CN109126217A - A kind of Chinese medicine flocculation clarification refining plant - Google Patents
A kind of Chinese medicine flocculation clarification refining plant Download PDFInfo
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- CN109126217A CN109126217A CN201811324749.6A CN201811324749A CN109126217A CN 109126217 A CN109126217 A CN 109126217A CN 201811324749 A CN201811324749 A CN 201811324749A CN 109126217 A CN109126217 A CN 109126217A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/01—Separation of suspended solid particles from liquids by sedimentation using flocculating agents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/2488—Feed or discharge mechanisms for settling tanks bringing about a partial recirculation of the liquid, e.g. for introducing chemical aids
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/28—Mechanical auxiliary equipment for acceleration of sedimentation, e.g. by vibrators or the like
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2221/00—Applications of separation devices
- B01D2221/10—Separation devices for use in medical, pharmaceutical or laboratory applications, e.g. separating amalgam from dental treatment residues
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
It flocculates the invention discloses a kind of Chinese medicine and clarifies refining plant, including the first basin, second basin, third basin, 4th basin and reactor tank, first basin and the second basin pass through the first pipeline connection, third basin and the 4th basin pass through the second pipeline connection, several sieve plates are provided in reactor tank, reactor tank top and bottom have been respectively communicated with the first small basin and the second small basin, first basin and the second small basin pass through third pipeline connection, third basin and the first small basin pass through the 4th pipeline connection, second small basin and the 4th basin pass through the 5th pipeline connection, first small basin is connected to the second basin by overflow passage, first basin is for containing flocculant, third basin is for containing Chinese medicine extract.Chinese medicine production is carried out using Chinese medicine flocculation clarification refining plant of the invention, with short production cycle, effective components of Chinese medicinal is high, and strong operability, composition is cheap, remarkable benefit.
Description
Technical field
The present invention relates to pharmaceutical machinery technical fields, flocculate more particularly to a kind of Chinese medicine and clarify refining plant.
Background technique
In recent years, it in the extraction process of Chinese medicine, largely studies and facts have proved using traditional water extract-alcohol precipitation device
While removing invalid components in decocting for Chinese herbal medicine liquid, it will cause a large amount of losses of effective ingredient, it is difficult to which guarantee finished product preparation has
Effect property and stability it is poor.Flocculation clarification purification techniques has the advantage that one, water extraction and alcohol precipitation method high to effective component retention rate
System makes its dehydration generate flocculation sedimentation by changing colloidal substance solubility, often destroys the natural colloid of former Chinese medicine extract
Stabilising system, total solid matters and polar component, microelement, polysaccharide component loss are serious, affect the treatment.Clarificant method is
A kind of Old Region is added in Chinese medicine extract and removes biggish suspension in solution in a manner of adsorption bridging and charge neutrality
Particle, therefore do not interfere with the effective components such as amino acid, vitamin, polypeptide, polysaccharide.And colloid protective effect is utilized, thus energy
More retain the effective component in Chinese medicine extract, preferably embodies the multicomponent traditional characteristics of traditional Chinese medicine；Two, clarification effect
Fruit is preferable, and under the conditions ofs suitable PH, Chinese medicine extract concentration etc., finished product obtained by adsorption-flocculation clarifying agent eliminates shakiness
Fixed suspended particles and macromolecular substances, the hydrophilic colloid solution of obtained approach true solution, filtrate absorbance become smaller, clarity
It improves, keeps stable state for a long time, generated almost without precipitating, stability is higher than alcohol deposition method and supercentrifugal process；Three, process
Simple at low cost, most Old Regions are added in drug extract after taking direct or simple preparation, can be added while hot, stir
Several minutes, time of repose is short.Relative to water extraction and alcohol precipitation method, the production cycle shortens, and strong operability is low in cost, effect
It is beneficial significant；Four, safe and non-toxic, be widely used, many adsorption-flocculation clarifying agent such as ZTC, chitin, 101 fruit juice clarifiers etc. are
Wholefood animal extracts, have the characteristics that safely, effectively, it is nontoxic, without side-effects, be widely used in field of medicaments.Such as
The A of ZTC, B component are through safety evaluatio, acute toxic test, and LD50 > 15g/kg belongs to nontoxic.Salmonella reversion test has no that cause is prominent
Denaturation, use are very safe.Clarifying agent also food, health care product, cosmetics, in terms of also have extensive use.Such as
II 1 type of ZTC- can be used for decolourizing clarifying；Chitin also has the effects that disintegration, is used as the disintegrating agent of tablet, and is manyization
The additive etc. of chemical product；Five, flocculation clarification technique development prospect compared with other technologies is wide, and flocculation technique both can be independent
Operation can also be applied in combination, as pretreatment, intermediate treatment or advanced treating with solid-liquid separating methods such as filtering, centrifugations
Means, compared with high-speed centrifugation technology, its equipment investment is few, less energy consumption, at low cost；Compared with hyperfiltration technique, skill of flocculating
Art also without film design, fouling membrane the problem of.Clarificant method have high treating effect, it is easily operated, have a wide range of application, can be with
The advantages that other methods are used in combination has vast potential for future development in cmm of simple prescription and compound preparation clarification purifying technique.
