soybean polysaccharide continuously extracts reaction
Device including plug flow reaction tube, is arranged in the piston flow reactor end cap of plug flow reaction tube upper and lower ends and is arranged flat-pushing
The spiral plate inside reaction tube is flowed, the spiral plate middle position inside the plug flow reaction tube is fixedly welded among spiral plate
Axis, the upper and lower ends of the spiral plate jackshaft are fixedly welded with screw-jointing seat, and the screw-jointing seat is far from spiral plate jackshaft
One end is equipped with bolt apertures, is connected with the column that is spirally connected by being threadedly engaged in bolt apertures, and the described one end of column far from screw-jointing seat that is spirally connected is solid
Surely it is welded in the fixed plate of end, the end fixed plate is fixedly welded on piston flow reactor cover internal, the plug flow
External screw thread is equipped at the upper and lower ends outer ring of reaction tube, the piston flow reactor end cap is made of fixing end and connecting pin,
The end fixed plate is fixedly welded in the fixing end inner wall of piston flow reactor cover internal.
Preferably, the plug flow reaction tube is in the cylinder-like structure of upper and lower opening, is consolidated in the inner wall of plug flow reaction tube
Surely it is fitted with wear-resistant layer.
Preferably, fixing end structure hemispherical, the cylindrical structure in connecting pin, connecting pin and fixing end are integrally set
It sets, and the u-shaped structure in cross section of piston flow reactor end cap that connecting pin and fixing end collectively constitute.
Preferably, the internal diameter of the connecting pin is consistent with the outer diameter of plug flow reaction tube, and connecting pin passes through the interior spiral shell of inner ring
It is connected with each other between line and the external screw thread of plug flow reaction tube end outer ring.
Preferably, clockwise thread company is threaded between the plug flow reaction tube, piston flow reactor end cap
It connects, described be spirally connected between column, screw-jointing seat is threaded to anti-clockwise thread connection.
Compared with prior art, the beneficial effects of the present invention are:
1. the present invention changes traditional reaction kettle extraction process, realizes that serialization biology extracts, mentioned for industrialization, serialization biology
It takes;
2. the present invention realizes large-scale industrial production, the technological parameter difference between batch processed is eliminated, realizes automation control,
Reduce manual control bring uncertain factor;
3. the spiral plate that the present invention uses has guide functions, that is, realize traditional plug flow reaction purpose, and eliminate
Reaction caused by delay, back-mixing caused by current difference radially (center flow velocity is maximum) etc. is unbalanced;
4. spiral plate of the invention has guide functions, while realizing without dead zone flowing, the mixing of local material is increased,
Improve the uniformity and reaction efficiency of reaction;
5. the piston flow reactor end cap at plug flow reaction tube both ends is connected to plug flow reaction tube by being threadedly engaged in device
End, the screw-jointing seat that internal spiral board ends are fixedly welded are connected to piston flow reactor cover internal by being threadedly engaged
It is spirally connected on column, integral disassembly, assembly is convenient;
6. the wear-resistant layer on plug flow reaction tube inner wall reduces the abrasion between plug flow reaction tube inner wall and spiral plate, increase
The service life of device is added;
7. being threaded to clockwise thread connection between plug flow reaction tube and piston flow reactor end cap, be spirally connected column and spiral shell
It is threaded to anti-clockwise thread connection between joint chair, the two rotating Vortex clockwise the more can turn the more tight, counterclockwise rotation in the same direction
Turn the more to turn the more loose, be easy to use, is suitble to promote.
Detailed description of the invention
Fig. 1 is schematic structural view of the invention;
Fig. 2 is spiral plate structural schematic diagram of the present invention;
Fig. 3 is plug flow reaction process figure of the present invention.
