CN108993345A - A kind of experiment porch of adsorbent research and development - Google Patents
A kind of experiment porch of adsorbent research and development Download PDFInfo
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- CN108993345A CN108993345A CN201811087813.3A CN201811087813A CN108993345A CN 108993345 A CN108993345 A CN 108993345A CN 201811087813 A CN201811087813 A CN 201811087813A CN 108993345 A CN108993345 A CN 108993345A
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- Prior art keywords
- reaction kettle
- autoclave body
- tracheae
- kettle autoclave
- experiment porch
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- 239000003463 adsorbent Substances 0.000 title claims abstract description 34
- 238000002474 experimental method Methods 0.000 title claims abstract description 27
- 238000012827 research and development Methods 0.000 title claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 87
- 238000007789 sealing Methods 0.000 claims abstract description 69
- 239000004809 Teflon Substances 0.000 claims abstract description 16
- 229920006362 Teflon® Polymers 0.000 claims abstract description 16
- 238000010079 rubber tapping Methods 0.000 claims description 8
- 239000011521 glass Substances 0.000 claims description 5
- 239000007789 gas Substances 0.000 description 35
- 229910000831 Steel Inorganic materials 0.000 description 8
- 239000010959 steel Substances 0.000 description 8
- 229910018503 SF6 Inorganic materials 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 5
- 238000013461 design Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 239000010935 stainless steel Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000007747 plating Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 231100001010 corrosive Toxicity 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000012212 insulator Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- WRQGPGZATPOHHX-UHFFFAOYSA-N ethyl 2-oxohexanoate Chemical compound CCCCC(=O)C(=O)OCC WRQGPGZATPOHHX-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 239000005431 greenhouse gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000005316 response function Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- SFZCNBIFKDRMGX-UHFFFAOYSA-N sulfur hexafluoride Chemical compound FS(F)(F)(F)(F)F SFZCNBIFKDRMGX-UHFFFAOYSA-N 0.000 description 1
- 229960000909 sulfur hexafluoride Drugs 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0245—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of synthetic organic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0295—Synthetic organic materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention patent discloses a kind of experiment porch of adsorbent research and development, experiment porch includes reaction kettle autoclave body, the first tracheae and sealing device, the first tracheae is connected on reaction kettle autoclave body side wall, pressure vacuum gauge is provided on first tracheae, first tracheae is provided with valve far from one end of reaction kettle autoclave body, the opening of reaction kettle autoclave body is provided with sealing device, the inner wall and reaction kettle autoclave body bottom of reaction kettle autoclave body are coated with Teflon film, realize the purpose screened for the adsorbent of different insulating gas.
Description
Technical field
The invention patent relates to high pressure electrical domains, more specifically to a kind of experiment porch of adsorbent research and development.
Background technique
For the insulating gas inside high voltage electric equipment once because the factors such as shelf depreciation cause to decompose to generate
Some gases, this portion gas insulation, arc extinguishing, in terms of all show very severe performance, such as SF6Gas
SO is easily generated under micro- water micro-oxygen conditions2And H2S、HF、SOF2Equal acidic corrosives gas, decomposes the active gases of generation
Will accelerating solid insulator arrangement aging, corrosion is generated to equipment, and the appearance of these situations will seriously affect the peace of equipment
Row for the national games, the personal safety also great threat to staff.Therefore existing with SF6To be placed in the equipment of dielectric
Adsorbent avoids it from affecting equipment life to adsorb to acid and toxic corrosive gas, moisture etc..
