CN108936594A - A kind of anti-oxidant compositions comprising tea polyphenols - Google Patents
A kind of anti-oxidant compositions comprising tea polyphenols Download PDFInfo
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- CN108936594A CN108936594A CN201810411241.3A CN201810411241A CN108936594A CN 108936594 A CN108936594 A CN 108936594A CN 201810411241 A CN201810411241 A CN 201810411241A CN 108936594 A CN108936594 A CN 108936594A
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- tea polyphenols
- oxidant
- oxidant compositions
- glutathione
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- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 70
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 67
- 235000006708 antioxidants Nutrition 0.000 title claims abstract description 67
- 150000008442 polyphenolic compounds Chemical class 0.000 title claims abstract description 44
- 235000013824 polyphenols Nutrition 0.000 title claims abstract description 44
- 239000000203 mixture Substances 0.000 title claims abstract description 42
- 241001122767 Theaceae Species 0.000 title claims 10
- RWSXRVCMGQZWBV-WDSKDSINSA-N glutathione Chemical compound OC(=O)[C@@H](N)CCC(=O)N[C@@H](CS)C(=O)NCC(O)=O RWSXRVCMGQZWBV-WDSKDSINSA-N 0.000 claims abstract description 55
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 42
- 108010024636 Glutathione Proteins 0.000 claims abstract description 27
- 229960003180 glutathione Drugs 0.000 claims abstract description 27
- 235000003969 glutathione Nutrition 0.000 claims abstract description 26
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 21
- 235000010323 ascorbic acid Nutrition 0.000 claims abstract description 21
- 229960005070 ascorbic acid Drugs 0.000 claims abstract description 21
- 239000011668 ascorbic acid Substances 0.000 claims abstract description 21
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 11
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 11
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 11
- 229940046009 vitamin E Drugs 0.000 claims abstract description 11
- 239000011709 vitamin E Substances 0.000 claims abstract description 11
- 244000269722 Thea sinensis Species 0.000 abstract description 36
- 235000019483 Peanut oil Nutrition 0.000 abstract description 11
- 239000000312 peanut oil Substances 0.000 abstract description 11
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- 235000013616 tea Nutrition 0.000 description 34
- 238000002360 preparation method Methods 0.000 description 11
- 210000002966 serum Anatomy 0.000 description 11
- 238000002156 mixing Methods 0.000 description 7
- 239000002002 slurry Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 238000010008 shearing Methods 0.000 description 6
- 241000208340 Araliaceae Species 0.000 description 5
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 5
- 235000003140 Panax quinquefolius Nutrition 0.000 description 5
- 235000008434 ginseng Nutrition 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 108090000765 processed proteins & peptides Proteins 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 230000006870 function Effects 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 150000003254 radicals Chemical class 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 2
- 235000005487 catechin Nutrition 0.000 description 2
- 229950001002 cianidanol Drugs 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- XUJNEKJLAYXESH-UHFFFAOYSA-N cysteine Natural products SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 description 2
- 235000018417 cysteine Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- GDSOZVZXVXTJMI-SNAWJCMRSA-N (e)-1-methylbut-1-ene-1,2,4-tricarboxylic acid Chemical compound OC(=O)C(/C)=C(C(O)=O)\CCC(O)=O GDSOZVZXVXTJMI-SNAWJCMRSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- 244000080767 Areca catechu Species 0.000 description 1
- 235000006226 Areca catechu Nutrition 0.000 description 1
- 201000001320 Atherosclerosis Diseases 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 description 1
- XUJNEKJLAYXESH-REOHCLBHSA-N L-Cysteine Chemical compound SC[C@H](N)C(O)=O XUJNEKJLAYXESH-REOHCLBHSA-N 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 229940123973 Oxygen scavenger Drugs 0.000 description 1
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 238000010420 art technique Methods 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000036983 biotransformation Effects 0.000 description 1
- QKSKPIVNLNLAAV-UHFFFAOYSA-N bis(2-chloroethyl) sulfide Chemical compound ClCCSCCCl QKSKPIVNLNLAAV-UHFFFAOYSA-N 0.000 description 1
- 239000013522 chelant Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004737 colorimetric analysis Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000012458 free base Substances 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- JDNTWHVOXJZDSN-UHFFFAOYSA-N iodoacetic acid Chemical compound OC(=O)CI JDNTWHVOXJZDSN-UHFFFAOYSA-N 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 210000005229 liver cell Anatomy 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 229960005489 paracetamol Drugs 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 230000004962 physiological condition Effects 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229940068041 phytic acid Drugs 0.000 description 1
- 235000002949 phytic acid Nutrition 0.000 description 1
- 239000000467 phytic acid Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a kind of anti-oxidant compositions comprising tea polyphenols, the raw material comprising following parts by weight: 13-15 parts of tea polyphenols, 8-10 parts of glutathione, 3-5 parts of ascorbic acid, 3-5 parts of polyethylene glycol.Present invention anti-oxidant compositions as made from combining tea polyphenols, glutathione, ascorbic acid with polyethylene glycol, can significantly reduce the anti-oxidant value of peanut oil, and showing has good synergistic function between these components.Simultaneously surprisingly, it was found that vitamin E is further added into above-mentioned anti-oxidant compositions can reduce the anti-oxidant value of peanut oil more significantly, superior antioxidant effect is shown.
