CN109045555A - A kind for the treatment of process of organosilicon slag slurry - Google Patents
A kind for the treatment of process of organosilicon slag slurry Download PDFInfo
- Publication number
- CN109045555A CN109045555A CN201811087660.2A CN201811087660A CN109045555A CN 109045555 A CN109045555 A CN 109045555A CN 201811087660 A CN201811087660 A CN 201811087660A CN 109045555 A CN109045555 A CN 109045555A
- Authority
- CN
- China
- Prior art keywords
- support plate
- slag slurry
- organosilicon slag
- cylindrical tube
- connecting rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002002 slurry Substances 0.000 title claims abstract description 74
- 239000002893 slag Substances 0.000 title claims abstract description 64
- 238000000034 method Methods 0.000 title claims abstract description 24
- 238000009835 boiling Methods 0.000 claims abstract description 36
- 239000012528 membrane Substances 0.000 claims abstract description 21
- 238000004821 distillation Methods 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 239000007787 solid Substances 0.000 claims abstract description 8
- 230000006835 compression Effects 0.000 claims description 17
- 238000007906 compression Methods 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 16
- 239000011229 interlayer Substances 0.000 claims description 8
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000012216 screening Methods 0.000 claims description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 3
- 238000009434 installation Methods 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract description 8
- 229910052710 silicon Inorganic materials 0.000 abstract description 7
- 239000010703 silicon Substances 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000005054 agglomeration Methods 0.000 description 9
- 230000002776 aggregation Effects 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 238000004140 cleaning Methods 0.000 description 4
- 239000000178 monomer Substances 0.000 description 3
- 238000003672 processing method Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- YGZSVWMBUCGDCV-UHFFFAOYSA-N chloro(methyl)silane Chemical compound C[SiH2]Cl YGZSVWMBUCGDCV-UHFFFAOYSA-N 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- OGFYGJDCQZJOFN-UHFFFAOYSA-N [O].[Si].[Si] Chemical compound [O].[Si].[Si] OGFYGJDCQZJOFN-UHFFFAOYSA-N 0.000 description 1
- QZOVMCPHIQVUGV-UHFFFAOYSA-N [Si].[C].[Si] Chemical compound [Si].[C].[Si] QZOVMCPHIQVUGV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 238000007701 flash-distillation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- SBEQWOXEGHQIMW-UHFFFAOYSA-N silicon Chemical compound [Si].[Si] SBEQWOXEGHQIMW-UHFFFAOYSA-N 0.000 description 1
- 239000011863 silicon-based powder Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
- A62D3/00—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances
- A62D3/30—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances by reacting with chemical agents
- A62D3/35—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances by reacting with chemical agents by hydrolysis
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
- A62D3/00—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances
- A62D3/40—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances by heating to effect chemical change, e.g. pyrolysis
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
- A62D2203/00—Aspects of processes for making harmful chemical substances harmless, or less harmful, by effecting chemical change in the substances
- A62D2203/02—Combined processes involving two or more distinct steps covered by groups A62D3/10 - A62D3/40
Landscapes
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Business, Economics & Management (AREA)
- Emergency Management (AREA)
- Silicon Compounds (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention belongs to technical field of organic silicon production, specifically a kind for the treatment of process of organosilicon slag slurry, the technique uses distillation still, the distillation still includes top end socket, cylindrical tube, conical shell, solid discharge and stirring module, stirring module includes cylinder, support plate, connecting rod and arc shaped slider, one group of support plate is equipped at intervals in the middle part of cylinder push-rod, support plate outer ring is equipped with one group of connecting rod being arranged radially along support plate；Connecting rod one end is fixedly connected with arc shaped slider side, and elastic membrane is equipped in through slot, and elastic membrane side and through slot side are connected, and the elastic membrane other end is fixedly connected with sliding panel, perforative notch is equipped in the middle part of elastic membrane, sliding panel sliding is for controlling notch closing or opening.The present invention drives support plate to move up and down by push rod, and when sliding into cylindrical tube with arc shaped slider, sliding panel is displaced outwardly, notch is opened, to increase the flow path of organosilicon slag slurry, so that the convection current of organosilicon slag slurry is more abundant, that improves high-boiling components steams efficiency.
Description
Technical field
The invention belongs to technical field of organic silicon production, specifically a kind for the treatment of process of organosilicon slag slurry.