Although sulfur hexafluoride (SF6) because of its nontoxicity, the good physics and chemistry such as insulation, arc extinction performance are good, and reactivity is low
Characteristic is widely used in gas-insulated assembling device (GIS), power transfer conduit (GIL), cable (GIC), transformer (GIT), breaks
In the equipment for power transmission and distribution such as road device (GCB), but SF6Because of the potential value of its high greenhouse effects, in an atmosphere the factors quilt such as service life length
It is classified as one of the greenhouse gases of 6 kinds of Limited uses.To be further reduced power industry to SF6The dependence of gas, reducing it makes
Dosage, many scholars actively probe into SF in recent years6Substitution gas be used for gas insulated electric apparatus.It has now been found that
C4F7N,C5F10O,C6F12The insulation characterisitic of the substances such as O is excellent, and environmental protection characteristic is prominent and nontoxic, has substitution tradition SF6Gas
The potentiality of body.With C4F7N,C5F10O,C6F12The buffer gas such as O etc. and nitrogen, which are mixed in a certain ratio, to be formed mixed gas and is
The electrical equipment of dielectric is with step by step input trial operation.However, C4F7N,C5F10O,C6F12The physicochemical property and SF of O etc.6Gas
There are larger difference, the decomposition product types and SF of generation of decomposing under the conditions ofs electric discharge, hot-spot etc.6Completely not
Together, and C4F7N,C5F10O,C6F12The self structures such as O are complicated.In large-scale promotion application C4F7N,C5F10O,C6F12The gaseous mixtures such as O
Before body insulator arrangement, need to develop a kind of suitable for C4F7N,C5F10O,C6F12The adsorbent of the mixed gas such as O, the adsorbent
On the one hand can satisfy not with C4F7N,C5F10O,C6F12O has an effect or has an effect minimum, on the other hand can effectively adsorb
C4F7N,C5F10O,C6F12The decomposition components and moisture of O.
For the adsorbent screening and development for different insulative gas, needing to design one can adapt to equipment gas
The experiment porch that pressure range, structural material do not react with insulating gas.
Summary of the invention
The purpose of the embodiment of the present invention is that providing a kind of experiment porch of adsorbent research and development, realize for different
The purpose that the adsorbent of insulating gas is screened.
A kind of experiment porch of adsorbent research and development, the experiment porch include reaction kettle autoclave body, the first tracheae and
Sealing device is connected with the first tracheae on the reaction kettle autoclave body side wall, is provided with pressure vacuum gauge on first tracheae, institute
It states the first tracheae and one end of reaction kettle autoclave body is provided with valve, the opening of the reaction kettle autoclave body is provided with sealing dress
It sets, the inner wall of the reaction kettle autoclave body and the bottom of reaction kettle autoclave body are coated with Teflon film.
Preferably, the sealing device includes sealing cover, and the sealing cover is detachably connected with reaction kettle autoclave body open end.
Preferably, the first tracheae outer wall is provided with sealing shroud close to reaction kettle autoclave body end, and the sealing shroud is embedded in anti-
Kettle autoclave body outer wall is answered, first tracheae is plugged in sealing shroud.
Preferably, shell is provided with outside the reaction kettle autoclave body.
Preferably, the sealing cover is provided with several equally distributed through-holes, and the opening of the shell is provided with and seals
The corresponding self tapping hole of the through-hole of lid, the sealing cover and reaction kettle autoclave body are by screw connection.
Preferably, the opening of the shell of the reaction kettle autoclave body is provided with and the consistent arc groove of autoclave body inner diameter size, institute
The inside that arc groove is located at self tapping hole is stated, is provided with sealing ring in the arc groove.
Preferably, the sealing cover uses organic glass.
Preferably, first tracheae is plugged with the second tracheae, the second tracheae plating far from one end of reaction kettle autoclave body
There is Teflon film.
Preferably, the reaction kettle autoclave body bottom is provided with the culture dish placed for adsorbent.
Preferably, the sealing ring outer wall is coated with Teflon film.