Description
Technical field
The invention belongs to tea extract manufacture fields, and in particular to a kind of anti-oxidant compositions comprising tea polyphenols.
Background technique
There is many kinds of chemical components in tealeaves, have apparent health-care effect to human body, wherein most importantly
Tea polyphenols.Tea polyphenols are the compounds with phenol chemical structure for being present in tea, it has been found that have more than 30 kinds, wherein catechin is about
70% or so of tea polyphenols total amount is accounted for, one of the main body of tealeaves green tea ingredient is not only, and is why tealeaves has
The important component of healthcare function.Free radical is the arch-criminal for threatening human health, and the catechu in tea polyphenols is known as removing freely
The good effects of base.Further proved according to clinic study in recent years, the catechin in tea polyphenols have it is anti-oxidant,
Radiation protection, lipid-loweringing, anticancer, anti-aging and other effects.
Glutathione (glutathione, GSH) is combined by glutamic acid, cysteine and glycine, and sulfydryl is contained
Tripeptides has antioxidation and integrates detoxication.Sulfydryl on cysteine is glutathione active group (event gluathione
Peptide is often abbreviated as G-SH), easily with some drugs (such as paracetamol), toxin (such as free radical, iodoacetic acid, mustard gas, lead, mercury, arsenic
Equal heavy metals) etc. combine, and have and integrate detoxication.Therefore glutathione (glutathione especially in liver cell) can participate in
Biotransformation excretes external so that poisonous substance harmful in body is converted into harmless substance.Glutathione can also be helped
Help the function of keeping normal immune system.Glutathione has two kinds of forms of reduced form (G-SH) and oxidized form (G-S-S-G),
The overwhelming majority is accounted for reduced glutathione under physiological condition.The polyradical of crossing that body newly metabolism of old generation generates can damage biological
Film invades life macromolecule, accelerates body aging, and the generation of induced tumor or atherosclerosis.Glutathione is in human body
Interior chemical, biological defense system plays an important role, and has various physiological functions.Its major physiological effect is can to dispose
The intracorporal free radical of people, the antioxidant important as internal one kind, protects the sulfydryl in the molecules such as many protein and enzyme.
It needs to add a certain amount of antioxidant in food at present to protect nutritional ingredient not go bad because of oxidation.Often at present
Antioxidant can by sources be divided into artificial synthesized antioxidant (such as BHA, BHT, PG) and natural, and (such as tea is more
Phenol, phytic acid etc.).Antioxidant is broadly divided into two classes by dissolubility: oil-soluble inhibitor has BHA, BHT etc.;Water solubility is anti-
Oxidant has ascorbic acid, tea polyphenols etc..Antioxidant can be divided into free base absorbant, metal ion-chelant according to the mode of action
Agent, oxygen scavenger, peroxide decomposer, enzyme antioxidant, ultraviolet absorbing agent or singlet oxygen quencher etc..It is domestic at present
Research in terms of external composite antioxidant is also less, especially in terms of the composite antioxidant comprising tea polyphenols, is badly in need of related
It studies to reinforce the protective effect of nutritional ingredient in food.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of anti-oxidant compositions comprising tea polyphenols.
The present invention is achieved by the following technical programs.
The present invention provides a kind of anti-oxidant compositions comprising tea polyphenols, the raw material comprising following parts by weight: tea polyphenols
13-15 parts, 8-10 parts of glutathione, 3-5 parts of ascorbic acid, 3-5 parts of polyethylene glycol.
It further, also include 5-7 parts of vitamin E in the anti-oxidant compositions.
Further, the anti-oxidant compositions include the raw material of following parts by weight: 14 parts of tea polyphenols, glutathione 9
Part, 4 parts of ascorbic acid, 4 parts of polyethylene glycol.
Further, the anti-oxidant compositions are made of the raw material of following parts by weight: 14 parts of tea polyphenols, glutathione
9 parts, 4 parts of ascorbic acid, 4 parts of polyethylene glycol, 5-7 parts of vitamin E.
It further, also include 6 parts of vitamin E in the anti-oxidant compositions.
