CN108969405A - A kind of preparation method of stable stateization powder plant grease used for cosmetic - Google Patents
A kind of preparation method of stable stateization powder plant grease used for cosmetic Download PDFInfo
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- CN108969405A CN108969405A CN201810749290.8A CN201810749290A CN108969405A CN 108969405 A CN108969405 A CN 108969405A CN 201810749290 A CN201810749290 A CN 201810749290A CN 108969405 A CN108969405 A CN 108969405A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a kind of preparation methods of stable stateization powder plant grease used for cosmetic；This method is first configured to buffer with disodium hydrogen phosphate and sodium dihydrogen phosphate, and by starch buffer at starch milk, boiling water bath gelatinization cools down, and isoamylase enzymatic hydrolysis, enzyme deactivation obtains enzymolysis liquid；Enzymolysis liquid is uniformly mixed with vegetable oil, 55~65 DEG C of stirring in water bath reactions are cooled to room temperature, core material；Emulsified starch is uniformly mixed with maltodextrin and is configured to solution, stirring and dissolving stands defoaming, and wall material solution is made；Core material is mixed with wall material, thick lotion is made in high speed shear；After thick lotion homogeneous, stable stateization powder plant grease used for cosmetic is made in spray drying.Vegetable oil powdered oil stability produced by the present invention is strong, with it is simple using vegetable oil compared with core material, storage-stable improve 30% or so, shelf life can be greatly prolonged, expand vegetable oil used for cosmetic application effect benefit.
Description
Technical field
The present invention relates to filed of daily-use chemical industry, relate in particular to the preparation method of powder plant grease used for cosmetic.
Background technique
Grease crop base starting material occupies larger specific gravity in cosmetics, plays various effects, such as: shea butter can promote
Into reepithelialization, skin-nourishing is assigned；Grape seed oil is rich in vitamin E, has stronger inoxidizability；Coconut oil is available
In anti-aging etc..However, it is apt to deteriorate in processing, transport, storage process.The grease to have gone bad can generate bad smell,
Product sensory quality is influenced, or even generates the peroxide and free radical being harmful to the human body.How grease and its product oxygen are reduced
Change, promote product quality, Shelf-life increasingly with realistic meaning.
Powdered oil is that grease droplet is embedded in the film forming such as carbohydrate, protein using food micro capsule technology
In the good material of property, formulated food additive, manufactured solid powder product.Powdered oil is with stability is good, can grasp
The features such as property made is strong, convenient for storage and transport, has been widely used in the food such as dairy products, dispensed food for baby, cake, but
It is also uncommon in the application of filed of daily-use chemical industry.But powdered oil product currently on the market is low in the prevalence of embedding rate, steady
The features such as qualitative poor, mobility is bad, develop stability is strong, quality is high powdered oil used for cosmetic have it is highly important
Realistic meaning.
Summary of the invention
It is of the existing technology the purpose of the present invention is being to overcome the problems, such as, with simple using vegetable oil as core material phase
Than providing a kind of storage-stable and improving 27% or more, extend good used for cosmetic of stability of shelf life by a relatively large margin
The preparation method of powder plant grease.
It is a discovery of the invention that D- glucopyranose is a kind of straight chain spiral shell by the amylose that α-Isosorbide-5-Nitrae glucosides key connection is got up
Shape molecule is revolved, it can form weekly the spiral inclusion compound of 6~8 glucose residues with guest molecule；Starch is configured to form sediment
Powder cream and after being digested with isoamylase, enzymolysis liquid is uniformly mixed with vegetable oil, 55~65 DEG C of stirring in water bath are reacted, and room is cooled to
Temperature obtains starch enzymolysis liquid/vegetable oil mixt core material, and in the core material, the amylose of straight chain helical molecular is by grease
It is wrapped in cavity, while outer layer is wrapped up with wall material again, so that the chance that grease is contacted with external environment greatly reduces, significantly mentions
The embedding rate of vegetable oil is risen, the speed of product oxidation deterioration substantially reduces.At present using starch enzymolysis liquid as a part of core material
The method for preparing powdered oil has not been reported.The addition of starch enzymolysis liquid may greatly improve the stability of powdered oil.
