CN109111969A - The experimental provision and experimental method that gas hydrates generate when a kind of simulation pipeline sudden contraction - Google Patents

The experimental provision and experimental method that gas hydrates generate when a kind of simulation pipeline sudden contraction Download PDF

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Publication number
CN109111969A
CN109111969A CN201810736891.5A CN201810736891A CN109111969A CN 109111969 A CN109111969 A CN 109111969A CN 201810736891 A CN201810736891 A CN 201810736891A CN 109111969 A CN109111969 A CN 109111969A
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experimental
experiment
pipeline
gas
simulation
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何岩峰
夏程
夏一程
窦祥骥
王相
邓嵩
张世锋
徐慧
赵虹宇
刘成
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Changzhou University
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Changzhou University
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/10Working-up natural gas or synthetic natural gas
    • C10L3/108Production of gas hydrates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/002Component parts of these vessels not mentioned in B01J3/004, B01J3/006, B01J3/02 - B01J3/08; Measures taken in conjunction with the process to be carried out, e.g. safety measures

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Pipeline Systems (AREA)

Abstract

The experimental provision and experimental method generated the present invention provides gas hydrates when a kind of simulation pipeline sudden contraction, it rationally designs the experimental provision that gas hydrates generate when simulating pipeline sudden contraction and rationally designs experimental method, by the flowing velocity for controlling pipeline, and caliber is tested than the shape with sudden contraction connecting pipe by changing upstream and downstream, interior flow mechanism is managed in research, and in the formation mechenism of metallic conduit adhesion and aggregation after analog study gas hydrate synthesis, the transport of exploitation and natural gas to gas hydrates is significant.

