CN108940155A - A kind of reaction kettle heating device and its heat-exchange system - Google Patents

A kind of reaction kettle heating device and its heat-exchange system Download PDF

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Publication number
CN108940155A
CN108940155A CN201811199454.0A CN201811199454A CN108940155A CN 108940155 A CN108940155 A CN 108940155A CN 201811199454 A CN201811199454 A CN 201811199454A CN 108940155 A CN108940155 A CN 108940155A
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China
Prior art keywords
heating
floating body
rotating ball
heat
reaction kettle
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Granted
Application number
CN201811199454.0A
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Chinese (zh)
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CN108940155B (en
Inventor
毛燕婷
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Quzhou Kefeng New Material Co ltd
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Individual
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23JREMOVAL OR TREATMENT OF COMBUSTION PRODUCTS OR COMBUSTION RESIDUES; FLUES 
    • F23J15/00Arrangements of devices for treating smoke or fumes
    • F23J15/06Arrangements of devices for treating smoke or fumes of coolers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/08Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being otherwise bent, e.g. in a serpentine or zig-zag
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085Plates; Jackets; Cylinders
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E20/00Combustion technologies with mitigation potential
    • Y02E20/30Technologies for a more efficient combustion or heat usage

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention is a kind of reaction kettle heating device and its heat-exchange system, including autoclave body, interlayer, agitating device, transmission device, motor, cylinder;It can be realized the heating of the targetedly partial region of fluid in autoclave body, it is unbalanced that domain of the existence is heated when solving the problems, such as due to solid-liquid, simultaneously by adjusting heating method, also it is able to achieve the unified heating of all areas, it can satisfy different heating needs, the setting of rotating ball can be realized the effect heated while agitating, overcome the shortcomings that conventional heating stirring carries out respectively, effect by fluid to rotating ball, it can be realized the disturbed flow type heating method of fluid, so that heat exchange is more abundant, the setting of the shape and direction of blade and flow-disturbing pawl enables to flow-disturbing more efficient.