The object of the invention is achieved through the following technical solutions:
As shown in Figure 1, a kind of preparation method of stable stateization powder plant grease used for cosmetic, includes the following steps:
1) buffer of pH value 5.0~7.0 is configured to disodium hydrogen phosphate and sodium dihydrogen phosphate, respectively using g and mL as
Quality and volume unit, the starch milk for being 10%~15% at mass volume ratio by starch buffer, boiling water bath gelatinization,
Cool down, digest 3~5h with the isoamylase of 10~30U/g dried starch under the conditions of 40~60 DEG C, enzyme deactivation obtains enzymolysis liquid；
2) enzymolysis liquid is uniformly mixed with vegetable oil 2~4:1 in mass ratio, 55~65 DEG C of stirring in water bath reactions are cooled to
Room temperature obtains starch enzymolysis liquid/vegetable oil mixt, as core material；
3) respectively using g and mL as quality and volume unit, emulsified starch and maltodextrin 3:4~6 in mass ratio are mixed
It is configured to the solution that mass volume ratio is 30%~50% with distilled water after closing uniformly, stirring and dissolving stands defoaming, and wall material is made
Solution；
4) volume ratio of core material and wall material 1:3~5 by volume is mixed, thick lotion is made in high speed shear；
5) by after thick lotion homogeneous, stable stateization powder plant grease used for cosmetic is made in spray drying.
To further realize the object of the invention, it is preferable that starch described in step 1) is cornstarch, waxy corn shallow lake
One of powder, wheaten starch, potato starch, tapioca and starch from sweet potato are a variety of.
Preferably, vegetable oil described in step 2) is SIMMONDSIA CHINENSIS SEED OIL, shea butter, coconut oil, grape seed oil, galam butter
With one of apricot kernel oil or a variety of.
Preferably, emulsified starch described in step 3) and maltodextrin belong to food-grade.
Preferably, the time of the gelatinization of boiling water bath described in step 1) is 0.5~1.5h；The enzyme deactivation is gone out using boiling water bath
Enzyme.
Preferably, the time of the reaction of 55~65 DEG C of stirring in water bath described in step 2) is 1.5~2.5h.
Preferably, stirring and dissolving described in step 3) is carried out under the conditions of 50~70 DEG C of temperature.
Preferably, the defoaming of standing described in step 3) is to carry out at room temperature.
Preferably, high-pressure homogeneous described in step 3) carried out on high pressure homogenizer, and pressure is 60~100MPa.
Preferably, the revolving speed of high speed shear described in step 4) is 10000-20000rpm.
Compared with prior art, the invention has the advantages that
The present invention is using starch enzymolysis liquid/vegetable oil mixt as core material, the existence form of oily phase are as follows: amylose/plant
Object oil inclusion compound and the vegetable oil not included, wherein the vegetable oil not included can be emulsified starch emulsification again, product is stablized
Property greatly improves.With it is simple using vegetable oil as core material compared with, the storage-stable of powdered oil produced by the present invention improves
30% or so, shelf life can be greatly prolonged, the application mode of vegetable oil used for cosmetic is expanded, there is important social benefit
And economic benefit.
Detailed description of the invention
Attached drawing 1 is the process flow chart of stable stateization powder plant oil and fat preparation used for cosmetic.
Attached drawing 2 is the scanning electron microscope (SEM) photograph of the powdered oil of embodiment 1.
Specific embodiment
For the present invention there are many successful embodiment, following embodiment is only to illustrate the present invention, and not makees to the present invention
Limitation in any form.Any simple modification made based on technical spirit of the invention, part replacement, equivalent variations
Deng being intended to be within the scope of the claims of the invention.
Emulsified starch (CAPSUL) is purchased from suitable Ruian food ingredient Co., Ltd, maltodextrin (DE15~20) in embodiment
Purchased from Shandong Xiwang Sugar Co., Ltd.
