CN109112832A - A kind of method of collagen-Compound-acid modified cotton fabric - Google Patents
A kind of method of collagen-Compound-acid modified cotton fabric Download PDFInfo
- Publication number
- CN109112832A CN109112832A CN201810857982.4A CN201810857982A CN109112832A CN 109112832 A CN109112832 A CN 109112832A CN 201810857982 A CN201810857982 A CN 201810857982A CN 109112832 A CN109112832 A CN 109112832A
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- Prior art keywords
- compound
- acid
- cotton fabric
- collagen
- modified cotton
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/507—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
Abstract
The invention discloses a kind of collagen-Compound-acid modified cotton fabric methods, include: (1) by cotton fabric to be modified be respectively 95% with deionized water and concentration under the conditions of temperature is 80~100 DEG C dehydrated alcohol sonic oscillation cleans repeatedly, be dried for standby；(2) Compound-acid is added in deionized water with the volume ratio of 1:10~50,30~40min of magnetic agitation under 50~60 DEG C of water bath condition, obtain Compound-acid solution, wherein the Compound-acid is the mixture of the polylactic acid that the ratio between amount of substance is 1:1~3 and citric acid；(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges adhesive, stir 20~30min, the cotton fabric in step (1) is added, cotton fabric is arranged using " second dipping and rolling " technique, wherein, soaking temperature is 60 DEG C, soaking time is 30~40min, and drying obtains the modified cotton fabric of Compound-acid.In the present invention, there is preferable ultraviolet-resistent property using the modified cotton fabric of collagen-Compound-acid, and be unlikely to deform.
Description
Technical field
The present invention relates to fabric arts, more particularly to a kind of collagen-Compound-acid modified cotton fabric method.
Background technique
In recent years, the requirement with people to living standard is higher and higher, while cosily enjoying life, to atmosphere
A large amount of fluorine, the chlorine compound of middle discharge, the destruction for making ozone layer be on the rise.Reach the amount of ultraviolet irradiation on ground
Increase, it is also increasingly severe to the injury of human body, therefore the research of physical protection ultraviolet radiation is paid attention to.Clothes are
The most effective protection tool of human body so it is necessary to carry out anti-ultraviolet finishing to textile, and can prevent ultraviolet light pair
The injury of skin, but the research for being able to maintain the original performance of fabric has become one of important topic of Dyeing Industry.
Pure cotton fabric has good hygroscopicity, penetrability, and soft, comfortable and easy to wear, especially pure cotton poplin cloth is even more
High-grade wearing fabric, is typically used as high-grade underlinen fabric.However the garment material as summer, existing main problem are anti-
Imparted energy is undesirable, is easily deformed.In order to improve the uvioresistant performance of pure cotton fabric and reduce deformation extent, it is necessary to pure
Cotton fabric carries out functional treatment.
For this reason, it is necessary in view of the above-mentioned problems, a kind of method for proposing collagen-Compound-acid modified cotton fabric, energy
Enough solve problems of the prior art.
Summary of the invention
The purpose of the present invention is to provide a kind of collagen-Compound-acid modified cotton fabric methods, to overcome existing skill
Deficiency in art.
To achieve the above object, the invention provides the following technical scheme:
A kind of method of collagen-Compound-acid modified cotton fabric, comprising:
It (1) with deionized water and concentration is respectively 95% under the conditions of temperature is 80~100 DEG C by cotton fabric to be modified
Dehydrated alcohol repeatedly sonic oscillation clean, be dried for standby；
(2) Compound-acid is added in deionized water with the volume ratio of 1:10~50, the magnetic under 50~60 DEG C of water bath condition
Power stirs 30~40min, obtains Compound-acid solution, wherein the Compound-acid is the polylactic acid that the ratio between amount of substance is 1:1~3
With the mixture of citric acid；
(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges
Adhesive stirs 20~30min, adds the cotton fabric in step (1), is carried out using " second dipping and rolling " technique to cotton fabric whole
Reason, wherein soaking temperature is 60 DEG C, and soaking time is 30~40min, and drying obtains the modified cotton fabric of Compound-acid.