Description

A kind of reaction kettle heating device and its heat-exchange system
Technical field
The present invention relates to reaction kettle device, specially a kind of reaction kettle heating device and its heat-exchange system.
Background technique
Reaction kettle is the conventional heating or cooling device applied to petrochemical process medium, in conventional reaction kettle Heating or cooling procedure use jacket type or other modes, and are directed to different material media, not due to its internal component Together, when liquid coexists admittedly, it is uneven to be commonly present heat exchange, thus it is excessively high to appear in temperatures at localized regions, and temperatures at localized regions It is not achieved the problem of needing, and conventional way is to be stirred to make it uniformly using agitating device, and existing agitating device Mode is single, and material can not be made to realize uniform flowing, and can not achieve different depth material and carry out specific aim mixed flow Temperature intervention, and realize that the mode of temperature adjustment is excessively single only by stirring, and stirring and heating is separated mistake Journey, since the temperature being heated or cooled has differences, thus, specific aim cannot expire the needs that a certain region is heated or cooled Foot, versatility is not strong, does not adapt to the needs of various different heatings or cooling.When fluid flows in kettle, it is limited to single Flowing means of intervention, usually can flow-disturbing it is ineffective, cause the process efficiency being heated or cooled not high, be not able to satisfy practical need It wants.
Summary of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of reaction kettle heating device and its heat-exchange system, Neng Gouke Take disadvantages mentioned above in the prior art.
A kind of reaction kettle heating device, including autoclave body, interlayer, agitating device, transmission device, motor, cylinder, heating kettle One layer interlayer of outside setting, heating kettle are internally provided with agitating device, agitating device include agitating shaft, lateral floating body, installation axle, One end of rotating ball, press holder, agitating shaft is connect with the motor of heating kettle tip exterior, and agitating shaft is vertically arranged at heating kettle In, agitating shaft is arranged radially multiple lateral floating bodies, is arranged fluted on agitating shaft, and one end of lateral floating body is provided with and groove pair The protrusion answered, groove and the protrusion of lateral floating body one end are connected together, so that lateral floating body can slide up and down in a groove, laterally Multiple installation axles are provided on floating body, installation axle is hollow shape, and installation axle one end connects lateral floating body, and the other end is in inside along circle One circle groove of setting in circumferential direction, one end of rotating ball are connected with raised connecting rod, and connecting rod and installation axle pass through protrusion Be connected together with groove, rotating ball enable to rotate along the circumferential direction of installation axle, be provided in rotating ball multiple arcs blade and Flow-disturbing pawl;The upper end of lateral floating body is provided with press holder, and press holder is hollow cylindrical, and internal diameter is greater than the outer of agitating shaft Diameter, the top of press holder are connected with telescopic rod, are arranged on the cylinder of heating kettle tip exterior at the top of telescopic rod.
Further, the material of rotating ball, arc shaped blade and flow-disturbing pawl is heat transfer material, and setting is empty in lateral floating body Chamber, fills heat-storing material in cavity, rotating ball be also it is hollow, the heat-storing material in floating body cavity passes through installation axle inner cavity and rotation Spherical cavity connection.
Further, lateral floating body, connecting shaft, heat-storing material, rotating ball material density be less than water density.
Further, the arc shaped blade of rotating ball is the distribution of multilayer petal-shaped, and blade tip is tip-shape, medial surface shape For the arcuation first expanded outwardly along bottom to top, the arcuation of after-contraction, arc shaped blade of the tip towards rear side.
Further, the flow-disturbing pawl of rotating ball is arranged between arc shaped blade, and flow-disturbing pawl is arc, and the wide top in bottom is sharp, The arc tip direction of flow-disturbing pawl between the arc shaped blade of front and back is opposite with arc shaped blade tip direction.
Further, press holder and lateral floating body upper-end contact position are provided with the slide plate for being conducive to opposite sliding.
Further, a kind of heat-exchange system, including reaction kettle heating device as described above further include economizer, heat dissipation Device, cooling device;The interlayer fluid outlet of reaction kettle heating device is connect with economizer fluid hose import, economizer fluid outlet Connect with radiator medium entrance, radiator media outlet is connect with cooling device medium entrance, cooling device media outlet with The connection of interlayer fluid inlet.
Further, heat-exchange system further includes by-pass line, triple valve, and by-pass line is connected to heat dissipation by triple valve one end The import of device, the other end are connected between interlayer import and the outlet of cooler.
Further, by cooling layer connection, there are two support legs for the lower part of heating kettle, on the ground by support leg support.
Beneficial effects of the present invention:
Reaction kettle heating device of the invention can be realized the heating of the targetedly partial region of fluid in autoclave body, solve by Domain of the existence unbalanced problem is heated when solid-liquid, while by adjusting heating method, being also able to achieve all areas Unified heating, can satisfy different heating needs;
The setting of rotating ball can be realized the effect heated while agitating, overcome what conventional heating stirring carried out respectively Disadvantage;
Effect by fluid to rotating ball can be realized the disturbed flow type heating method of fluid so that heat exchange it is more abundant, blade and The shape of flow-disturbing pawl and the setting of direction enable to flow-disturbing more efficient;
In heat-exchange system, using sandwich-type heating is carried out after the flue gas waste heat for heat exchange of economizer, the energy is saved, heat is sufficiently provided Source.The setting of bypass line triple valve can freely control switching and autoclave body mode is heated or cooled, and technique is more convenient.
Detailed description of the invention
Fig. 1 is main structure schematic diagram of the present invention.
Fig. 2 is the lateral float structure schematic diagram of the present invention.
Fig. 3 is agitating shaft schematic diagram of the present invention.
