CN109126267A - The clarified separation equipment of calcium and magnesium crystallization in a kind of removing solution system - Google Patents
The clarified separation equipment of calcium and magnesium crystallization in a kind of removing solution system Download PDFInfo
- Publication number
- CN109126267A CN109126267A CN201710452406.7A CN201710452406A CN109126267A CN 109126267 A CN109126267 A CN 109126267A CN 201710452406 A CN201710452406 A CN 201710452406A CN 109126267 A CN109126267 A CN 109126267A
- Authority
- CN
- China
- Prior art keywords
- clarified separation
- pipeline
- slag charge
- peristaltic pump
- water phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/02—Settling tanks with single outlets for the separated liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/2444—Discharge mechanisms for the classified liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/245—Discharge mechanisms for the sediments
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/04—Combinations of filters with settling tanks
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
The present invention provides a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system, it is characterized by comprising slag slots, clarified separation pond, water phase baffle, water phase adjuster, oily phase baffle, oil trap, pipeline solid-liquid separator, wired hose, peristaltic pump, slag charge extractor, the slag charge extractor is connected with peristaltic pump, the peristaltic pump is connected by wired hose with clarified separation pond, clarified separation pond of the invention is to crystallize calcium and magnesium, the mixture of oil and water is extracted out from extraction box to carry out storing clear equipment, wired hose is the pipeline for connecting peristaltic pump and slag charge clarified separation pond；Pipeline solid-liquid separator is the pipeline type solid-liquid separator being mounted below slag charge clarifying basin, inside it equipment stainless steel metal net cage, and synthetic cotton is filled in net cage, for the interception to fine particle, prevent part slag charge from entering in solution, realization is completely separated, and guarantees the clarification of solution.
Description
Technical field
The present invention relates to clarified separation equipment, more particularly to remove the clarified separation equipment of calcium and magnesium crystallization in solution system.
Background technique
For most of hydrometallurgy industries, the concerned process steps of extraction are directed to, and in extraction production process,
The case where calcium and magnesium slag and other impurities crystallize in cabinet more or less can all occur, especially in feed liquid there are a large amount of calcium and magnesiums from
In the sulfuric acid system of son, it is easy to the crystallization of calcium and magnesium slag occur, blocks production equipment, influence normally to produce.
Existing processing method is, after crystallization content reaches a certain level in extraction box, carries out halt production centralized processing, is locating
It needs to pour out organic and sour whole in extraction box during reason, then manually be cleared up, the calcium and magnesium crystallization cleaned up
In be entrained with a large amount of acid and organic phase, cause the waste of organic phase and acid, while the slag charge cleaned up being made to be difficult to handle, and
And need the long period.
Before using Function Solution Handling Device Used of the invention, after crystallization content reaches a certain level in extraction box, stop production
Centralized processing, needs to pour out organic and sour whole in extraction box during processing, is then manually cleared up, cleaned out
It is entrained with a large amount of acid and organic phase in the calcium and magnesium crystallization come, causes the waste of organic phase and acid, while making the slag cleaned up
Material is difficult to handle, and needs the long period, influences the environmental sanitation on equipment itself and periphery, increases the labor of post operation personnel
Fatigue resistance directly contributes valuable metal loss and economic benefit loss.
Summary of the invention
According to the above technical problem, the present invention provides a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system,
It is characterized by comprising slag slot, clarified separation pond, water phase baffle, water phase adjuster, oily phase baffles, oil trap, pipeline solid-liquid
Separator, wired hose, peristaltic pump, slag charge extractor, the slag charge extractor are connected with peristaltic pump, and the peristaltic pump passes through steel
Silk hose is connected with clarified separation pond, and oily phase baffle is equipped on the upside of the clarified separation pond, is equipped on the oil phase baffle
Oil trap, oil phase baffle downside are equipped with water phase baffle, and the water phase baffle and oily phase baffle do not contact, the water phase gear
Water phase adjuster is installed on plate, offers water outlet, the water outlet and conveyance conduit one end on the downside of the clarified separation pond
Connection, the conveyance conduit other end are connected with pipeline solid-liquid separator, valve respectively, and slag slot is equipped on the downside of the valve.
