CN108936371A - A kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated - Google Patents
A kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated Download PDFInfo
- Publication number
- CN108936371A CN108936371A CN201810841947.3A CN201810841947A CN108936371A CN 108936371 A CN108936371 A CN 108936371A CN 201810841947 A CN201810841947 A CN 201810841947A CN 108936371 A CN108936371 A CN 108936371A
- Authority
- CN
- China
- Prior art keywords
- pressure
- grade breast
- fresh grade
- vacuum
- marinated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 210000000481 breast Anatomy 0.000 title claims abstract description 51
- 238000000034 method Methods 0.000 title claims abstract description 29
- 230000003750 conditioning effect Effects 0.000 title claims abstract description 26
- 230000008569 process Effects 0.000 title claims abstract description 23
- 238000010411 cooking Methods 0.000 claims abstract description 33
- 238000012545 processing Methods 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 238000005554 pickling Methods 0.000 claims abstract description 25
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 24
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims abstract description 18
- 229940048086 sodium pyrophosphate Drugs 0.000 claims abstract description 18
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims abstract description 18
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims abstract description 18
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 12
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims description 17
- 235000013372 meat Nutrition 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 10
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 claims description 10
- 235000021110 pickles Nutrition 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 7
- 229920002261 Corn starch Polymers 0.000 claims description 6
- 239000008120 corn starch Substances 0.000 claims description 6
- 229940099112 cornstarch Drugs 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 244000203593 Piper nigrum Species 0.000 claims description 5
- 235000008184 Piper nigrum Nutrition 0.000 claims description 5
- 244000273928 Zingiber officinale Species 0.000 claims description 5
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 5
- 235000010323 ascorbic acid Nutrition 0.000 claims description 5
- 229960005070 ascorbic acid Drugs 0.000 claims description 5
- 239000011668 ascorbic acid Substances 0.000 claims description 5
- 235000013614 black pepper Nutrition 0.000 claims description 5
- 210000002808 connective tissue Anatomy 0.000 claims description 5
- 235000008397 ginger Nutrition 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 239000001931 piper nigrum l. white Substances 0.000 claims description 5
- 238000004321 preservation Methods 0.000 claims description 5
- 235000020995 raw meat Nutrition 0.000 claims description 5
- 235000010288 sodium nitrite Nutrition 0.000 claims description 5
- 235000012424 soybean oil Nutrition 0.000 claims description 5
- 239000003549 soybean oil Substances 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 108010073771 Soybean Proteins Proteins 0.000 claims description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 4
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 4
- 239000005457 ice water Substances 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 235000019710 soybean protein Nutrition 0.000 claims description 4
- 241000206575 Chondrus crispus Species 0.000 claims description 2
- 235000013599 spices Nutrition 0.000 claims 1
- 241000287828 Gallus gallus Species 0.000 abstract description 28
- 239000000654 additive Substances 0.000 abstract description 21
- 230000000996 additive effect Effects 0.000 abstract description 21
- 238000002474 experimental method Methods 0.000 abstract description 13
- 235000013622 meat product Nutrition 0.000 abstract description 11
- 229920002472 Starch Polymers 0.000 abstract description 10
- 235000019698 starch Nutrition 0.000 abstract description 10
- 239000008107 starch Substances 0.000 abstract description 10
- 239000003795 chemical substances by application Substances 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 6
- 230000004044 response Effects 0.000 abstract description 4
- 235000013330 chicken meat Nutrition 0.000 description 34
- 206010016807 Fluid retention Diseases 0.000 description 21
- 235000013305 food Nutrition 0.000 description 14
- 238000012856 packing Methods 0.000 description 5
- 238000005303 weighing Methods 0.000 description 5
- 229910019142 PO4 Inorganic materials 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 4
- 239000010452 phosphate Substances 0.000 description 4
- 230000000630 rising effect Effects 0.000 description 4
- 206010034203 Pectus Carinatum Diseases 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000003292 glue Substances 0.000 description 3
- 238000003672 processing method Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 235000018102 proteins Nutrition 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 238000009938 salting Methods 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 238000009461 vacuum packaging Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000005138 cryopreservation Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- TVZISJTYELEYPI-UHFFFAOYSA-N hypodiphosphoric acid Chemical compound OP(O)(=O)P(O)(O)=O TVZISJTYELEYPI-UHFFFAOYSA-N 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000015277 pork Nutrition 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 235000013594 poultry meat Nutrition 0.000 description 1