In figure: plug flow reaction tube 1, piston flow reactor end cap 2, spiral plate 3, spiral plate jackshaft 4, end fixed plate
5, be spirally connected column 6, screw-jointing seat 7, wear-resistant layer 8, bolt apertures 9, external screw thread 10, fixing end 21, connecting pin 22.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Fig. 1-3 is please referred to, the present invention provides a kind of technical solution: a kind of soluble soybean polysaccharide continuous extraction reactor,
Including plug flow reaction tube 1, the piston flow reactor end cap 2 of 1 upper and lower ends of plug flow reaction tube is set and is arranged flat-pushing
The spiral plate 3 inside reaction tube 1 is flowed, 3 middle position of spiral plate inside plug flow reaction tube 1 is fixedly welded among spiral plate
Axis 4, the upper and lower ends of spiral plate jackshaft 4 are fixedly welded with screw-jointing seat 7, the one end of screw-jointing seat 7 far from spiral plate jackshaft 4
Equipped with bolt apertures 9, it is connected with the column 6 that is spirally connected by being threadedly engaged in bolt apertures 9, be spirally connected the fixed weldering in the one end of column 6 far from screw-jointing seat 7
It connects in end fixed plate 5, end fixed plate 5 is fixedly welded on inside piston flow reactor end cap 2, plug flow reaction tube 1
External screw thread 10 is equipped at upper and lower ends outer ring, piston flow reactor end cap 2 is made of fixing end 21 and connecting pin 22, and end is solid
Fixed board 5 is fixedly welded in 21 inner wall of fixing end inside piston flow reactor end cap 2.
Plug flow reaction tube 1 is in the cylinder-like structure of upper and lower opening, and fixation is fitted with anti-in the inner wall of plug flow reaction tube 1
Wearing layer 8.
The structure hemispherical of fixing end 21, the cylindrical structure in connecting pin 22, connecting pin 22 and fixing end 21 are wholely set,
And the u-shaped structure in cross section of piston flow reactor end cap 2 that connecting pin 22 and fixing end 21 collectively constitute.
The internal diameter of connecting pin 22 is consistent with the outer diameter of plug flow reaction tube 1, the internal screw thread peace that connecting pin 22 passes through inner ring
It is connected with each other between the external screw thread 10 of 1 end outer ring of plug-flow reaction tube.
It is threaded to clockwise thread connection between plug flow reaction tube 1, piston flow reactor end cap 2, be spirally connected column
6, anti-clockwise thread connection is threaded between screw-jointing seat 7.
Embodiment 1
A kind of soluble soybean polysaccharide continuous extraction reactor, including plug flow reaction tube 1, setting are on plug flow reaction tube 1
The piston flow reactor end cap 2 at lower both ends and the spiral plate 3 being arranged in inside plug flow reaction tube 1, the plug flow reaction tube 1
Internal 3 middle position of spiral plate is fixedly welded with spiral plate jackshaft 4, and the upper and lower ends of the spiral plate jackshaft 4 are solid
Surely it is welded with screw-jointing seat 7, the screw-jointing seat 7 is equipped with bolt apertures 9 far from one end of spiral plate jackshaft 4, passes through spiral shell in bolt apertures 9
Line is connected with the column 6 that is spirally connected, and the column 6 that is spirally connected is fixedly welded in end fixed plate 5 far from one end of screw-jointing seat 7, described
End fixed plate 5 is fixedly welded on inside piston flow reactor end cap 2, at the upper and lower ends outer ring of the plug flow reaction tube 1
It is equipped with external screw thread 10, the piston flow reactor end cap 2 is made of fixing end 21 and connecting pin 22, the end fixed plate 5
It is fixedly welded in 21 inner wall of fixing end inside piston flow reactor end cap 2.
