CN108929030A - A kind of production method of tempered glass - Google Patents

A kind of production method of tempered glass Download PDF

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Publication number
CN108929030A
CN108929030A CN201710386875.3A CN201710386875A CN108929030A CN 108929030 A CN108929030 A CN 108929030A CN 201710386875 A CN201710386875 A CN 201710386875A CN 108929030 A CN108929030 A CN 108929030A
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CN
China
Prior art keywords
parts
glass
production method
tempered glass
standing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710386875.3A
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Chinese (zh)
Inventor
徐作义
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Building Energy Saving Glass (guizhou) Co Ltd
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Building Energy Saving Glass (guizhou) Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Building Energy Saving Glass (guizhou) Co Ltd filed Critical Building Energy Saving Glass (guizhou) Co Ltd
Priority to CN201710386875.3A priority Critical patent/CN108929030A/en
Publication of CN108929030A publication Critical patent/CN108929030A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B27/00Tempering or quenching glass products
    • C03B27/012Tempering or quenching glass products by heat treatment, e.g. for crystallisation; Heat treatment of glass products before tempering by cooling
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C21/00Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
    • C03C21/001Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
    • C03C21/002Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions to perform ion-exchange between alkali ions

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  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Laminated Bodies (AREA)
  • Surface Treatment Of Glass (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)

Abstract

The invention discloses a kind of production methods of tempered glass, include the following steps:(1)Glass is put on roller-way, is sent into annealing furnace through roller-way in 600 DEG C of -610 DEG C of standing 10-15min;(2)Cool the temperature to 400 DEG C of -420 DEG C of standing 5-6min;(3)Temperature is risen into 700 DEG C of -720 DEG C of standing 5-6min;(4)By step(3)Glass from annealing furnace take out, glass surface temperature is down to 300-320 DEG C using high pressure is air-cooled;(5)By step(4)Glass be put into coating layer protecting film, be put into later potassium nitrate fused salt reaction 1-2h;(6)By step(5)It is put into 95-100 DEG C of hot water and impregnates 5-8min;(7)By step(6)Take out natural cooling to obtain the final product.The present invention has the characteristics that production yield is high, intensity is high.

Description

A kind of production method of tempered glass
Technical field
The present invention relates to a kind of glass processing field, especially a kind of production method of tempered glass.
Background technique
Tempered glass due to having many advantages, such as higher mechanical strength, excellent heatproof acute degeneration, good safety so that its It is widely used.Existing tempered glass production process mostly uses greatly the steel process using air as cooling medium, makes to be heated glass Glass carries out Quench processing by large quantity of air in a short time, to complete toughening process.In order to guarantee the performance of tempered glass, It usually requires to provide the air of very big flow in very short time, especially be become apparent when tempering is compared with thin glass, usually selected high Wind pressure, big flow high-power blower dry simultaneously.
The mode of glass tempering also has chemical tempering mode at present, and chemically toughened glass intensity connects with physical toughened glass Closely, but overlong time, low efficiency and high production cost.
Summary of the invention
The object of the present invention is to provide a kind of production methods of tempered glass.The present invention has production yield height, intensity High feature.
In order to solve the above technical problems, the present invention is implemented with the following technical solutions:
A kind of production method of tempered glass, includes the following steps:
(1)Glass is put on roller-way, is sent into annealing furnace through roller-way in 600 DEG C of -610 DEG C of standing 10-15min;
(2)Cool the temperature to 400 DEG C of -420 DEG C of standing 5-6min;
(3)Temperature is risen into 700 DEG C of -720 DEG C of standing 5-6min;
(4)By step(3)Glass from annealing furnace take out, glass surface temperature is down to 300-320 DEG C using high pressure is air-cooled;
(5)By step(4)Glass be put into coating layer protecting film, be put into later potassium nitrate fused salt reaction 1-2h;
(6)By step(5)It is put into 95-100 DEG C of hot water and impregnates 5-8min;
(7)By step(6)Take out natural cooling to obtain the final product.
In the production method of aforementioned tempered glass, the step(5)Protective film be made by following raw materials,
3-7 parts of metasilicic acid, 25-35 parts of silica,
2-5 parts of lithia, 0.5-1.5 parts of zinc oxide,
1-3 parts of disilicic acid, 30-50 parts of ethyl alcohol,
85-100 parts of distilled water.
In the production method of aforementioned tempered glass, the step(5)Protective film be made by following raw materials,
5-6 parts of metasilicic acid, 28-32 parts of silica,
2.5-4 parts of lithia, 0.8-1.2 parts of zinc oxide,
1.5-2.5 parts of disilicic acid, 32-45 parts of ethyl alcohol,
90-98 parts of distilled water.
In the production method of aforementioned tempered glass, the step(5)Protective film be made by following raw materials,
5.5 parts of metasilicic acid, 30 parts of silica,
3.5 parts of lithia, 1 part of zinc oxide,
1.8 parts of disilicic acid, 40 parts of ethyl alcohol,
95 parts of distilled water.
In the production method of tempered glass above-mentioned, the step(5)In, by step(4)Glass be put into coating one Layer protective film is put into potassium nitrate fused salt reaction 1.5h later.
Compared with prior art, the present invention is using heating, cold treatment stage by stage, to adjust glass surface stress distribution, It ensure that the flatness of tempered glass, and be coated with the effectively low machinery for increasing glass of layer protecting film by force in glass surface Glass, is put into potassium nitrate fused salt and hot water cools down by different level in addition to this, last natural cooling effectively prevent glass in life by degree It is revealed when production, improves production yield and production efficiency.
Specific embodiment:
Embodiment 1:
A kind of production method of tempered glass, includes the following steps:
(1)Glass is put on roller-way, is sent into annealing furnace through roller-way in 600 DEG C of -610 DEG C of standing 10-15min;
(2)Cool the temperature to 400 DEG C of -420 DEG C of standing 5-6min;
(3)Temperature is risen into 700 DEG C of -720 DEG C of standing 5-6min;
(4)By step(3)Glass from annealing furnace take out, glass surface temperature is down to 300-320 DEG C using high pressure is air-cooled;
(5)By step(4)Glass be put into coating layer protecting film, be put into later potassium nitrate fused salt reaction 1-2h;
(6)By step(5)It is put into 95-100 DEG C of hot water and impregnates 5-8min;
(7)By step(6)Take out natural cooling to obtain the final product.
Aforementioned step(5)Protective film be made by following raw materials,
3-7 parts of metasilicic acid, 25-35 parts of silica,
2-5 parts of lithia, 0.5-1.5 parts of zinc oxide,
1-3 parts of disilicic acid, 30-50 parts of ethyl alcohol,
85-100 parts of distilled water.
More preferably, aforementioned step(5)Protective film be made by following raw materials,
5-6 parts of metasilicic acid, 28-32 parts of silica,
2.5-4 parts of lithia, 0.8-1.2 parts of zinc oxide,
1.5-2.5 parts of disilicic acid, 32-45 parts of ethyl alcohol,
90-98 parts of distilled water.
More preferably, aforementioned step(5)Protective film be made by following raw materials,
5.5 parts of metasilicic acid, 30 parts of silica,
3.5 parts of lithia, 1 part of zinc oxide,
1.8 parts of disilicic acid, 40 parts of ethyl alcohol,
95 parts of distilled water.
More preferably, aforementioned step(5)In, by step(4)Glass be put into coating layer protecting film, be put into nitric acid later Potassium fused salt reacts 1.5h.

