CN109056110A - A kind of wig fiber with good friction performance - Google Patents
A kind of wig fiber with good friction performance Download PDFInfo
- Publication number
- CN109056110A CN109056110A CN201810841110.9A CN201810841110A CN109056110A CN 109056110 A CN109056110 A CN 109056110A CN 201810841110 A CN201810841110 A CN 201810841110A CN 109056110 A CN109056110 A CN 109056110A
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- China
- Prior art keywords
- weight
- wig
- parts
- friction performance
- good friction
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/12—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyamide as constituent
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
- A41G3/00—Wigs
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/10—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one other macromolecular compound obtained by reactions only involving carbon-to-carbon unsaturated bonds as constituent
Abstract
The invention discloses a kind of wig fibers with good friction performance, are related to wig technical field, the nano silica of the chlorinated polyethylene graft copolymer containing its quality 3.6-7.5% and 1.2-1.6% in the wig fiber with good friction performance；Wig fiber prepared by the present invention has good frictional behaviour, and especially by addition chlorinated polyethylene alkene copolymer and the synergistic effect Jing Guo pretreated nano silica, the frictional behaviour of wig fiber is greatly improved.
Description
Technical field
The invention belongs to wig technical fields, and in particular to a kind of wig fiber with good friction performance.
Background technique
With the raising of economic level development and living standards of the people, wig has become fashion decorations important in the modern life
Product, the every annual consumption in the whole world is at 150,000 tons or so.With going from strength to strength for hair product industry, human hair material rate is increasingly
Few, domestic and international human hair resource is gradually reduced.Therefore, artificial hair product industry need find a kind of new human hair substitution of resources product.It is false
Hair is generally divided into animal ceratin fiber hair and artificial synthesized wig, animal ceratin wig generally comprise human hair, horse hair, horse
Hair on the neck, yak hair, oxtail etc., animal ceratin wig simulation quality is preferable, but animal ceratin fiber production is low, price is high and raw
Long period is longer, is far from satisfying the wilderness demand in market, and increasing rapidly with domestic and international hair products demand, people
Work synthesis wig is more and more extensive, and still, the artificial synthesized wig frictional behaviour of prior art preparation is poor, the frictional property of wig
Can, there is large effect to the superiority and inferiority of wig quality, directly affects the complexity combed in wig daily life.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of wig fiber with good friction performance is provided.
The present invention is achieved by the following technical solutions:
A kind of wig fiber with good friction performance contains its quality in the wig fiber with good friction performance
The chlorinated polyethylene graft copolymer of 3.6-7.5% and the nano silica of 1.2-1.6%.
Further, the polyvinyl chloride graft copolymer the preparation method comprises the following steps:
(1) it is added the haloflex of 75 parts by weight into reaction kettle, the catalyst of 2.3 parts by weight, the solvent of 320 parts by weight,
It vacuumizes, stirs 55min；
(2) the octadecyl methyl acrylate of 6 parts by weight, the Isooctyl acrylate monomer of 1.2 parts by weight, 0.55 parts by weight are added
2- chloroaniline, the promotor of 0.012 parts by weight are heated to 76 DEG C, react 3.5 hours, then filter out precipitating, washed using clear water
Wash, drying to constant weight to get.
Further, the solvent is dehydrated alcohol.
Further, the catalyst is frerrous chloride.
Further, the promotor is triethylamine.
Further, the nano silica is by pretreatment:
Nano silica is evenly spread into the phenyl dichloro phosphorus solution that mass fraction is 5.2% under nitrogen atmosphere protection
In, 115 DEG C are heated to, 40min is kept the temperature, is then filtered, successively cleaned using dehydrated alcohol with deionized water, is dried
To constant weight.
Further, the phenyl dichloro phosphorus solution is to be dissolved in acetone after drying, then by phenyl dichloro phosphorus
Acetone obtains.
Further, the wig fiber with good friction performance further includes that following parts by weight of component is made: nylon
It is sliced 88, epoxidized soybean oil 1.5, odium stearate 2.6, pigment 0.6.
The present invention has the advantage that wig fiber prepared by the present invention has good frictional property compared with prior art
Can, especially by addition chlorinated polyethylene alkene copolymer and the synergistic effect Jing Guo pretreated nano silica, significantly
The frictional behaviour for improving wig fiber significantly reduce vacation so that manufactured wig quality is greatly ensured
The complexity combed in hair daily life.Wig fiber of the invention has good smoothness, excellent hydrofuge gas permeability,
It is 12 times higher than cotton wearability, send out high 25 times than true man, when being stretched to 6-7%, elastic recovery rate is amenable to up to 100%
Ten thousand times folding is scratched and not broken, can obviously improve or avoid to wear the entanglement in use process, it is random that long periods of wear is not easy fold hair.