- 235000020991 processed meat Nutrition 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005211 surface analysis Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/70—Tenderised or flavoured meat pieces; Macerating or marinating solutions specially adapted therefor
- A23L13/72—Tenderised or flavoured meat pieces; Macerating or marinating solutions specially adapted therefor using additives, e.g. by injection of solutions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/426—Addition of proteins, carbohydrates or fibrous material from vegetable origin other than sugars or sugar alcohols
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/428—Addition of flavours, spices, colours, amino acids or their salts, peptides, vitamins, yeast extract or autolysate, nucleic acid or derivatives, organic acidifying agents or their salts or acidogens, sweeteners, e.g. sugars or sugar alcohols; Addition of alcohol-containing products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/43—Addition of vegetable fats or oils; Addition of non-meat animal fats or oils; Addition of fatty acids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/432—Addition of inorganic compounds, e.g. minerals; oligo-elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/50—Poultry products, e.g. poultry sausages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/70—Tenderised or flavoured meat pieces; Macerating or marinating solutions specially adapted therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Mycology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Meat, Egg Or Seafood Products (AREA)
Abstract
The present invention discloses a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated, belong to field of meat product processing, the present invention is to improve chicken water retention and cooking loss rate as index, tumbling time, water-retaining agent additive amount, super-pressure time and pressure are optimized by single factor experiment and response surface experiments, to determine optimal processing parameter.The result shows that: when vacuum degree 0.06Mpa, tumbling time 30min, tumbling effect is best.Pickling liquid proportion water retention in sodium pyrophosphate 0.2%, starch 7%, sodium bicarbonate 1.5% is best.When the ultra high pressure treatment time is 10min, processing pressure is 200Mpa, effect is best.
Description
Technical field
The present invention relates to field of meat product processing, marinated more particularly to a kind of conditioning Fresh Grade Breast vacuum combination super-pressure
Process.
Background technique
Currently, chicken has become the second largest meat for being only second to pork in the world.China is raw as the main chicken in the whole world
Produce state and country of consumption.In recent years, chicken production and consumption is still in rising trend.2014, Chinese broiler chicken butchered working ability
The 70% of industry supply capacity is accounted for, and preliminary working and deep processing chicken meat product develop slowly.Currently, poultry husbandry is from a list
One health product chicken development is high quality, high value-added product.Recuperating chicken breast product refers to using fresh chicken breast meat as raw material,
It is aided with marinated and seasoning.By processing appropriate, such as cutting, stirring, molding and conditioning, saves, transports under the conditions of cryo-conservation
Defeated and sale.Chicken products are a kind of novel instant foods, it is only necessary to which it can be served after simple processing or heat treatment.Its generation
The table developing direction of the following chicken deep processing.
Processed meat products processing in, tumbling is most common processing method, it be improve product water-retaining property, yield rate,
The important means of food quality and organoleptic quality.By mechanical movement, the mechanical strength of meat fiber weakens, final fracture, knot
Toughness reduction, the musculature softening of tissue are formed, product yield and food quality greatly improve.Because intercellular gap increases
Greatly, salt water is easier to be distributed and absorb, so that the dosage of pickling liquid be made to reduce.During tumbling, the items such as time and additive
Part can all generate different degrees of influence to the quality characteristic of meat.
Water-retaining property refers to meat products processing, storage, in storage process, such as pressure effect, chopping, heating, freezing, thaw,
Pickle the holding capacity during waiting to moisture.Water-retaining property directly affects the quality of meat, is the evaluation most important index of meat products
One of, there is important economic significance.In order to promote the water-retaining property of meat, the water-retaining agent based on phosphate is led in meat products processing
Domain is widely used, and is capable of the quality of the improvement meat products of high degree.But human body, which takes in excessive phosphate, will lead to human body pair
The absorbability of calcium declines, thus unhealthful.And meat products raw material inherently has certain phosphate, slightly has without paying attention to
Add the excessive risk of phosphate.Low-phosphorous water-retaining agent compares phosphate-free water-retaining agent, and cost is relatively low, it can be ensured that food safety guarantees meat
Product water retention has preferable market prospects.