Fig. 4 is rotating ball schematic diagram of the present invention.
Fig. 5 is flow-disturbing pawl schematic diagram of the present invention.
In figure: 1- autoclave body, 2- interlayer, 3- motor, 4- cylinder, 5- agitating shaft, 6- telescopic rod, 7- economizer, 8- radiator, 9- cooling device, 10- transverse direction floating body, 11- press holder, 12- installation axle, 13- rotating ball, 14- arc shaped blade, 15- heat-dissipating pipe, 16- flow-disturbing pawl, 17- triple valve, 18- bypass, 19- connecting rod.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
A kind of reaction kettle heating device, including heating kettle 1, interlayer 2, agitating device, transmission device, motor 3, cylinder 4 add A layer interlayer 2 is arranged in the external of hot kettle 1, and heating kettle 1 is internally provided with agitating device, and agitating device includes agitating shaft 5, laterally floats One end of body 10, installation axle 12, rotating ball 13, press holder 11, agitating shaft 5 is connect with the motor 3 of 1 tip exterior of heating kettle, Agitating shaft 5 is vertically arranged in heating kettle 1, and agitating shaft 5 is arranged radially multiple lateral floating bodies 10, be arranged on agitating shaft 5 it is fluted, One end of lateral floating body 10 is provided with protrusion corresponding with groove, and groove and the protrusion of 10 one end of lateral floating body are connected together, make Obtaining lateral floating body can slide up and down in a groove, and multiple installation axles 12 are provided on lateral floating body 10, and installation axle 12 is hollow shape, 12 one end of installation axle connects lateral floating body 10, and the other end is in internal along the circumferential direction upper one circle groove of setting, and the one of rotating ball 13 End is connected with raised connecting rod 19, and connecting rod 19 is connected together with installation axle 12 by protrusion and groove, makes rotating ball 13 It can be rotated along the circumferential direction of installation axle 12, multiple arcs blade 14 and flow-disturbing pawl 16 are provided in rotating ball 13;Lateral floating body 10 upper end is provided with press holder 11, and press holder 11 is hollow cylindrical, and internal diameter is greater than the outer diameter of agitating shaft 5, pressure holding dress The top for setting 11 is connected with telescopic rod, is arranged on the cylinder 4 of heating kettle tip exterior at the top of telescopic rod;Rotating ball 13, arc The material of shape blade 14 and flow-disturbing pawl 16 is heat transfer material, and cavity is arranged in lateral floating body, fills heat-storing material in cavity, turns Dynamic ball 13 be also it is hollow, the heat-storing material in floating body cavity is connected to by 12 inner cavity of installation axle with spherical cavity is rotated, lateral floating body 10, Connecting rod 19, heat-storing material, rotating ball material density be less than the density of water, the arc shaped blade 14 of rotating ball 13 is multilayer petal Shape distribution, 14 top of blade be it is tip-shape, medial surface shape is the arcuation first expanded outwardly along bottom to top, the arc of after-contraction Shape, tip is towards the arc shaped blade of rear side, and between arc shaped blade 14, flow-disturbing pawl 16 is for the setting of flow-disturbing pawl 16 of rotating ball 13 Arc, the wide top in bottom point, the arc tip of the flow-disturbing pawl between the arc shaped blade of front and back towards with arc shaped blade tip towards phase Instead, press holder 11 and 10 upper-end contact position of lateral floating body are provided with the slide plate for being conducive to opposite sliding;A kind of heat-exchange system, packet Reaction kettle heating device as described above is included, further includes economizer 7, radiator 8, cooling device 9;The folder of reaction kettle heating device 2 fluid outlet of layer are connect with 7 fluid hose import of economizer, and 7 fluid outlet of economizer is connect with 8 medium entrance of radiator, heat dissipation 8 media outlet of device is connect with 9 medium entrance of cooling device, and 9 media outlet of cooling device is connect with 2 fluid inlet of interlayer, heat exchange System further includes by-pass line 18, triple valve 17, and by-pass line 18 is connected to the import of radiator 8 by 17 one end of triple valve, The other end is connected between interlayer import and the outlet of cooler, and by cooling layer connection, there are two supports for the lower part of heating kettle Foot, on the ground by support leg support.
The course of work of the invention are as follows: under heating mode, starting cylinder can push telescopic rod to move up and down press holder, It can be slided up and down in slot to press lateral floating body, starting cylinder extends constrictor, so that press contacts under press holder Lateral floating body after reaching specified mixing position, is closed cylinder, is opened so that lateral floating body is moved down along vertical agitating shaft Motor drives agitating shaft rotation, so that lateral floating body is driven to rotate around agitating shaft, the position that press holder is contacted with lateral floating body The slide plate for being equipped with and being conducive to opposite sliding material is installed, can make it that can be freely rotated under press holder pressure, on lateral floating body Rotating ball due to arc shaped blade and flow-disturbing pawl, in kettle under the action of media flow, around installation axle rotate, thus to range Interior liquid carries out further flow-disturbing agitation and heating;When needing to carry out heating stirring for different height or layer, it is only necessary to adjust The telescopic height of press holder is to realize.Under heating mode, interlayer is heating liquid, and triple valve is by by-path turn-on, fluid at this time Without radiator and cooler, medium in interlayer heating kettle is directly reached after being heated in economizer.
In addition, control heating and agitation mode can also according to be evenly heated or specific aim heating carry out adjust Whole, when such as needing to be evenly heated, adjustable cylinder was depressed and is lifted according to certain intermittent time, controlled press holder pressure When lower, floating body is pressed into bottommost, and then cylinder is withdrawn, and floating body floats by buoyancy, in the process can be to vertical direction On different height fluid all carry out disturbance formula heating stirring, floating body reaches top exhaust hood and repeats to push, and circulation carries out.
After reaching heating temperature, medium exports kettle chamber in kettle, and autoclave body temperature is higher at this time, further to drop to it Temperature can control triple valve connection radiator and cooler to become cold at this point, fluid reaches interlayer by radiator and cooler But medium cools down to kettle chamber.Both of which is controlled by triple valve and is converted.