Background technique
Organosilicon slag slurry is generated waste in organic silicon monomer especially methyl chlorosilane monomer synthesis process,
Mainly by a large amount of high-boiling components and a small amount of fluidized bed take unreacted silicon powder out of, copper powder forms, high-boiling components refer to methylchlorosilane
70.3~250 DEG C of the boiling range generated in monomer synthesis process, the height based on silicon-silicon key, silicon-carbon-silicon key, silicon-oxygen-silicon
Boiling point multi-silane mixture.If the exposure of this partial material is in air, it will burn or form strong acid mist or liquid, therefore such as
Fruit direct emission can cause environment seriously to pollute, it is necessary to carry out Harmless processing.
Currently, manufacturing enterprise is all to be recycled the lower substance of its mid-boiling point by flash distillation to the processing method of slurry, give up
Slag is directly discharged into water and hydrolyzes.This processing method does not only recycle high-boiling components a large amount of in slurry, causes effectively to provide
A large amount of wastes in source, it is often more important that the copper powder in slurry in the presence of high-boiling components, meet air or open fire can cause fire or
Explosion, brings serious security risk.
Also occur the technical solution of some organosilicon slag slurries processing in the prior art, such as application No. is
2008101953752 Chinese patent discloses the processing method and its device of a kind of organosilicon slag slurry, by organosilicon slag
After slurry preheating, it is passed through taper evaporator, steams high-boiling components by stirring, condensation is collected to storage tank, residual residue discharge.
The technical solution can steam high-boiling components, but the program carries out organosilicon slag slurry using Stirring mode
Stirring, so that the organosilicon slag slurry temperature near bucket inner wall is higher, the convection current of organosilicon slag slurry is not enough, and restricts high-boiling components
Efficiency is steamed, so that the treatment effeciency of machine silicon slurry is lower.
Summary of the invention
In order to make up for the deficiencies of the prior art, a kind for the treatment of process of organosilicon slag slurry proposed by the present invention, the technique make
With distillation still, which drives support plate to move up and down by push rod, and the arc shaped slider on the outside of support plate is located at conical shell
When, the elastic membrane in through slot is pressurized and closes notch, and when sliding into cylindrical tube with arc shaped slider, sliding panel is moved out
Dynamic, notch is opened, to increase the flow path of organosilicon slag slurry, so that the convection current of organosilicon slag slurry is more abundant, so that having
Machine silicon slurry is heated evenly, and that improves high-boiling components steams efficiency.
The technical solution adopted by the present invention to solve the technical problems is: a kind of place of organosilicon slag slurry of the present invention
Science and engineering skill, the technique the following steps are included:
S1: calcium carbonate is added in organosilicon slag slurry, and is stirred evenly, in order to improve screenings obtained solid object after distillation
Sponginess；
S2: the mixed organosilicon slag slurry of S1 is pumped into distillation still by conveyance conduit, steams high-boiling components, conveyance conduit
Outer ring coiling has heating tube, preheats to organosilicon slag slurry；
S3: the screenings after S2 is distilled, which is added in aqueous sodium carbonate, to be hydrolyzed；
S4: the high-boiling components steamed are sent into condenser after the heating tube of S2, and the heat of gaseous high-boiling components is to organosilicon
Slurry is preheated, to achieve the effect that energy saving；
S5: the high-boiling components that S4 is condensed are delivered to high-boiling components cracker and crack；
Wherein, the distillation still includes top end socket, cylindrical tube, up big and down small conical shell, solid discharge and stirs
Module, controller are mixed, the controller is mounted on the outside of the end socket of top, and the controller is used to control distillation still automatic running,
It is exported on the end socket of top equipped with material inlet and flashed vapour, top end socket is fixedly connected on the upside of cylindrical tube, cylindrical tube bottom
Portion is connected to conical shell, and conical shell bottom is equipped with solid discharge, exports on the cylindrical tube equipped with heat-conducting medium, described
Conical shell side is equipped with heat-conducting medium entrance, and cylindrical tube is connected with the interlayer of conical shell and for filling heat-conductive medium；
The stirring module includes cylinder, support plate, connecting rod and arc shaped slider, and the cylinder is mounted at the top of the end socket of top, cylinder
One group of support plate is equipped at intervals in the middle part of push rod, the support plate is disc, and support plate outer ring is equipped with one group along support plate radial direction
The connecting rod of setting；Described connecting rod one end is fixedly connected with arc shaped slider side, and the arc shaped slider can be in conical shell or cylinder
Cylinder inboard wall sliding, the connecting rod other end are fixedly connected with sliding panel side, and the sliding panel is slidably installed on the supporting plate, and
Spring is equipped in its sliding slot, the support plate is equipped with one group of perforative through slot, is equipped with elastic membrane, the elasticity in the through slot
Film side and through slot side are connected, and the elastic membrane other end is fixedly connected with sliding panel, are equipped with and run through in the middle part of the elastic membrane
Notch, sliding panel sliding for control notch closing or open.In use, push rod drives support plate to move up and down, support plate
When the arc shaped slider in outside is located at conical shell, the elastic membrane in through slot is pressurized and closes notch, as arc shaped slider slides
When to cylindrical tube, sliding panel is displaced outwardly, and notch is opened, to increase the flow path of organosilicon slag slurry, so that organosilicon
The convection current of slurry is more abundant, so that organosilicon slag slurry is heated evenly, that improves high-boiling components steams efficiency.