Superhigh pressure technique, which refers to, is at high or low temperatures put into food in liquid medium, and carry out 100 to it~
The HIGH PRESSURE TREATMENT technology of 1000MPa.The ultra high pressure treatment time is where appropriate, non-covalent bond (hydrogen bond, ionic bond and hydrophobic in food
Key etc.) it is destroyed or is formed, the enzyme, protein, starch and other biological macromolecule in food lose activity, are denaturalized or are gelatinized,
The harmful microorganism in food can be killed and improve food quality.It is keeping being processed food natural color and nutrition
In terms of ingredient, superhigh pressure technique has comparable superiority.Meanwhile it can be efficiently against traditional heat using superhigh pressure technique
Processing method handles defect brought by food.In the manufacturing process of meat products, meat products is can be enhanced in ultra high pressure treatment
Coagulability and water holding capacity.
The research to conditioning chicken external in recent years lays particular emphasis on quality control primarily with respect to the application of new and high technology.In
The characteristics of state's chicken processing industry is the value Transfer of industrial chain to deep processing stage, stronger tune processing method and residue detection.
The present invention passes through tumbling time, low-phosphorous water-retaining agent, ultra high pressure and time pair in research recuperating chicken breast product tumbling procedure
The water retention of Fresh Grade Breast and the influence of cooking loss rate, to make product reach higher water-retaining property, to obtain optimal add
Work process conditions.
Summary of the invention
The object of the present invention is to provide a kind of processes that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated, on solving
Problem of the existing technology is stated, to improve conditioning Water-holding Capacity of Chicken Meat, reduces its cooking loss rate.
To achieve the above object, the present invention provides following schemes:
The present invention provides a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated, comprising the following steps:
(1) raw meat pre-processes: selecting the excellent Fresh Grade Breast of meat, is placed on 0-4 DEG C of preservation 12h of refrigerator, cleans and reject
It is spare to be cut into the placement of 5cm × 10cm × 2cm strip for fat and connective tissue;
(2) it pickles, tumbling: step (1) processed Fresh Grade Breast is put into vacuum tumbler, pickling liquid, vacuum rolling is added
Rub 10-50min;
(3) be vacuum-packed: the Fresh Grade Breast packing that step (2) is disposed and vacuum bag are sealed with sealing machine, in boiling water
Middle cooking 10min takes out, and placement is cooled to room temperature;
(4) ultra high pressure treatment: the Fresh Grade Breast that step (3) is disposed is placed in high-tension apparatus, pressure 50-500Mpa,
Ultra high pressure treatment 1-20min;
(5) it refrigerates: the Fresh Grade Breast that step (4) is disposed is refrigerated.
Preferably, the pickling liquid in the step (2) includes following component according to Fresh Grade Breast percent by weight: corn forms sediment
Powder 1-9%, sodium bicarbonate 0.3-1.8%, sodium pyrophosphate 0.05-0.3%, sodium nitrite 0.02%, ascorbic acid 0.05%, ice
It is water 20%, five-spice powder 0.5%, salt 1.5%, cooking wine 2.0%, ginger powder 0.2%, white pepper powder 0.2%, soybean oil 2.5%, big
Beans protein isolate 1.0%, carragheen 0.9%.
Preferably, the cornstarch proportion is 7%.
Preferably, the sodium bicarbonate proportion is 1.5%.
Preferably, the sodium pyrophosphate proportion is 0.2%.
Preferably, vacuum tumbling time is 30min, vacuum degree 0.06Mpa in the step (2).
Preferably, ultra high pressure treatment pressure is 200Mpa in the step (4).
Preferably, the ultra high pressure treatment time is 10min in the step (4).
The invention discloses following technical effects:
1, the present invention by high-quality Fresh Grade Breast and pickling liquid, pickle in vacuum tumbler jointly by tumbling, super-pressure, Ke Yiti
High product water-retaining property, yield rate, food quality and organoleptic quality;
2, pickling liquid of the present invention uses hypophosphate formula, and cost is relatively low, it can be ensured that food safety guarantees that meat products is protected
Water rate has preferable market prospects;
3, it is an advantage of the invention that pickling process combination, vacuum and super-pressure is front and rear combined to be combined marinated, improves meat
Rotten quality.It is marinated uniform that vacuum promotes the seepage velocity of pickling liquid, super-pressure further to make, and improves marinated effect, improves meat gruel
Quality.