Embodiment 1
The preparation method of stable stateization powder plant grease used for cosmetic, the specific steps are as follows:
(1) it is configured to the buffer of pH value 6.0 with disodium hydrogen phosphate and sodium dihydrogen phosphate, cornstarch buffer is matched
The starch milk of 10% (g/mL, w/v) is made, boiling water bath is gelatinized 0.5h, cools down, and the different shallow lake of 10U/g dried starch is used under the conditions of 40 DEG C
Powder enzyme (08124-5MU, Sigma-aldrich) digests 3h, and boiling water bath enzyme deactivation obtains cornstarch enzymolysis liquid.
(2) appropriate SIMMONDSIA CHINENSIS SEED OIL is weighed, enzymolysis liquid is uniformly mixed with SIMMONDSIA CHINENSIS SEED OIL 3:1 in mass ratio, 55 DEG C of water-baths are stirred
Reaction 1.5h is mixed, is slowly cooled to room temperature, cornstarch enzymolysis liquid/SIMMONDSIA CHINENSIS SEED OIL mixture is obtained, as core material.
(3) emulsified starch is uniformly mixed with maltodextrin 3:5 in mass ratio, being configured to concentration with distilled water is 30%
The solution of (g/mL, w/v), the stirring and dissolving at 50 DEG C, it is to be dissolved completely after, at room temperature stand defoaming, be made wall material solution.
(4) ratio of core material and wall material 1:3 by volume are mixed, thick lotion is made with high-speed shearing machine, and (revolving speed is
15000rpm)。
(5) with high pressure homogenizer by thick lotion after homogeneous under 60MPa, spray drying, be made SIMMONDSIA CHINENSIS SEED OIL powdered oil,
It is denoted as experimental group.
Meanwhile one group of production is free of cornstarch enzymolysis liquid, only using equivalent SIMMONDSIA CHINENSIS SEED OIL as the powdered oil of core material,
Its same the present embodiment, as a control group.
Product obtained is white powder through the invention, and powder micromorphology and size are shown in Fig. 2, are put into 65 DEG C of baking ovens and add
After speed oxidation 30d, control group peroxide value is 10.16meq/kg, and experimental group peroxide value is 7.39meq/kg, with control group phase
Than storage-stable improves 27.26%.The present embodiment product storage-stable significantly improves compared with the control group, it may be possible to
Because grease is wrapped in cavity by the amylose in cornstarch enzymolysis liquid first, outer layer is wrapped up with wall material again, so that oily
The chance that rouge is contacted with external environment greatly reduces, and the speed of product oxidation deterioration substantially reduces.
The storage-stable of powder plant grease used for cosmetic is measured with the following method:
The powdered oil of spray drying preparation is equably layered on conical flask bottom, progress grease in 65 DEG C of insulating boxs is put into and adds
Fast oxidation test surveys a peroxide value (POV) every 5d.Storage-stable increase rate is calculated according to following formula:
The measurement of peroxide value: referring to national standard GB/T 5538-2005 " animal and plant fat determination of POV ".
Embodiment 2
The preparation method of stable stateization powder plant grease used for cosmetic, the specific steps are as follows:
(1) it is configured to the buffer of pH value 7.0 with disodium hydrogen phosphate and sodium dihydrogen phosphate, waxy corn starch is buffered
Liquid is configured to the starch milk of 11% (g/mL, w/v), and boiling water bath is gelatinized 1h, cools down, and the different of 15U/g dried starch is used under the conditions of 50 DEG C
Amylase enzymolysis 4h, boiling water bath enzyme deactivation obtain waxy corn starch enzymolysis liquid.
(2) appropriate shea butter is weighed, enzymolysis liquid is uniformly mixed with shea butter 2:1 in mass ratio, 60 DEG C of water-baths are stirred
Reaction 2h is mixed, is slowly cooled to room temperature, waxy corn starch enzymolysis liquid/shea butter mixture is obtained, as core material.
(3) emulsified starch is uniformly mixed with maltodextrin 3:4 in mass ratio, being configured to concentration with distilled water is 35%
The solution of (g/mL, w/v), the stirring and dissolving at 55 DEG C, it is to be dissolved completely after, at room temperature stand defoaming, be made wall material solution.
(4) ratio of core material and wall material 1:4 by volume are mixed, thick lotion is made with high-speed shearing machine, and (revolving speed is
13000rpm)。
(5) with high pressure homogenizer by thick lotion after homogeneous under 80MPa, spray drying, be made shea butter powdered oil,
It is denoted as experimental group.