Preferably, the support plate top and bottom are arranged to cambered surface, with moving up and down for support plate, push organosilicon slag slurry
Flowing improves the convection current for increasing organosilicon slag slurry, so that organosilicon slag slurry is heated evenly, that improves high-boiling components steams efficiency.
Preferably, elastic wire arranged in a crossed manner is equipped in the notch, elastic wire end and notch inner wall are connected, with
The sliding of sliding panel, notch open, with moving up and down for support plate, elastic wire shears the material of agglomeration, just
In subsequent deslagging, the treatment effeciency of organosilicon slag slurry is improved.
Preferably, it is equipped with the first magnet in the arc shaped slider, is equipped in the interlayer of the cylindrical tube and conical shell
Second magnet attracting with the first magnet.Second magnet is slided with the first magnet, is stirred to the heat-conducting medium in interlayer,
Increase the mobility for importing medium, so that organosilicon slag slurry is heated evenly, that improves high-boiling components steams efficiency.
Preferably, waviness is arranged in the cylindrical tube inner wall.Arc shaped slider slides on wavy inner wall, so that
Sliding panel reciprocatingly slides, and the organosilicon slag slurry in through slot moves back and forth, and increases the mobility of organosilicon slag slurry, so that organosilicon slag
Slurry is heated evenly, and improves the efficiency that steams of high-boiling components, meanwhile, the material of some agglomerations is crushed, and is convenient for subsequent deslagging, is improved
The treatment effeciency of organosilicon slag slurry.
Preferably, one end of flexible arc plate is fixedly connected in the middle part of the connecting rod, the flexible arc plate other end is fixed
It is connected to sleeve outer ring, the sleeve is slidably mounted on push rod outer ring, is equipped between the sleeve and support plate and is socketed in push rod
On compression bag, the compression bag surface be equipped with one group of stomata.Connecting rod is mobile and flexible arc plate is pressurized and pushes sleeve
Along push rod outer ring upward sliding, with the reciprocating motion of connecting rod, sleeve periodically squeezes compression bag, the air blast effect of compression bag
Under, the material that agglomeration is attached in support plate is washed from, to improve the efficiency of subsequent cleaning.
Beneficial effects of the present invention are as follows:
1. a kind for the treatment of process of organosilicon slag slurry of the invention, which uses distillation still, which passes through push rod
Support plate is driven to move up and down, when the arc shaped slider on the outside of support plate is located at conical shell, the elastic membrane in through slot is pressurized and seals
Notch is closed, when sliding into cylindrical tube with arc shaped slider, sliding panel is displaced outwardly, and notch is opened, to increase organosilicon
The flow path of slurry, so that organosilicon slag slurry is heated evenly, improves high-boiling components so that the convection current of organosilicon slag slurry is more abundant
Steam efficiency.
2. a kind for the treatment of process of organosilicon slag slurry of the invention, which uses distillation still, which passes through in slot
Elastic wire arranged in a crossed manner is equipped in mouthful, elastic wire end and notch inner wall are connected, with the sliding of sliding panel, notch
It opens, with moving up and down for support plate, elastic wire shears the material of agglomeration, is convenient for subsequent deslagging, improves organic
The treatment effeciency of silicon slurry.
