CN109085101A - A kind of flue gas soluble matter continuously monitors analysis method and system on-line - Google Patents
A kind of flue gas soluble matter continuously monitors analysis method and system on-line Download PDFInfo
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- CN109085101A CN109085101A CN201811253645.0A CN201811253645A CN109085101A CN 109085101 A CN109085101 A CN 109085101A CN 201811253645 A CN201811253645 A CN 201811253645A CN 109085101 A CN109085101 A CN 109085101A
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- flue gas
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- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 title claims abstract description 125
- 239000003546 flue gas Substances 0.000 title claims abstract description 125
- 238000004458 analytical method Methods 0.000 title claims abstract description 16
- 238000001514 detection method Methods 0.000 claims abstract description 35
- 239000007788 liquid Substances 0.000 claims abstract description 31
- 239000013618 particulate matter Substances 0.000 claims abstract description 30
- 238000009833 condensation Methods 0.000 claims abstract description 19
- 230000005494 condensation Effects 0.000 claims abstract description 19
- 238000005070 sampling Methods 0.000 claims abstract description 18
- 239000002245 particle Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000012544 monitoring process Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- 230000008569 process Effects 0.000 claims abstract description 10
- 238000005259 measurement Methods 0.000 claims abstract description 5
- 150000001450 anions Chemical class 0.000 claims description 22
- 239000002184 metal Substances 0.000 claims description 18
- 238000006073 displacement reaction Methods 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- 230000005684 electric field Effects 0.000 claims description 9
- 239000010419 fine particle Substances 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 230000002262 irrigation Effects 0.000 abstract 1
- 238000003973 irrigation Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 9
- 150000003839 salts Chemical class 0.000 description 7
- 235000019504 cigarettes Nutrition 0.000 description 4
- 239000000523 sample Substances 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 230000005611 electricity Effects 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000443 aerosol Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000029058 respiratory gaseous exchange Effects 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000008247 solid mixture Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/06—Investigating concentration of particle suspensions
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- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The present invention relates to environmental monitoring technology field, in particular to a kind of flue gas soluble matter continuously monitors analysis method and system on-line, and drip irrigation device includes the following steps: the flue gas that sampling is taken out out of chimney, and is monitored to the flue gas flow F1 of sampling;Condensation process is carried out to flue gas and forms droplet so that particulate matter is attached in condensed condensation particle water;Droplet capture and is collected to form detection liquid;The salinity C1 and detection flow quantity F2 of measurement detection liquid;2=F2*C1/F1 of concentration C of the soluble matter particulate matter of flue gas is calculated, realizes the monitoring to soluble matter in flue gas, convenient for carrying out specific aim control to flue gas emission, provides basic data to the research haze origin cause of formation.
Description
Technical field
The present invention relates to environmental monitoring technology field, in particular to a kind of flue gas soluble matter continuously monitors analysis method on-line
And system.
Background technique
Since entering 21st century with China, economic development drives the development of every field, and industrial circle is also therewith
Grow up, while environmental problem also becomes the maximum of China's industrial realization modernization and hinders, air pollution is environmental pollution
In the matter of utmost importance that should study, in order to which China can realize sound and fast development under the premise of environmental protection, to related flue gas
The flue gas monitoring engineering for discharging industry is duty-bound, and it is modern industry management that pollution control is carried out in the technology for collect parameter
Matter of utmost importance.
Flue gas after sulfur removal technology, is foring the higher flue gas of low temperature humidity, takes out of in flue gas a large amount of ultra-fine
Soluble matter exists with aerosol form, when the concentration of this particulate matter is higher, will threaten to human health, especially to heavy breathing
Breathing heavily patient and other has the crowd of respiratory disorder, and this soluble matter particulate matter can also propagate fungi and virus, this will lead
Cause the prevalence and outburst of some regional diseases.But at present, in fume continuous monitoring system, majority is to flue gas temperature
Degree, flue gas pressures, flue gas flow rate, granularity concentration, NOx, SO2, HCl, CO etc. monitoring, wherein the current particulate matter surveyed
Concentration is far below the concentration actually excluded, and mainly existing detection device is difficult effectively to capture superfine particulate matter,
And salt is discharged into atmosphere, forms aerosol as " nuclei of condensation ", is had key effect for the generation of haze, is so made
Obtaining becomes particularly difficult to the control of discharge flue gas, is badly in need of a kind of for flue gas after desulfurization soluble matter continuous monitor system.