Description

The experimental provision and experiment that gas hydrates generate when a kind of simulation pipeline sudden contraction Method
Technical field
The present invention relates to natural when gas hydrates production and transport technical field more particularly to a kind of simulation pipeline sudden contraction The experimental provision and experimental method that gas hydrate generates.
Background technique
With the increasingly deficient of landing field petroleum resources and people are more and more to the exploration of Marine oil and gas resource, naturally Gas hydrate is resourceful, especially payes attention to the exploitation to deep water hydrocarbon resource.Obtaining from underwater installation is especially exploited under deep water conditions Have become possibility with production conveying petroleum resources, but there is many important in gas hydrates production and transport Problem, wherein most obviously be also most serious be exactly variable diameter sudden contraction transport pipeline blocking accident.The blocking of transport pipeline can make It at the interruption of transport, causes to leak, pollutes environment, so that oil gas transportation industry is difficult to normal operation, consequence is very serious.
But for a long time, people to hydrate produce and transportational process in encounter the research of variable diameter sudden contraction and few, And also not deep enough to research forming process of the pipe shape thickness to gas hydrate synthesis, at home and abroad there is no simulations to manage at present The experimental provision and method that hydrate when road sudden contraction generates.These all fully understand that different pipeline diameter combination variable diameters are prominent to us It contracts the blocking of hydrate and how to cope with this blocking and cause very big difficulty.
Summary of the invention
The technical problem to be solved by the present invention is in order to not there is hydrate when simulation pipeline sudden contraction to generate in the prior art Experimental provision and experimental method, the present invention provide it is a kind of different pipeline diameters can be combined the blocking of hydrate under variable diameter sudden contraction with And gas hydrates generate when how should be to a kind of simulation pipeline sudden contraction that this blocking is tested experimental provision and reality Proved recipe method.
The technical solution adopted by the present invention to solve the technical problems is: hydrate generates when a kind of simulation pipeline sudden contraction Experimental provision, including experimental simulation system, infusion fluid systems, the circulatory system, temperature control system, pressure-measuring system, pressure Force control system and monitoring storage system, infusion fluid systems and circulatory system piping connection simultaneously provide multiphase for the circulatory system Stream, the pressure-measuring system are arranged between infusion fluid systems and experimental simulation system pipeline, the monitoring storage In experimental simulation system side, monitoring storage system includes monitoring the acoustic detection of sound wave inside experimental simulation system for system setting The high-speed camera of device and storage experimentation;The experimental simulation system includes experiment bin and is fixed by mounting flange Main experimental channel in experiment bin, the main experimental channel includes downstream experimental channel and upstream experimental channel, under described It swims between experimental channel and upstream experimental channel through connecting pipe pipeline connection, the control pressurer system and downstream experiment tube Road pipeline connection, the circulatory system, control pressurer system and upstream experimental channel pipeline connection are corresponding in the experiment bin Visual windows are provided at connecting line, the high-speed camera corresponds to visual windows setting, and the temperature control system includes Temperature control equipment below experiment bin is set.
Further, pass through flanged joint between downstream experimental channel, connecting pipe and upstream experimental channel.Downstream experiment Other dismountable connection methods such as threaded connection can also be used between pipeline, connecting pipe and upstream experimental channel.
Further, the experiment bin of the experimental simulation system is fixed on experiment rotatable platform.
Further, the circulatory system includes solution liquid pool and connection solution liquid pool and experimental simulation system The circulation line between mounting flange under the upstream experimental channel of circulation line, the solution liquid pool and experimental simulation system On be also successively arranged recirculated water water inlet control valve, intake pump, force (forcing) pump and recirculated water outlet water control valve.
Further, infusion fluid systems include multiphase flow splitting device, and the multiphase flow splitting device and solution match liquid Slot pipeline connection.
Further, pressure-measuring system piping connection is in multiphase flow splitting device and experimental simulation system downstream experiment tube Between the mounting flange of road, including the relief valve, safety overflow valve and flowmeter being successively set on pipeline.