Embodiment 2
A kind of soluble soybean polysaccharide continuous extraction reactor, including plug flow reaction tube 1, setting are on plug flow reaction tube 1
The piston flow reactor end cap 2 at lower both ends and the spiral plate 3 being arranged in inside plug flow reaction tube 1, the plug flow reaction tube 1
Internal 3 middle position of spiral plate is fixedly welded with spiral plate jackshaft 4, and the upper and lower ends of the spiral plate jackshaft 4 are solid
Surely it is welded with screw-jointing seat 7, the screw-jointing seat 7 is equipped with bolt apertures 9 far from one end of spiral plate jackshaft 4, passes through spiral shell in bolt apertures 9
Line is connected with the column 6 that is spirally connected, and the column 6 that is spirally connected is fixedly welded in end fixed plate 5 far from one end of screw-jointing seat 7, described
End fixed plate 5 is fixedly welded on inside piston flow reactor end cap 2, at the upper and lower ends outer ring of the plug flow reaction tube 1
It is equipped with external screw thread 10, the piston flow reactor end cap 2 is made of fixing end 21 and connecting pin 22, the end fixed plate 5
It is fixedly welded in 21 inner wall of fixing end inside piston flow reactor end cap 2.
The plug flow reaction tube 1 is in the cylinder-like structure of upper and lower opening, fixed fitting in the inner wall of plug flow reaction tube 1
There is wear-resistant layer 8.
Embodiment 3
A kind of soluble soybean polysaccharide continuous extraction reactor, including plug flow reaction tube 1, setting are on plug flow reaction tube 1
The piston flow reactor end cap 2 at lower both ends and the spiral plate 3 being arranged in inside plug flow reaction tube 1, the plug flow reaction tube 1
Internal 3 middle position of spiral plate is fixedly welded with spiral plate jackshaft 4, and the upper and lower ends of the spiral plate jackshaft 4 are solid
Surely it is welded with screw-jointing seat 7, the screw-jointing seat 7 is equipped with bolt apertures 9 far from one end of spiral plate jackshaft 4, passes through spiral shell in bolt apertures 9
Line is connected with the column 6 that is spirally connected, and the column 6 that is spirally connected is fixedly welded in end fixed plate 5 far from one end of screw-jointing seat 7, described
End fixed plate 5 is fixedly welded on inside piston flow reactor end cap 2, at the upper and lower ends outer ring of the plug flow reaction tube 1
It is equipped with external screw thread 10, the piston flow reactor end cap 2 is made of fixing end 21 and connecting pin 22, the end fixed plate 5
It is fixedly welded in 21 inner wall of fixing end inside piston flow reactor end cap 2.
The plug flow reaction tube 1 is in the cylinder-like structure of upper and lower opening, fixed fitting in the inner wall of plug flow reaction tube 1
There is wear-resistant layer 8.
The fixing end 21 structure hemispherical, the cylindrical structure in connecting pin 22,21 one of connecting pin 22 and fixing end
Setting, and the u-shaped structure in cross section of piston flow reactor end cap 2 that connecting pin 22 and fixing end 21 collectively constitute.
Embodiment 4
A kind of soluble soybean polysaccharide continuous extraction reactor, including plug flow reaction tube 1, setting are on plug flow reaction tube 1
The piston flow reactor end cap 2 at lower both ends and the spiral plate 3 being arranged in inside plug flow reaction tube 1, the plug flow reaction tube 1
Internal 3 middle position of spiral plate is fixedly welded with spiral plate jackshaft 4, and the upper and lower ends of the spiral plate jackshaft 4 are solid
Surely it is welded with screw-jointing seat 7, the screw-jointing seat 7 is equipped with bolt apertures 9 far from one end of spiral plate jackshaft 4, passes through spiral shell in bolt apertures 9
Line is connected with the column 6 that is spirally connected, and the column 6 that is spirally connected is fixedly welded in end fixed plate 5 far from one end of screw-jointing seat 7, described
End fixed plate 5 is fixedly welded on inside piston flow reactor end cap 2, at the upper and lower ends outer ring of the plug flow reaction tube 1
It is equipped with external screw thread 10, the piston flow reactor end cap 2 is made of fixing end 21 and connecting pin 22, the end fixed plate 5
It is fixedly welded in 21 inner wall of fixing end inside piston flow reactor end cap 2.