Specific embodiment
Below in conjunction with the specific embodiment of the invention, technical solution in the embodiment of the present invention is carried out clearly and completely
Description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on this hair
Embodiment in bright, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, With reference to embodiment
The present invention is described in further detail.
Embodiment 1
(1) raw meat pre-processes: selecting the excellent Fresh Grade Breast of meat, is placed on 0-4 DEG C of preservation 12h of refrigerator, cleans and reject
It is spare to be cut into the placement of 5cm × 10cm × 2cm strip for fat and connective tissue;
(2) it pickles, tumbling: preparing pickling liquid, formula is calculated as cornstarch 1%, carbonic acid according to Fresh Grade Breast weight percent
Hydrogen sodium 0.3%, sodium pyrophosphate 0.05%, sodium nitrite 0.02%, ascorbic acid 0.05%, ice water 20%, five-spice powder 0.5%,
Salt 1.5%, cooking wine 2.0%, ginger powder 0.2%, white pepper powder 0.2%, soybean oil 2.5%, soybean protein isolate 1.0%, card
Draw glue 0.9%.
Step (1) processed Fresh Grade Breast is put into vacuum tumbler, pickling liquid, vacuum tumbling 10min, vacuum degree is added
0.06Mpa;
(3) be vacuum-packed: the Fresh Grade Breast packing that step (2) is disposed and vacuum bag are sealed with sealing machine, in boiling water
Middle cooking 10min takes out, and placement is cooled to room temperature;
(4) ultra high pressure treatment: the Fresh Grade Breast that step (3) is disposed is placed in high-tension apparatus, pressure 50Mpa, superelevation
Pressure processing 1min;
(5) it refrigerates: the Fresh Grade Breast that step (4) is disposed is refrigerated.
The conditioning Water-holding Capacity of Chicken Meat obtained of the present embodiment 1 is 11.23%, and cooking loss rate is 20.66%.
Embodiment 2
(1) raw meat pre-processes: selecting the excellent Fresh Grade Breast of meat, is placed on 0-4 DEG C of preservation 12h of refrigerator, cleans and reject
It is spare to be cut into the placement of 5cm × 10cm × 2cm strip for fat and connective tissue;
(2) it pickles, tumbling: preparing pickling liquid, formula is calculated as cornstarch 7%, carbonic acid according to Fresh Grade Breast weight percent
Hydrogen sodium 1.5%, sodium pyrophosphate 0.2%, sodium nitrite 0.02%, ascorbic acid 0.05%, ice water 20%, five-spice powder 0.5%, food
Salt 1.5%, cooking wine 2.0%, ginger powder 0.2%, white pepper powder 0.2%, soybean oil 2.5%, soybean protein isolate 1.0%, OK a karaoke club
Glue 0.9%.
Step (1) processed Fresh Grade Breast is put into vacuum tumbler, pickling liquid, vacuum tumbling 30min, vacuum degree is added
0.06Mpa;
(3) be vacuum-packed: the Fresh Grade Breast packing that step (2) is disposed and vacuum bag are sealed with sealing machine, in boiling water
Middle cooking 10min takes out, and placement is cooled to room temperature;
(4) ultra high pressure treatment: the Fresh Grade Breast that step (3) is disposed is placed in high-tension apparatus, pressure 200Mpa, is surpassed
HIGH PRESSURE TREATMENT 10min;
(5) it refrigerates: the Fresh Grade Breast that step (4) is disposed is refrigerated.
The conditioning Water-holding Capacity of Chicken Meat obtained of the present embodiment 2 is 13.66%, and cooking loss rate is 20.45%.
Embodiment 3
(1) raw meat pre-processes: selecting the excellent Fresh Grade Breast of meat, is placed on 0-4 DEG C of preservation 12h of refrigerator, cleans and reject
It is spare to be cut into the placement of 5cm × 10cm × 2cm strip for fat and connective tissue;
(2) it pickles, tumbling: preparing pickling liquid, formula is calculated as cornstarch 9%, carbonic acid according to Fresh Grade Breast weight percent
Hydrogen sodium 1.8%, sodium pyrophosphate 0.3%, sodium nitrite 0.02%, ascorbic acid 0.05%, ice water 20%, five-spice powder 0.5%, food
Salt 1.5%, cooking wine 2.0%, ginger powder 0.2%, white pepper powder 0.2%, soybean oil 2.5%, soybean protein isolate 1.0%, OK a karaoke club
Glue 0.9%.