Compared with prior art, a kind of experiment porch of adsorbent research and development disclosed by the invention, experiment porch include
Reaction kettle autoclave body, the first tracheae and sealing device are connected with the first tracheae on reaction kettle autoclave body side wall, are arranged on the first tracheae
There is pressure vacuum gauge, the first tracheae is provided with valve far from one end of reaction kettle autoclave body, and the opening of reaction kettle autoclave body is provided with
Sealing device, the inner wall of reaction kettle autoclave body and bottom are coated with Teflon film, by first by the culture of reaction kettle autoclave body bottom
It is put into adsorbent in ware, then seals reaction kettle autoclave body with sealing device, insulating gas enters reaction kettle autoclave body from the first tracheae, absolutely
Edge gas observes the atmospheric pressure value of pressure vacuum gauge by adsorbent, and control valve makes to control the intake velocity of insulating gas
The adsorbent of insulating gas can be screened by obtaining experiment porch.
By plating Teflon film in reaction kettle inner wall of kettle and bottom, so that the insulating gas being filled in kettle will not be interior
Wall is adsorbed or is reacted with inner wall, and the decomposition product for also avoiding being filled with the insulating gas in kettle is reacted with inner wall of kettle, shadow
Ring the accuracy of experimental result.
Since the sealing cover on reaction kettle is made using organic glass, so that the pattern of the adsorbent in reaction kettle can
With directly observed.
Due to being provided with pressure vacuum gauge on the first tracheae, so that the variation of reaction kettle air pressure inside is directly by vacuum pressure
The registration of table shows.
Since the first tracheae outer wall is provided with sealing shroud close to reaction kettle autoclave body end, sealing shroud is outside reaction kettle autoclave body
Wall, the first tracheae are plugged in sealing shroud, so that the air-tightness of whole device is more preferable.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the experiment porch of adsorbent research and development in the embodiment of the present invention.
It illustrates:
1, steel ring；2, sealing cover；3, sealing ring；4, reaction kettle autoclave body；5, inner wall；6, through-hole；7, sealing shroud；8, vacuum pressure
Power table；9, valve；10, screw；11, the second tracheae；12, the first tracheae；13, shell.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
As shown in Figure 1, a kind of experiment porch of adsorbent research and development, experiment porch includes reaction kettle autoclave body 4, the first gas
Pipe 12 and sealing device, reaction kettle is hollow cylindrical body in the present embodiment, and reaction kettle includes reaction kettle autoclave body 4 and shell
13, the first tracheae 12 passes through shell 13 and is connected to 4 side wall of reaction kettle autoclave body, and pressure vacuum gauge 8 is connected on the first tracheae 12, the
One tracheae 12 is connected with valve 9 far from one end of reaction kettle autoclave body 4, and the opening of reaction kettle autoclave body 4 is removably connected with sealing
Device, the inner wall 5 of reaction kettle autoclave body 4 and 4 bottom of reaction kettle autoclave body are coated with Teflon film, reaction kettle inner wall in the present embodiment
5 and bottom plating Teflon film be 2mm.
Sealing device includes sealing cover 2 in the present embodiment, and sealing cover 2 is detachably connected with 4 open end of reaction kettle autoclave body, close
Capping 2 is in the same size with the open end of reaction kettle autoclave body 4, and sealing cover 2 uses organic glass, and sealing cover 2 is cylindrical body, and thick
3cm, steel ring 1 is connected on sealing cover 2, and steel ring 1 uses stainless steel material, 1 thickness 1cm of stainless steel steel ring；Sealing cover 2 and steel ring 1
Circumferential direction along sealing cover 2 is provided with eight evenly distributed through-holes 6, and not tapping, and 4 opening of reaction kettle autoclave body is provided with eight certainly
Emptying aperture, and tapping are attacked, through-hole 6 and self tapping empty position correspond；4 opening of reaction kettle autoclave body is provided with and autoclave body inner diameter size one
The arc groove of cause, arc groove are located at the inside in self tapping hole, and sealing ring 3 is placed in arc groove, and sealing ring 3 is matched with arc groove size
And the depth of arc groove is identical as the cross sectional radius of sealing ring 3, the outer wall of sealing ring 3 is coated with Teflon film, and reaction kettle passes through
Butterfly screws 10 successively compress steel ring 1, sealing cover 2, sealing ring 3 and reaction kettle, are formed and are sealed to reaction kettle.