The plug flow reaction tube 1 is in the cylinder-like structure of upper and lower opening, fixed fitting in the inner wall of plug flow reaction tube 1
There is wear-resistant layer 8.
The fixing end 21 structure hemispherical, the cylindrical structure in connecting pin 22,21 one of connecting pin 22 and fixing end
Setting, and the u-shaped structure in cross section of piston flow reactor end cap 2 that connecting pin 22 and fixing end 21 collectively constitute.
The internal diameter of the connecting pin 22 is consistent with the outer diameter of plug flow reaction tube 1, the internal screw thread that connecting pin 22 passes through inner ring
It is connected with each other between the external screw thread 10 of 1 end outer ring of plug flow reaction tube.
Embodiment 5
A kind of soluble soybean polysaccharide continuous extraction reactor, including plug flow reaction tube 1, setting are on plug flow reaction tube 1
The piston flow reactor end cap 2 at lower both ends and the spiral plate 3 being arranged in inside plug flow reaction tube 1, the plug flow reaction tube 1
Internal 3 middle position of spiral plate is fixedly welded with spiral plate jackshaft 4, and the upper and lower ends of the spiral plate jackshaft 4 are solid
Surely it is welded with screw-jointing seat 7, the screw-jointing seat 7 is equipped with bolt apertures 9 far from one end of spiral plate jackshaft 4, passes through spiral shell in bolt apertures 9
Line is connected with the column 6 that is spirally connected, and the column 6 that is spirally connected is fixedly welded in end fixed plate 5 far from one end of screw-jointing seat 7, described
End fixed plate 5 is fixedly welded on inside piston flow reactor end cap 2, at the upper and lower ends outer ring of the plug flow reaction tube 1
It is equipped with external screw thread 10, the piston flow reactor end cap 2 is made of fixing end 21 and connecting pin 22, the end fixed plate 5
It is fixedly welded in 21 inner wall of fixing end inside piston flow reactor end cap 2.
The plug flow reaction tube 1 is in the cylinder-like structure of upper and lower opening, fixed fitting in the inner wall of plug flow reaction tube 1
There is wear-resistant layer 8.
The fixing end 21 structure hemispherical, the cylindrical structure in connecting pin 22,21 one of connecting pin 22 and fixing end
Setting, and the u-shaped structure in cross section of piston flow reactor end cap 2 that connecting pin 22 and fixing end 21 collectively constitute.
The internal diameter of the connecting pin 22 is consistent with the outer diameter of plug flow reaction tube 1, the internal screw thread that connecting pin 22 passes through inner ring
It is connected with each other between the external screw thread 10 of 1 end outer ring of plug flow reaction tube.
Clockwise thread connection, institute are threaded between the plug flow reaction tube 1, piston flow reactor end cap 2
It states to be spirally connected between column 6, screw-jointing seat 7 and is threaded to anti-clockwise thread connection.
