CN109020184A - A kind of production method and equipment of porous basalt cellucotton - Google Patents

A kind of production method and equipment of porous basalt cellucotton Download PDF

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Publication number
CN109020184A
CN109020184A CN201810748561.8A CN201810748561A CN109020184A CN 109020184 A CN109020184 A CN 109020184A CN 201810748561 A CN201810748561 A CN 201810748561A CN 109020184 A CN109020184 A CN 109020184A
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CN
China
Prior art keywords
basalt
parts
cellucotton
production method
porous
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CN201810748561.8A
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Chinese (zh)
Inventor
袁彬
李阳明
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Sichuan Thousand Ran Technology Co Ltd
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Sichuan Thousand Ran Technology Co Ltd
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Priority to CN201810748561.8A priority Critical patent/CN109020184A/en
Publication of CN109020184A publication Critical patent/CN109020184A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C13/00Fibre or filament compositions
    • C03C13/06Mineral fibres, e.g. slag wool, mineral wool, rock wool

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Artificial Filaments (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Chemical Treatment Of Fibers During Manufacturing Processes (AREA)

Abstract

The invention discloses the production method and equipment of a kind of porous basalt cellucotton, preparation step: basalt, quartz and inorganic salts are put into pulverizer and are crushed, mixed powder is made;The powder being mixed to get is added in blast furnace, and being heated to 1450 DEG C ~ 1500 DEG C melts powder, and solution is made;Toughener is added in solution, being sufficiently stirred makes its cooling, and spinning melt is made;Obtained spinning melt is stood, and nylon is added, and basalt composite fibre cotton is made by bushing;Obtained basalt composite fibre cotton immerses size, makes sufficiently its cooling;Obtained composite fibre, which is immersed in water, to be dissolved, and addition ultrasonic oscillator accelerates dissolution, dries to obtain porous basalt cellucotton;Porous basalt cellucotton is made by techniques such as stock, melting, mixing, spinning, cooling, dissolutions using basalt raw material, quartz, nylon, toughener, inorganic salts on material of the present invention.