Step (1) processed Fresh Grade Breast is put into vacuum tumbler, pickling liquid, vacuum tumbling 50min, vacuum degree is added
0.06Mpa;
(3) be vacuum-packed: the Fresh Grade Breast packing that step (2) is disposed and vacuum bag are sealed with sealing machine, in boiling water
Middle cooking 10min takes out, and placement is cooled to room temperature;
(4) ultra high pressure treatment: the Fresh Grade Breast that step (3) is disposed is placed in high-tension apparatus, pressure 500Mpa, is surpassed
HIGH PRESSURE TREATMENT 20min;
(5) it refrigerates: the Fresh Grade Breast that step (4) is disposed is refrigerated.
The conditioning Water-holding Capacity of Chicken Meat obtained of the present embodiment 3 is 12.13%, and cooking loss rate is 15.63%.
Embodiment 4
(1) influence of the tumbling time to conditioning chicken
It takes the chicken cut to be grouped two-by-two, is marked with multi-color cord, weigh m1, prepare pickling liquid.By the chicken of weighing and pickle
Liquid is put into tumbler together and carries out tumbling processing, with tumbling time 0min, 10min, 20min, 30min, 40min, 50min difference
It is experiment of single factor, vacuum degree 0.06Mpa.Chicken is placed on mesh screen and stands after tumbling, and there is no claim when drop infiltration is fallen
Weight m2, measure its water retention.
Packing chicken is sealed in vacuum bag with sealing machine after measuring water retention, and 10min is cooked in boiling water and is taken out, is placed cold
But to room temperature, weigh m after being dried with gauze3, measure its cooking loss rate.
As the result is shown: with the increase of tumbling time, Water-holding Capacity of Chicken Meat is in the trend risen.Tumbling time 10min with
Without tumbling processing group, 20min with 10min processing group, 40min compared with 30min processing group, water retention dramatically increases (P <
0.05).For tumbling time 30min with 20min processing group, 50min compared with 40min processing group, difference is not significant (P > 0.05).
With the increase of tumbling time, Fresh Grade Breast cooking loss rate is in the trend risen.Tumbling time 10min is handled with without tumbling
With 20min processing group, 50min compared with 40min processing group, cooking loss rate dramatically increases (P < 0.05) by group, 30min.Tumbling
For time 20min compared with 10min processing group, difference is not significant (P > 0.05).Tumbling time 40min and 30min processing group phase
Than cooking loss rate is remarkably decreased (P < 0.05).Comprehensive water retention and cooking loss rate compare, select tumbling time for
30min。
(2) influence of the sodium pyrophosphate additive amount to conditioning chicken
It takes the chicken cut to be grouped two-by-two, is marked with multi-color cord, weigh m1, prepare pickling liquid.With sodium pyrophosphate 0.05%,
0.1%, 0.15%, 0.2%, 0.25%, 0.3% experiment of single factor is done respectively.The chicken of weighing and pickling liquid are put into together
Tumbler carries out tumbling and handles 20min, vacuum degree 0.06Mpa.Measure water retention and cooking loss rate.
As the result is shown: with the increase of sodium pyrophosphate additive amount, under Water-holding Capacity of Chicken Meat and cooking loss take the lead in after rising
Drop.Sodium pyrophosphate additive amount from 0.05% increase to 0.2% when water retention increase significant (P < 0.05), sodium pyrophosphate additive amount
Water retention difference is not significant (P > 0.05) when rising to 0.25% from 0.2%, and sodium pyrophosphate additive amount rises to from 0.25%
Water retention declines significant (P < 0.05) when 0.3%.Sodium pyrophosphate additive amount from 0.05% rise to 0.1% when cooking loss rate
Increase significant (P < 0.05), sodium pyrophosphate additive amount from 0.1% rise to 0.1% when cooking loss rate decline significant (P <
0.05)。
(3) influence of the starch additive amount to conditioning chicken
It takes the chicken cut to be grouped two-by-two, is marked with multi-color cord, weigh m1, prepare pickling liquid.With starch 1%, 3%, 5%,
7%, 9% experiment of single factor is done respectively.The chicken of weighing and pickling liquid are put into tumbler together and carry out tumbling processing 20min,
Vacuum degree 0.06Mpa.Measure water retention and cooking loss rate.