Summary of the invention
It flocculates clarification refining plant the object of the present invention is to provide a kind of Chinese medicine, to solve above-mentioned of the existing technology ask
Topic is improved production cycle shortening, effective component of chinese medicine.
To achieve the above object, the present invention provides following schemes:
The present invention provides a kind of Chinese medicine flocculate clarification refining plant, including the first basin, the second basin, third basin,
4th basin and reactor tank, first basin and second basin pass through the first pipeline connection, the third basin and institute
It states the 4th basin and passes through the second pipeline connection, several sieve plates, the reactor tank top and bottom point are provided in the reactor tank
It is not communicated with the first small basin and the second small basin, first basin and the described second small basin pass through third pipeline connection,
By the 4th pipeline connection, the second small basin passes through with the 4th basin for the third basin and the described first small basin
5th pipeline connection, the first small basin are connected to second basin by overflow passage, and first basin is for containing
Flocculant is filled, the third basin is for containing Chinese medicine extract.
Preferably, pump one, institute are provided on the third pipeline that first basin is connected to the described second small basin
It states and is provided with pump two on the 4th pipeline that third basin is connected to the described first small basin.
Preferably, first basin, second basin, the third basin, the 4th basin, described first small
Liquidometer is provided on basin and the second small basin.
Preferably, it is provided with the first valve on first pipeline, is provided with the second valve on second pipeline, also wraps
The first detection valve and the second detection valve are included, between the first detection valve and first valve and second basin
First pipeline connection, it is described second detection valve and second valve and the 4th basin between described second
Pipeline connection.
Preferably, third pipeline one end is connected with first spray head, and the first spray head is arranged in the described second small storage
In tank, be provided with the first control valve on the third pipeline between the first spray head and the pump one, the pump one with
It is provided with the second control valve on the third pipeline between first basin, further includes the first charging valve, described first
The third pipeline connection between charging valve and the pump one and second control valve.
Preferably, described 4th pipeline one end is connected with second spray head, and the second spray head is arranged in the described first small storage
In tank, be provided with third control valve on the 4th pipeline between the second spray head and the pump two, the pump two with
The 4th control valve is provided on the 4th pipeline between the third basin.
Preferably, it is provided with third valve on the 5th pipeline, further includes the 4th valve and the 5th valve, the described 4th
Valve is connected to the 4th pipeline and the third valve and described second between the third control valve and the pump two
The 5th pipeline between small basin, the 5th valve are connected between the third control valve and the second spray head
The 5th pipeline between 4th pipeline and the third valve and the 4th basin.
It preferably, further include first row air valve, second row air valve, third exhaust valve, the 4th exhaust valve and the 5th exhaust valve,
The first row air valve is connected to described between first basin and the third control valve and the first small basin
Four pipelines, the second row air valve are arranged on second basin, and the third exhaust valve is connected to the third basin and institute
The 5th pipeline between the 4th basin and the third valve is stated, the 4th exhaust valve is arranged in the 4th basin
On, the 5th pipeline connection between the 5th exhaust valve and the 4th basin and the third valve.
It preferably, further include pump three, the pump three is connected to by the 6th pipeline with the upper end of the described second small basin, described
The 5th control valve is provided on 6th pipeline, the pump three is connected to by the 7th pipeline with the lower end of the described second small basin,
The 6th control valve is provided on 7th pipeline；The pump three is intermittent pump；The second small tank bottom is provided with
Tapping valve.
Preferably, further include purge valve, the purge valve is connected to the overflow passage, the sieve plate be porous sieve plate and
It is set side by side with several.
The present invention achieves following technical effect compared with the existing technology:
Flocculant in first basin is passed through in the second small basin of reactor tank lower end by the present invention, will be in third basin
Chinese medicine extract is passed through in the first small basin of reactor tank upper end, with the slowly sinking of Chinese medicine extract, Chinese medicine extract with
Flocculant chemically reacts in reactor tank, and the anti-big floc sedimentation generated disperses to precipitate by sieve plate, forms supernatant and gives up turbid
Liquid flows into the second small basin, and supernatant is flowed into the 4th basin by the 5th pipeline.It is flocculated and is clarified using Chinese medicine of the invention
Refining plant carries out Chinese medicine production, with short production cycle, and effective components of Chinese medicinal is high, and strong operability, composition is cheap, remarkable benefit.