A round hole is provided in the middle part of 4 side wall of reaction kettle autoclave body, the diameter of round hole is 3cm, is embedded in round hole close
The internal diameter of big envelope 7, sealing shroud 7 is identical in the outer diameter size of the first tracheae 12, and the first tracheae 12 is plugged in sealing shroud 7, vacuum pressure
Power table 8 is located between valve 9 and the sealing shroud 7 for connecting autoclave body, and tracheae is plugged in the second tracheae 11 far from one end of reaction kettle body,
Second tracheae 11 is coated with Teflon film, and the second tracheae 11 is connected with gas cylinder or vacuum pump.
The broad understanding of reaction kettle has the rustless steel container physically or chemically reacted, according to different process conditions demands
The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards,
To realize the mixture response function of heating, evaporation that technique requires, cooling and low high speed.Pressure vessel must comply with GB150 (steel
Pressing pressure container) standard.The pressure requirements in reaction process are not also identical to the design requirement of container therewith.Production must be tight
Lattice are processed, detected according to corresponding standard and trial operation.Stainless steel cauldron according to different production technologies, operating condition not
Identical, the design structure and parameter of reaction kettle are different, i.e. the structural style of reaction kettle is different, belong to nonstandard tankage.
It is poly- that Teflon film is also referred to as polytetrafluoroethylene film, be by suspension polytetrafluoroethylene resin through molding, sintering,
It is cooled to blank, then is made by turning and rolling.
The culture dish for being placed with adsorbent is put in the bottom of reaction kettle autoclave body 4, successively by sealing cover 2 and stainless steel coil 1
It is placed on 4 opening of reaction kettle autoclave body, then tightens butterfly screws 10, after washing kettle by tracheae multi-time inflating, will be reacted with vacuum pump
Kettle is evacuated to vacuum, and the insulating gas of required absorption is filled with reaction kettle autoclave body 4 by gas tube orifice, is seen according to pressure vacuum gauge 8
The air pressure inside for examining detection reaction kettle controls the speed of air inlet by the valve 9 connecting with pressure vacuum gauge 8, through sealing cover 2
Reaction in observing response kettle.
Since the air pressure of gas insulated combined electrical equipment (GIS) inner inflatable is mostly in 0.3Mpa~0.5Mpa, gas-insulated ring
Net cabinet inner gas pressure is less than 0.15Mpa mostly, sealing device, reaction kettle autoclave body 4 and bottom, tracheae on reaction kettle autoclave body 4
The device of the sealing of composition can bear the gas pressure from vacuum to 0.8Mpa.
By being coated with Teflon film in the inner wall 5 of reaction kettle autoclave body 4 and bottom, so that the insulating gas being filled in kettle is not
It can be adsorbed or reacted with inner wall 5 by inner wall 5, also avoid being filled with the decomposition product and inner wall of kettle of the insulating gas in kettle
5 reactions, influence the accuracy of experimental result, thus the adsorbent that experiment porch can preferably to insulating gas and its decomposition product
It is screened.
Since the sealing cover 2 on reaction kettle autoclave body 4 is made using organic glass, so that the adsorbent in reaction kettle
Pattern can be directly observed.
Due to being provided with pressure vacuum gauge 8 on the first tracheae 12, so that the variation of reaction kettle air pressure inside is directly by vacuum
The registration of pressure gauge 8 shows.
Since 12 outer wall of the first tracheae is provided with sealing shroud 7 close to 4 end of reaction kettle autoclave body, sealing shroud 7 is embedded in reaction kettle kettle
4 outer wall of body, the first tracheae 12 is plugged in sealing shroud 7, so that the air-tightness of whole device is more preferable.
Due to being coated with Teflon film on sealing ring 3, sealing ring 3 can not only make reaction kettle autoclave body 4 send out better tightness,
And it is also prevented from the insulating gas being filled in reaction kettle autoclave body 4 and reacts with sealing ring 3.
Since the first tracheae 12 is plugged with the second tracheae 11, convenient for the pumping and inflation in reaction kettle.