Description

A kind of production method and equipment of porous basalt cellucotton
Technical field
The present invention relates to the production methods and equipment of a kind of porous basalt cellucotton, belong to basalt fiber cotton manufacture skill Art field.
Background technique
Basalt fibre is a kind of emerging novel inorganic environment-friendly and green high performance fibre material, is following China's emphasis One of the four big high-performance fibers of development, it is aoxidized by silica, aluminium oxide, calcium oxide, iron oxide and titanium dioxide etc. The basalt building stones of object composition are prepared after high-temperature fusion by spinning technique.Basalt continuous fiber is not only stable Property it is good, but also there are a variety of excellent properties such as electrical insulating property, anticorrosive, flame resistant, high temperature resistant, moreover, basalt fibre The waste that production technology generates is few, and environmental pollution is small, can directly be transferred in ecological environment after product abandonment, without any danger Evil, thus be the qualified green of one kind, environment-friendly materials.Basalt fibre fibre reinforced composites, friction material, The many aspects such as shipbuilding materials, heat-barrier material, automobile industry, high temperature filtration fabric and protection field have obtained widely answering With.
Basalt fibre is added together in cotton spinning, can form basalt fiber cotton, but existing basalt fiber cotton Have the defects that water penetration, drainage performance are poor, intensity is inadequate.
Summary of the invention
The present invention provides the production method and equipment of a kind of porous basalt cellucotton.
In order to solve the above-mentioned technical problems, the present invention provides the following technical solutions:
A kind of production method of porous basalt cellucotton of the present invention, preparation step are as follows:
S1) basalt, quartz and inorganic salts are put into pulverizer and are crushed, mixed powder is made;
S2) powder being mixed to get in step S1) is added in blast furnace, being heated to 1450 DEG C ~ 1500 DEG C melts powder, is made Solution;
S3 toughener) is added in the solution of step S2), being sufficiently stirred makes its cooling, and spinning melt is made;
S4) step S3) obtained spinning melt is stood, and nylon is added, basalt composite fibre cotton is made by bushing;
S5) the basalt composite fibre cotton for obtaining S4) immerses size, makes sufficiently its cooling;
S6) the obtained composite fibre of S5) is immersed in water and is dissolved, addition ultrasonic oscillator accelerates dissolution, dries to obtain more Hole basalt fiber cotton.
As a preferred technical solution of the present invention, raw material is prepared including following parts by weight: basalt raw material 35-45 Part, 10-15 parts of quartz, 35-45 parts of nylon, 1-5 parts of toughener, 4-7 parts of inorganic salts.
As a preferred technical solution of the present invention, raw material is prepared including following parts by weight: 40 parts of basalt raw material, Quartzy 10 parts, 40 parts of nylon, 5 parts of toughener, 5 parts of inorganic salts.
As a preferred technical solution of the present invention, ceramic raw material includes that following parts by weight prepare raw material: porcelain stone powder 50 parts, 20 parts of kaolin, 10 parts of lime stone, 10 parts of cullet, 10 parts of quartz
As a preferred technical solution of the present invention, toughener is silica, silicon carbide, silicon nitride particle, titanium nitride, carbon Change one of aluminium, calcium silicide or a variety of.
As a preferred technical solution of the present invention, in the size aqueous polyurethane, water-soluble epoxy resin It is one or more.
As a preferred technical solution of the present invention, the infiltration temperature of the size is 0-50 degrees Celsius.
The present invention also provides the making apparatus of above-mentioned porous basalt cellucotton:
It is set including ore melt furnace 1, heating device 2, mixing plant 3, microwave concussion equipment 4, size coating apparatus 5 and drying Standby 6.Wherein ore melt furnace 1 includes melting furnace, input and output material equipment and fume extractor with bushing.