Working principle: the present invention changes traditional reaction kettle extraction process, realizes that serialization biology extracts, to industrialize, even
Continuous metaplasia object extracts;
It realizes large-scale industrial production, eliminates the technological parameter difference between batch processed, realize automation control, reduce artificial
Control bring uncertain factor;
Spiral plate 3 has guide functions, that is, realizes traditional plug flow reaction purpose, and eliminate flow velocity radially
Reaction caused by delay, back-mixing caused by difference (center flow velocity is maximum) etc. is unbalanced;
Spiral plate 3 has guide functions, while realizing without dead zone flowing, increases the mixing of local material, improves anti-
The uniformity and reaction efficiency answered;
The piston flow reactor end cap 2 at 1 both ends of plug flow reaction tube is connected to plug flow reaction tube 1 by being threadedly engaged in device
End, the screw-jointing seat 7 that internal 3 both ends of spiral plate are fixedly welded are connected in piston flow reactor end cap 2 by being threadedly engaged
Portion is spirally connected on column 6, and integral disassembly, assembly is convenient;
Wear-resistant layer 8 on 1 inner wall of plug flow reaction tube reduces the abrasion between 1 inner wall of plug flow reaction tube and spiral plate 3,
Increase the service life of device;
It is threaded to clockwise thread connection between plug flow reaction tube 1 and piston flow reactor end cap 2, be spirally connected 6 He of column
It is threaded to anti-clockwise thread connection between screw-jointing seat 7, the two rotating Vortex clockwise the more can turn the more tight, counterclockwise in the same direction
Rotation the more can turn the more loose, be easy to use, and be suitble to promote.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (5)
1. a kind of soluble soybean polysaccharide continuous extraction reactor, including plug flow reaction tube (1), setting are in plug flow reaction tube
(1) spiral plate (3) of the piston flow reactor end cap (2) of upper and lower ends and setting in plug flow reaction tube (1) inside, feature
Be: internal spiral plate (3) middle position of the plug flow reaction tube (1) is fixedly welded with spiral plate jackshaft (4), described
The upper and lower ends of spiral plate jackshaft (4) are fixedly welded with screw-jointing seat (7), and the screw-jointing seat (7) is far from spiral plate jackshaft
(4) one end is equipped with bolt apertures (9), is connected with the column that is spirally connected (6) in bolt apertures (9) by being threadedly engaged, and the column that is spirally connected (6) is remote
One end from screw-jointing seat (7) is fixedly welded on end fixed plate (5), and the end fixed plate (5) is fixedly welded on plug flow
Reactor end cap (2) is internal, is equipped with external screw thread (10) at the upper and lower ends outer ring of the plug flow reaction tube (1), described flat
Plug-flow reactor end cap (2) is made of fixing end (21) and connecting pin (22), and the end fixed plate (5) is fixedly welded on flat-pushing
In internal fixing end (21) inner wall of flow reactor end cap (2).
2. a kind of soluble soybean polysaccharide continuous extraction reactor according to claim 1, it is characterised in that: described flat-pushing
The cylinder-like structure that reaction tube (1) is in upper and lower opening is flowed, fixation is fitted with wear-resistant layer in the inner wall of plug flow reaction tube (1)
(8).
3. a kind of soluble soybean polysaccharide continuous extraction reactor according to claim 1, it is characterised in that: the fixation
(21) structure hemispherical, connecting pin (22) cylindrical structure are held, connecting pin (22) and fixing end (21) are wholely set, and even
Connect end (22) and the u-shaped structure in cross section of piston flow reactor end cap (2) that fixing end (21) collectively constitutes.
4. a kind of soluble soybean polysaccharide continuous extraction reactor according to claim 1, it is characterised in that: the connection
Hold the internal diameter of (22) consistent with the outer diameter of plug flow reaction tube (1), connecting pin (22) are anti-by the internal screw thread and plug flow of inner ring
It answers and is connected with each other between the external screw thread (10) of cylinder (1) end outer ring.
5. a kind of soluble soybean polysaccharide continuous extraction reactor according to claim 1, it is characterised in that: described flat-pushing
The clockwise thread that is threaded between stream reaction tube (1), piston flow reactor end cap (2) connects, the column that is spirally connected (6),
Anti-clockwise thread connection is threaded between screw-jointing seat (7).
Priority Applications (1)
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CN201810695693.9A CN109126680A (en) | 2018-06-29 | 2018-06-29 | A kind of soluble soybean polysaccharide continuous extraction reactor |
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CN201810695693.9A CN109126680A (en) | 2018-06-29 | 2018-06-29 | A kind of soluble soybean polysaccharide continuous extraction reactor |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111394124A (en) * | 2020-05-07 | 2020-07-10 | 中国石油大学(华东) | Hydrocarbon raw material heat treatment process and device |
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US4460278A (en) * | 1981-01-28 | 1984-07-17 | Toyo Engineering Corporation | Continuous bulk polymerization reactor |
CN101024540A (en) * | 2007-02-02 | 2007-08-29 | 浙江大学 | Spiral self-circulation anaerobic biological reactor |
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