Further, control pressurer system includes gas source and is connected under gas source and experimental simulation system upstream experiment pipeline Mounting flange between pressure piping, be successively arranged gas control on the pressure piping between the gas source and mounting flange Valve, gas booster pump and pressure gauge.
A kind of experimental method for the experimental provision that hydrate generates when simulation pipeline sudden contraction, including following experimental procedure:
A, the Preparatory work of experiment stage:
First with getting the solution of required concentration ready in solution matching slot, closed safe relief valve, recirculated water water inlet control valve, Experiment bin is opened, checks that the docking of pipeline coincide, screws pipeline mounting flange, close experiment bin;Open recirculated water water inlet control Valve, starting intake pump, liquid needed for injecting into experiment simulation storehouse, flooding circulating water pipeline outlet up to liquid level is Only, it is then shut off recirculated water water inlet control valve and intake pump, makes water circulation in experimental temperature control device, makes temperature control Device processed reaches experiment required temperature, starts intake pump and force (forcing) pump, guarantees the liquid flowing in the combination of experiment bin inner tube;It opens Gas booster pump and gas control valve, starting gas booster pump are started to work, and pressure in pressure gauge are read, to pressure interior in pipeline After reaching pressure needed for operating condition of test, gas booster pump is closed, opens overflow relief valve;Light source is opened, from form is illuminated to reality Polishing in testing position, starting high-speed camera, acoustic detection device and computer, guarantees high-speed camera and acoustic detection device pair Quasi- observation window completes the Preparatory work of experiment stage;
B, the progress stage is tested:
When temperature reaches experiment set temperature in experiment bin, gas injection control valve is opened, gas boosting is then opened Pump controls gas flowmeter flow, starts to simulate the experiment of the confluence flowing in main experimental channel, is grabbed automatically with high-speed camera Mobility status of the bubble on main experimental channel is clapped, adsorbs situation, Yi Jishui with the aggregation of acoustic detection device detection hydrate Formation and the aggregation blocking of object are closed, gas flow is certain, and circulating water flow is certain, and observes that pipeline has hydrate shape As only, an experimentation terminates, and the image data that high-speed camera is captured passes to computer by data line and stored;
C, pipe stage is replaced:
After upper one group of experiment, first closing temperature control device opens the safety relief valve pressure release of experimental channel, closes Closed loop water water inlet control valve and recirculated water outlet water control valve are opened the drain valve of experiment bin lower end, are discharged in main experimental channel Medium replace next group of experimental channel combination, repeat upper two step and continue to test, if you need to be further added by according to requirement of experiment Experimental channel combination repeats A, B, step C is tested;
D, ending phase is tested:
First closing temperature control device opens the safety relief valve pressure release of experimental channel, closes recirculated water water inlet control valve With recirculated water outlet water control valve, closed safe overflow valve opens the drain valve of experiment bin lower end, after this is tested in experiment bin Sewage be vented to pond, experiment terminates.
The invention has the advantages that the reality that gas hydrates generate when a kind of simulation pipeline sudden contraction provided by the invention Experiment device and experimental method rationally design the experimental provision that gas hydrates generate when simulating pipeline sudden contraction and rationally design reality Proved recipe method tests caliber than the shape with sudden contraction connecting pipe by controlling the flowing velocity of pipeline, and by changing upstream and downstream Interior flow mechanism is managed in shape, research, and in the formation mechenism of metallic conduit adhesion and aggregation after analog study gas hydrate synthesis, to natural The exploitation of gas hydrate and the transport of natural gas are significant.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is the structural schematic diagram of optimum embodiment of the present invention.
Fig. 2 is the structural schematic diagram of experimental simulation system in the present invention.
Fig. 3 is the schematic diagram that kinds of experiments pipeline combines in experimental simulation system in the present invention.
1 in figure, solution matching slot 2, recirculated water water inlet control valve 3, intake pump 4, force (forcing) pump 5-1, spend control device 6, experiment bin 6-1, upstream experimental channel 6-2, connecting pipe 6-3, downstream experimental channel 6-4, mounting flange 6-5, visual Window 7, experiment rotatable platform 8, flowmeter 9, safety overflow valve 10, multiphase flow splitting device 11, relief valve 12, gas Body booster pump 13, gas control valve 14,15 acoustic detection device 16 of pressure gauge, high-speed camera.