Specific embodiment
Embodiment 1
A kind of wig fiber with good friction performance contains its quality in the wig fiber with good friction performance
The chlorinated polyethylene graft copolymer of 3.6-7.5% and the nano silica of 1.2-1.6%.
Further, the polyvinyl chloride graft copolymer the preparation method comprises the following steps:
(1) it is added the haloflex of 75 parts by weight into reaction kettle, the catalyst of 2.3 parts by weight, the solvent of 320 parts by weight,
It vacuumizes, stirs 55min；
(2) the octadecyl methyl acrylate of 6 parts by weight, the Isooctyl acrylate monomer of 1.2 parts by weight, 0.55 parts by weight are added
2- chloroaniline, the promotor of 0.012 parts by weight are heated to 76 DEG C, react 3.5 hours, then filter out precipitating, washed using clear water
Wash, drying to constant weight to get.
Further, the solvent is dehydrated alcohol.
Further, the catalyst is frerrous chloride.
Further, the promotor is triethylamine.
Further, the nano silica is by pretreatment:
Nano silica is evenly spread into the phenyl dichloro phosphorus solution that mass fraction is 5.2% under nitrogen atmosphere protection
In, 115 DEG C are heated to, 40min is kept the temperature, is then filtered, successively cleaned using dehydrated alcohol with deionized water, is dried
To constant weight.
Further, the phenyl dichloro phosphorus solution is to be dissolved in acetone after drying, then by phenyl dichloro phosphorus
Acetone obtains.
Further, the wig fiber with good friction performance further includes that following parts by weight of component is made: nylon
It is sliced 88, epoxidized soybean oil 1.5, odium stearate 2.6, pigment 0.6.
Embodiment 2
A kind of wig fiber with good friction performance contains its quality in the wig fiber with good friction performance
The chlorinated polyethylene graft copolymer of 3.6-7.5% and the nano silica of 1.2-1.6%.
Further, the polyvinyl chloride graft copolymer the preparation method comprises the following steps:
(1) it is added the haloflex of 75 parts by weight into reaction kettle, the catalyst of 2.3 parts by weight, the solvent of 320 parts by weight,
It vacuumizes, stirs 55min；
(2) the octadecyl methyl acrylate of 6 parts by weight, the Isooctyl acrylate monomer of 1.2 parts by weight, 0.55 parts by weight are added
2- chloroaniline, the promotor of 0.012 parts by weight are heated to 76 DEG C, react 3.5 hours, then filter out precipitating, washed using clear water
Wash, drying to constant weight to get.
Further, the solvent is dehydrated alcohol.
Further, the catalyst is frerrous chloride.
Further, the promotor is triethylamine.
Further, the nano silica is by pretreatment:
Nano silica is evenly spread into the phenyl dichloro phosphorus solution that mass fraction is 5.2% under nitrogen atmosphere protection
In, 115 DEG C are heated to, 40min is kept the temperature, is then filtered, successively cleaned using dehydrated alcohol with deionized water, is dried
To constant weight.
Further, the phenyl dichloro phosphorus solution is to be dissolved in acetone after drying, then by phenyl dichloro phosphorus
Acetone obtains.
Further, the wig fiber with good friction performance further includes that following parts by weight of component is made: nylon
It is sliced 88, epoxidized soybean oil 1.5, odium stearate 2.6, pigment 0.6.
Embodiment 3
A kind of wig fiber with good friction performance contains its quality in the wig fiber with good friction performance
The chlorinated polyethylene graft copolymer of 3.6-7.5% and the nano silica of 1.2-1.6%.
Further, the polyvinyl chloride graft copolymer the preparation method comprises the following steps:
(1) it is added the haloflex of 75 parts by weight into reaction kettle, the catalyst of 2.3 parts by weight, the solvent of 320 parts by weight,
It vacuumizes, stirs 55min；
(2) the octadecyl methyl acrylate of 6 parts by weight, the Isooctyl acrylate monomer of 1.2 parts by weight, 0.55 parts by weight are added
2- chloroaniline, the promotor of 0.012 parts by weight are heated to 76 DEG C, react 3.5 hours, then filter out precipitating, washed using clear water
Wash, drying to constant weight to get.
Further, the solvent is dehydrated alcohol.
Further, the catalyst is frerrous chloride.