Claims (9)

1. a kind of reaction kettle heating device, including heating kettle, interlayer, agitating device, transmission device, motor, cylinder, heating kettle One layer interlayer of outside setting, heating kettle are internally provided with agitating device, agitating device include agitating shaft, lateral floating body, installation axle, One end of rotating ball, press holder, agitating shaft is connect with the motor of heating kettle tip exterior, and agitating shaft is vertically arranged at heating kettle In, agitating shaft is arranged radially multiple lateral floating bodies, is arranged fluted on agitating shaft, and one end of lateral floating body is provided with and groove pair The protrusion answered, groove and the protrusion of lateral floating body one end are connected together, so that lateral floating body can slide up and down in a groove, laterally Multiple installation axles are provided on floating body, installation axle is hollow shape, and installation axle one end connects lateral floating body, and the other end is in inside along circle One circle groove of setting in circumferential direction, one end of rotating ball are connected with raised connecting rod, and connecting rod and installation axle pass through protrusion Be connected together with groove, rotating ball enable to rotate along the circumferential direction of installation axle, be provided in rotating ball multiple arcs blade and Flow-disturbing pawl;The upper end of lateral floating body is provided with press holder, and press holder is hollow cylindrical, and internal diameter is greater than the outer of agitating shaft Diameter, the top of press holder are connected with telescopic rod, are arranged on the cylinder of heating kettle tip exterior at the top of telescopic rod.
2. a kind of reaction kettle heating device according to claim 1, it is characterised in that: rotating ball, arc shaped blade and flow-disturbing The material of pawl is heat transfer material, and cavity is arranged in lateral floating body, fills heat-storing material in cavity, rotating ball be also it is hollow, float Heat-storing material in body cavity is connected to by installation axle inner cavity with rotation spherical cavity.
3. a kind of reaction kettle heating device according to claim 1, lateral floating body, connecting shaft, heat-storing material, rotating ball material The density of matter is less than the density of water.
4. a kind of reaction kettle heating device according to claim 1, the arc shaped blade of rotating ball is the distribution of multilayer petal-shaped, Blade tip be it is tip-shape, medial surface shape is the arcuation first expanded outwardly along bottom to top, the arcuation of after-contraction, tip court To the arc shaped blade of rear side.
5. the flow-disturbing pawl of a kind of reaction kettle heating device according to claim 1, rotating ball is arranged between arc shaped blade, Flow-disturbing pawl is arc, and the wide top in bottom is sharp, the arc tip direction and arc shaped blade point of the flow-disturbing pawl between the arc shaped blade of front and back End is towards on the contrary.
6. a kind of reaction kettle heating device according to claim 1, press holder is set with lateral floating body upper-end contact position It is equipped with the slide plate for being conducive to opposite sliding.
7. a kind of heat-exchange system, including reaction kettle heating device described in any one of claims 1-6 further include economizer, dissipate Hot device, cooling device;The interlayer fluid outlet of reaction kettle heating device is connect with economizer fluid hose import, and economizer fluid goes out Mouth is connect with radiator medium entrance, and radiator media outlet is connect with cooling device medium entrance, cooling device media outlet It is connect with interlayer fluid inlet.
It further include by-pass line 8. a kind of heat-exchange system according to claim 7, triple valve, by-pass line passes through threeway Valve one end is connected to the import of radiator, and the other end is connected between interlayer import and the outlet of cooler.
9. a kind of heat-exchange system according to claim 8, by cooling layer connection, there are two supports for the heating kettle lower part Foot, on the ground by support leg support.
CN201811199454.0A 2018-10-16 2018-10-16 Reation kettle heating device and heat transfer system thereof Active CN108940155B (en)