Preferably, in step (2), the ratio between volume of the Compound-acid and the ionized water is 1:30.
Preferably, in step (2), the ratio between amount of substance of the polylactic acid and the citric acid is 1:2.
Preferably, in step (3), the mass fraction of collagen is 1~3% in the finishing fluid.
Preferably, the mass fraction of collagen is 2% in the finishing fluid.
Preferably, in step (3), described adhesive is selected from aliphatic polyurethane binders or palyacrylate binder.
Compared with the prior art, the advantages of the present invention are as follows: in the present invention, using the modified cotton of collagen-Compound-acid
Fabric has preferable ultraviolet-resistent property, and is unlikely to deform.
Specific embodiment
The present invention is described further by the following example: according to following embodiments, the present invention may be better understood.
However, as it will be easily appreciated by one skilled in the art that specific material ratio, process conditions and its result described in embodiment are only used
In illustrating the present invention, without the present invention described in detail in claims should will not be limited.
A kind of method that the present invention discloses collagen-Compound-acid modified cotton fabric, comprising:
It (1) with deionized water and concentration is respectively 95% under the conditions of temperature is 80~100 DEG C by cotton fabric to be modified
Dehydrated alcohol repeatedly sonic oscillation clean, be dried for standby；
(2) Compound-acid is added in deionized water with the volume ratio of 1:10~50, the magnetic under 50~60 DEG C of water bath condition
Power stirs 30~40min, obtains Compound-acid solution, wherein the Compound-acid is the polylactic acid that the ratio between amount of substance is 1:1~3
With the mixture of citric acid；
(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges
Adhesive stirs 20~30min, adds the cotton fabric in step (1), is carried out using " second dipping and rolling " technique to cotton fabric whole
Reason, wherein soaking temperature is 60 DEG C, and soaking time is 30~40min, and drying obtains the modified cotton fabric of Compound-acid.
In step (2), the ratio between volume of the Compound-acid and the ionized water is 1:30；The polylactic acid and the lemon
The ratio between amount of substance of acid is 1:2.
In step (3), the mass fraction of collagen is 1~3% in the finishing fluid, it is preferred that in the finishing fluid
The mass fraction of collagen is 2%；Described adhesive is selected from aliphatic polyurethane binders or palyacrylate binder.
It is following that collagen in the present invention-Compound-acid modified cotton fabric method is illustrated with specifically embodiment.
Embodiment 1
(1) by cotton fabric to be modified under the conditions of temperature is 80 DEG C respectively with deionized water and concentration be 95% it is anhydrous
Sonic oscillation cleans ethyl alcohol repeatedly, is dried for standby；
(2) Compound-acid is added in deionized water with the volume ratio of 1:10, the magnetic agitation under 50 DEG C of water bath condition
30min obtains Compound-acid solution, wherein the Compound-acid is the mixing of the polylactic acid that the ratio between amount of substance is 1:1 and citric acid
Object；
(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges
Adhesive is stirred 20min, adds the cotton fabric in step (1), arranged using " second dipping and rolling " technique to cotton fabric,
Wherein, soaking temperature is 60 DEG C, soaking time 30min, drying, obtains the modified cotton fabric of Compound-acid.
Embodiment 2
(1) by cotton fabric to be modified under the conditions of temperature is 90 DEG C respectively with deionized water and concentration be 95% it is anhydrous
Sonic oscillation cleans ethyl alcohol repeatedly, is dried for standby；
(2) Compound-acid is added in deionized water with the volume ratio of 1:30, the magnetic agitation under 55 DEG C of water bath condition
35min obtains Compound-acid solution, wherein the Compound-acid is the mixing of the polylactic acid that the ratio between amount of substance is 1:2 and citric acid
Object；
(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges
Adhesive is stirred 25min, adds the cotton fabric in step (1), arranged using " second dipping and rolling " technique to cotton fabric,
Wherein, soaking temperature is 60 DEG C, soaking time 35min, drying, obtains the modified cotton fabric of Compound-acid.