Further, the promotor is triethylamine.
Further, the nano silica is by pretreatment:
Nano silica is evenly spread into the phenyl dichloro phosphorus solution that mass fraction is 5.2% under nitrogen atmosphere protection
In, 115 DEG C are heated to, 40min is kept the temperature, is then filtered, successively cleaned using dehydrated alcohol with deionized water, is dried
To constant weight.
Further, the phenyl dichloro phosphorus solution is to be dissolved in acetone after drying, then by phenyl dichloro phosphorus
Acetone obtains.
Further, the wig fiber with good friction performance further includes that following parts by weight of component is made: nylon
It is sliced 88, epoxidized soybean oil 1.5, odium stearate 2.6, pigment 0.6.
Comparative example 1: it is only that with the difference of embodiment 1 and does not add chlorinated polyethylene alkene copolymer.
Comparative example 2: it is only that and is not added by pretreated nano silica with the difference of embodiment 1.
Comparative example 3: it is only that nano silica without pretreatment with the difference of embodiment 1.
Comparative example 4: by octadecyl methyl acrylic acid when being only that prepared by chlorinated polyethylene alkene copolymer with the difference of embodiment 1
Ester replaces with alkyl methacrylate.
Comparative example 5: it is only that with the difference of embodiment 1 and chlorinated polyethylene alkene copolymer is replaced with into polyethylene.
Control group: Zhen Renfa.
Test
Performance is carried out to the wig fiber of the same size (diameter is 66.35 ± 0.002 μm) of embodiment and comparative example preparation
Detection:
When test, sample is first put into standard testing room and carries out the pretreatment of damping for 24 hours, since true man send out along the hair tip to root of hair diameter
There is certain difference, general hair root is thicker, and it is thinner at the more past hair tip, therefore intercepted in experiment in the middle part of hair as real
Sample is tested, after true man's hair is organized into the concordant fibre bundle in one end, falls staple fiber with comb comb, in the middle part of scissors clip wig beam
Fiber is spare；And chemical fibre wig diameter edge is axial more uniform, has no this requirement, 50 wig fibers of experiment test, are tested every time
The size of average friction force between wig fiber and mahogany；
Table 1
As can be seen from Table 1, wig fiber prepared by the present invention has good frictional behaviour, poly- especially by addition chlorination
Ethylene copolymer and the synergistic effect Jing Guo pretreated nano silica, are greatly improved the frictional property of wig fiber
Can, so that manufactured wig quality is greatly ensured, significantly reduce the difficulty or ease journey combed in wig daily life
Degree.
Embodiment wig fibre diameter is 66.35 ± 0.002 μm of intensity average out to 4.65cN/dtex, and 1 wig of comparative example
Fibre diameter is 66.35 ± 0.002 μm of intensity average out to 3.82cN/dtex, it is seen then that chlorinated polyethylene alkene copolymer being capable of certain journey
The intensity of wig fiber is improved on degree.
Claims (8)
1. a kind of wig fiber with good friction performance, which is characterized in that the wig with good friction performance is fine
The nano silica of chlorinated polyethylene graft copolymer and 1.2-1.6% containing its quality 3.6-7.5% in dimension.
2. a kind of wig fiber with good friction performance according to claim 1, which is characterized in that the polychlorostyrene second
Alkene graft copolymer the preparation method comprises the following steps:
(1) it is added the haloflex of 75 parts by weight into reaction kettle, the catalyst of 2.3 parts by weight, the solvent of 320 parts by weight,
It vacuumizes, stirs 55min；
(2) the octadecyl methyl acrylate of 6 parts by weight, the Isooctyl acrylate monomer of 1.2 parts by weight, 0.55 parts by weight are added
2- chloroaniline, the promotor of 0.012 parts by weight are heated to 76 DEG C, react 3.5 hours, then filter out precipitating, washed using clear water
Wash, drying to constant weight to get.
3. a kind of wig fiber with good friction performance according to claim 2, which is characterized in that the solvent is
Dehydrated alcohol.
4. a kind of wig fiber with good friction performance according to claim 2, which is characterized in that the catalyst
For frerrous chloride.
5. a kind of wig fiber with good friction performance according to claim 2, which is characterized in that the promotor
For triethylamine.
6. a kind of wig fiber with good friction performance according to claim 1, which is characterized in that the nanometer two
Silica is by pretreatment:
Nano silica is evenly spread into the phenyl dichloro phosphorus solution that mass fraction is 5.2% under nitrogen atmosphere protection
In, 115 DEG C are heated to, 40min is kept the temperature, is then filtered, successively cleaned using dehydrated alcohol with deionized water, is dried
To constant weight.