The slag charge extractor is the tool for being directly inserted into the crystallization position of extraction box and being detached to crystallization, wherein
Main body is etch-proof DN50 pipeline, is used to connect wired hose above pipeline, lower section is connected with the suction nozzle of dustpan shape, the suction
Head entrance is reticular structure.
The solid-liquid separator internal unit stainless steel metal net cage, net cage is interior to be filled with synthetic cotton.
The invention has the benefit that the present invention is a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system,
The grease that simultaneously slag charge can be taken out of carries out separation and recycling, and solves and there is a situation where the water of aniseed and oil in calcium and magnesium slag,
Being automatically separated for oil, water and slag charge is realized, the treatment effeciency of calcium and magnesium crystallization is improved.Using can be effective after the invention equipment
During continuous production in extraction box calcium and magnesium crystallization handle, while can guarantee acid and organic phase must return
It receives, the promotion of making by oneself degree greatly reduces the labor intensity of post operation personnel, has prevented solution loss, improves operation ring
Border.
Clarified separation pond of the invention be by calcium and magnesium crystallization, oil and water mixture extracted out from extraction box store it is clear
Clear equipment, clarified separation pond inside is equipped with water phase baffle and oily phase baffle, in the west side equipment water phase height tune of water phase baffle
Device is saved, is equipped with oil trap, the organic phase that recycling clarified separation goes out in the upper end of oily phase baffle；Slag charge extractor is to be directly inserted into
The tool that the crystallization position of extraction box detaches crystallization, wherein main body is etch-proof DN50 pipeline, is used above pipeline one
In connection wired hose, lower section is connected with the suction nozzle of dustpan shape, does latticed processing in the entrance of suction nozzle, prevent bulk slag charge
Block the pump housing；Wired hose is the pipeline for connecting peristaltic pump and slag charge clarified separation pond；Pipeline solid-liquid separator is to be mounted on slag
Expect the pipeline type solid-liquid separator below clarifying basin, inside it equipment stainless steel metal net cage, synthetic cotton be filled in net cage,
For the interception to fine particle, prevent part slag charge from entering in solution, realization is completely separated, and guarantees the clarification of solution.
Detailed description of the invention
Fig. 1 is schematic structural view of the invention.
Such as figure, slag slot -1, clarified separation pond -2, water phase baffle -3, water phase adjuster -4, oily phase baffle -5, oil trap -
6, pipeline solid-liquid separator -7, wired hose -8, peristaltic pump -9, slag charge extractor -10.
Specific embodiment
According to Fig. 1, invention is further explained:
Embodiment 1
The present invention provides a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system, including slag slot 1, clarification point
From pond 2, water phase baffle 3, water phase adjuster 4, oily phase baffle 5, oil trap 6, pipeline solid-liquid separator 7, wired hose 8, hose
9, slag charge extractor 10 are pumped, slag charge extractor 10 and peristaltic pump 9 connect, and peristaltic pump 9 passes through wired hose 8 and clarified separation pond 2
It connects, oily phase baffle 5 is installed on the upside of clarified separation pond 2, oil trap 6 is installed on oily phase baffle 5, is pacified on the downside of oily phase baffle 5
Equipped with water phase baffle 3, water phase baffle 3 and oily phase baffle 5 are not contacted, and water phase adjuster 4, clarification point are equipped on water phase baffle 3
From water outlet is offered on the downside of pond 2, water outlet is connected with conveyance conduit one end, and the conveyance conduit other end divides with pipeline solid-liquid respectively
It is connected from device 7, valve, slag slot 1 is equipped on the downside of valve.Slag charge extractor 10 be the crystallization position for being directly inserted into extraction box
To the tool that crystallization is detached, wherein main body is etch-proof DN50 pipeline, is used to connect wired hose 8 above pipeline, under
Side is connected with the suction nozzle of dustpan shape, and suction nozzle entrance is reticular structure.Solid-liquid separator internal unit stainless steel metal net cage, net
Synthetic cotton is filled in case.
Embodiment 2
The present invention carries out greatly reducing post employee to there are calcium and magnesium slags to handle in extraction box using above equipment
Labor intensity, while it is synchronous with water phase to be able to achieve organic phase, about save it is artificial from the aspect of, can at least reduce post
1 people of staffing can reduce expenses 70,000 yuan or so estimated every year according to the average salary level calculation of Tianjin.