Detailed description of the invention
It in order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, below will be to institute in embodiment
Attached drawing to be used is needed to be briefly described, it should be apparent that, the accompanying drawings in the following description is only some implementations of the invention
Example, for those of ordinary skill in the art, without creative efforts, can also obtain according to these attached drawings
Obtain other attached drawings.
Fig. 1 is Chinese medicine flocculation clarification refining plant schematic diagram of the invention；
Fig. 2 is the sieve plate schematic diagram in the present invention；
Wherein: the first basin of 1-, the second basin of 2-, 3- third basin, the 4th basin of 4-, 5- reactor tank, the first pipeline of 6-,
The second pipeline of 7-, 8- sieve plate, the small basin of 9- first, the small basin of 10- second, 11- third pipeline, the 4th pipeline of 12-, 13- the 5th
Pipeline, 14- overflow passage, 15- pump one, 16- pump two, 17- pump three, 18- liquidometer, the first valve of 19-, the second valve of 20-,
21- first detects valve, and 22- second detects valve, 23- first spray head, 24- second spray head, the first control valve of 25-, 26- the
Two control valves, the first charging valve of 27-, 28- third control valve, the 4th control valve of 29-, 30- third valve, 31- the 4th
Valve, the 5th valve of 32-, 33- first row air valve, 34- second row air valve, 35- third exhaust valve, the 4th exhaust valve of 36-, 37-
5th exhaust valve, the 6th pipeline of 38-, the 5th control valve of 39-, the 7th pipeline of 40-, the 6th control valve of 41-, 42- tapping valve,
43- purge valve.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art under the premise of not making the creative labor it is obtained it is all its
His embodiment, shall fall within the protection scope of the present invention.
It flocculates clarification refining plant the object of the present invention is to provide a kind of Chinese medicine, to solve above-mentioned of the existing technology ask
Topic is improved production cycle shortening, effective component of chinese medicine.
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, with reference to the accompanying drawing and specific real
Applying mode, the present invention is described in further detail.
It is as shown in Figs. 1-2: to present embodiments provide a kind of Chinese medicine flocculation clarification refining plant, including the first basin 1, second
Basin 2, third basin 3, the 4th basin 4 and reactor tank 5.First basin 1 is connected to the second basin 2 by the first pipeline 6, and first
The first valve 19 is provided on pipeline 6；Third basin 3 is connected to the 4th basin 4 by the second pipeline 7, is arranged on the second pipeline 7
There is the second valve 20；It further include the first detection valve 21 and the second detection valve 22, first detects valve 21 and the first valve 19
And second the first pipeline 6 connection between basin 2, the between the second detection valve 22 and the second valve 20 and the 4th basin 4
The connection of two pipelines 7.
In the present embodiment, sieve plate 8 is provided in reactor tank 5, sieve plate 8 is porous sieve plate and is set side by side with several.Instead
5 top and bottom of tank are answered to be respectively communicated with the first small basin 9 and the second small basin 10, the first basin 1 and the second small basin 10 are logical
The connection of third pipeline 11 is crossed, third basin 3 is connected to the first small basin 9 by the 4th pipeline 12, the second small basin 10 and the 4th
Basin 4 is connected to by the 5th pipeline 13.First small basin 9 is connected to the second basin 2 by overflow passage 14, further includes purge valve
43, purge valve 43 is connected to overflow passage 14.First basin 1 is for containing flocculant, and third basin 3 is for containing traditional Chinese medicine extraction
Liquid.It is respectively provided on first basin 1, the second basin 2, third basin 3, the 4th basin 4, the first small basin 9 and the second small basin 10
There is liquidometer 18.
