CN108914585A - Natural silk antiseptic underwear - Google Patents
Natural silk antiseptic underwear Download PDFInfo
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- CN108914585A CN108914585A CN201810528970.7A CN201810528970A CN108914585A CN 108914585 A CN108914585 A CN 108914585A CN 201810528970 A CN201810528970 A CN 201810528970A CN 108914585 A CN108914585 A CN 108914585A
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- Prior art keywords
- silk
- antiseptic
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- underwear
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention provides a kind of natural silk antiseptic underwear, and silk is immersed in antimicrobial fluid, and the two solid-to-liquid ratio is 1:15-25;In 50-70 DEG C of immersion 1-3h of temperature;Using silk and fleece-flower root vinc fiber, the two ratio is 5-8:1, blended silk thread progress is blended to be made into fabric;Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, actual conditions are as follows:PH value 6.5-7.5, refining agent are bathed in desizing:2-4g/L, sodium bicarbonate:3-5g/L, bath raio:1:10-12, temperature:80-90 DEG C, the time:8-12min;It then arranged, be formed, drying and processing, the antiseptic underwear can be obtained.
Description
Technical field
The present invention relates to the preparation technical fields of underwear, and in particular to the preparation of natural silk antiseptic underwear.
Background technique
Existing knitted underwear clothes, most of to be made of woven, although comfortable and easy to wear, warmth retention property is poor,
And dress occurs after a long time compared with bad smell.With the improvement of living standards, people increasingly pay attention to the quality of life, it is desirable to
The living environment of the clothing and hygiene and health that have comfort can be obtained.It is higher and higher for the requirement of various textiles,
Especially safely, feel at ease, comfortably, the formation of health, health, " green " idea such as cleaning, make the antibacterial, mould proof, anti-of textile
Smelly final finishing processing is more valued by people.In life, people inevitably touch various bacteriums, true
The microorganisms such as bacterium, these microorganisms can breed rapidly under suitable external condition, and be spread the disease by modes such as contacts,
Influence the health and normal work, studying and living of people.Fiber belongs to porous material, again can shape after superposition braiding
At the layered body in countless gaps, therefore fabric is easier to absorption mushroom.Antibiotic finish is exactly to have fabric to inhibit fungus grown
Function, maintain health clothing living environment, guarantee human health.
Silk is most light most soft most thin natural fiber in nature, can easily be restored to the original state after cancelling external force, the inner tube of a tyre is not
Molding, not stuffy, purse up, homogeneous soft, can not exempt from permanently to turn over use.Silk quilt, using first-class silk, with novel fine footpath between fields
Structure makes steam free flow.In addition the distinctive ventilative, water vapour permeability of silk itself, is perceived silk more sliding, feels well not
Temperature, it is warm but not dry.Mulberry silk is mainly made of animal protein, rich in amino acid necessary to 18 kinds of human bodies, can promote skin
Cell viability, anti-vascular sclerosis, long-time service can anti-skin aging, have special antipruritic effect to certain skin diseases.Currently, existing
There is the multi-functional underwear of comprehensive utilization natural silk preparation in technology not yet to have been reported that.
Summary of the invention
The purpose of the present invention is provide a kind of natural silkworm for underwear preparation process above shortcomings in the prior art
Silk antiseptic underwear is aided with other compositions and obtains multi-functional underwear, met underwear in people based on natural silk
The current demand of health care.
In order to achieve the above objectives, the technical solution adopted by the present invention is that:
Natural silk antiseptic underwear, includes the following steps:
S1:Silk is immersed in antimicrobial fluid, the two solid-to-liquid ratio is 1:15-25;In 50-70 DEG C of immersion 1-3h of temperature;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 5-8:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 6.5-7.5, refining agent are bathed in desizing:2-4g/L, sodium bicarbonate:3-5g/L, bath raio:1:10-12, temperature:
80-90 DEG C, the time:8-12min;
S4:It then arranged, be formed, drying and processing, the antiseptic underwear can be obtained.
Preferably, the configuration process of antimicrobial fluid is as follows in step S1:Take 20-30 parts of glycerol, 10-20 parts of allyl glycidyls sweet
Oily ether, 3-7 part ammonium citrate, 5-10 parts of radix scutellariaes, 3-8 portions of Cortex Phellodendris, 4-8 portions of folium artemisiae argyis and 30-60 parts of distilled water increase temperature extremely
100-120 DEG C, 2-4h is stirred, supernatant antimicrobial fluid is then filtered to obtain;Both silk and antimicrobial fluid solid-to-liquid ratio are 1:20;In temperature 55
DEG C impregnate 2h.
Preferably, the configuration process of antimicrobial fluid is as follows:Take 25 parts of glycerol, 15 parts of allyl glycidyl ethers, 5 parts of citric acids
Ammonium, 7 parts of radix scutellariaes, 6 portions of Cortex Phellodendris, 5 portions of folium artemisiae argyis and 45 parts of distilled water increase temperature to 110 DEG C, stir 3h, then filter to obtain supernatant
Antimicrobial fluid.
Preferably, both silk and the fleece-flower root vinc fiber ratio are 6 in step S2:1.
