CN109021656A - Putty material, preparation method and application method - Google Patents
Putty material, preparation method and application method Download PDFInfo
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- CN109021656A CN109021656A CN201710437427.1A CN201710437427A CN109021656A CN 109021656 A CN109021656 A CN 109021656A CN 201710437427 A CN201710437427 A CN 201710437427A CN 109021656 A CN109021656 A CN 109021656A
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- weight
- putty material
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- rice
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
This disclosure relates to putty material and preparation method thereof.The putty material includes: bonding colloid；Auxiliary binder；Preservative；Lemon juice；And glycerol；Wherein, it is described bonding colloid be by by include rice, water and boric acid mixture freezing after carry out cooking aging, then mill.In some embodiments, the putty material also includes plant amylum.In some embodiments, the putty material also includes pigment and/or filler material.
Description
Technical field
The disclosure belongs to house decorative material field, specifically, this disclosure relates to putty material and preparation method thereof.
Background technique
Putty is the common construction material of indoor decoration, with flourishing for indoor decoration decoration, to putty material
Expect that the requirement of the Safety and Environmental Protection of itself is higher and higher.Existing commercially available petrochemical industry/chemical industry synthesis putty product it is basic composition include:
(1) auxiliary binder/chemical synthesis resin: for example, pure acrylic acid condensate -- emulsifying and solvent type；Styrene
With acrylic acid copolymer zoarium -- emulsifying and solvent type；Vinyl acetate condensate -- emulsifying and solvent type；And polyvinyl alcohol
Condensate -- water soluble type.
(2) solvent: water and coalescing agent (ether, alcohols high boiling solvent)；And organic solvent (such as toluene, esters, alcohols
Deng)；
(3) additive；
(4) pigment: white pigment is mainly titanium dioxide, and colored pigment is mainly inorganic pigment and organic pigment；And
(5) filler etc..
Resin, solvent and the additive overwhelming majority therein are all to be closed using chemical industry/petrochemical material by multiple chemistry
At made of reaction, pigment titanium white be by being completed via pickling and chemical reaction manufacture after mining ilmenite, raw material sources and
Manufacture course of products causes the serious destruction and pollution of environment.Therefore, made by these chemical industry/petrochemical materials and mineral products material
At existing various coating for wall surface and putty have can not it is recycled, non-renewable, can not degrade/decompose, preparation method
Or the problems such as distributing noxious material when derived contaminants environment, use for a long time and poison health.
Summary of the invention
On the one hand, the disclosure provides putty material, it includes:
Wherein, it is described bonding colloid be by by include rice, water and boric acid mixture freezing after carry out cooking aging,
Then it mills.
In some embodiments, the auxiliary binder is selected from gelatin, egg white and combinations thereof.
In some embodiments, the preservative is selected from carbohydrate, plant ash and combinations thereof.
In some embodiments, the putty material also includes pigment and/or filler material.
In some embodiments, the pigment is selected from conch meal, edible pigment, natural mineral matter pigment and their times
Meaning combination.
In some embodiments, the filler material is selected from conch meal, calcium carbonate, talcum powder and their any combination.
In some embodiments, when in putty material including conch meal, the conch meal is with soaked by 10-30 days
Made of shell slurry form be added.
In some embodiments, putty material includes:
Wherein, it is described bonding colloid be by by include rice, water and boric acid mixture freezing after carry out cooking aging,
Then it mills.
In some embodiments, the auxiliary binder is selected from gelatin, egg white and combinations thereof.
In some embodiments, the preservative is selected from carbohydrate, plant ash and combinations thereof.
On the other hand, the preparation method of putty material described in the disclosure is also provided comprising:
By comprising carrying out cooking aging after the freezing of the mixture of rice, water and boric acid, then mills and bonding colloid is made；
The bonding colloid and preservative, glycerol and optional water are mixed；
Then the other components being added in the putty material are mixed；Condition is: the filler material in addition to conch meal
It in addition system and is mixed before lemon juice is added, and conch meal is adding when in putty material including conch meal
Enter after lemon juice in addition system and is mixed；And when in putty material including egg white, egg white is eventually adding and mixes
Close stirring.