In the present embodiment, pump 1, third are provided on the third pipeline 11 that the first basin 1 is connected to the second small basin 10
Pump 2 16 is provided on the 4th pipeline 12 that basin 3 is connected to the first small basin 9.11 one end of third pipeline is connected with first spray head
23, first spray head 23 is arranged in the second small basin 10, is provided on the third pipeline 11 between first spray head 23 and pump 1
The second control valve 26 is provided on first control valve 25, pump 1 and the first third pipeline 11 between basin 1, first adjusts
Section valve 25 and the second control valve 26 are used to adjust the flow of third pipeline 11, further include the first charging valve 27, the first liquid feeding
Valve 27 is used for into the first basin 1 plus flocculant, the third between the first charging valve 27 and pump 1 and the second control valve 26
Pipeline 11 is connected to.4th pipeline, 12 one end is connected with second spray head 24, and second spray head 24 is arranged in the first small basin 9, and second
The position of spray head 24 is lower than overflow passage 14, and the 5th pipeline 13 is inverted U shape with 4 connectivity part of the 4th basin, and enters with the 4th basin 4
The position of 5th pipeline 13 of mouth connection is lower than the position of second spray head 24.The 4th pipeline between second spray head 24 and pump 2 16
It is provided with third control valve 28 on 12, is provided with the 4th regulating valve on the 4th pipeline 12 between pump 2 16 and third basin 3
Door 29, third control valve 28 and the 4th control valve 29 are used to adjust the flow of the 4th pipeline 12.It is arranged on 5th pipeline 13
There is third valve 30, further include the 4th valve 31 and the 5th valve 32, the 4th valve 31 is connected to third control valve 28 and pump two
The 5th pipeline 13 between the 4th pipeline 12 between 16 and third valve 30 and the second small basin 10, the 5th valve 32 connection the
The 5th pipeline between the 4th pipeline 12 and third valve 30 and the 4th basin 4 between three control valves 28 and second spray head 24
13。
The present embodiment further includes first row air valve 33, second row air valve 34, third exhaust valve 35, the 4th exhaust valve 36 and
Five exhaust valves 37, first row air valve 33, second row air valve 34, third exhaust valve 35, the 4th exhaust valve 36 and the 5th exhaust valve 37
It is used to discharge air, first row air valve 33 is connected to the between the first basin 1 and third control valve 28 and the first small basin 9
Four pipelines 12, second row air valve 34 are arranged on the second basin 2, third exhaust valve 35 be connected to third basin 3 and the 4th basin 4 with
The 5th pipeline 13 between third valve 30, the 4th exhaust valve 36 are arranged on the 4th basin 4, the 5th exhaust valve 37 and the 4th storage
The 5th pipeline 13 connection between tank 4 and third valve 30.
The present embodiment further includes pump 3 17, and pump 3 17 is connected to by the 6th pipeline 38 with the upper end of the second small basin 10, the
The 5th control valve 39 is provided on six pipelines 38, the 5th control valve 39 is used to adjust the flow of the 6th pipeline 38, pump 3 17
It is connected to by the 7th pipeline 40 with the lower end of the second small basin 10, is provided with the 6th control valve 41 on the 7th pipeline 40, the 6th
Control valve 41 is used to adjust the flow of the 7th pipeline 40；3 17 are pumped as intermittent pump；Second small 10 bottom of basin is provided with row
Liquid valve 42, tapping valve 42 are used to for the useless turbid in the second small basin 10 being discharged.
The Chinese medicine flocculation clarification refining plant of the present embodiment is in use, the first control valve 25 and the second control valve 26 are beaten
It opens, remaining each valve is closed, and the flocculant of the first basin 1 is passed through the second small storage by first spray head 23 under the action of pumping 1
In tank 10, when flocculant is full of the first small basin 9, reactor tank 5 and the second small basin 10, pump 1 stops working, and closes first
Control valve 25 and the second control valve 26；Open third control valve 28 and the 4th control valve 29, the Chinese medicine of third basin 3
Extracting solution is slowly introducing in the first small basin 9 under the action of pumping 2 16 by second spray head 24, with leading to for Chinese medicine extract
Enter, extra flocculant flows into the second basin 2 by overflow passage 14 in the first small basin 9；The density of Chinese medicine extract is greater than
The density of flocculant, Chinese medicine extract slowly decline, and the sieve plate 8 in reactor tank 5 plays stirring action, Chinese medicine extract and flocculation
The mixed liquor of agent reacts in the first small basin 9, reactor tank 5 and the second small basin 10；Open the 3 17, the 5th control valve 39 of pump
With the 6th control valve 41, Chinese medicine extract and flocculant circulation are pushed, its reaction is accelerated；After reaction sufficiently, supernatant is formed
Liquid and useless turbid open third valve 30, and supernatant enters the 4th basin 4 by the 5th pipeline 13 under the action of siphon, lead to
It whether qualified crosses the supernatant that the second detection valve 22 takes liquid to carry out in the 4th basin 4 of detection, if unqualified, opens the second valve
Door 20 makes underproof liquid flow into third basin 3, is reacted again.