Specific embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These attached drawings are simplified schematic diagram, only with Illustration illustrates basic structure of the invention, therefore it only shows the composition relevant to the invention.
The experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as shown in Figure 1 to Figure 3, including experiment simulation system System, infusion fluid systems, the circulatory system, temperature control system, pressure-measuring system, control pressurer system and monitoring storage system System.
Infusion fluid systems and circulatory system piping connection simultaneously provide multiphase flow, the pressure measurement system for the circulatory system System is arranged between infusion fluid systems and experimental simulation system pipeline, and the monitoring storage system setting is in experiment simulation system System side, monitoring storage system include monitoring the acoustic detection device 15 of sound wave inside experimental simulation system and storing experimentation High-speed camera 16.
It tests simulation system and provides the metallic conduit environment that Hydrate Plugging is formed under simulated high-pressure, low temperature to test.Experiment The main experimental channel that simulation system includes experiment bin 6 and is fixed in experiment bin 6 by mounting flange 6-4.Experimental simulation system Experiment bin 6 be fixed on experiment rotatable platform 7 on.Rotatable platform 7 can top experiment bin carry out angular adjustment, Ke Yijin The pipeline experiment of the horizontal positioned angle of row can also be carried out placing pipeline experiment vertically, can also be carried out with certain tilt angle Place the experiment of pipeline.It influences, plays caused by being generated by the flowing of 7 analog gravity convection body of rotatable platform and hydrate Pipeline is not fixed the effect of the experiment simulation of angle placement in Practical Project.
Main experimental channel includes downstream experimental channel 6-3 and upstream experimental channel 6-1, the downstream experimental channel 6-3 and Pass through connecting pipe 6-2 pipeline connection, the control pressurer system and downstream experimental channel 6-3 between the experimental channel 6-1 of upstream Pipeline connection, the circulatory system, control pressurer system and upstream experimental channel 6-1 pipeline connection are right in the experiment bin 6 It answers and is provided with visual windows 6-5 at connecting line 6-2, the corresponding visual windows 6-5 setting of the high-speed camera 16.
Temperature control system provides required temperature environment for experimental model system, and the temperature control system includes setting Set the temperature control equipment 5-1 below experiment bin 6.
Further, connected between downstream experimental channel 6-3, connecting pipe 6-2 and upstream experimental channel 6-1 by flange It connects.Threaded connection etc. can also be used between downstream experimental channel 6-3, connecting pipe 6-2 and upstream experimental channel 6-1, and other are removable The connection method unloaded.In specific experiment, a variety of downstream experimental channel 6-3 and upstream experimental channel 6-1 can be designed as needed Between caliber ratio, the sudden contraction shape of a variety of connecting pipe 6-2 is provided, replaces and tests in an experiment.
Corresponding main experimental channel, also has the drainage system for being connected to 6 lower end of experiment bin, including be connected under experiment bin 6 The drain valve at end, for testing after sewage discharge.
The circulatory system then provides for experimental model system into dress liquid.The circulatory system can effectively simulate pipeline liquid flowing ring Border.The circulatory system includes solution liquid pool 1 and the circulation line for connecting solution liquid pool 1 and experimental simulation system, the solution It is also successively set on the circulation line between mounting flange 6-4 under the upstream experimental channel 6-1 of liquid pool 1 and experimental simulation system There are recirculated water water inlet control valve 2, intake pump 3, force (forcing) pump 4 and recirculated water outlet water control valve.
Infusion fluid systems are that solution liquid pool 1 injects multiphase flow.Infusion fluid systems include multiphase flow splitting device 10, The multiphase flow splitting device 10 and 1 pipeline connection of solution liquid pool.
Pressure-measuring system can effectively measure the pressure after main experimental channel confluence gas, pressure-measuring system piping connection Between the mounting flange 6-4 on multiphase flow splitting device 10 and experimental simulation system downstream experiment pipeline 6-3, including successively set Set relief valve 11, safety overflow valve 9 and flowmeter 8 on pipeline.
Control pressurer system include gas source and be connected to gas source and experimental simulation system upstream experiment pipeline 6-1 under fixation Pressure piping between flange 6-4 is successively arranged gas control valve on the pressure piping between the gas source and mounting flange 6-4 13, gas booster pump 12 and pressure gauge 14.