As the result is shown: with the increase of starch additive amount, Water-holding Capacity of Chicken Meat and cooking loss take the lead in declining after rising.It forms sediment
Powder additive amount from 1% increase to 5% when water retention increase significant (P < 0.05), starch additive amount from 5% rise to 9% when guarantor
Water rate declines significant (P < 0.05).Starch additive amount from 1% increase to 3% when cooking loss rate increase significant (P < 0.05),
Starch additive amount from 3% increase to 9% when cooking loss rate decline significant (P < 0.05).
(4) influence of the sodium bicarbonate additive amount to conditioning chicken
It takes the chicken cut to be grouped two-by-two, is marked with multi-color cord, weigh m1, prepare pickling liquid.With sodium bicarbonate 0.3%,
0.6%, 0.9%, 1.2%, 1.5%, 1.8% experiment of single factor is done respectively.The chicken of weighing and pickling liquid are put into rolling together
It rubs machine and carries out tumbling processing 20min, vacuum degree 0.06Mpa.Measure water retention and cooking loss rate.
As the result is shown: with the increase of sodium bicarbonate additive amount, the water retention of Fresh Grade Breast increases significant (P < 0.05),
Sodium bicarbonate additive amount reaches highest level when being 1.2%, and difference is not significant (P > 0.05) when increasing to 1.5%, continues growing
(P < 0.05) is remarkably decreased when to 1.8%.With the increase of sodium bicarbonate additive amount, the cooking loss rate decline of Fresh Grade Breast is aobvious
It writes (P < 0.05), when sodium bicarbonate additive amount increases to 1.5% from 1.2%, difference is not significant (P > 0.05), continues growing
(P < 0.05) is remarkably decreased when to 1.8%.
(5) orthogonal test
It takes the chicken cut to be grouped two-by-two, is marked with multi-color cord, weigh m1, prepare pickling liquid.With sodium pyrophosphate 0.15%,
0.2%, 0.25%;Starch is with 5%, 7%, 9%;Sodium bicarbonate does orthogonal experiment with 0.9%, 1.2%, 1.5%.By weighing
Chicken and pickling liquid are put into tumbler together and carry out tumbling processing 20min, vacuum degree 0.06Mpa.Measure water retention and boiling damage
Mistake rate.Quadrature analysis selects best water-retaining agent proportion.
(6) super-pressure is tested
Super high-pressure single Factor Experiment is carried out according to the optimum formula of measured tumbling time, low-phosphorous water-retaining agent.
A, influence of the ultra high pressure to conditioning chicken
By the good Fresh Grade Breast vacuum packaging of knead-salting, it is placed in high-tension apparatus and is handled.With pressure 50,100,150,
200,250,300,400,500Mpa does experiment of single factor respectively, measures water retention and cooking loss rate.
B, influence of the super-pressure time to conditioning chicken
By the good Fresh Grade Breast vacuum packaging of knead-salting, it is placed in high-tension apparatus and is handled.With super-pressure time 1,3,
5,7,10,15,20min does experiment of single factor respectively, measures water retention and cooking loss rate.
The present embodiment 4 is by single factor experiment and response surface experiments to tumbling time, water-retaining agent additive amount, super-pressure time
It is optimized with pressure.Show that best tumbling time is 30min, the best ultra high pressure treatment time is by experiment of single factor
10min, processing pressure 200Mpa.By response surface analysis, optimal water retention proportion is obtained are as follows: sodium pyrophosphate 0.2%, starch
7%, sodium bicarbonate 1.5%.It carries out three groups of parallel laboratory tests with this condition to be verified, average water retention is 13.67%, phase
To error less than 1%, thus it is accurate and reliable based on the resulting Optimal Parameters of Response Surface Method, and obtained optimum process condition has
Practical application value.
It can be obtained by experimental data, the water retention 1.70% of vacuum tumbling control group, ultra high pressure treatment control is
11.32%, substantially less than vacuum tumbling-ultra high pressure treatment group water retention 13.57%.Vacuum-ultra high pressure treatment meat gruel
Cooking loss rate is 25.19%, and control group is up to 31.83%.Meat gruel quality is significantly promoted accordingly.
Embodiment described above is only that preferred embodiment of the invention is described, and is not carried out to the scope of the present invention
It limits, without departing from the spirit of the design of the present invention, those of ordinary skill in the art make technical solution of the present invention
Various changes and improvements, should all fall into claims of the present invention determine protection scope in.