Summary of the invention
The first purpose of the invention is to provide a kind of flue gas soluble matter continuously to monitor analysis method on-line, has and realizes cigarette
The purpose of soluble matter particle concentration in gas.
Above-mentioned technical purpose of the invention has the technical scheme that
A kind of flue gas soluble matter continuously monitors analysis method on-line, includes the following steps:
The flue gas of sampling is taken out out of chimney, and the flue gas flow F1 of sampling is monitored;
Condensation process is carried out to flue gas and forms droplet so that particulate matter is attached in condensed condensation particle water;
Droplet capture and is collected to form detection liquid;
The salinity C1 and detection flow quantity F2 of measurement detection liquid;
2=F2*C1/F1 of concentration C of the soluble matter particulate matter of flue gas is calculated.
Through the above technical solutions, by flue gas from chimney and after being detected to flue gas flow F1, by condensing to high temperature
Flue gas carry out cooling condensation process flue-gas temperature is reduced, make high-temperature gas be condensed into water droplet, suspended particulate after cooling
Object is then adsorbed in condensing drip and forms droplet, forms the particulate matter of droplet at this point, capturing and collecting to be attached in water droplet with shape
It at detection liquid, is detected by the salinity C1 and detection flow quantity F2 to detection liquid, and combines flue gas flow F1, calculated
Soluble matter particle concentration out, and then realize the monitoring to soluble salt in flue gas, convenient for carrying out specific aim control to flue gas emission.
The present invention is further arranged to: when carrying out capturing collection to form detection liquid to droplet, comprising:
High voltage electric field is applied to flue gas;
The anion ionized out under high pressure power plant drives droplet displacement;
Displacement droplet is intercepted and captured.
Through the above technical solutions, strong electrical field is formed in the environment that flue gas passes through after being powered, to ionize out in free
The anion of state, this part anion displacement.At this point, the droplet in flue gas after heat exchange during constant flow with
The anion of free state combines, and anion drives droplet displacement, realizes the separation of soluble matter particulate matter and flue gas.
A second object of the present invention is to provide a kind of flue gas soluble matter continuously to monitor analysis system on-line, has and realizes cigarette
The purpose of soluble matter particle concentration in gas.
Above-mentioned technical purpose of the invention has the technical scheme that
A kind of flue gas soluble matter continuously monitors analysis system on-line, which is characterized in that including following station:
S1, by sampler by flue gas from chimney from taking-up;
S2, sampling flue gas flow F1 is detected by flue gas flow meter;
S3, cooling condensation process is carried out to flue gas by condensing unit, and the particulate matter in flue gas is driven to be adsorbed in condensing drip
Middle formation droplet;
S4, Charged Droplet is collected by superfine particulate matter capture device and forms detection liquid;
S5, it is detected by flow F2 of the solution micro-flowmeter to detection liquid, and dense by salt of the salinity meter to detection liquid
Degree C1 is detected;
S6, the solvable composition granule that flue gas is calculated in conjunction with the parameter that flue gas flow meter, solution micro-flowmeter, salinity meter detect
2=F2*C1/F1 of concentration C of object.
Through the above technical solutions, detected by the flue gas flow that flue gas flow meter takes out sampler, due to
Flue gas is high temperature, gas, solid mixture, therefore is passed through and condensing unit carries out cooling condensation process to flue gas, and condensing unit is passed through
So that flue-gas temperature reduces, so that high-temperature gas is condensed into water droplet, suspended particulate substance is then adsorbed in condensing drip and forms droplet,
Condensed flue gas captures droplet by superfine particulate matter capture device, forms droplet at this point, being attached in water droplet
Particulate matter is collected to form detection liquid, by solution micro-flowmeter and salinity meter to the flow of detection liquid and salinity into
Row detection, and combine flue gas flow meter to calculate soluble matter particle concentration, and then realize the monitoring to soluble salt in flue gas, it is convenient for
Specific aim control is carried out to flue gas emission.