The above is a preferred embodiment of the present invention, it is noted that for those skilled in the art
For, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also considered as
Protection scope of the present invention.
Claims (10)
1. a kind of experiment porch of adsorbent research and development, which is characterized in that the experiment porch include reaction kettle autoclave body (4),
First tracheae (12) and sealing device are connected with the first tracheae (12) on reaction kettle autoclave body (4) side wall, first gas
It is provided with pressure vacuum gauge (8) on pipe (12), first tracheae (12) is provided with valve far from the one end of reaction kettle autoclave body (4)
(9), the opening of the reaction kettle autoclave body (4) is provided with sealing device, the inner wall (5) of the reaction kettle autoclave body (4) and anti-
The bottom of kettle autoclave body (4) is answered to be coated with Teflon film.
2. a kind of experiment porch of adsorbent research and development as described in claim 1, which is characterized in that the sealing device packet
It includes sealing cover (2), the sealing cover (2) is detachably connected with reaction kettle autoclave body (4) open end.
3. a kind of experiment porch of adsorbent research and development as described in claim 1, which is characterized in that first tracheae
(12) outer wall is provided with sealing shroud (7) close to reaction kettle autoclave body (4) end, and the sealing shroud (7) is embedded in reaction kettle autoclave body (4) outside
Wall, first tracheae (12) are plugged in sealing shroud (7).
4. a kind of experiment porch of adsorbent research and development as described in claim 1, which is characterized in that the reaction kettle autoclave body
(4) shell (13) are provided with outside.
5. a kind of experiment porch of adsorbent research and development as claimed in claim 2, which is characterized in that the sealing cover (2)
Several equally distributed through-holes (6) are provided with, the opening of the shell (13) is provided with opposite with the through-hole (6) of sealing cover (2)
The self tapping hole answered, the sealing cover (2) and reaction kettle autoclave body (4) are connected by screw (10).
6. a kind of experiment porch of adsorbent research and development as claimed in claim 2, which is characterized in that the reaction kettle autoclave body
(4) opening of shell (13), which is provided with, is located at the interior of self tapping hole with the consistent arc groove of autoclave body inner diameter size, the arc groove
Side is provided with sealing ring (3) in the arc groove.
7. a kind of experiment porch of adsorbent research and development as claimed in claim 2, which is characterized in that the sealing cover (2)
Using organic glass.
8. a kind of experiment porch of adsorbent research and development as described in claim 1, which is characterized in that first tracheae
(12) one end far from reaction kettle autoclave body (4) is plugged with the second tracheae (11), and second tracheae (11) is coated with Teflon film.
9. a kind of experiment porch of adsorbent research and development as described in claim 1, which is characterized in that the reaction kettle autoclave body
(4) bottom is provided with the culture dish placed for adsorbent.
10. a kind of experiment porch of adsorbent research and development as claimed in claim 5, which is characterized in that the sealing ring (3)
Outer wall is coated with Teflon film.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811087813.3A CN108993345A (en) | 2018-09-18 | 2018-09-18 | A kind of experiment porch of adsorbent research and development |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811087813.3A CN108993345A (en) | 2018-09-18 | 2018-09-18 | A kind of experiment porch of adsorbent research and development |
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| CN108993345A true CN108993345A (en) | 2018-12-14 |
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| CN201811087813.3A Pending CN108993345A (en) | 2018-09-18 | 2018-09-18 | A kind of experiment porch of adsorbent research and development |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111195504A (en) * | 2020-01-21 | 2020-05-26 | 国网重庆市电力公司检修分公司 | Environment-friendly insulating gas photo-thermal combined reaction experimental device |
| CN111638433A (en) * | 2020-06-10 | 2020-09-08 | 广西电网有限责任公司电力科学研究院 | Experimental equipment and method for partial discharge decomposition of insulating silicone oil with adjustable environmental humidity |
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| CN206215175U (en) * | 2016-11-11 | 2017-06-06 | 浙江科技学院 | A kind of autoclave |
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