In some embodiments, also include in the mixture to be frozen in the method for preparing putty material
Plant is rich in starch position.
In some embodiments, in the method for preparing putty material, when in putty material including conch meal,
Conch meal addition in the form of shell slurry made of soaked by 10-30 days.
In some embodiments, -5 DEG C ± 2 DEG C of temperature is frozen in described in the method for putty material in described prepare
Under carry out about 4-6 hours.
In some embodiments, stirring described in the method for putty material is prepared 600RPM-800RPM's described
It is carried out under speed.
In some embodiments of any of the above-described aspect, the rice is selected from glutinous rice, polished rice or combinations thereof.
In the preferred embodiment of any of the above-described aspect, the rice is the combination of glutinous rice and polished rice.
In some embodiments of any of the above-described aspect, the rice accounts for 6% weight of the putty material in terms of dry weight
Measure % to 15 weight %.
In some embodiments of any of the above-described aspect, the putty material also includes plant amylum.In some implementations
In scheme, the plant amylum accounts for the 0.5 weight % to 1 weight % of the putty material.In some embodiments, the shallow lake
Powder is from including but not limited to: Chinese yam, cassava, potato, corn, rhizoma polygonati and their any combination.
In the preferred embodiment of any of the above-described aspect, the putty material includes the carbon of 30 weight % to 40 weight %
The talcum powder of sour calcium and 5 weight % to 10 weight %.In some embodiments, the fineness 400-600 purpose of the calcium carbonate
Calcium carbonate accounts for 80-85%, and the calcium carbonate of 800-1000 mesh accounts for 15-20%.In some embodiments, the fineness of the talcum powder
For 600-800 mesh.
In some embodiments of any of the above-described aspect, the putty material includes the shellfish of 20 weight % to 30 weight %
Shell powder.
In the preferred embodiment of any of the above-described aspect, the conch meal with by 10-30 days it is soaked made of shell
The form of slurry is added.In some embodiments, the shell powder fineness is 800-1000 mesh, whiteness higher than 90, conch meal
The pH value of slurry is 9-10, specific gravity 2.8.
In the preferred embodiment of any of the above-described aspect, the boric acid accounts for 0.05 weight % to 1 of the putty material
Weight %.
In the preferred embodiment of any of the above-described aspect, the preservative is made of carbohydrate and plant ash, the carbohydrate
The 1 weight % to 3 weight % of the putty material is each accounted for plant ash.
Specific embodiment
On the one hand, the disclosure provides putty material, it includes:
Bond colloid；
Auxiliary binder；
Preservative；
Lemon juice；And
Glycerol；
Wherein, it is described bonding colloid be by by include rice, water and boric acid mixture freezing after carry out cooking aging,
Then it mills.
In some embodiments, the auxiliary binder is selected from gelatin (including but not limited to food-grade gelatin), egg white
And combinations thereof.
In some embodiments, the preservative is selected from carbohydrate, plant ash and combinations thereof.
In some embodiments, the putty material also may include pigment and/or filler material.
In some embodiments, the pigment is selected from conch meal, edible pigment, natural mineral matter pigment and their times
Meaning combination；
In some embodiments, the filler material is selected from conch meal, calcium carbonate, talcum powder and their any combination.
In some embodiments, the putty material of the disclosure may include at least 20 weight % and at most 30 weight % (examples
Such as 21 weight %, 22 weight %, 23 weight %, 24 weight %, 25 weight %, 26 weight %, 27 weight %, 28 weight %, 29
Weight % or 30 weight %) bonding colloid.
In some embodiments, the rice accounts for the 6% weight % to 15 weight % of the putty material in terms of dry weight
(such as 6 weight %, 7 weight %, 8 weight %, 9 weight %, 10 weight %, 11 weight %, 12 weight %, 13 weight %, 14 weights
Measure % or 15 weight %).