Main experimental channel flow pressure drop under certain temperature, pressure condition can be measured using above-mentioned experimental provision, it can be achieved that Different upstream and downstream caliber ratios, the drop measurement of different medium;Main pipeline under certain temperature, pressure condition can be simulated to obtain and divided The confluence flowing and the formation of hydrate of branch pipe(tube);Pipelines combination can be tested, pipelines angle provides for experiment Diversity choice;Acoustic detection device 15 and high-speed camera 16 are circumscribed with computer, can receive sound wave by computer and visit The data that device 15 and high-speed camera 16 are collected are surveyed, by storing image data in processing computer, can analyze difference Caliber is than the gas hydrate synthesis mechanism under, gas with various flow velocity, different solid phase particles concentration, flow rate of liquid.
Using above-mentioned experimental provision, gas hydrates are generated when analog pipeline sudden contraction, have following experimental procedure:
A, the Preparatory work of experiment stage:
First with the solution for getting required concentration ready, closed safe relief valve 11, recirculated water water inlet control in solution matching slot 1 Valve 2 opens experiment bin 6, checks that the docking of pipeline coincide, screws pipeline mounting flange 6-4, close experiment bin 6;Open recirculated water Water inlet control valve 2 starts intake pump 3, liquid needed for injecting into experiment simulation storehouse, until liquid level floods circulating water pipe Until road exports, it is then shut off recirculated water water inlet control valve 2 and intake pump 3, recycles water in experimental temperature control device 5-1 Circulation makes temperature control equipment reach experiment required temperature, starts intake pump 3 and force (forcing) pump 4, guarantees the combination of 6 inner tube of experiment bin In liquid flowing;Gas booster pump 12 and gas control valve 13 are opened, starting gas booster pump 12 is started to work, and pressure is read Pressure in table 14 closes gas booster pump 20 after pressure interior in pipeline reaches pressure needed for operating condition of test, opens overflow safety Valve 9;Light source is opened, from illumination form polishing into experiment bin 6, starting high-speed camera 16, acoustic detection device 15 and calculating Machine guarantees that high-speed camera 16 and acoustic detection device 15 are directed at observation window, completes the Preparatory work of experiment stage;
B, the progress stage is tested:
When temperature reaches experiment set temperature in experiment bin 6, gas injection control valve 13 is opened, gas is then opened and increases Press pump 12 controls gas flowmeter flow, starts to simulate the experiment of the confluence flowing in main experimental channel, with high-speed camera 16 The automatic mobility status for capturing bubble on main experimental channel adsorbs feelings with the aggregation that acoustic detection device 15 detects hydrate The formation of condition and hydrate and aggregation blocking, gas flow is certain, and circulating water flow is certain, and observes pipeline Until having gas hydrate synthesis, an experimentation terminates, and the image data that high-speed camera 16 is captured passes to meter by data line Calculation machine is stored;
C, pipe stage is replaced:
After upper one group of experiment, first closing temperature control device 5-1, the safety relief valve 11 for opening experimental channel is let out Pressure closes recirculated water water inlet control valve 2 and recirculated water outlet water control valve, opens the drain valve of 6 lower end of experiment bin, main experiment is discharged Medium in pipeline replaces next group of experimental channel combination, repeats upper two step and continue to test according to requirement of experiment, if you need to It is further added by experimental channel combination, repeats A, B, step C is tested;
D, ending phase is tested:
First closing temperature control device 5-1 opens 11 pressure release of safety relief valve of experimental channel, closes recirculated water water inlet control Valve 2 and recirculated water outlet water control valve processed, closed safe overflow valve 9 open the drain valve of 6 lower end of experiment bin, after this is tested Sewage in experiment bin 6 is vented to pond, and experiment terminates.
The experimental provision and method that gas hydrates generate when a kind of simulation pipeline sudden contraction being designed in this way, rationally design Simulate pipeline sudden contraction when gas hydrates generate experimental provision and rationally design experimental method, pass through control pipeline flowing Speed, and caliber is tested than the shape with sudden contraction connecting pipe by changing upstream and downstream, interior flow mechanism is managed in research, and is simulated In the formation mechenism of metallic conduit adhesion and aggregation, the fortune of exploitation and natural gas to gas hydrates after research gas hydrate synthesis It is defeated significant.
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.

