CN109115138A - A kind of boiler tube inner wall oxide film ultrasonic measurement couplant and preparation method thereof - Google Patents
A kind of boiler tube inner wall oxide film ultrasonic measurement couplant and preparation method thereof Download PDFInfo
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- CN109115138A CN109115138A CN201810919968.2A CN201810919968A CN109115138A CN 109115138 A CN109115138 A CN 109115138A CN 201810919968 A CN201810919968 A CN 201810919968A CN 109115138 A CN109115138 A CN 109115138A
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- couplant
- raw material
- preparation
- honey
- oxide film
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01B—MEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
- G01B17/00—Measuring arrangements characterised by the use of infrasonic, sonic or ultrasonic vibrations
- G01B17/02—Measuring arrangements characterised by the use of infrasonic, sonic or ultrasonic vibrations for measuring thickness
- G01B17/025—Measuring arrangements characterised by the use of infrasonic, sonic or ultrasonic vibrations for measuring thickness for measuring thickness of coating
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/22—Details, e.g. general constructional or apparatus details
- G01N29/28—Details, e.g. general constructional or apparatus details providing acoustic coupling, e.g. water
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/02—Indexing codes associated with the analysed material
- G01N2291/028—Material parameters
- G01N2291/02854—Length, thickness
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/02—Indexing codes associated with the analysed material
- G01N2291/028—Material parameters
- G01N2291/0289—Internal structure, e.g. defects, grain size, texture
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- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses a kind of boiler tube inner wall oxide film ultrasonic measurement couplants and preparation method thereof, its be formulated include following component raw material: honey 40-66%, glycerol 10-15%, 2-3% parts of antirust agent, viscosity agent 1-8% and surplus distilled water, by preparation step S1, the preparation of raw material；Couplant can be made in S2 after the operation of the mixing of raw material.The main component honey of raw material and glycerol is cheap in the present invention, and acquisition modes are convenient, reduce costs；Honey uses natural honey, highly-safe, and is using preceding filtering and impurity removing, purity is high, and be free from side effects, highly-safe；With excellent rustless property；The viscosity of couplant is suitable for various ultrasonic detection instruments in 300~85000mpa.s；Preparation method is simple, easy to operate.
Description
Technical field
The present invention relates to couplant and preparation method thereof technical field more particularly to a kind of boiler tube inner wall oxide film ultrasounds
Wave measurement couplant and preparation method thereof.
Background technique
Ultrasonic detecting equipment is that it is anti-to be based on ultrasonic pulse using newest high-performance, low-power microprocessor technology
Principle is penetrated, the thickness of metal and other multiple materials can be measured, the velocity of sound of material can also be measured.When probe emits
Ultrasonic pulse when reaching material interface by testee, pulse is reflected back toward probe by precise measurement ultrasonic wave
The time propagated in the material determines the thickness of measured material.Ultrasonic detecting equipment can be to pipes various in production equipment
Road and pressure vessel carry out thickness measure, monitor the thinned degree after they are corroded in use, can also be to various
Plate and various processing parts make precise measurement.
Couplant is a kind of water soluble polymer colloid, it is made for excluding the air between probe and testee
Ultrasonic energy effectively penetrates measured object and reaches effective testing goal.Industrial couplant be for exclude probe and testee it
Between air, so that ultrasonic energy is effectively penetrated the product that workpiece reaches testing goal.Currently, in industrial application, in order to drop
Low production cost, general industry couplant is mainly with machine oil, transformer oil, lubricating grease, glycerol, waterglass (sodium metasilicate
Na2SiO3) or industrial glue, chemical paste, or the dedicated couplant of ultrasound detection of commercialization, mostly liquid；Solid-state
Less, such as aluminium foil.But coupling tightness degree of the solid couplant under low-stress is very poor, and the scope of application is too small；
And when using industrial glue, chemical paste, machine oil these liquid couplant when, due to viscosity, although can be by vertical
Wave, but it cannot be only applicable to longitudinal wave detection, we have devised a kind of boiler tube thus by most of high-frequency shear wave
Inner wall oxide film ultrasonic measurement solves problem above with couplant and preparation method thereof.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of boiler tube inner wall oxide proposed
Film ultrasonic measurement couplant and preparation method thereof.