The above is only a preferred embodiment of the present invention, it is noted that for the common skill of the art
For art personnel, without departing from the principle of the present invention, several improvement can also be made, these improvement also should be regarded as this hair
Bright protection scope.
Claims (3)
1. a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system, it is characterised in that including slag slot, clarified separation
Pond, water phase baffle, water phase adjuster, oily phase baffle, oil trap, pipeline solid-liquid separator, wired hose, peristaltic pump, slag charge are inhaled
Device is taken, the slag charge extractor is connected with peristaltic pump, and the peristaltic pump is connected by wired hose with clarified separation pond, described clear
Oily phase baffle is installed on the upside of clear separate tank, oil trap is installed on the oil phase baffle, is equipped on the downside of the oil phase baffle
Water phase baffle, the water phase baffle and oily phase baffle do not contact, and water phase adjuster, the clarification are equipped on the water phase baffle
Water outlet is offered on the downside of separate tank, the water outlet connect with conveyance conduit one end, the conveyance conduit other end respectively with
Pipeline solid-liquid separator, valve connection, the valve downside are equipped with slag slot.
2. a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system described in accordance with the claim 1, it is characterised in that
The slag charge extractor is the tool for being directly inserted into the crystallization position of extraction box and being detached to crystallization, and wherein main body is anti-
The DN50 pipeline of corrosion, for connecting wired hose, lower section is connected with the suction nozzle of dustpan shape, the suction nozzle entrance for pipeline top
For reticular structure.
3. a kind of clarified separation equipment for removing calcium and magnesium crystallization in solution system described in accordance with the claim 1, it is characterised in that
The solid-liquid separator internal unit stainless steel metal net cage, net cage is interior to be filled with synthetic cotton.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710452406.7A CN109126267A (en) | 2017-06-15 | 2017-06-15 | The clarified separation equipment of calcium and magnesium crystallization in a kind of removing solution system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710452406.7A CN109126267A (en) | 2017-06-15 | 2017-06-15 | The clarified separation equipment of calcium and magnesium crystallization in a kind of removing solution system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109126267A true CN109126267A (en) | 2019-01-04 |
Family
ID=64829979
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710452406.7A Pending CN109126267A (en) | 2017-06-15 | 2017-06-15 | The clarified separation equipment of calcium and magnesium crystallization in a kind of removing solution system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109126267A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113549759A (en) * | 2021-06-02 | 2021-10-26 | 浙江天能新材料有限公司 | Complete device for cleaning calcium slag of extraction box in wet metallurgy industry |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202682834U (en) * | 2012-05-21 | 2013-01-23 | 贵州顶效开发区宏达金属综合回收有限公司 | Box-type mixing, settling and extracting tank facilitating removal of crystalline deposits |
| AU2012245059A1 (en) * | 2011-04-20 | 2013-02-28 | Hatch Pty Ltd | Re-entrainment prevention apparatus |
| CN103706147A (en) * | 2013-12-25 | 2014-04-09 | 江西稀有稀土金属钨业集团有限公司 | Method of improving phase separation speed of organic phase and water phase in extraction tank |
-
2017
- 2017-06-15 CN CN201710452406.7A patent/CN109126267A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2012245059A1 (en) * | 2011-04-20 | 2013-02-28 | Hatch Pty Ltd | Re-entrainment prevention apparatus |
| CN202682834U (en) * | 2012-05-21 | 2013-01-23 | 贵州顶效开发区宏达金属综合回收有限公司 | Box-type mixing, settling and extracting tank facilitating removal of crystalline deposits |
| CN103706147A (en) * | 2013-12-25 | 2014-04-09 | 江西稀有稀土金属钨业集团有限公司 | Method of improving phase separation speed of organic phase and water phase in extraction tank |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113549759A (en) * | 2021-06-02 | 2021-10-26 | 浙江天能新材料有限公司 | Complete device for cleaning calcium slag of extraction box in wet metallurgy industry |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190104 |
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| RJ01 | Rejection of invention patent application after publication |