3. a kind for the treatment of process of organosilicon slag slurry of the invention, which uses distillation still, which passes through setting
Flexible arc plate, connecting rod is mobile and flexible arc plate is pressurized and pushes sleeve along push rod outer ring upward sliding, with connecting rod
Reciprocating motion, sleeve periodically squeezes compression bag, under the air blast effect of compression bag, the material quilt of agglomeration attached in support plate
It washes from, to improve the efficiency of subsequent cleaning.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is process flow chart of the invention；
Fig. 2 is the main view of distillation still of the invention；
Fig. 3 is A-A cross-sectional view in Fig. 2；
Fig. 4 is B-B cross-sectional view in Fig. 3；
Fig. 5 is partial enlarged view at E in Fig. 4；
In figure: top end socket 11, cylindrical tube 12, conical shell 13, solid discharge 14, material inlet 15, flashed vapour go out
Mouth 16, stirring module 2, heat-conducting medium export 3, heat-conducting medium entrance 4, push rod 23, support plate 24, through slot 241, connecting rod 25, arc
Shape sliding block 26, sliding panel 27, elastic membrane 28, notch 281, elastic wire 5, the first magnet 61, the second magnet 62, flexible arc plate
7, sleeve 8, compression bag 9.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As shown in Figures 1 to 5, the treatment process of a kind of organosilicon slag slurry of the present invention, the technique include following step
It is rapid:
S1: calcium carbonate is added in organosilicon slag slurry, and is stirred evenly, in order to improve screenings obtained solid object after distillation
Sponginess；
S2: the mixed organosilicon slag slurry of S1 is pumped into distillation still by conveyance conduit, steams high-boiling components, conveyance conduit
Outer ring coiling has heating tube, preheats to organosilicon slag slurry；
S3: the screenings after S2 is distilled, which is added in aqueous sodium carbonate, to be hydrolyzed；
S4: the high-boiling components steamed are sent into condenser after the heating tube of S2, and the heat of gaseous high-boiling components is to organosilicon
Slurry is preheated, to achieve the effect that energy saving；
S5: the high-boiling components that S4 is condensed are delivered to high-boiling components cracker and crack；
Wherein, the distillation still includes that top end socket 11, cylindrical tube 12, up big and down small conical shell 13, residue go out
Mouth 14 and stirring module 2, controller, the controller are mounted on 11 outside of top end socket, and the controller is for control distillation
Kettle automatic running, equipped with material inlet 15 and flashed vapour outlet 16 on top end socket 11, top end socket 11 is fixedly connected on cylinder
12 upside of cylinder, 12 bottom of cylindrical tube are connected to conical shell 12, and 12 bottom of conical shell is equipped with solid discharge 14, the circle
On column casing body 12 equipped with heat-conducting medium outlet 3,12 side of conical shell be equipped with heat-conducting medium entrance 4, cylindrical tube 12 with
The interlayer of conical shell 12 is connected and is used for filling heat-conductive medium；The stirring module 2 includes cylinder, support plate 24, connecting rod 25
With arc shaped slider 26, the cylinder is mounted on 11 top of top end socket, is equipped at intervals with one group of support plate in the middle part of the push rod 23 of cylinder
24, the support plate 24 is disc, and 24 outer ring of support plate is equipped with one group of connecting rod 25 being arranged radially along support plate 24；The company
25 one end of bar is fixedly connected with 26 side of arc shaped slider, and the arc shaped slider 26 can be in 12 inner wall of conical shell 13 or cylindrical tube
Sliding, 25 other end of connecting rod are fixedly connected with 27 side of sliding panel, and the sliding panel 27 is slidably mounted in support plate 24, and
Spring is equipped in its sliding slot, the support plate 24 is equipped with one group of perforative through slot 241, is equipped with elastic membrane in the through slot 241
28,28 side of elastic membrane and 241 side of through slot are connected, and 28 other end of elastic membrane is fixedly connected with sliding panel 27, institute
It states and is equipped with perforative notch 281 in the middle part of elastic membrane 28, the sliding of sliding panel 27 is for controlling the closing of notch 281 or opening.In use,
Push rod 23 drives support plate 24 to move up and down, when the arc shaped slider 26 in 24 outside of support plate is located at conical shell 12, in through slot 241
Elastic membrane 28 be pressurized and close notch 281, when sliding into cylindrical tube 12 with arc shaped slider 26, sliding panel 27 is moved out
Dynamic, notch 281 is opened, thus increase the flow path of organosilicon slag slurry, so that the convection current of organosilicon slag slurry is more abundant, so that
Organosilicon slag slurry is heated evenly, and that improves high-boiling components steams efficiency.