To achieve the goals above, present invention employs following technical solutions:
A kind of boiler tube inner wall oxide film ultrasonic measurement couplant, the raw material including following component: honey 40-66%, glycerol
10-15%, 2-3% parts of antirust agent, viscosity agent 1-8% and surplus distilled water.
Preferably, the distilled water of honey 56%, glycerol 12%, 2% part of antirust agent, viscosity agent 3% and surplus.
Preferably, the antirust agent is morpholine.
Preferably, the viscosity agent is gel-type vehicle.
A kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that including following
Step,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 40-66%, glycerol 10-15%, 2-3% parts of antirust agent, viscosity agent 1-8%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, and then heating stirring 30-50 minutes, heating
Temperature is 40-60 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent is added in last 3-5 minutes of stirring, stirs
After mixing technology, makes mixture natural cooling, couplant can be obtained.
Preferably, the sieve in the S1 is 200 mesh.
The invention has the benefit that raw material main component honey and glycerol it is cheap, and acquisition modes are convenient,
It reduces costs；Honey uses natural honey, highly-safe, and is using preceding filtering and impurity removing, purity is high, and be free from side effects,
It is highly-safe；With excellent rustless property；The viscosity of couplant is suitable for various ultrasonic waves in 300~85000mpa.s
Detecting instrument；Preparation method is simple, easy to operate.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.
Embodiment one
A kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that include the following steps,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 40%, glycerol 10%, 2% part of antirust agent, viscosity agent 1%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, then heating stirring 30 minutes, heating temperature
Degree is 40 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent, stirring technique is added in last 3 minutes of stirring
Afterwards, make mixture natural cooling, couplant can be obtained.
Embodiment two
A kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that include the following steps,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 45%, glycerol 12%, 2.2% part of antirust agent, viscosity agent 5%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, then heating stirring 35 minutes, heating temperature
Degree is 46 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent, stirring technique is added in last 4 minutes of stirring
Afterwards, make mixture natural cooling, couplant can be obtained.
Embodiment three
A kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that include the following steps,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 48%, glycerol 13%, 2.4% part of antirust agent, viscosity agent 6%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, then heating stirring 40 minutes, heating temperature
Degree is 52 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent, stirring technique is added in last 4 minutes of stirring
Afterwards, make mixture natural cooling, couplant can be obtained.
Example IV
A kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that include the following steps,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 56%, glycerol 14%, 2.8% part of antirust agent, viscosity agent 7%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, then heating stirring 45 minutes, heating temperature
Degree is 55 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent, stirring technique is added in last 5 minutes of stirring
Afterwards, make mixture natural cooling, couplant can be obtained.
Embodiment five
A kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that include the following steps,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 66%, glycerol 15%, 3% part of antirust agent, viscosity agent 8%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, then heating stirring 50 minutes, heating temperature
Degree is 60 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent, stirring technique is added in last 5 minutes of stirring
Afterwards, make mixture natural cooling, couplant can be obtained.
In the above-described embodiments, the additive amount that viscosity agent is adjusted in proportional region needs to make the viscosity of couplant obtained
In the range of 300~85000mpa.s.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (6)
1. a kind of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that the raw material including following component: bee
Sweet 40-66%, glycerol 10-15%, 2-3% parts of antirust agent, viscosity agent 1-8% and surplus distilled water.
2. a kind of boiler tube inner wall oxide film ultrasonic measurement couplant according to claim 1, which is characterized in that bee
Sweet 56%, the distilled water of glycerol 12%, 2% part of antirust agent, viscosity agent 3% and surplus.
3. a kind of boiler tube inner wall oxide film ultrasonic measurement couplant according to claim 1, which is characterized in that institute
Stating antirust agent is morpholine.
4. a kind of boiler tube inner wall oxide film ultrasonic measurement couplant according to claim 1, which is characterized in that institute
Stating viscosity agent is gel-type vehicle.
5. a kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant, which is characterized in that including following step
Suddenly,
S1, the preparation of raw material: the natural honey in raw material is filtered using sieve, by the contaminant filter plate in natural honey
Fall, then proportionally weighs raw material, honey 40-66%, glycerol 10-15%, 2-3% parts of antirust agent, viscosity agent 1-8%；
S2, the mixing of raw material: honey and distilled water are first added in reaction kettle, and then heating stirring 30-50 minutes, heating
Temperature is 40-60 DEG C, and glycerol and antirust agent are sequentially added in whipping process, viscosity agent is added in last 3-5 minutes of stirring, stirs
After mixing technology, makes mixture natural cooling, couplant can be obtained.