Meanwhile one group of production is free of waxy corn starch enzymolysis liquid, only using equivalent shea butter as the powder of core material oil
Rouge, other same the present embodiment, as a control group.
Product obtained is white powder through the invention, and powder micromorphology and size are close with embodiment 1, are put into 65
After DEG C baking oven accelerated oxidation 30d, control group peroxide value is 10.37meq/kg, and experimental group peroxide value is 7.42meq/kg, with
Control group is compared, and storage-stable improves 28.45%.
Embodiment 3
The preparation method of stable stateization powder plant grease used for cosmetic, the specific steps are as follows:
(1) it is configured to the buffer of pH value 5.0 with disodium hydrogen phosphate and sodium dihydrogen phosphate, wheaten starch buffer is matched
The starch milk of 12% (g/mL, w/v) is made, boiling water bath is gelatinized 1.5h, cools down, and the different shallow lake of 20U/g dried starch is used under the conditions of 60 DEG C
Powder enzyme digests 5h, and boiling water bath enzyme deactivation obtains wheaten starch enzymolysis liquid.
(2) appropriate coconut oil is weighed, enzymolysis liquid is uniformly mixed with coconut oil 4:1 in mass ratio, 65 DEG C of stirring in water bath are anti-
2.5h is answered, is slowly cooled to room temperature, wheaten starch enzymolysis liquid/coconut oil blend is obtained, as core material.
(3) emulsified starch is uniformly mixed with maltodextrin 3:6 in mass ratio, being configured to concentration with distilled water is 40%
The solution of (g/mL, w/v), the stirring and dissolving at 60 DEG C, it is to be dissolved completely after, at room temperature stand defoaming, be made wall material solution.
(4) ratio of core material and wall material 1:5 by volume are mixed, thick lotion is made with high-speed shearing machine, and (revolving speed is
10000rpm)。
(5) with high pressure homogenizer by thick lotion after homogeneous under 100MPa, spray drying, be made coconut oil powdered oil,
It is denoted as experimental group.
Meanwhile one group of production is free of wheaten starch enzymolysis liquid, it is other only using equivalent coconut oil as the powdered oil of core material
Same the present embodiment, as a control group.
Product obtained is white powder through the invention, and powder micromorphology is close with embodiment 1, and size is smaller, puts
After entering 65 DEG C of baking oven accelerated oxidation 30d, control group peroxide value is 10.71meq/kg, and experimental group peroxide value is 7.49meq/
Kg, compared with the control group, storage-stable improve 30.07%.
Embodiment 4
The preparation method of stable stateization powder plant grease used for cosmetic, the specific steps are as follows:
(1) buffer of pH value 5.0 is configured to disodium hydrogen phosphate and sodium dihydrogen phosphate, by potato starch buffer
It is configured to the starch milk of 14% (g/mL, w/v), boiling water bath is gelatinized 0.5h, cools down, and the different of 25U/g dried starch is used under the conditions of 40 DEG C
Amylase enzymolysis 4h, boiling water bath enzyme deactivation obtain potato starch enzymolysis liquid.
(2) appropriate grape seed oil is weighed, enzymolysis liquid is uniformly mixed with grape seed oil 2:1 in mass ratio, 65 DEG C of water-baths are stirred
Reaction 1.5h is mixed, is slowly cooled to room temperature, potato starch enzymolysis liquid/grape seed oil mixture is obtained, as core material.
(3) emulsified starch is uniformly mixed with maltodextrin 3:5 in mass ratio, being configured to concentration with distilled water is 45%
The solution of (g/mL, w/v), the stirring and dissolving at 65 DEG C, it is to be dissolved completely after, at room temperature stand defoaming, be made wall material solution.
(4) ratio of core material and wall material 1:4 by volume are mixed, thick lotion is made with high-speed shearing machine, and (revolving speed is
20000rpm)。
(5) with high pressure homogenizer by thick lotion after homogeneous under 90MPa, spray drying, be made grape seed oil powdered oil,
It is denoted as experimental group.
Meanwhile one group of production without potato starch enzymolysis liquid, only using equivalent grape seed oil as the powdered oil of core material,
Other same the present embodiment, as a control group.