As one embodiment of the present invention, 24 top and bottom of support plate are arranged to cambered surface, with support plate 24
It moves up and down, pushes organosilicon slag slurry flowing, improve the convection current for increasing organosilicon slag slurry, so that organosilicon slag slurry is heated evenly,
That improves high-boiling components steams efficiency.
As one embodiment of the present invention, elastic wire 5 arranged in a crossed manner, Elastic Steel are equipped in the notch 281
5 ends of silk and 281 inner wall of notch are connected, and with the sliding of sliding panel 27, notch 281 opens, with moving down in support plate 24
Dynamic, the material of 5 pairs of elastic wire agglomerations is sheared, and is convenient for subsequent deslagging, is improved the treatment effeciency of organosilicon slag slurry.
As one embodiment of the present invention, the first magnet 61, the cylindrical tube are equipped in the arc shaped slider 26
12 and conical shell 13 interlayer in be equipped with second magnet 62 attracting with the first magnet 61.Second magnet 62 is with the first magnet
61 slidings, stir the heat-conducting medium in interlayer, increase the mobility for importing medium, so that organosilicon slag slurry is heated equal
Even, that improves high-boiling components steams efficiency.
As one embodiment of the present invention, waviness is arranged in 12 inner wall of cylindrical tube.Arc shaped slider 26 exists
It is slided on wavy inner wall, so that sliding panel 27 reciprocatingly slides, the organosilicon slag slurry in through slot 241 is moved back and forth, and increase has
The mobility of machine silicon slurry improves the efficiency that steams of high-boiling components so that organosilicon slag slurry is heated evenly, meanwhile, some agglomerations
Material is crushed, and is convenient for subsequent deslagging, is improved the treatment effeciency of organosilicon slag slurry.
As one embodiment of the present invention, one end of flexible arc plate 7 is fixedly connected in the middle part of the connecting rod 25, it is described
7 other end of flexible arc plate is fixedly connected on 8 outer ring of sleeve, and the sleeve 8 is slidably mounted on 23 outer ring of push rod, the sleeve 8
The compression bag 9 being socketed on push rod 23 is equipped between support plate 24,9 surface of compression bag is equipped with one group of stomata.Connecting rod 25
It moves and flexible arc plate 7 is pressurized and pushes sleeve 8 along 23 outer ring upward sliding of push rod, with the reciprocal fortune of connecting rod 25
It moves, the periodically extruding compression bag 9 of sleeve 8, under the air blast effect of compression bag 9, the material that agglomeration is attached in support plate 24 is rushed
From to improve the efficiency of subsequent cleaning.
In use, push rod 23 drives support plate 24 to move up and down, the arc shaped slider 26 in 24 outside of support plate is located at conically shaped
When body 12, the elastic membrane 28 in through slot 241 is pressurized and closes notch 281, as arc shaped slider 26 slides into cylindrical tube 12
When, sliding panel 27 is displaced outwardly, and notch 281 is opened, thus increase the flow path of organosilicon slag slurry, so that organosilicon slag slurry
Convection current is more abundant, so that organosilicon slag slurry is heated evenly, that improves high-boiling components steams efficiency；
Further, one end of flexible arc plate 7 is fixedly connected in the middle part of connecting rod 25,7 other end of flexible arc plate is fixed
It is connected to 8 outer ring of sleeve, the sleeve 8 is slidably mounted on 23 outer ring of push rod, and socket is equipped between the sleeve 8 and support plate 24
Compression bag 9 on push rod 23,9 surface of compression bag are equipped with one group of stomata.Connecting rod 25 it is mobile and make flexible arc plate 7 by
It presses and pushes sleeve 8 along 23 outer ring upward sliding of push rod, with the reciprocating motion of connecting rod 25, sleeve 8 periodically squeezes compression
Capsule 9, under the air blast effect of compression bag 9, the material that agglomeration is attached in support plate 24 is washed from, to improve the effect of subsequent cleaning
Rate.