Claims (8)
1. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated, it is characterised in that: the following steps are included:
(1) raw meat pre-processes: selecting the excellent Fresh Grade Breast of meat, is placed on 0-4 DEG C of preservation 12h of refrigerator, cleans and reject fat
And connective tissue, it is spare to be cut into the placement of 5cm × 10cm × 2cm strip;
(2) it pickles, tumbling: step (1) processed Fresh Grade Breast being put into vacuum tumbler, pickling liquid, vacuum tumbling 10- is added
50min;
(3) it is vacuum-packed: the Fresh Grade Breast that step (2) is disposed being sub-packed in vacuum bag, is sealed with sealing machine, is boiled in boiling water
10min processed takes out, and placement is cooled to room temperature;
(4) ultra high pressure treatment: the Fresh Grade Breast that step (3) is disposed is placed in high-tension apparatus, pressure 50-500Mpa, superelevation
Pressure processing 1-20min;
(5) it refrigerates: the Fresh Grade Breast that step (4) is disposed is refrigerated.
2. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 1, feature exist
In: pickling liquid in the step (2) includes following component according to Fresh Grade Breast percent by weight: cornstarch 1-9%, carbonic acid
Hydrogen sodium 0.3-1.8%, sodium pyrophosphate 0.05-0.3%, sodium nitrite 0.02%, ascorbic acid 0.05%, ice water 20%, spices
Powder 0.5%, salt 1.5%, cooking wine 2.0%, ginger powder 0.2%, white pepper powder 0.2%, soybean oil 2.5%, soybean protein isolate
1.0%, carragheen 0.9%.
3. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 2, feature exist
In: the cornstarch proportion is 7%.
4. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 2, feature exist
In: the sodium bicarbonate proportion is 1.5%.
5. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 2, feature exist
In: the sodium pyrophosphate proportion is 0.2%.
6. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 1, feature exist
In: vacuum tumbling time is 30min, vacuum degree 0.06Mpa in the step (2).
7. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 1, feature exist
In: ultra high pressure treatment pressure is 200Mpa in the step (4).
8. a kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated according to claim 1, feature exist
In: the ultra high pressure treatment time is 10min in the step (4).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810841947.3A CN108936371A (en) | 2018-07-27 | 2018-07-27 | A kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810841947.3A CN108936371A (en) | 2018-07-27 | 2018-07-27 | A kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated |
Publications (1)
Publication Number | Publication Date |
---|---|
CN108936371A true CN108936371A (en) | 2018-12-07 |
Family
ID=64465921
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810841947.3A Pending CN108936371A (en) | 2018-07-27 | 2018-07-27 | A kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN108936371A (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109924429A (en) * | 2019-04-18 | 2019-06-25 | 彭为锋 | A kind of production method of soft dried beef |
CN110110926A (en) * | 2019-05-06 | 2019-08-09 | 武汉轻工大学 | Optimization method, equipment, storage medium and the device of grain processing link |
CN110692936A (en) * | 2019-11-21 | 2020-01-17 | 安徽万礼食品有限责任公司 | Processing technology of spiced pig ears |
CN111480801A (en) * | 2019-01-25 | 2020-08-04 | 上海联豪食品有限公司 | Conditioning chicken steak and preparation method thereof |
CN114343000A (en) * | 2021-12-07 | 2022-04-15 | 福建省亚明食品有限公司 | Method for improving quality of medium-sized dishes of spareribs |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070237865A1 (en) * | 2006-04-05 | 2007-10-11 | Robert Love | Method for manufacturing high pressure processed food products |
CN102125269A (en) * | 2010-01-13 | 2011-07-20 | 天津科技大学 | Method for producing low-temperature and low-salt ham by utilizing ultrahigh pressure |
CN103976324A (en) * | 2014-05-30 | 2014-08-13 | 辽宁禾丰食品有限公司 | Rattan pepper-flavor quick-frozen chicken breast seasoning formula and using method thereof |
CN105581273A (en) * | 2015-12-23 | 2016-05-18 | 宁夏大学 | Preparation method of Muslim low-temperature mutton ham |
CN107373420A (en) * | 2017-07-12 | 2017-11-24 | 必斐艾食品有限公司 | A kind of processing method of curry chicken |