Further, the preparation method of the anti-oxidant compositions, comprising the following steps:
(1) polyethylene glycol is melted at 60-80 DEG C, shearing obtains slurries to clarifying, and the water-soluble of tea polyphenols is then added
Liquid, high speed shear obtain mixed serum after mixing;
(2) glutathione, ascorbic acid are successively added into step (1) resulting mixed serum, after high speed shear mixes,
It is spray-dried to obtain the anti-oxidant compositions through cryogenic vacuum.
Further, vitamin E is further added into mixed serum after ascorbic acid is added in step (2).
Further, step used in above-mentioned preparation method and parameter can use routine well known in the prior art
Technique and parameter carry out.
The beneficial effects of the present invention are:
Present invention antioxidant group as made from combining tea polyphenols, glutathione, ascorbic acid with polyethylene glycol
Object is closed, the anti-oxidant value of peanut oil can be significantly reduced, showing has good synergistic function between these components.Together
When surprisingly, it was found that vitamin E is further added into above-mentioned anti-oxidant compositions can reduce peanut more significantly
The anti-oxidant value of oil, shows superior antioxidant effect.
Specific embodiment
Technical solution of the present invention is described further below by specific embodiment, but following specific embodiments do not have to
In the limitation present invention.It is all within spirit of that invention and principle, any modification, equivalent replacement, improvement and so on should all include
Within protection scope of the present invention.
Embodiment 1
A kind of anti-oxidant compositions comprising tea polyphenols, are made of the raw material of following parts by weight: 14 parts of tea polyphenols, paddy Guang
9 parts of sweet peptide, 4 parts of ascorbic acid, 4 parts of polyethylene glycol.
The preparation method of the anti-oxidant compositions comprising tea polyphenols, comprising the following steps:
(1) polyethylene glycol is melted at 60-80 DEG C, shearing obtains slurries to clarifying, and the water-soluble of tea polyphenols is then added
Liquid, high speed shear obtain mixed serum after mixing;
(2) glutathione, ascorbic acid are successively added into step (1) resulting mixed serum, after high speed shear mixes,
It is spray-dried to obtain the anti-oxidant compositions through cryogenic vacuum.
Step used in above-mentioned preparation method and parameter can use common process well known in the prior art and ginseng
Number carries out.
Embodiment 2
A kind of anti-oxidant compositions comprising tea polyphenols, are made of the raw material of following parts by weight: 14 parts of tea polyphenols, paddy Guang
9 parts of sweet peptide, 4 parts of ascorbic acid, 4 parts of polyethylene glycol, 6 parts of vitamin E.
(1) polyethylene glycol is melted at 60-80 DEG C, shearing obtains slurries to clarifying, and the water-soluble of tea polyphenols is then added
Liquid, high speed shear obtain mixed serum after mixing;
(2) glutathione, ascorbic acid, vitamin E is successively added into step (1) resulting mixed serum, cuts at a high speed
After cutting mixing, it is spray-dried to obtain the anti-oxidant compositions through cryogenic vacuum.
Step used in above-mentioned preparation method and parameter can use common process well known in the prior art and ginseng
Number carries out.
Embodiment 3
A kind of anti-oxidant compositions comprising tea polyphenols, are made of the raw material of following parts by weight: 14 parts of tea polyphenols, anti-bad
4 parts of hematic acid.Preparation method is to mix tea polyphenols and ascorbic acid according to the weight ratio.
Embodiment 4
A kind of anti-oxidant compositions comprising tea polyphenols, are made of the raw material of following parts by weight: 14 parts of tea polyphenols, paddy Guang
9 parts of sweet peptide, 4 parts of polyethylene glycol.
(1) polyethylene glycol is melted at 60-80 DEG C, shearing obtains slurries to clarifying, and the water-soluble of tea polyphenols is then added
Liquid, high speed shear obtain mixed serum after mixing;
(2) glutathione is added into step (1) resulting mixed serum to spray after high speed shear mixes through cryogenic vacuum
Mist is dried to obtain the anti-oxidant compositions.
Step used in above-mentioned preparation method and parameter can use common process well known in the prior art and ginseng
Number carries out.
Embodiment 5
A kind of anti-oxidant compositions are made of the raw material of following parts by weight: 9 parts of glutathione, 4 parts of ascorbic acid, being gathered
4 parts of ethylene glycol.
The preparation method of the anti-oxidant compositions, comprising the following steps:
(1) polyethylene glycol is melted at 60-80 DEG C, shearing obtains slurries to clarifying, and the water-soluble of glutathione is then added
Liquid, high speed shear obtain mixed serum after mixing;
(2) ascorbic acid is added into step (1) resulting mixed serum to spray after high speed shear mixes through cryogenic vacuum
Mist is dried to obtain the anti-oxidant compositions.
Step used in above-mentioned preparation method and parameter can use common process well known in the prior art and ginseng
Number carries out.