In some embodiments, the dosage of the boric acid accounts for the weight % (example of 0.05 weight % to 1 of the putty material
As 0.05 weight %, 0.06 weight %, 0.07 weight %, 0.08 weight %, 0.09 weight %, 0.1 weight %, 0.2 weight %,
0.3 weight %, 0.4 weight %, 0.5 weight %, 0.6 weight %, 0.7 weight %, 0.8 weight %, 0.9 weight % or 1.0 weights
Measure %) boric acid.In the disclosure, boric acid can provide chelating thickening function.
In some embodiments, the putty material of the disclosure may include at least 8 weight % and at most 10 weight % (such as
8 weight %, 8.5 weight %, 9 weight %, 9.5 weight % or 10 weight %) auxiliary binder.
In some embodiments, the putty material of the disclosure may include at least 1 weight % and at most 6 weight % (such as 1
Weight %, 2 weight %, 3 weight %, 4 weight %, 5 weight % or 6 weight %) preservative.
In some embodiments, the putty material of the disclosure may include at least 0.5 weight % and at most 5 weight % (examples
Such as the lemon juice of 0.5 weight %, 1 weight %, 1.5 weight %, 2 weight %, 3 weight %, 4 weight % or 5 weight %).At this
The dosage of lemon juice used in open is the dosage based on the not diluted or not concentrated lemon juice squeezed.It can manage
Its dosage can be not diluted or not concentrated based on squeezing for the disclosure when use is through dilution or concentrated lemon juice for solution
The dosage of lemon juice calculated that therefore the use through dilution or concentrated lemon juice is also fallen into the scope of the present disclosure.
In some embodiments, the putty material of the disclosure may include at least 0.1 weight % and at most 0.4 weight %
The glycerol of (such as 0.1 weight %, 0.2 weight %, 0.3 weight % or 0.4 weight %).In the disclosure, glycerol can provide guarantor
Wet function.
Suitable pigment and its dosage can be selected as needed, and shell can be used when required color is white or pearl
Powder then uses natural mineral matter and edible pigment to replace as pigment, other colors.
On the other hand, the disclosure also provides the preparation method of putty material described in the disclosure comprising:
By comprising carrying out cooking aging after the freezing of the mixture of rice, water and boric acid, then mills and bonding colloid is made；
The bonding colloid and preservative, glycerol and optional water are mixed；
Then the other components being added in the putty material are mixed；Condition is: the filler material in addition to conch meal
It in addition system and is mixed before lemon juice is added, and conch meal is adding when in putty material including conch meal
Enter after lemon juice in addition system and is mixed；And when in putty material including egg white, egg white is eventually adding and mixes
Close stirring.
Water is added or is added without water it will be appreciated by persons skilled in the art that optional water refers to, if be added water with
And the amount for the water being added can be set according to the actual situation by those skilled in the art.
In some embodiments, also include in the mixture to be frozen in the method for preparing putty material
Plant is rich in starch position.
In some embodiments, in the method for preparing putty material, when in putty material including conch meal,
The conch meal is added in the form by (such as 10-30 days, more preferable 20 days) for a long time shell slurry made of soaked.
In some embodiments, -5 DEG C ± 2 DEG C of temperature is frozen in described in the method for putty material in described prepare
Under carry out about 4-6 hours.
In some embodiments, stirring described in the method for putty material is prepared 600RPM-800RPM's described
It is carried out under speed.
In some embodiments, the preparation method of putty material described in the disclosure includes:
By comprising carrying out cooking aging after the freezing of the mixture of rice, water and boric acid, then this mixture cured is existed
After being stirred under the revolving speed of 600RPM-800RPM, mills and bonding colloid is made；
The bonding colloid is mixed with preservative, glycerol and optional water and is stirred under the revolving speed of 600RPM-800RPM
It mixes；
Then the filler material (such as calcium carbonate, talcum powder etc.) in addition to conch meal is added to turn in 600RPM-800RPM
After fast lower stirring, lemon juice is added and is mixed, adds conch meal mixing and (held when in putty material including conch meal
This step of row, does not execute this step when not including conch meal in putty material)；And when in putty material including egg white,
Egg white is eventually adding and is mixed.In addition to this, the addition sequence of other components is not particularly limited.