Embodiment 3
(1) nothing for being respectively 95% with deionized water and concentration under the conditions of temperature is 100 DEG C by cotton fabric to be modified
Sonic oscillation cleans water-ethanol repeatedly, is dried for standby；
(2) Compound-acid is added in deionized water with the volume ratio of 1:50, the magnetic agitation under 60 DEG C of water bath condition
40min obtains Compound-acid solution, wherein the Compound-acid is the mixing of the polylactic acid that the ratio between amount of substance is 1:3 and citric acid
Object；
(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges
Adhesive is stirred 30min, adds the cotton fabric in step (1), arranged using " second dipping and rolling " technique to cotton fabric,
Wherein, soaking temperature is 60 DEG C, soaking time 40min, drying, obtains the modified cotton fabric of Compound-acid.
Uvioresistant experiment is carried out to the cotton fabric arranged using the above method, the results showed that, the sun-proof finger of the cotton fabric
Number UPF can reach 35+~40+；Morphotropism test is carried out to the cotton fabric, the results showed that, which has preferable resistance
Shape ability.
Finally, it is to be noted that, the terms "include", "comprise" or its any other variant be intended to it is non-exclusive
Property include so that include a series of elements process, method, article or equipment not only include those elements, but also
Further include other elements that are not explicitly listed, or further include for this process, method, article or equipment it is intrinsic
Element.
Claims (6)
1. a kind of collagen-Compound-acid modified cotton fabric method characterized by comprising
(1) nothing for being respectively 95% with deionized water and concentration under the conditions of temperature is 80~100 DEG C by cotton fabric to be modified
Sonic oscillation cleans water-ethanol repeatedly, is dried for standby；
(2) Compound-acid is added in deionized water with the volume ratio of 1:10~50, magnetic force stirs under 50~60 DEG C of water bath condition
30~40min is mixed, Compound-acid solution is obtained, wherein the Compound-acid is the polylactic acid and lemon that the ratio between amount of substance is 1:1~3
The mixture of lemon acid；
(3) collagen is dissolved in the Compound-acid solution and is configured to certain density finishing fluid, clothing is added and arranges bonding
Agent is stirred 20~30min, adds the cotton fabric in step (1), arranged using " second dipping and rolling " technique to cotton fabric,
Wherein, soaking temperature is 60 DEG C, and soaking time is 30~40min, and drying obtains the modified cotton fabric of Compound-acid.
2. collagen according to claim 1-Compound-acid modified cotton fabric method, which is characterized in that step (2)
In, the ratio between volume of the Compound-acid and the ionized water is 1:30.
3. collagen according to claim 1-Compound-acid modified cotton fabric method, which is characterized in that step (2)
In, the ratio between amount of substance of the polylactic acid and the citric acid is 1:2.
4. collagen according to claim 1-Compound-acid modified cotton fabric method, which is characterized in that step (3)
In, the mass fraction of collagen is 1~3% in the finishing fluid.
5. collagen according to claim 4-Compound-acid modified cotton fabric method, which is characterized in that the arrangement
The mass fraction of collagen is 2% in liquid.
6. collagen according to claim 1-Compound-acid modified cotton fabric method, which is characterized in that step (3)
In, described adhesive is selected from aliphatic polyurethane binders or palyacrylate binder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810857982.4A CN109112832A (en) | 2018-07-31 | 2018-07-31 | A kind of method of collagen-Compound-acid modified cotton fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810857982.4A CN109112832A (en) | 2018-07-31 | 2018-07-31 | A kind of method of collagen-Compound-acid modified cotton fabric |
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| Publication Number | Publication Date |
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| CN109112832A true CN109112832A (en) | 2019-01-01 |
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| CN201810857982.4A Pending CN109112832A (en) | 2018-07-31 | 2018-07-31 | A kind of method of collagen-Compound-acid modified cotton fabric |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110106706A (en) * | 2019-05-23 | 2019-08-09 | 叶盛 | A kind of preparation method of modified protein UV resistance finishing agent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110106706A (en) * | 2019-05-23 | 2019-08-09 | 叶盛 | A kind of preparation method of modified protein UV resistance finishing agent |
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