The present invention is further arranged to: the superfine particulate matter capture device includes shell, is connected to leading for outer casing inner wall
Torch, the metalwork being arranged in conductive tube and drive that conductive tube is positively charged and the electronegative power supply of metalwork.
Through the above technical solutions, forming strong electrical field between conductive tube and metalwork, and constantly ionize after being powered
Flue gas between conductive tube and metalwork, to ionize out the anion in free state, this part anion is moved towards conductive tube
It is dynamic.At this point, pouring the flue gas after heat exchange into shell, the anion of free state can be attached on condensed droplet, and band
Dynamic droplet is mobile towards anode electrode pipe, so that droplet be made to be attached on conductive tube inner wall, and as the more poly- droplet the more, droplet with
Conductive tube flowing, realize that droplet is separated and collected from flue gas, and since conductive tube and metalwork are through in outer cylinder, therefore electric
The collection efficiency of droplet is improved full of in shell in field.
The present invention is further arranged to: the metalwork is hollow setting and the metal mesh that flue gas is passed through out of metalwork
Cylinder.
Through the above technical solutions, by the interception of the logical achievable major diameter droplets particles of metal net cylinder, and flue gas is being worn
When crossing metal net cylinder, metal net cylinder can be to droplet direct charging, that is, part anion is transmitted on droplet, finally, this part
The droplet for being attached with anion can more directly, more arrive at rapidly the inner wall of conductive tube, to improve the collection efficiency of droplet.
The present invention is further arranged to: the level-one condensing unit selects heat exchanger.
Through the above technical solutions, heat exchanger is realized to flue gas cool-down, by the air-liquid state water condensation in flue gas.
In conclusion the invention has the following advantages:
Flue gas is cooled down after stack sampling, is condensed, particulate matter adheres to form droplet, flue gas is ionized, and to band
Droplet after point is separated and is collected, and detection liquid is formed, and carries out salinity detection to liquid is detected after separation, and cigarette is calculated
The soluble matter particle concentration of gas.
Detailed description of the invention
Fig. 1 is the entire block diagram of embodiment 2;
Fig. 2 is the structural schematic diagram of superfine particulate matter capture device in embodiment 2.
Appended drawing reference: 1, sampler;2, flue gas flow meter;3, condensing unit;4, superfine particulate matter capture device;5, molten
Liquid micro-flowmeter;6, salinity meter;7, sampling probe;8, sampling pump;9, seizure pipe;10, shell;11, conductive tube;12, metal
Part.
Specific embodiment
Below in conjunction with attached drawing, invention is further described in detail.
Embodiment 1:
A kind of flue gas soluble matter continuously monitors analysis method on-line, includes the following steps:
The flue gas of sampling is taken out out of chimney, and the flue gas flow F1 of sampling is monitored;
Condensation process is carried out to flue gas and forms droplet so that particulate matter is attached in condensed condensation particle water;
Droplet capture and is collected to form detection liquid;
The salinity C1 and detection flow quantity F2 of measurement detection liquid;
2=F2*C1/F1 of concentration C of the soluble matter particulate matter of flue gas is calculated.
Wherein, when carrying out capturing collection to form detection liquid to droplet, comprising:
High voltage electric field is applied to flue gas;
The anion ionized out under high pressure power plant drives droplet displacement;
Displacement droplet is intercepted and captured.
By flue gas from chimney and after detecting to flue gas flow F1, cooling condensation is carried out to the flue gas of high temperature by condensation
Processing makes high-temperature gas be condensed into water droplet, suspended particulate substance is then adsorbed in condensing drip so that flue-gas temperature reduction after cooling
Middle formation droplet.
After energization, strong electrical field is formed in the environment that flue gas passes through, to ionize out the anion in free state, this part
Anion displacement.At this point, the droplet in flue gas after heat exchange during constant flow with the anion knot of free state
It closes, anion drives droplet displacement, realizes the separation of soluble matter particulate matter and flue gas.