Although the present invention be illustrated by specific embodiment, it will be appreciated by those skilled in the art that, do not departing from
In the case where the scope of the invention, various transformation and equivalent substitute can also be carried out to the present invention.In addition, being directed to particular condition or material
Material, can do various modifications to the present invention, without departing from the scope of the present invention.Therefore, the present invention is not limited to disclosed tool
Body embodiment, and should include the whole embodiments fallen within the scope of the appended claims.
Claims (6)
1. a kind for the treatment of process of organosilicon slag slurry, which is characterized in that the technique the following steps are included:
S1: calcium carbonate is added in organosilicon slag slurry, and is stirred evenly；
S2: the mixed organosilicon slag slurry of S1 is pumped into distillation still by conveyance conduit, steams high-boiling components, conveyance conduit outer ring
Coiling has heating tube, preheats to organosilicon slag slurry；
S3: the screenings after S2 is distilled, which is added in aqueous sodium carbonate, to be hydrolyzed；
S4: the high-boiling components steamed are sent into condenser after the heating tube of S2；
S5: the high-boiling components that S4 is condensed are delivered to high-boiling components cracker and crack；
Wherein, the distillation still includes top end socket (11), cylindrical tube (12), up big and down small conical shell (13), residue
(14) and stirring module (2), controller are exported, the controller is mounted on the outside of top end socket (11), and the controller is used for
Distillation still automatic running is controlled, material inlet (15) and flashed vapour outlet (16), top end socket are housed on top end socket (11)
(11) it is fixedly connected on the upside of cylindrical tube (12), cylindrical tube (12) bottom is connected to conical shell (12), conical shell
(12) bottom is equipped with solid discharge (14), equipped with heat-conducting medium outlet (3), the conical shell on the cylindrical tube (12)
(12) side is equipped with heat-conducting medium entrance (4), and cylindrical tube (12) is connected with the interlayer of conical shell (12) and leads for injecting
Thermal medium；The stirring module (2) includes cylinder, support plate (24), connecting rod (25) and arc shaped slider (26), the cylinder installation
On top at the top of end socket (11), it is equipped at intervals with one group of support plate (24) in the middle part of the push rod (23) of cylinder, the support plate (24) is
Disc, support plate (24) outer ring are equipped with one group of connecting rod (25) being arranged radially along support plate (24)；Described connecting rod (25) one end
It is fixedly connected with arc shaped slider (26) side, the arc shaped slider (26) can be in conical shell (13) or cylindrical tube (12) inner wall
Sliding, connecting rod (25) other end are fixedly connected with sliding panel (27) side, and the sliding panel (27) is slidably mounted on support plate
(24) on, and spring is equipped in its sliding slot, the support plate (24) is equipped with one group of perforative through slot (241), the through slot
(241) elastic membrane (28) are equipped in, elastic membrane (28) side and through slot (241) side are connected, and the elastic membrane (28) is another
One end is fixedly connected with sliding panel (27), is equipped with perforative notch (281) in the middle part of the elastic membrane (28), sliding panel (27) sliding
For controlling notch (281) closing or opening.
2. a kind for the treatment of process of organosilicon slag slurry according to claim 1, it is characterised in that: on the support plate (24)
Following settings is at cambered surface.
3. a kind for the treatment of process of organosilicon slag slurry according to claim 2, it is characterised in that: in the notch (281)
Equipped with elastic wire (5) arranged in a crossed manner, elastic wire (5) end and notch (281) inner wall are connected.
4. a kind for the treatment of process of organosilicon slag slurry according to claim 3, it is characterised in that: the arc shaped slider (26)
It is inside equipped with the first magnet (61), is equipped with and the first magnet (61) phase in the interlayer of the cylindrical tube (12) and conical shell (13)
The second magnet (62) inhaled.
5. a kind for the treatment of process of organosilicon slag slurry according to claim 4, it is characterised in that: the cylindrical tube (12)
Waviness is arranged in inner wall.