7. a kind of wig fiber with good friction performance according to claim 6, which is characterized in that the phenyl two
Chlorination phosphorus solution be by acetone after drying, then phenyl dichloro phosphorus is dissolved in acetone and is obtained.
8. a kind of wig fiber with good friction performance according to claim 1, which is characterized in that described with good
The wig fiber of good frictional behaviour further includes that following parts by weight of component is made: nylon chips 88, epoxidized soybean oil 1.5, stearic acid
Sodium 2.6, pigment 0.6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810841110.9A CN109056110A (en) | 2018-07-27 | 2018-07-27 | A kind of wig fiber with good friction performance |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810841110.9A CN109056110A (en) | 2018-07-27 | 2018-07-27 | A kind of wig fiber with good friction performance |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109056110A true CN109056110A (en) | 2018-12-21 |
Family
ID=64836581
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810841110.9A Pending CN109056110A (en) | 2018-07-27 | 2018-07-27 | A kind of wig fiber with good friction performance |
Country Status (1)
| Country | Link |
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| CN (1) | CN109056110A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112921446A (en) * | 2021-01-27 | 2021-06-08 | 李生达 | Synthetic fiber with strong wear resistance and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1287819A (en) * | 1999-09-13 | 2001-03-21 | 克劳斯·迪特里希·萨尔兹西德尔 | Method for mfg. durable wigs |
| CN102443218A (en) * | 2011-09-23 | 2012-05-09 | 郑勇 | Thermoplastic rubber composition and preparation method thereof |
| CN103755877A (en) * | 2013-12-21 | 2014-04-30 | 山东日科橡塑科技有限公司 | Production process for ACM (Chlorinated Polyethylene-Alkyl Acrylate Interpenetrating Network Copolymer) with high elongation at rupture |
| CN105887238A (en) * | 2016-05-23 | 2016-08-24 | 太和县蓝翎养殖有限公司 | Flame-retardant artificial wig fibers containing peacock feather |
| CN107118306A (en) * | 2017-06-09 | 2017-09-01 | 江苏科利新材料有限公司 | A kind of chlorinated polyethylene graft copolymer and preparation method thereof |
| CN107805853A (en) * | 2017-10-24 | 2018-03-16 | 许昌鸿洋生化实业发展有限公司 | It is a kind of to be used to manufacture high temperature resistant nylon fiber of wig and preparation method thereof |
| CN107938015A (en) * | 2017-10-24 | 2018-04-20 | 许昌鸿洋生化实业发展有限公司 | A kind of dumb light high temperature resistant nylon wig fiber and preparation method thereof |
-
2018
- 2018-07-27 CN CN201810841110.9A patent/CN109056110A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1287819A (en) * | 1999-09-13 | 2001-03-21 | 克劳斯·迪特里希·萨尔兹西德尔 | Method for mfg. durable wigs |
| CN102443218A (en) * | 2011-09-23 | 2012-05-09 | 郑勇 | Thermoplastic rubber composition and preparation method thereof |
| CN103755877A (en) * | 2013-12-21 | 2014-04-30 | 山东日科橡塑科技有限公司 | Production process for ACM (Chlorinated Polyethylene-Alkyl Acrylate Interpenetrating Network Copolymer) with high elongation at rupture |
| CN105887238A (en) * | 2016-05-23 | 2016-08-24 | 太和县蓝翎养殖有限公司 | Flame-retardant artificial wig fibers containing peacock feather |
| CN107118306A (en) * | 2017-06-09 | 2017-09-01 | 江苏科利新材料有限公司 | A kind of chlorinated polyethylene graft copolymer and preparation method thereof |
| CN107805853A (en) * | 2017-10-24 | 2018-03-16 | 许昌鸿洋生化实业发展有限公司 | It is a kind of to be used to manufacture high temperature resistant nylon fiber of wig and preparation method thereof |
| CN107938015A (en) * | 2017-10-24 | 2018-04-20 | 许昌鸿洋生化实业发展有限公司 | A kind of dumb light high temperature resistant nylon wig fiber and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112921446A (en) * | 2021-01-27 | 2021-06-08 | 李生达 | Synthetic fiber with strong wear resistance and preparation method thereof |
| CN112921446B (en) * | 2021-01-27 | 2022-02-22 | 合肥清华胜嘉服饰有限公司 | Synthetic fiber with strong wear resistance and preparation method thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181221 |
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