Product obtained is white powder through the invention, and powder micromorphology and size are close with embodiment 1, are put into 65
After DEG C baking oven accelerated oxidation 30d, control group peroxide value is 10.54meq/kg, and experimental group peroxide value is 7.21meq/kg, with
Control group is compared, and storage-stable improves 31.59%.
Embodiment 5
The preparation method of stable stateization powder plant grease used for cosmetic, the specific steps are as follows:
(1) it is configured to the buffer of pH value 7.0 with disodium hydrogen phosphate and sodium dihydrogen phosphate, tapioca buffer is matched
The starch milk of 15% (g/mL, w/v) is made, boiling water bath is gelatinized 1.5h, cools down, and the different shallow lake of 30U/g dried starch is used under the conditions of 60 DEG C
Powder enzyme digests 5h, and boiling water bath enzyme deactivation obtains tapioca enzymolysis liquid.
(2) appropriate galam butter is weighed, enzymolysis liquid is uniformly mixed with galam butter 3:1 in mass ratio, 55 DEG C of water-baths are stirred
Reaction 2.5h is mixed, is slowly cooled to room temperature, tapioca enzymolysis liquid/galam butter mixture is obtained, as core material.
(3) emulsified starch is uniformly mixed with maltodextrin 3:6 in mass ratio, being configured to concentration with distilled water is 50%
The solution of (g/mL, w/v), the stirring and dissolving at 70 DEG C, it is to be dissolved completely after, at room temperature stand defoaming, be made wall material solution.
(4) ratio of core material and wall material 1:5 by volume are mixed, thick lotion is made with high-speed shearing machine, and (revolving speed is
10000rpm)。
(5) with high pressure homogenizer by thick lotion after homogeneous under 80MPa, spray drying, be made galam butter powdered oil,
It is denoted as experimental group.
Meanwhile one group of production without tapioca enzymolysis liquid, only using equivalent galam butter as the powdered oil of core material,
Its same the present embodiment, as a control group.
Product obtained is shallow green powder through the invention, and powder micromorphology is close with embodiment 1, and size is bigger,
After being put into 65 DEG C of baking oven accelerated oxidation 30d, control group peroxide value is 9.96meq/kg, and experimental group peroxide value is 7.11meq/
Kg, compared with the control group, storage-stable improve 28.61%.
Embodiment 6
The preparation method of stable stateization powder plant grease used for cosmetic, the specific steps are as follows:
(1) it is configured to the buffer of pH value 6.0 with disodium hydrogen phosphate and sodium dihydrogen phosphate, starch from sweet potato buffer is matched
The starch milk of 13% (g/mL, w/v) is made, boiling water bath is gelatinized 1h, cools down, and the different starch of 20U/g dried starch is used under the conditions of 50 DEG C
Enzyme digests 3h, and boiling water bath enzyme deactivation obtains starch from sweet potato enzymolysis liquid.
(2) appropriate apricot kernel oil is weighed, enzymolysis liquid is uniformly mixed with apricot kernel oil 4:1 in mass ratio, 60 DEG C of stirring in water bath are anti-
2h is answered, is slowly cooled to room temperature, starch from sweet potato enzymolysis liquid/almond oil mixture is obtained, as core material.
(3) emulsified starch is uniformly mixed with maltodextrin 3:4 in mass ratio, being configured to concentration with distilled water is 40%
The solution of (g/mL, w/v), the stirring and dissolving at 60 DEG C, it is to be dissolved completely after, at room temperature stand defoaming, be made wall material solution.
(4) ratio of core material and wall material 1:3 by volume are mixed, thick lotion is made with high-speed shearing machine, and (revolving speed is
15000rpm)。
(5) with high pressure homogenizer by thick lotion after homogeneous under 70MPa, spray drying, be made apricot kernel oil powdered oil, note
For experimental group.
Meanwhile one group of production is free of starch from sweet potato enzymolysis liquid, only using equivalent apricot kernel oil as the powdered oil of core material, it is other
Same the present embodiment, as a control group.