6. a kind for the treatment of process of organosilicon slag slurry according to claim 5, it is characterised in that: in the middle part of the connecting rod (25)
It is fixedly connected with one end of flexible arc plate (7), flexible arc plate (7) other end is fixedly connected on sleeve (8) outer ring, described
Sleeve (8) is slidably mounted on push rod (23) outer ring, is equipped with and is socketed on push rod (23) between the sleeve (8) and support plate (24)
Compression bag (9), compression bag (9) surface be equipped with one group of stomata.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811087660.2A CN109045555B (en) | 2018-09-18 | 2018-09-18 | Treatment process of organic silicon slag slurry |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811087660.2A CN109045555B (en) | 2018-09-18 | 2018-09-18 | Treatment process of organic silicon slag slurry |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109045555A true CN109045555A (en) | 2018-12-21 |
| CN109045555B CN109045555B (en) | 2020-12-15 |
Family
ID=64761984
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811087660.2A Active CN109045555B (en) | 2018-09-18 | 2018-09-18 | Treatment process of organic silicon slag slurry |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109045555B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111925819A (en) * | 2020-07-23 | 2020-11-13 | 内蒙古翔泰环境科技有限公司 | System and method for preparing coal tar and medium-temperature pitch from coal-prepared oil residues |
-
2018
- 2018-09-18 CN CN201811087660.2A patent/CN109045555B/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111925819A (en) * | 2020-07-23 | 2020-11-13 | 内蒙古翔泰环境科技有限公司 | System and method for preparing coal tar and medium-temperature pitch from coal-prepared oil residues |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109045555B (en) | 2020-12-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108220611B (en) | A kind of aluminium slag reclaimer and aluminium slag recovery process | |
| CN204193944U (en) | A kind of reactor dewater unit | |
| CN208684745U (en) | A kind of mud drying device | |
| CN109045555A (en) | A kind for the treatment of process of organosilicon slag slurry | |
| CN109224490A (en) | A kind of organosilicon synthesis recovery and reuse of waste device | |
| CN209109168U (en) | It is a kind of to be mixed with device for N- cyanoethyl aniline | |
| CN205516576U (en) | Washing type stills is exempted from in saving | |
| CN209155154U (en) | M-aminophenol filter cake vacuum distillation plant | |
| CN208815094U (en) | A kind of ferronickel waste residue waste-heat recovery device | |
| CN209123924U (en) | A kind of device synthesizing casting silane coupling agent | |
| CN109157852A (en) | A kind of organosilicon slag slurry processing unit | |
| CN208975787U (en) | A kind of high-efficiency heating reaction kettle of circulation stirring stirring | |
| CN202509007U (en) | Methacrylic acid heavy component recovery device | |
| CN210186935U (en) | Energy-efficient material preheating device | |
| CN205362124U (en) | Jar is washd in quartz sand purification | |
| CN209049055U (en) | A kind of rosemary Continuous Countercurrent Extraction unit | |
| CN220981973U (en) | Preheating furnace for expanded perlite production | |
| CN220169985U (en) | Energy-saving preheating furnace for processing expanded perlite | |
| CN219879922U (en) | Reation kettle that plastic production was used | |
| CN113698119B (en) | Cement production equipment convenient for waste heat recovery and utilization and use method thereof | |
| CN215946955U (en) | Waste liquid treatment device for chemical laboratory | |
| CN109548903A (en) | A kind of intelligent process units and application method of collection tea rolling and drying one | |
| CN218709895U (en) | Heated air circulation mud minimizing device | |
| CN220745976U (en) | Iron-making device capable of utilizing blast furnace slag waste heat | |
| CN216125636U (en) | Enamel reaction kettle with preheating function |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20201124 Address after: 239400 industrial concentration zone, Suxiang Town, Mingguang City, Chuzhou City, Anhui Province Applicant after: Anhui cansen New Energy Technology Co.,Ltd. Address before: 211189 Southeast University, No. 2 Southeast University Road, Jiangning District, Nanjing City, Jiangsu Province Applicant before: LAN Feng |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240603 Address after: 838299 West of Kekeya Road, Stone Industrial Park, Shanshan County, Turpan, Xinjiang Uygur Autonomous Region (Hesheng Industrial Park) Patentee after: Xinjiang Hesheng Silicon New Materials Co.,Ltd. Country or region after: China Address before: 239400 industrial concentration zone, Suxiang Town, Mingguang City, Chuzhou City, Anhui Province (plant 3) Patentee before: Anhui cansen New Energy Technology Co.,Ltd. Country or region before: China |
|
| TR01 | Transfer of patent right |