At this point, detecting by the salinity C1 and detection flow quantity F2 to detection liquid, and flue gas flow F1 is combined, meter
Calculation obtains soluble matter particle concentration, and then realizes the monitoring to soluble salt in flue gas, convenient for carrying out specific aim to flue gas emission
Control.
Embodiment 2:
A kind of flue gas soluble matter continuously monitors analysis system on-line, as shown in Figure 1, including following station:
1, by sampler 1 by flue gas from chimney from taking-up;
2, it is detected by 2 couples of sampling flue gas flow F1 of flue gas flow meter;
3, cooling condensation process is carried out to flue gas by condensing unit 3, and the particulate matter in flue gas is driven to be adsorbed in condensing drip
Middle formation droplet;
4, Charged Droplet is collected by superfine particulate matter capture device 4 and forms detection liquid;
5, the flow F2 for detecting liquid by 5 couples of solution micro-flowmeter is detected, and dense by the salt of 6 pairs of salinity meter detection liquid
Degree C1 is detected;
6, the soluble matter of flue gas is calculated in conjunction with the parameter that flue gas flow meter 2, solution micro-flowmeter 5, salinity meter 6 detect
2=F2*C1/F1 of concentration C of grain object.
Sampler 1 is that the sampling probe 7 extended in chimney is used for 7 end of sampling probe is fixedly connected on by chimney
Interior flue gas draws the sampling pump 8 of chimney and sampling probe 7.
In the present embodiment, condensing unit 3 and selection heat exchanger, heat exchanger is not outer under the action of realizing to flue gas cool-down to be added
Steam is in flue gas, to further increase the measurement accuracy of soluble matter particle concentration C2 in flue gas.
Superfine particulate matter capture device 4 include shell 10, be connected to 10 inner wall of shell conductive tube 11, be arranged in conductive tube
Metalwork 12 in 11 and drive conductive tube 11 positively charged and the electronegative power supply of metalwork 12, wherein shell 10 is selected
Insulating materials production.
In the present embodiment, metalwork 12 is hollow setting and the metal net cylinder that flue gas is passed through out of metalwork 12.
Power supply is high-voltage DC power supply, and the anode of high-voltage DC power supply is coupled to conductive tube 11, high straightening by conducting wire
The cathode in galvanic electricity source is coupled to metal net cylinder by conducting wire.
After power supply is connected, strong electrical field is formed between conductive tube 11 and metal net cylinder, and metal net cylinder access negative electricity is simultaneously
Anion can be discharged, at this point, being passed through flue gas into metal net cylinder, strong electrical field is persistently ionized between conductive tube 11 and metal net cylinder
Flue gas, to ionize out the anion in free state, this part anion is mobile towards conductive tube 11.And the anion of free state
It can be attached on condensed droplet, and drive droplet mobile towards anode electrode pipe, be attached to droplet on 11 inner wall of conductive tube,
And as the more poly- droplet the more, droplet is flowed with conductive tube 11, realizes that droplet is separated and collected from flue gas, and due to conduction
Cylinder 11 and metal net cylinder are through in outer cylinder, therefore electric field improves the charged and collection efficiency of droplet full of in shell 10.
Simultaneously as metal net cylinder has mesh, therefore the droplet that diameter is greater than mesh is intercepted in metal net cylinder, and
It is fallen after accumulation, and since metal net cylinder access negative electricity can also discharge anion simultaneously, therefore flue gas is when passing through metal net cylinder, it is golden
Belong to net cylinder can be to droplet direct charging, that is, part anion is transmitted on droplet, finally, this part be attached with bear from
The droplet of son can more directly, more arrive at rapidly the inner wall of conductive tube 11, to improve the collection efficiency of droplet.