The present invention a kind of production method and equipment of porous basalt cellucotton, wherein process equipment is mainly molten including ore Change furnace 1, heating device 2, mixing plant 3, microwave concussion equipment 4, size coating apparatus 5 and drying equipment 6, in process In, it is necessary first to former stone is processed into powder, then passes through the techniques machine-shaping such as thawing, mixing, spinning, cooling, dissolution process, Porous basalt cellucotton is made, the fibre diameter of finished product is 0.5-50 μm, porosity 10%-80%;With good permeable, guarantor Water, orientation drainage performance, have some strength.
The beneficial effects obtained by the present invention are as follows being: on material of the present invention using basalt raw material, quartz, nylon, toughener, Porous basalt cellucotton is made by techniques such as stock, melting, mixing, spinning, cooling, dissolutions in inorganic salts, and finished product is whole Permeable, water conservation, drainage performance it is good, and operation difficulty is low in entire manufacturing process, and the processing is simple, and finished product also has good Intensity;It is suitble to promote the use of.
Detailed description of the invention
Fig. 1 is a kind of production equipment structural schematic diagram of porous basalt cellucotton of the present invention;
In figure: 1, ore melt furnace;2, heating device;3, mixing plant;4, microwave shakes equipment;5, size coating apparatus; 6, drying equipment.
Specific embodiment
Hereinafter, preferred embodiments of the present invention will be described, it should be understood that preferred embodiment described herein is only used In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1
A kind of production method of porous basalt cellucotton of invention, preparation step are as follows:
S1) basalt, quartz and inorganic salts are put into pulverizer and are crushed, mixed powder is made;
S2) powder being mixed to get in step S1) is added in blast furnace, being heated to 1450 DEG C ~ 1500 DEG C melts powder, is made Solution;
S3 toughener) is added in the solution of step S2), being sufficiently stirred makes its cooling, and spinning melt is made;
S4) step S3) obtained spinning melt is stood, and nylon is added, basalt composite fibre cotton is made by bushing;
S5) the basalt composite fibre cotton for obtaining S4) immerses size, makes sufficiently its cooling;
S6) the obtained composite fibre of S5) is immersed in water and is dissolved, addition ultrasonic oscillator accelerates dissolution, dries to obtain more Hole basalt fiber cotton.
Prepare raw material including following parts by weight: 35-45 parts of basalt raw material, 35-45 parts of nylon, increases 10-15 parts of quartz Tough dose 1-5 parts, 4-7 parts of inorganic salts.Raw material is prepared including following parts by weight: 40 parts of basalt raw material, quartzy 10 parts, nylon 40 Part, 5 parts of toughener, 5 parts of inorganic salts.The toughener be silica, silicon carbide, silicon nitride particle, titanium nitride, aluminium carbide, One of calcium silicide is a variety of.One of the size aqueous polyurethane, water-soluble epoxy resin are a variety of.The leaching The infiltration temperature for moistening agent is 0-50 degrees Celsius.
Making apparatus are as follows:
It is set including ore melt furnace 1, heating device 2, mixing plant 3, microwave concussion equipment 4, size coating apparatus 5 and drying Standby 6.Wherein ore melt furnace 1 includes melting furnace, input and output material equipment and fume extractor with bushing.
The present invention a kind of production method and equipment of porous basalt cellucotton, wherein process equipment is mainly molten including ore Change furnace 1, heating device 2, mixing plant 3, microwave concussion equipment 4, size coating apparatus 5 and drying equipment 6, in process In, it is necessary first to former stone is processed into powder, then passes through the techniques machine-shaping such as thawing, mixing, spinning, cooling, dissolution process, Porous basalt cellucotton is made, the fibre diameter of finished product is 0.5-50 μm, porosity 10%-80%;With good permeable, guarantor Water, orientation drainage performance, have some strength.
In conclusion basalt raw material, quartz, nylon, toughener, inorganic salts are used on material of the present invention, by stocking up, Porous basalt cellucotton, finished product whole permeable, water conservation, draining is made in the techniques such as melting, mixing, spinning, cooling, dissolution Performance is good, and operation difficulty is low in entire manufacturing process, and the processing is simple, and finished product also has good intensity;Suitable popularization makes With.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention, Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features. All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention Within protection scope.