In some embodiments of any of the above-described aspect, the rice is selected from glutinous rice, polished rice or combinations thereof.
In the preferred embodiment of any of the above-described aspect, the rice is the combination of glutinous rice and polished rice.
In some embodiments of any of the above-described aspect, the putty material also may include at least 0.5 weight % and extremely
More 1 weight % (such as 0.5 weight %, 0.6 weight %, 0.7 weight %, 0.8 weight %, 0.9 weight % or 1.0 weight %)
Plant amylum.In the disclosure, plant amylum can provide hydrogen bond thickening function.
In some embodiments, the starch source is in including but not limited to: Chinese yam, cassava, potato, corn, Huang
Essence and their any combination.
In the preferred embodiment of any of the above-described aspect, the putty material includes the carbon of 30 weight % to 40 weight %
The talcum powder of sour calcium and 5 weight % to 10 weight %.In some embodiments, the fineness 400-600 purpose of the calcium carbonate
Calcium carbonate accounts for 80-85%, and the calcium carbonate of 800-1000 mesh accounts for 15-20%.In some embodiments, the fineness of the talcum powder
For 600-800 mesh.
In some embodiments, when calcium carbonate is used, the putty material includes 30 weight %, 31 weight %, 32
Weight %, 33 weight %, 34 weight %, 35 weight %, 36 weight %, 37 weight %, 38 weight %, 39 weight % or 40 weights
Measure the calcium carbonate of %.In the disclosure, calcium carbonate can provide filler/polishing function.
In some embodiments, when using talcum powder, the putty material includes 5 weight %, 6 weight %, 7 weights
Measure the talcum powder of %, 8 weight %, 9 weight % or 10 weight %.In the disclosure, talcum powder, which has, improves hardness/increase whiteness
Function.
In the preferred embodiment of any of the above-described aspect, the putty material includes that conch meal as pigment and/or is filled out
Charge.In some embodiments, when in putty material including conch meal, the conch meal is by (such as 10- for a long time
30 days, more preferable 20 days) it is soaked made of shell slurry form be added.In preferred embodiments, the conch meal
Average to be greater than 90 less than 1000 mesh, whiteness, the pH value of shell slurry is 9-10, specific gravity 2.8.It is described greasy when using conch meal
Sub- material include at least 20 weight % and at most 30 weight % (such as 20 weight %, 21 weight %, 22 weight %, 23 weight %,
24 weight %, 25 weight %, 26 weight %, 27 weight %, 28 weight %, 29 weight % or 30 weight %) conch meal.
In the preferred embodiment of any of the above-described aspect, the preservative is made of carbohydrate and plant ash, the carbohydrate
The 1 weight % to 3 weight % (such as 1 weight %, 2 weight % and 3 weight %) of the putty material is each accounted for plant ash.
Detailed description of the invention
Fig. 1: wall schematic diagram to be onstructed.
Fig. 2: the schematic diagram of the putty material product of embodiment 1.
Fig. 3: effect diagram of the putty material product construction of embodiment 1 on wall.
Fig. 4: the effect diagram that the putty material product of embodiment 1 is constructed on wall after polishing.
Embodiment
Below with reference to embodiment, the specific embodiment of the disclosure is described in further detail.Following embodiment is only used
In the purpose of explanation, rather than it is used to limit the scope of the present disclosure.
Embodiment 1:
The formula of putty material: glutinous rice 60g (dry weight), polished rice 20g (dry weight), water 193g, boric acid 1g, egg white 80g, vegetation
Grey 10g, lemon juice 10g, glycerol 3g, shell starch 250g, 400 mesh calcium carbonate 260g, 1000 mesh calcium carbonate 60g, 800 mesh talcum powder
50g, white sugar 3g.