Claims (5)

1. a kind of production method of tempered glass, it is characterised in that:Include the following steps:
(1)Glass is put on roller-way, is sent into annealing furnace through roller-way in 600 DEG C of -610 DEG C of standing 10-15min;
(2)Cool the temperature to 400 DEG C of -420 DEG C of standing 5-6min;
(3)Temperature is risen into 700 DEG C of -720 DEG C of standing 5-6min;
(4)By step(3)Glass from annealing furnace take out, glass surface temperature is down to 300-320 DEG C using high pressure is air-cooled;
(5)By step(4)Glass be put into coating layer protecting film, be put into later potassium nitrate fused salt reaction 1-2h;
(6)By step(5)It is put into 95-100 DEG C of hot water and impregnates 5-8min;
(7)By step(6)Take out natural cooling to obtain the final product.
2. the production method of tempered glass according to claim 1, it is characterised in that:The step(5)Protective film by Following raw materials are made,
3-7 parts of metasilicic acid, 25-35 parts of silica,
2-5 parts of lithia, 0.5-1.5 parts of zinc oxide,
1-3 parts of disilicic acid, 30-50 parts of ethyl alcohol,
85-100 parts of distilled water.
3. the production method of tempered glass according to claim 2, it is characterised in that:The step(5)Protective film by Following raw materials are made,
5-6 parts of metasilicic acid, 28-32 parts of silica,
2.5-4 parts of lithia, 0.8-1.2 parts of zinc oxide,
1.5-2.5 parts of disilicic acid, 32-45 parts of ethyl alcohol,
90-98 parts of distilled water.
4. the production method of tempered glass according to claim 3, it is characterised in that:The step(5)Protective film by Following raw materials are made,
5.5 parts of metasilicic acid, 30 parts of silica,
3.5 parts of lithia, 1 part of zinc oxide,
1.8 parts of disilicic acid, 40 parts of ethyl alcohol,
95 parts of distilled water.
5. the production method of tempered glass according to claim 4, it is characterised in that:The step(5)In, by step (4)Glass be put into coating layer protecting film, be put into later potassium nitrate fused salt reaction 1.5h.
CN201710386875.3A 2017-05-26 2017-05-26 A kind of production method of tempered glass Pending CN108929030A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710386875.3A CN108929030A (en) 2017-05-26 2017-05-26 A kind of production method of tempered glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710386875.3A CN108929030A (en) 2017-05-26 2017-05-26 A kind of production method of tempered glass

Publications (1)

Publication Number Publication Date
CN108929030A true CN108929030A (en) 2018-12-04

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CN201710386875.3A Pending CN108929030A (en) 2017-05-26 2017-05-26 A kind of production method of tempered glass

Country Status (1)

Country Link
CN (1) CN108929030A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113185120A (en) * 2021-04-20 2021-07-30 常熟明阳玻璃制品有限公司 Novel super-strength toughened glass and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113185120A (en) * 2021-04-20 2021-07-30 常熟明阳玻璃制品有限公司 Novel super-strength toughened glass and preparation method thereof

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Application publication date: 20181204

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