CN108112859A (en) * | 2017-12-13 | 2018-06-05 | 成都大学 | A kind of Novel dried meat and its processing method |
-
2018
- 2018-07-27 CN CN201810841947.3A patent/CN108936371A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070237865A1 (en) * | 2006-04-05 | 2007-10-11 | Robert Love | Method for manufacturing high pressure processed food products |
CN102125269A (en) * | 2010-01-13 | 2011-07-20 | 天津科技大学 | Method for producing low-temperature and low-salt ham by utilizing ultrahigh pressure |
CN103976324A (en) * | 2014-05-30 | 2014-08-13 | 辽宁禾丰食品有限公司 | Rattan pepper-flavor quick-frozen chicken breast seasoning formula and using method thereof |
CN105581273A (en) * | 2015-12-23 | 2016-05-18 | 宁夏大学 | Preparation method of Muslim low-temperature mutton ham |
CN107373420A (en) * | 2017-07-12 | 2017-11-24 | 必斐艾食品有限公司 | A kind of processing method of curry chicken |
CN108112859A (en) * | 2017-12-13 | 2018-06-05 | 成都大学 | A kind of Novel dried meat and its processing method |
Non-Patent Citations (1)
Title |
---|
杨宝进: "《现代畜产食品加工学》", 30 September 2007, 中国农业大学出版社 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111480801A (en) * | 2019-01-25 | 2020-08-04 | 上海联豪食品有限公司 | Conditioning chicken steak and preparation method thereof |
CN109924429A (en) * | 2019-04-18 | 2019-06-25 | 彭为锋 | A kind of production method of soft dried beef |
CN110110926A (en) * | 2019-05-06 | 2019-08-09 | 武汉轻工大学 | Optimization method, equipment, storage medium and the device of grain processing link |
CN110692936A (en) * | 2019-11-21 | 2020-01-17 | 安徽万礼食品有限责任公司 | Processing technology of spiced pig ears |
CN114343000A (en) * | 2021-12-07 | 2022-04-15 | 福建省亚明食品有限公司 | Method for improving quality of medium-sized dishes of spareribs |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN108936371A (en) | A kind of process that conditioning Fresh Grade Breast vacuum combination super-pressure is marinated | |
CN101861992A (en) | Method for improving gelling performance of minced Tilapia mossambica products | |
CN109259123A (en) | A kind of processing method of vacuum and low temperature preconditioned sturgeon meat products | |
KR101111590B1 (en) | A Method for Producing Instant Retort Fotiaoqiang | |
CN103340432B (en) | Method for processing normal-temperature storage type roasted goose | |
CN103610122A (en) | Production method of ready-to-eat canned abalone | |
CN110800936A (en) | Processing method of quick-frozen pork balls | |
CN109195459A (en) | The processed food for preparing the method for processed food and being prepared with same method | |
CN106376830A (en) | Preserved egg and shredded pork congee, and manufacturing method thereof | |
JP7144876B2 (en) | Non-thermal processing method for fresh bird's nest and fresh bird's nest | |
Matella et al. | Hydration, blanching and thermal processing of dry beans | |
CN107373300A (en) | A kind of popcorn chicken and its processing method | |
CN110754638A (en) | Preparation method of pre-cooked Fotiaoqiang frozen bag | |
CN105533670A (en) | Instant pleurotus cornucopiae and processing method thereof | |
CN111955674A (en) | Collagen skin jelly and preparation method thereof | |
CN107518272A (en) | A kind of modification method of quick-freezing boiled dumplings | |
CN106942631A (en) | Tasty and refreshing crisp chicken row preparation method Fresh & Tender in Texture | |
JP6782020B2 (en) | Food protein binders, food compositions containing them, and methods for producing foods using them. | |
CN110192615A (en) | A method of addition lysine pickles less salt and forms ham | |
KR101105469B1 (en) | Product of retort crab meat soup distributable at the normal temperature and method for preparation thereof | |
CN105054121A (en) | Method for tenderizing salamander meat | |
Mishra et al. | Hydration, Blanching and Thermal Processing of Dry Beans | |
CN108041477A (en) | A kind of pickled chicken claw and preparation method thereof | |
CN110897105A (en) | Processing method of minced fillet food compounded by vegetable grains and minced fillet | |
CN109007756A (en) | A method of high-quality fish sauce is prepared using leftovers of tilapia |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181207 |
|
RJ01 | Rejection of invention patent application after publication |