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Application Number Priority Date Filing Date Title
CN201811199454.0A CN108940155B (en) 2018-10-16 2018-10-16 Reation kettle heating device and heat transfer system thereof

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CN108940155B CN108940155B (en) 2019-12-31

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111006530A (en) * 2019-11-18 2020-04-14 榆林学院 Heat exchanger device and heat exchange system for inner component of crescent fan
CN113618993A (en) * 2021-08-10 2021-11-09 黄山菲英汽车零部件有限公司 Manufacturing process of drum type friction plate for water passing tank vehicle
CN114623723A (en) * 2022-02-28 2022-06-14 呼伦贝尔安泰热电有限责任公司满洲里热电厂 Head convenient to dismantle
CN114688909A (en) * 2022-02-28 2022-07-01 呼伦贝尔安泰热电有限责任公司满洲里热电厂 Heating network heater
CN115430390A (en) * 2022-11-09 2022-12-06 山东法拉第氘源科技有限公司 Processing and preparation device and processing and preparation method of deuterated bromobenzene

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DE102007004925B3 (en) * 2007-02-01 2008-04-03 Christian-Albrechts-Universität Zu Kiel Mixing container for mixing liquid materials in analytical chemistry comprises a rod arranged on the lower side of the container and rotating on the container using a ball joint and a weight arranged on both sides of the ball joint
CN204891848U (en) * 2015-08-27 2015-12-23 浙江华洲药业有限公司 Reaction still is opened to red copper
CN205499907U (en) * 2016-03-31 2016-08-24 天孚控股集团有限公司 Glue pot preventing surface layer from becoming dry and crusted
CN207774829U (en) * 2018-01-24 2018-08-28 云南酉兑科技有限公司 A kind of ice crystal synth sink
CN108514829A (en) * 2018-03-21 2018-09-11 林巧鸿 Coating machine slurry device

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Publication number Priority date Publication date Assignee Title
DE102007004925B3 (en) * 2007-02-01 2008-04-03 Christian-Albrechts-Universität Zu Kiel Mixing container for mixing liquid materials in analytical chemistry comprises a rod arranged on the lower side of the container and rotating on the container using a ball joint and a weight arranged on both sides of the ball joint
CN204891848U (en) * 2015-08-27 2015-12-23 浙江华洲药业有限公司 Reaction still is opened to red copper
CN205499907U (en) * 2016-03-31 2016-08-24 天孚控股集团有限公司 Glue pot preventing surface layer from becoming dry and crusted
CN207774829U (en) * 2018-01-24 2018-08-28 云南酉兑科技有限公司 A kind of ice crystal synth sink
CN108514829A (en) * 2018-03-21 2018-09-11 林巧鸿 Coating machine slurry device

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111006530A (en) * 2019-11-18 2020-04-14 榆林学院 Heat exchanger device and heat exchange system for inner component of crescent fan
CN113618993A (en) * 2021-08-10 2021-11-09 黄山菲英汽车零部件有限公司 Manufacturing process of drum type friction plate for water passing tank vehicle
CN113618993B (en) * 2021-08-10 2023-01-10 黄山菲英汽车零部件有限公司 Manufacturing process of drum type friction plate for water passing tank vehicle
CN114623723A (en) * 2022-02-28 2022-06-14 呼伦贝尔安泰热电有限责任公司满洲里热电厂 Head convenient to dismantle
CN114688909A (en) * 2022-02-28 2022-07-01 呼伦贝尔安泰热电有限责任公司满洲里热电厂 Heating network heater
CN115430390A (en) * 2022-11-09 2022-12-06 山东法拉第氘源科技有限公司 Processing and preparation device and processing and preparation method of deuterated bromobenzene

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