Embodiment 6
A kind of anti-oxidant compositions are made of the raw material of following parts by weight: 9 parts of glutathione, 4 parts of polyethylene glycol.
The preparation method of the anti-oxidant compositions, comprising the following steps:
(1) polyethylene glycol is melted at 60-80 DEG C, shearing obtains slurries to clarifying;
(2) aqueous solution of glutathione is added into step (1) resulting slurries, it is true through low temperature after high speed shear mixes
Sky spray drying obtains the anti-oxidant compositions.
Step used in above-mentioned preparation method and parameter can use common process well known in the prior art and ginseng
Number carries out.
Embodiment 7
Take 700 grams of peanut oil to be divided into 7 parts of equivalent, 100 grams every part, will wherein 1 part be used as blank control group, to other 6
Anti-oxidant compositions obtained in embodiment 1-6 are added respectively as processing according to the 0.02% of peanut oil weight in part
This 7 groups of samples are placed in constant temperature oven (50 ± 0.5 DEG C) by group after mixing, primary every stirring in 24 hours.In the 10th He
Using the anti-oxidant value (meq/kg) of colorimetric method for determining peanut oil as defined in GB/T5009.37-2003 at 20 days, as peanut oil
The evaluation index of degree of oxidation carrys out the antioxidant activity height of anti-oxidant compositions added by comparison with this.Each group is in the 10th He
The anti-oxidant value (meq/kg) of measured peanut oil is sampled at 20 days referring to the following table 1.
Influence of the different anti-oxidant compositions of table 1 to the anti-oxidant value of peanut oil
Group | 10th day anti-oxidant value meq/kg | 20th day anti-oxidant value meq/kg |
Embodiment 1 | 1.85 | 3.32 |
Embodiment 2 | 0.49 | 0.96 |
Embodiment 3 | 5.83 | 11.84 |
Embodiment 4 | 4.98 | 9.93 |
Embodiment 5 | 6.77 | 14.32 |
Embodiment 6 | 7.26 | 16.58 |
Blank control group | 9.19 | 27.86 |
Due to peanut oil (wherein containing oleic acid 41.2%, linoleic acid 37.6%) containing 80% or more unsaturated fatty acid, ratio
Other edible vegetable oils are easier to be oxidized.By the result in upper table it can be found that the present invention is by by tea polyphenols, gluathione
Peptide, ascorbic acid combine anti-oxidant compositions obtained with polyethylene glycol, can significantly reduce the anti-oxidant value of peanut oil,
Showing has good synergistic function between these components.Meanwhile comparing tea polyphenols, glutathione, ascorbic acid, dimension
For any two or three of combination in raw element E and these ingredients of polyethylene glycol, the specific group of 4 kinds or 5 kinds raw materials is selected
Conjunction also shows that significant progress effect.Therefore, technical solution of the present invention compared to existing technologies, shows significance difference
It is different, unexpected technical effect is obtained in the combined aspects of antioxidant composition.
Concrete scheme and main feature of the invention has been shown and described above, and to a certain extent by test data
Embody advantages of the present invention.It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, above-mentioned reality
It applies and only illustrates concrete scheme of the invention described in example and specification, in the premise for not departing from spirit and scope of the invention
Under, various changes and improvements may be made to the invention, and these changes and improvements all fall within the protetion scope of the claimed invention.This hair
Bright claimed range is defined by the appending claims and its equivalent thereof.
Claims (6)
1. a kind of anti-oxidant compositions comprising tea polyphenols, which is characterized in that the raw material comprising following parts by weight: tea polyphenols
13-15 parts, 8-10 parts of glutathione, 3-5 parts of ascorbic acid, 3-5 parts of polyethylene glycol.
2. as described in claim 1 including the anti-oxidant compositions of tea polyphenols, which is characterized in that the antioxidant combination
It also include 5-7 parts of vitamin E in object.
3. as described in claim 1 including the anti-oxidant compositions of tea polyphenols, which is characterized in that the antioxidant combination
Object includes the raw material of following parts by weight: 14 parts of tea polyphenols, 9 parts of glutathione, 4 parts of ascorbic acid, 4 parts of polyethylene glycol.
4. as described in claim 1 including the anti-oxidant compositions of tea polyphenols, which is characterized in that the antioxidant combination
Object is made of the raw material of following parts by weight: 14 parts of tea polyphenols, 9 parts of glutathione, and 4 parts of ascorbic acid, 4 parts of polyethylene glycol, dimension life
Plain E 5-7 parts.
5. the anti-oxidant compositions as claimed in claim 1 or 3 comprising tea polyphenols, which is characterized in that the antioxidant
It also include 6 parts of vitamin E in composition.
6. the anti-oxidant compositions as claimed in claim 2 or 4 comprising tea polyphenols, which is characterized in that the antioxidant
The usage ratio of vitamin E is 6 parts in composition.
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