Product obtained is white powder through the invention, and powder micromorphology and size are close with embodiment 1, are put into 65
After DEG C baking oven accelerated oxidation 30d, control group peroxide value is 10.12meq/kg, and experimental group peroxide value is 7.13meq/kg, with
Control group is compared, and storage-stable improves 29.55%.
As described above, the present invention can be realized preferably.
Above embodiment just for the sake of clearly demonstrating examples made by the present invention is implemented to the present invention
The restriction of mode.For those of ordinary skill in the art, not similar shape can also be made on the basis of the above description
The variation or variation of formula.There is no necessity and possibility to exhaust all the enbodiments.It is all in the spirit and principles in the present invention
Within made any modifications, equivalent replacements, and improvements etc., be all contained within the scope of protection of the claims of the present invention.
Claims (10)
1. a kind of preparation method of stable stateization powder plant grease used for cosmetic, it is characterised in that include the following steps:
1) buffer of pH value 5.0~7.0 is configured to disodium hydrogen phosphate and sodium dihydrogen phosphate, respectively using g and mL as quality
And volume unit, the starch milk for being 10%~15% at mass volume ratio by starch buffer, boiling water bath gelatinization, drop
Temperature, digests 3~5h with the isoamylase of 10~30U/g dried starch under the conditions of 40~60 DEG C, and enzyme deactivation obtains enzymolysis liquid；
2) enzymolysis liquid being uniformly mixed with vegetable oil 2~4:1 in mass ratio, 55~65 DEG C of stirring in water bath reactions are cooled to room temperature,
Starch enzymolysis liquid/vegetable oil mixt is obtained, as core material；
3) respectively using g and mL as quality and volume unit, emulsified starch is mixed with maltodextrin 3:4~6 in mass ratio
It is configured to the solution that mass volume ratio is 30%~50% with distilled water after even, stirring and dissolving stands defoaming, and it is molten that wall material is made
Liquid；
4) volume ratio of core material and wall material 1:3~5 by volume is mixed, thick lotion is made in high speed shear；
5) by after thick lotion homogeneous, stable stateization powder plant grease used for cosmetic is made in spray drying.
2. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
1) starch described in is in cornstarch, waxy corn starch, wheaten starch, potato starch, tapioca and starch from sweet potato
It is one or more.
3. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
2) vegetable oil described in be one of SIMMONDSIA CHINENSIS SEED OIL, shea butter, coconut oil, grape seed oil, galam butter and apricot kernel oil or
It is a variety of.
4. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
3) emulsified starch and maltodextrin described in belong to food-grade.
5. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
1) time of the boiling water bath gelatinization described in is 0.5~1.5h；The enzyme deactivation uses boiling water bath enzyme deactivation.
6. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
2) time of 55~65 DEG C of stirring in water bath reaction described in is 1.5~2.5h.
7. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
3) stirring and dissolving described in is carried out under the conditions of 50~70 DEG C of temperature.
8. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
3) the standing defoaming described in is to carry out at room temperature.
9. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
3) high-pressure homogeneous described in is carried out on high pressure homogenizer, and pressure is 60~100MPa.
10. the preparation method of stable stateization powder plant grease used for cosmetic according to claim 1, it is characterised in that: step
It is rapid 4) described in high speed shear revolving speed be 10000-20000rpm.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022033524A1 (en) * | 2020-08-12 | 2022-02-17 | 华南理工大学 | Starch-based steady-state vegetable oil compound and preparation method therefor |
| CN116285014A (en) * | 2022-12-22 | 2023-06-23 | 佛山市国农淀粉有限公司 | Pregelatinized starch for liquid substance adsorption and preparation method and application thereof |
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| JP2000256135A (en) * | 1999-03-04 | 2000-09-19 | L'oreal Sa | Cosmetic composition in the form of powder containing specific ester |
| CN104961837A (en) * | 2015-06-30 | 2015-10-07 | 华南理工大学 | Preparation method of starch and fatty acid compound |
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| CN107418988A (en) * | 2017-08-31 | 2017-12-01 | 华南理工大学 | A kind of resistant starch and its preparation method and application |
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| WO2022033524A1 (en) * | 2020-08-12 | 2022-02-17 | 华南理工大学 | Starch-based steady-state vegetable oil compound and preparation method therefor |
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