Preparation process:
1. the boric acid that 1g is added mixes by the water of the polished rice and 150g of the glutinous rice of 60g and 20g, it is put into -5 DEG C
Freezer freezes 5 hours.
2. taking out this frozen material, carry out cooking aging about 1 hour
3. after this mixture cured is stirred 45 minutes under the revolving speed of 600RPM, then being milled into uniform adhesive glue
Body.
4. bonding colloid is added together in the revolving speed of 600RPM in the glycerol of the water of 43g, the plant ash of 10g, the sugar of 3g, 3g
Lower stirring 20 minutes.
5. the calcium carbonate of the calcium carbonate of 260g (400 mesh), 60g (1000 mesh) is added, 15 are stirred under the revolving speed of 750RPM
After minute, the talcum powder for adding 50g (800 mesh) is stirred for 10 minutes.
6. will be stirred 10 minutes in the lemon juice addition system of 10g again.
7. the shell slurry 250g for adding and (impregnating 20 sky and water), is stirred 20 minutes.
8. will be finally stirred for 20 minutes in the egg white addition system of 80g.
Embodiment 2:
In addition to being additionally added potato in mixture to be frozen, it is made and is implemented with preparation process same as Example 1
The putty material of example 2.
The performance test results of putty material made from the disclosure:
The putty fineness of testing example 1-2 standard up to specification.According to " architecture indoor putty " JG/T298-
The regulation of 2010 standards is tested for the property embodiment 1-2 referring to attached drawing 1-4, and test result is as follows shown in table 1:
Table 1
* the temperature-time of cold cycling: -5 DEG C ± 2 DEG C standing time 18 hours, 23 DEG C of ± 2 DEG C of standing times 4 of room temperature are small
When.
In addition, being detected to whether there is harmful substance in the putty material of embodiment 1-2, testing result such as the following table 2:
Table 2
* wherein N.D expression is not detected.
By the testing result of above-mentioned Tables 1 and 2 as it can be seen that putty material of the invention does not contain volatile organic compound not only
Poisonous and harmful substances such as object, heavy metal, and application property, grinability, water resistance, caking property and have good stability, not light,
Water, tide, cold and hot influence.
Claims (10)
1. putty material, it includes:
Wherein, it is described bonding colloid be by by include rice, water and boric acid mixture freezing after carry out cooking aging, then
It mills；
Optionally, the auxiliary binder is selected from gelatin, egg white and combinations thereof；
Optionally, the preservative is selected from carbohydrate, plant ash and combinations thereof.
2. putty material as described in claim 1, the putty material also includes pigment and/or filler material；
Optionally, the pigment is selected from conch meal, edible pigment, natural mineral matter pigment and their any combination；
Optionally, the filler material is selected from conch meal, calcium carbonate, talcum powder and their any combination.
3. putty material, it includes:
Wherein, it is described bonding colloid be by by include rice, water and boric acid mixture freezing after carry out cooking aging, then
It mills；
Optionally, the auxiliary binder is selected from gelatin, egg white and combinations thereof；
Optionally, the preservative is selected from carbohydrate, plant ash and combinations thereof.
4. the preparation method of putty material of any of claims 1-3 comprising:
By comprising carrying out cooking aging after the freezing of the mixture of rice, water and boric acid, then mills and bonding colloid is made；
The bonding colloid and preservative, glycerol and optional water are mixed；
Then the other components being added in the putty material are mixed；Condition is: the filler material in addition to conch meal exists
It in addition system and is mixed before lemon juice is added, and lemon is being added in conch meal when in putty material including conch meal
It in addition system and is mixed after lemon juice；And when in putty material including egg white, egg white is eventually adding and mixes and stirs
It mixes；
Optionally, starch position also is rich in comprising plant in the mixture to be frozen.