Using the present embodiment Chinese medicine flocculation clarification refining plant carry out Chinese medicine production, it is with short production cycle, Chinese medicine effectively at
Part is high, and strong operability, composition is cheap, remarkable benefit.
Apply that a specific example illustrates the principle and implementation of the invention in this specification, above embodiments
Explanation be merely used to help understand method and its core concept of the invention；At the same time, for those skilled in the art,
According to the thought of the present invention, there will be changes in the specific implementation manner and application range.In conclusion in this specification
Appearance should not be construed as limiting the invention.
Claims (10)
1. a kind of Chinese medicine flocculation clarification refining plant, it is characterised in that: including the first basin, the second basin, third basin, the 4th
Basin and reactor tank, first basin and second basin are by the first pipeline connection, the third basin and described the
Four basins pass through the second pipeline connection, are provided with several sieve plates in the reactor tank, the reactor tank top and bottom connect respectively
It is connected with the first small basin and the second small basin, first basin and the described second small basin are described by third pipeline connection
By the 4th pipeline connection, the second small basin passes through the 5th with the 4th basin for third basin and the described first small basin
Pipeline connection, the first small basin are connected to second basin by overflow passage, and first basin is for containing wadding
Solidifying agent, the third basin is for containing Chinese medicine extract.
2. Chinese medicine according to claim 1 flocculation clarification refining plant, it is characterised in that: first basin and described the
It is provided with pump one on the third pipeline of two small basin connections, the third basin is connected to described with the described first small basin
Pump two is provided on 4th pipeline.
3. Chinese medicine according to claim 1 flocculation clarification refining plant, it is characterised in that: first basin, described the
Liquid level is provided on two basins, the third basin, the 4th basin, the first small basin and the second small basin
Meter.
4. Chinese medicine flocculation clarification refining plant according to claim 1, it is characterised in that: be provided on first pipeline
First valve is provided with the second valve on second pipeline, further includes the first detection valve and the second detection valve, and described the
First pipeline connection between one detection valve and first valve and second basin, the second detection valve
With second pipeline connection between second valve and the 4th basin.
5. Chinese medicine flocculation clarification refining plant according to claim 2, it is characterised in that: the connection of third pipeline one end
There is first spray head, the first spray head is arranged in the described second small basin, the institute between the first spray head and the pump one
It states and is provided with the first control valve on third pipeline, be arranged on the third pipeline between the pump one and first basin
Have the second control valve, further include the first charging valve, first charging valve and it is described pump one and second control valve it
Between the third pipeline connection.
6. Chinese medicine flocculation clarification refining plant according to claim 2, it is characterised in that: the 4th pipeline one end connection
There is second spray head, the second spray head is arranged in the described first small basin, the institute between the second spray head and the pump two
It states and is provided with third control valve on the 4th pipeline, be arranged on the 4th pipeline between the pump two and the third basin
There is the 4th control valve.
7. Chinese medicine flocculation clarification refining plant according to claim 6, it is characterised in that: be provided on the 5th pipeline
Third valve, further includes the 4th valve and the 5th valve, and the 4th valve is connected to the third control valve and the pump two
Between the 4th pipeline and the third valve and the second small basin between the 5th pipeline, the 5th valve
Door is connected to the 4th pipeline between the third control valve and the second spray head and the third valve and described the
The 5th pipeline between four basins.
8. Chinese medicine according to claim 7 flocculation clarification refining plant, it is characterised in that: further include first row air valve, the
Two exhaust valves, third exhaust valve, the 4th exhaust valve and the 5th exhaust valve, the first row air valve are connected to first basin and institute
The 4th pipeline between third control valve and the first small basin is stated, the second row air valve is arranged described second
On basin, the third exhaust valve is connected to described between the third basin and the 4th basin and the third valve
Five pipelines, the 4th exhaust valve are arranged on the 4th basin, the 5th exhaust valve and the 4th basin and described
The 5th pipeline connection between third valve.
9. Chinese medicine flocculation clarification refining plant according to claim 1, it is characterised in that: it further include pump three, the pump three
It is connected to by the 6th pipeline with the upper end of the described second small basin, is provided with the 5th control valve on the 6th pipeline, it is described
Pump three is connected to by the 7th pipeline with the lower end of the described second small basin, is provided with the 6th control valve on the 7th pipeline；
The pump three is intermittent pump；The second small tank bottom is provided with tapping valve.
10. Chinese medicine flocculation clarification refining plant according to claim 1, it is characterised in that: it further include purge valve, it is described clear
It washes valve to be connected to the overflow passage, the sieve plate is porous sieve plate and is set side by side with several.
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