6. a kind of preparation method of boiler tube inner wall oxide film ultrasonic measurement couplant according to claim 5,
It is characterized in that, the sieve in the S1 is 200 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810919968.2A CN109115138A (en) | 2018-08-14 | 2018-08-14 | A kind of boiler tube inner wall oxide film ultrasonic measurement couplant and preparation method thereof |
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|---|---|---|---|
| CN201810919968.2A CN109115138A (en) | 2018-08-14 | 2018-08-14 | A kind of boiler tube inner wall oxide film ultrasonic measurement couplant and preparation method thereof |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10338063A1 (en) * | 2003-08-19 | 2005-03-17 | Daimlerchrysler Ag | Ultrasonic method for measuring the cylinder lining thickness in a crankcase, in which a liquid couplant is used to couple the ultrasonic probe to the cylinder lining |
| CN105194695A (en) * | 2015-10-28 | 2015-12-30 | 湖南工程学院 | Coupling agent and preparation method thereof |
| CN105259258A (en) * | 2015-10-28 | 2016-01-20 | 湘乡宏进电子科技有限公司 | Coupling agent for ultrasonic measurement of boiler pipe inner wall oxidation film and preparation method thereof |
| CN105371791A (en) * | 2015-10-28 | 2016-03-02 | 湘潭宏远电子科技有限公司 | Industrial coupling agent for metal thickness measurement, and preparation method therefor |
| CN105423968A (en) * | 2015-10-28 | 2016-03-23 | 湘潭宏远电子科技有限公司 | Transverse wave couplant for power station boiler steel pipe inner wall oxide-film high frequency ultrasonic measurement, and preparation method thereof |
| CN106645431A (en) * | 2015-10-28 | 2017-05-10 | 湘潭宏远电子科技有限公司 | Industrial couplant used for metal defect detection, and preparation method thereof |
| CN108132307A (en) * | 2017-10-26 | 2018-06-08 | 湖南金化科技集团有限公司 | A kind of rail examination industry couplant and preparation method thereof |
| CN108287198A (en) * | 2017-01-07 | 2018-07-17 | 北京鑫泽源铁路技术发展有限公司 | Steel rail ultrasonic flaw detecting couplant and its preparation method |
-
2018
- 2018-08-14 CN CN201810919968.2A patent/CN109115138A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10338063A1 (en) * | 2003-08-19 | 2005-03-17 | Daimlerchrysler Ag | Ultrasonic method for measuring the cylinder lining thickness in a crankcase, in which a liquid couplant is used to couple the ultrasonic probe to the cylinder lining |
| CN105194695A (en) * | 2015-10-28 | 2015-12-30 | 湖南工程学院 | Coupling agent and preparation method thereof |
| CN105259258A (en) * | 2015-10-28 | 2016-01-20 | 湘乡宏进电子科技有限公司 | Coupling agent for ultrasonic measurement of boiler pipe inner wall oxidation film and preparation method thereof |
| CN105371791A (en) * | 2015-10-28 | 2016-03-02 | 湘潭宏远电子科技有限公司 | Industrial coupling agent for metal thickness measurement, and preparation method therefor |
| CN105423968A (en) * | 2015-10-28 | 2016-03-23 | 湘潭宏远电子科技有限公司 | Transverse wave couplant for power station boiler steel pipe inner wall oxide-film high frequency ultrasonic measurement, and preparation method thereof |
| CN106645431A (en) * | 2015-10-28 | 2017-05-10 | 湘潭宏远电子科技有限公司 | Industrial couplant used for metal defect detection, and preparation method thereof |
| CN106643590A (en) * | 2015-10-28 | 2017-05-10 | 湘潭宏远电子科技有限公司 | Transverse wave couplant and preparation method thereof |
| CN108287198A (en) * | 2017-01-07 | 2018-07-17 | 北京鑫泽源铁路技术发展有限公司 | Steel rail ultrasonic flaw detecting couplant and its preparation method |
| CN108132307A (en) * | 2017-10-26 | 2018-06-08 | 湖南金化科技集团有限公司 | A kind of rail examination industry couplant and preparation method thereof |
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Application publication date: 20190101 |