Claims (8)

1. a kind of production method of porous basalt cellucotton, which is characterized in that preparation step is as follows:
S1 it) crushes: basalt, quartz and inorganic salts being put into pulverizer and are crushed, mixed powder is made;
S2) heating and melting: the powder being mixed to get in step S1) is added in blast furnace, being heated to 1450 DEG C ~ 1500 DEG C makes powder Melt, solution is made;
S3) cool down: toughener being added in the solution of step S2), being sufficiently stirred makes its cooling, and spinning melt is made;
S4) step S3) obtained spinning melt is stood, and nylon is added, basalt composite fibre cotton is made by bushing;
S5) cooling: the basalt composite fibre cotton that S4) is obtained immerses size, makes sufficiently its cooling;
S6 it) dissolves drying: the obtained composite fibre of S5) being immersed in water and is dissolved, addition ultrasonic oscillator accelerates dissolution, dries in the air It is dry to obtain porous basalt cellucotton.
2. a kind of production method of porous basalt cellucotton according to claim 1, which is characterized in that including following heavy Amount part prepares raw material: 35-45 parts of basalt raw material, 10-15 parts of quartz, 35-45 parts of nylon, 1-5 parts of toughener, inorganic salts 4- 7 parts.
3. a kind of production method of porous basalt cellucotton according to claim 2, which is characterized in that including following heavy Amount part prepares raw material: 40 parts of basalt raw material, quartzy 10 parts, 40 parts of nylon, 5 parts of toughener, 5 parts of inorganic salts.
4. a kind of production method of porous basalt cellucotton according to claim 3, which is characterized in that the toughener For one of silica, silicon carbide, silicon nitride particle, titanium nitride, aluminium carbide, calcium silicide or a variety of.
5. a kind of production method of porous basalt cellucotton according to claim 1, which is characterized in that the size One of aqueous polyurethane, water-soluble epoxy resin are a variety of.
6. a kind of production method of porous basalt cellucotton according to claim 5, which is characterized in that the size Infiltration temperature be 0-50 degrees Celsius.
7. a kind of making apparatus of porous basalt cellucotton according to claim 1, which is characterized in that molten including ore Change furnace (1), heating device (2), mixing plant (3), microwave concussion equipment (4), size coating apparatus (5) and drying equipment (6).
8. a kind of making apparatus of porous basalt cellucotton according to claim 7, which is characterized in that ore melt furnace It (1) include melting furnace, input and output material equipment and fume extractor with bushing.
CN201810748561.8A 2018-07-10 2018-07-10 A kind of production method and equipment of porous basalt cellucotton Pending CN109020184A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109678340A (en) * 2019-02-26 2019-04-26 东南大学 A kind of basaltic magma adjustable microwave heating wire-drawing frame and drawing process
CN111470779A (en) * 2020-04-03 2020-07-31 深圳中科氢能科技有限公司 Process for manufacturing basalt capillary tube by using stretching method
CN112080815A (en) * 2020-08-29 2020-12-15 河南交通职业技术学院 Extrusion type basalt steel fiber production equipment
CN113860796A (en) * 2021-10-29 2021-12-31 北京金隅节能保温科技(大厂)有限公司 Ecological porous cellucotton and preparation process thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1789187A (en) * 2004-12-14 2006-06-21 玄武岩纤维复合材料科技发展有限公司 Method and equipment for producing basalt fiber
CN101492243A (en) * 2009-03-13 2009-07-29 宋朋泽 Method for producing ultra-fine basalt continuous filament
KR100919638B1 (en) * 2009-05-08 2009-09-30 경기수 Underfloor-heating using the power wave water and porous whinstone
CN102786220A (en) * 2012-08-07 2012-11-21 宋朋泽 Production method for ultrafine continuous basalt fibers
CN105506782A (en) * 2015-12-29 2016-04-20 四川力久知识产权服务有限公司 Preparation method of porous basalt fibers

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1789187A (en) * 2004-12-14 2006-06-21 玄武岩纤维复合材料科技发展有限公司 Method and equipment for producing basalt fiber
CN101492243A (en) * 2009-03-13 2009-07-29 宋朋泽 Method for producing ultra-fine basalt continuous filament
KR100919638B1 (en) * 2009-05-08 2009-09-30 경기수 Underfloor-heating using the power wave water and porous whinstone
CN102786220A (en) * 2012-08-07 2012-11-21 宋朋泽 Production method for ultrafine continuous basalt fibers
CN105506782A (en) * 2015-12-29 2016-04-20 四川力久知识产权服务有限公司 Preparation method of porous basalt fibers

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109678340A (en) * 2019-02-26 2019-04-26 东南大学 A kind of basaltic magma adjustable microwave heating wire-drawing frame and drawing process
CN109678340B (en) * 2019-02-26 2021-07-02 东南大学 Adjustable microwave heating wire drawing device and method for basalt slurry
CN111470779A (en) * 2020-04-03 2020-07-31 深圳中科氢能科技有限公司 Process for manufacturing basalt capillary tube by using stretching method
CN112080815A (en) * 2020-08-29 2020-12-15 河南交通职业技术学院 Extrusion type basalt steel fiber production equipment
CN112080815B (en) * 2020-08-29 2022-09-09 河南交通职业技术学院 Extrusion type basalt steel fiber production equipment
CN113860796A (en) * 2021-10-29 2021-12-31 北京金隅节能保温科技(大厂)有限公司 Ecological porous cellucotton and preparation process thereof

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Application publication date: 20181218