Claims (8)

1. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction, it is characterised in that: including experimental simulation system, fluid Injected system, the circulatory system, temperature control system, pressure-measuring system, control pressurer system and monitoring storage system, fluid note Enter system and circulatory system piping connection and provide multiphase flow for the circulatory system, the pressure-measuring system setting is infused in fluid Enter between system and experimental simulation system pipeline, the monitoring storage system is arranged in experimental simulation system side, and monitoring is deposited Storage system includes the high-speed camera for monitoring the acoustic detection device (15) of sound wave and storage experimentation inside experimental simulation system Machine (16);The experimental simulation system includes experiment bin (6) and is fixed in experiment bin (6) by mounting flange (6-4) Main experimental channel, the main experimental channel include downstream experimental channel (6-3) and upstream experimental channel (6-1), the downstream Pass through connecting pipe (6-2) pipeline connection, pressure control system between experimental channel (6-3) and upstream experimental channel (6-1) System and downstream experimental channel (6-3) pipeline connection, the circulatory system, control pressurer system and upstream experimental channel (6-1) are managed Road connection, interior be correspondingly connected at pipeline (6-2) of the experiment bin (6) are provided with visual windows (6-5), the high-speed camera (16) corresponding visual windows (6-5) setting, the temperature control system include the temperature control being arranged below experiment bin (6) Device (5-1).
2. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as described in claim 1, it is characterised in that: described Downstream experimental channel (6-3), between connecting pipe (6-2) and upstream experimental channel (6-1) pass through flanged joint.
3. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as described in claim 1, it is characterised in that: described Experimental simulation system experiment bin (6) be fixed on experiment rotatable platform (7) on.
4. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as described in claim 1, it is characterised in that: described The circulatory system include solution liquid pool (1) and connect solution liquid pool (1) and experimental simulation system circulation line, it is described molten On the circulation line between mounting flange (6-4) under the upstream experimental channel (6-1) of liquid liquid pool (1) and experimental simulation system Also it is successively arranged recirculated water water inlet control valve (2), intake pump (3) and force (forcing) pump (4).
5. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as claimed in claim 4, it is characterised in that: described Infusion fluid systems include multiphase flow splitting device (10), the multiphase flow splitting device (10) and solution liquid pool (1) are managed Road connection.
6. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as claimed in claim 5, it is characterised in that: described Pressure-measuring system piping connection multiphase flow splitting device (10) and experimental simulation system downstream experiment pipeline (6-3) on Between mounting flange (6-4), including the relief valve (11), safety overflow valve (9) and flowmeter (8) being successively set on pipeline.
7. the experimental provision that hydrate generates when a kind of simulation pipeline sudden contraction as described in claim 1, it is characterised in that: described Control pressurer system include gas source and be connected to gas source and experimental simulation system upstream experiment pipeline (6-1) under mounting flange Pressure piping between (6-4) is successively arranged gas control valve on the pressure piping between the gas source and mounting flange (6-4) (13), gas booster pump (12) and pressure gauge (14).
8. a kind of experimental method for the experimental provision that hydrate generates when simulation pipeline sudden contraction, it is characterised in that: including following real Test step:
A, the Preparatory work of experiment stage:
First with the solution for getting required concentration ready, closed safe relief valve (11), recirculated water water inlet control in solution matching slot (1) Valve (2) is opened experiment bin (6), is checked that the docking of pipeline coincide, is screwed pipeline mounting flange (6-4), close experiment bin (6);It beats Open cycle water water inlet control valve (2) starts intake pump (3), liquid needed for injecting into experiment simulation storehouse, until liquid level Until flooding circulating water pipeline outlet, it is then shut off recirculated water water inlet control valve (2) and intake pump (3), makes water in experimental temperature Circulation in control device (5-1) makes temperature control equipment reach experiment required temperature, starts intake pump (3) and force (forcing) pump (4), guarantee the liquid flowing in the combination of experiment bin (6) inner tube;It opens gas booster pump (12) and gas control valve (13), starting Gas booster pump (12) is started to work, and is read pressure in pressure gauge (14), is reached pressure needed for operating condition of test to pressure interior in pipeline It after power, closes gas booster pump (20), opens overflow relief valve (9);Light source is opened, is beaten from illumination form in experiment bin (6) Light, starting high-speed camera (16), acoustic detection device (15) and computer guarantee high-speed camera (16) and acoustic detection dress (15) alignment observation window is set, the Preparatory work of experiment stage is completed;
B, the progress stage is tested:
It when the interior temperature of experiment bin (6) reaches experiment set temperature, opens gas injection control valve (13), then opens gas and increase Press pump (12) controls gas flowmeter flow, starts to simulate the experiment of the confluence flowing in main experimental channel, uses high-speed camera (16) mobility status of the bubble on main experimental channel is captured automatically, is inhaled with the aggregation of acoustic detection device (15) detection hydrate The formation of attached situation and hydrate and aggregation blocking, gas flow is certain, and circulating water flow is certain, and observes Until pipeline has gas hydrate synthesis, an experimentation terminates, and the image data that high-speed camera (16) is captured passes through data line Computer is passed to be stored;
C, pipe stage is replaced:
After upper one group of experiment, first closing temperature control device (5-1), the safety relief valve (11) for opening experimental channel is let out Pressure closes recirculated water water inlet control valve (2) and recirculated water outlet water control valve, opens the drain valve of experiment bin (6) lower end, discharge master Medium in experimental channel replaces next group of experimental channel combination, repeats upper two step and continue to test according to requirement of experiment, If you need to be further added by experimental channel combination, A, B is repeated, step C is tested;
D, ending phase is tested:
First closing temperature control device (5-1) opens safety relief valve (11) pressure release of experimental channel, closes recirculated water water inlet control Valve (2) processed and recirculated water outlet water control valve, closed safe overflow valve (9) open the drain valve of experiment bin (6) lower end, by this Sewage after experiment in experiment bin (6) is vented to pond, and experiment terminates.
CN201810736891.5A 2018-07-06 2018-07-06 The experimental provision and experimental method that gas hydrates generate when a kind of simulation pipeline sudden contraction Pending CN109111969A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201749071U (en) * 2010-07-01 2011-02-16 青岛海洋地质研究所 Experimental device for natural gas hydrate gas storage determination
CN102392646A (en) * 2011-12-07 2012-03-28 常州大学 Marine gas hydrate electronic-spraying pump composite exploitation method and apparatus
CN202746940U (en) * 2012-09-18 2013-02-20 成都鼎鸿石油技术有限公司 Prevention and control tool of natural gas hydrate
CN106908446A (en) * 2017-03-01 2017-06-30 中国石油大学(华东) Gas hydrate choking mechanism analogue experiment installation and method under bubble flow

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201749071U (en) * 2010-07-01 2011-02-16 青岛海洋地质研究所 Experimental device for natural gas hydrate gas storage determination
CN102392646A (en) * 2011-12-07 2012-03-28 常州大学 Marine gas hydrate electronic-spraying pump composite exploitation method and apparatus
CN202746940U (en) * 2012-09-18 2013-02-20 成都鼎鸿石油技术有限公司 Prevention and control tool of natural gas hydrate
CN106908446A (en) * 2017-03-01 2017-06-30 中国石油大学(华东) Gas hydrate choking mechanism analogue experiment installation and method under bubble flow

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
刘有智: "超重力旋转填料床中天然气水合物含气量研究", 《化工进展》 *
时君友等: "《可再生能源概述》", 30 June 2017, 电子科技大学出版社 *
胡德芬: "重庆气矿天然气集输系统水合物成因及防治对策", 《天然气勘探与开发》 *
袁亮: "《煤与瓦斯共采》", 31 December 2016, 中国矿业大学出版社 *

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Application publication date: 20190101