5. method as claimed in claim 4, wherein
It is described be frozen in -5 DEG C ± 2 DEG C at a temperature of carry out about 4-6 hours；
Optionally, the stirring carries out under the speed of 600RPM-800RPM.
6. putty material as claimed in any one of claims 1-3 or method as described in claim 4 or 5, wherein institute
It states rice and is selected from glutinous rice, polished rice or combinations thereof；Optionally, the rice is the combination of glutinous rice and polished rice；Optionally, in terms of dry weight
The rice accounts for the 6% weight % to 15 weight % of the putty material.
7. putty material as claimed in any one of claims 1-3 or method as described in claim 4 or 5, described greasy
Sub- material also includes plant amylum；
Optionally, the plant amylum accounts for the 0.5 weight % to 1 weight % of the putty material；
Optionally, the starch source is in Chinese yam, cassava, potato, corn, rhizoma polygonati and their any combination.
8. putty material as claimed in any one of claims 1-3 or method as described in claim 4 or 5, wherein institute
Stating putty material includes the calcium carbonate of 30 weight % to 40 weight % and the talcum powder of 5 weight % to 10 weight %；Optionally, institute
The calcium carbonate for stating the fineness 400-600 mesh of calcium carbonate accounts for 80-85%, and the calcium carbonate of 800-1000 mesh accounts for 15-20%；Optionally,
The fineness of the talcum powder is 600-800 mesh.
9. putty material as claimed in any one of claims 1-3 or method as described in claim 4 or 5, wherein institute
State the conch meal that putty material includes 20 weight % to 30 weight %；Optionally, the conch meal with by 10-30 days it is soaked and
At shell slurry form be added；Optionally, the shell powder fineness is 800-1000 mesh, whiteness higher than 90；Shell slurry
PH value be 9-12, specific gravity 2.8.
10. putty material as claimed in any one of claims 1-3 or method as described in claim 4 or 5, wherein institute
State the 0.05 weight % to 1 weight % that boric acid accounts for the putty material；Optionally, wherein the preservative is by carbohydrate and plant ash
Composition, the carbohydrate and plant ash each account for the 1 weight % to 3 weight % of the putty material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710437427.1A CN109021656A (en) | 2017-06-09 | 2017-06-09 | Putty material, preparation method and application method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710437427.1A CN109021656A (en) | 2017-06-09 | 2017-06-09 | Putty material, preparation method and application method |
Publications (1)
| Publication Number | Publication Date |
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| CN109021656A true CN109021656A (en) | 2018-12-18 |
Family
ID=64629255
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710437427.1A Pending CN109021656A (en) | 2017-06-09 | 2017-06-09 | Putty material, preparation method and application method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111944349A (en) * | 2020-08-21 | 2020-11-17 | 北京七特丽装饰材料有限公司 | Coating containing herbal plant extract, preparation method and application thereof |
| CN113735519A (en) * | 2021-09-14 | 2021-12-03 | 北京科技大学 | Filling material and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1580143A (en) * | 2003-08-13 | 2005-02-16 | 上海大作为铜管道有限公司 | Shell interior wall putty powder |
| CN105524511A (en) * | 2016-01-28 | 2016-04-27 | 任甜甜 | Exterior wall putty with capacity of energy saving and heat preservation and preparation method |
-
2017
- 2017-06-09 CN CN201710437427.1A patent/CN109021656A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1580143A (en) * | 2003-08-13 | 2005-02-16 | 上海大作为铜管道有限公司 | Shell interior wall putty powder |
| CN105524511A (en) * | 2016-01-28 | 2016-04-27 | 任甜甜 | Exterior wall putty with capacity of energy saving and heat preservation and preparation method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111944349A (en) * | 2020-08-21 | 2020-11-17 | 北京七特丽装饰材料有限公司 | Coating containing herbal plant extract, preparation method and application thereof |
| CN113735519A (en) * | 2021-09-14 | 2021-12-03 | 北京科技大学 | Filling material and application thereof |
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Application publication date: 20181218 |