The course of work:
It is detected by the flue gas flow that flue gas flow meter 2 takes out sampler 1, since flue gas is high temperature, gas, solid mixing
Object, therefore pass through and condensing unit 3 carries out cooling condensation process to flue gas, by condensing unit 3 flue-gas temperature is reduced, from
And high-temperature gas is condensed into water droplet, suspended particulate substance, which is then adsorbed in condensing drip, forms droplet, and condensed flue gas is by super
Fine particle capture device 4 captures droplet, at this point, the particulate matter for being attached to formation droplet in water droplet is collected shape
It at detection liquid, is detected by solution micro-flowmeter 5 and 6 pairs of the salinity meter flows for detecting liquid and salinity, and combines cigarette
Air-flow meter 2 calculates soluble matter particle concentration, and then realizes the monitoring to soluble salt in flue gas, convenient for carrying out to flue gas emission
Specific aim control.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, those skilled in the art
Member can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as at this
All by the protection of Patent Law in the scope of the claims of invention.
Claims (6)
1. a kind of flue gas soluble matter continuously monitors analysis method on-line, which comprises the steps of:
The flue gas of sampling is taken out out of chimney, and the flue gas flow F1 of sampling is monitored;
Condensation process is carried out to flue gas and forms droplet so that particulate matter is attached in condensed condensation particle water;
Droplet capture and is collected to form detection liquid;
The salinity C1 and detection flow quantity F2 of measurement detection liquid;
2=F2*C1/F1 of concentration C of the soluble matter particulate matter of flue gas is calculated.
2. a kind of flue gas soluble matter according to claim 1 continuously monitors analysis method on-line, which is characterized in that droplet
When carrying out capturing collection to form detection liquid, comprising:
High voltage electric field is applied to flue gas;
The anion ionized out under high pressure power plant drives droplet displacement;
Displacement droplet is intercepted and captured.
3. a kind of flue gas soluble matter continuously monitors analysis system on-line, which is characterized in that including following station:
S1, by sampler (1) by flue gas from chimney from taking-up;
S2, sampling flue gas flow F1 is detected by flue gas flow meter (2);
S3, cooling condensation process is carried out to flue gas by condensing unit (3), and the particulate matter in flue gas is driven to be adsorbed in condensed water
Droplet is formed in drop;
S4, Charged Droplet is collected by superfine particulate matter capture device (4) and forms detection liquid;
S5, it is detected by flow F2 of the solution micro-flowmeter (5) to detection liquid, and by salinity meter (6) to detection liquid
Salinity C1 detected;
S6, flue gas is calculated in conjunction with the parameter that flue gas flow meter (2), solution micro-flowmeter (5), salinity meter (6) detect
2=F2*C1/F1 of concentration C of soluble matter particulate matter.
4. a kind of flue gas soluble matter according to claim 3 continuously monitors analysis system on-line, it is characterised in that: described super
Fine particle capture device (4) includes shell (10), the conductive tube (11) for being connected to shell (10) inner wall, is arranged in conductive tube
(11) metalwork (12) in and drive conductive tube (11) positively charged and metalwork (12) electronegative power supply.
5. continuously monitoring analysis system on-line according to a kind of flue gas soluble matter that claim 4 is stated, it is characterised in that: the metal
Part (12) is hollow setting and the metal net cylinder that flue gas is passed through out of metalwork (12).
6. continuously monitoring analysis system on-line according to a kind of flue gas soluble matter that claim 3 is stated, it is characterised in that: the condensation
Device (3) selects heat exchanger.
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CN110118711A (en) * | 2019-06-11 | 2019-08-13 | 江苏钛科圈物联网科技有限公司 | Room air bacteria containing amount real-time detection and analysis method, system based on Internet of Things |
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CN110118711A (en) * | 2019-06-11 | 2019-08-13 | 江苏钛科圈物联网科技有限公司 | Room air bacteria containing amount real-time detection and analysis method, system based on Internet of Things |
CN110118711B (en) * | 2019-06-11 | 2019-12-31 | 江苏钛科圈物联网科技有限公司 | Indoor air bacteria content real-time detection and analysis method and system based on Internet of things |
CN113865943A (en) * | 2021-08-25 | 2021-12-31 | 安徽元琛环保科技股份有限公司 | Industrial flue gas particulate matter sampling analysis system and method |
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