Preferably, pH value 7, refining agent are bathed in desizing described in step S3:3g/L, sodium bicarbonate:4g/L, bath raio:1:11, temperature
Degree:85 DEG C, the time:10min.
Preferably, arrangement process described in step S4 is as follows:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with
Mass ratio 2-3:1,3-5h is reacted at 150-160 DEG C, finishing agent is prepared;After embryo cloth is added, control bath raio is 1:14-
16, in 20-30 DEG C of processing 30-40min.
Preferably, the arrangement process is as follows:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio
2.3:1,3.5h is reacted at 155 DEG C, finishing agent is prepared;After embryo cloth is added, control bath raio is 1:15, it is handled at 25 DEG C
35min。
Preferably, sizing, drying course described in step S4 are as follows:In 115 DEG C of processing 40s of temperature.
Beneficial effect:
The preparation of natural silk antiseptic underwear of the present invention, first configures suitable antimicrobial fluid to silk antimicrobial treatment,
It is then blended at embryo cloth with fleece-flower root vinc fiber, arrange by refining, finishing agent, be formed, dry etc., it obtains having silk, resist
The functions such as bacterium, tranquilizing soporific can satisfy the plurality kinds of health care demand of people.
Specific embodiment
Further illustrate that the present invention, following embodiments are merely to illustrate the present invention below in conjunction with following embodiments, and
The unrestricted present invention.
Embodiment 1
S1:Take 20 parts of glycerol, 10 parts of allyl glycidyl ethers, 3 parts of ammonium citrates, 5 parts of radix scutellariaes, 3 portions of Cortex Phellodendris, 4 portions of folium artemisiae argyis and
30 parts of distilled water increase temperature to 100 DEG C, stir 2h, then filter to obtain supernatant antimicrobial fluid;Silk is immersed in antimicrobial fluid, two
Person's solid-to-liquid ratio is 1:15;1h is impregnated in temperature 50 C;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 5:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 6.5, refining agent are bathed in desizing:2g/L, sodium bicarbonate:3g/L, bath raio:1:10, temperature:80 DEG C, the time:
8min;
S4:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 2:1,3h is reacted at 150 DEG C, is prepared into
To finishing agent;After embryo cloth is added, control bath raio is 1:14, in 20 DEG C of processing 30min;In 115 DEG C of processing 40s of temperature.
Embodiment 2
S1:Take 30 parts of glycerol, 20 parts of allyl glycidyl ethers, 7 parts of ammonium citrates, 10 parts of radix scutellariaes, 8 portions of Cortex Phellodendris, 8 portions of folium artemisiae argyis and
60 parts of distilled water increase temperature to 120 DEG C, stir 4h, then filter to obtain supernatant antimicrobial fluid;Silk is immersed in antimicrobial fluid, two
Person's solid-to-liquid ratio is 1:25;3h is impregnated in temperature 70 C;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 8:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 7.5, refining agent are bathed in desizing:4g/L, sodium bicarbonate:5g/L, bath raio:1:12, temperature:90 DEG C, the time:
12min;
S4:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 3:1,5h is reacted at 160 DEG C, is prepared into
To finishing agent;After embryo cloth is added, control bath raio is 1:16, in 30 DEG C of processing 40min;In 115 DEG C of processing 40s of temperature.
Embodiment 3
S1:Take 22 parts of glycerol, 14 parts of allyl glycidyl ethers, 4 parts of ammonium citrates, 7 parts of radix scutellariaes, 4 portions of Cortex Phellodendris, 5 portions of folium artemisiae argyis and
40 parts of distilled water increase temperature to 105 DEG C, stir 2.5h, then filter to obtain supernatant antimicrobial fluid;Silk is immersed in antimicrobial fluid,
The two solid-to-liquid ratio is 1:18;In 55 DEG C of immersion 1.5h of temperature;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 6:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 6.8, refining agent are bathed in desizing:2.5g/L, sodium bicarbonate:3.5g/L, bath raio:1:10, temperature:85 DEG C, when
Between:10min;
S4:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 2.5:1,3.5h is reacted at 152 DEG C, is made
It is standby to obtain finishing agent;After embryo cloth is added, control bath raio is 1:15, in 23 DEG C of processing 35min;In 115 DEG C of processing 40s of temperature.
Embodiment 4
S1:Take 26 parts of glycerol, 18 parts of allyl glycidyl ethers, 6 parts of ammonium citrates, 9 parts of radix scutellariaes, 7 portions of Cortex Phellodendris, 7 portions of folium artemisiae argyis and
50 parts of distilled water increase temperature to 115 DEG C, stir 3.5h, then filter to obtain supernatant antimicrobial fluid;Silk is immersed in antimicrobial fluid,
The two solid-to-liquid ratio is 1:23;In 65 DEG C of immersion 2.5h of temperature;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 8:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 7.2, refining agent are bathed in desizing:3.5g/L, sodium bicarbonate:4.5g/L, bath raio:1:12, temperature:90 DEG C, when
Between:12min;
S4:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 3.0:1,4h is reacted at 158 DEG C, is prepared
Obtain finishing agent;After embryo cloth is added, control bath raio is 1:16, in 27 DEG C of processing 40min;In 115 DEG C of processing 40s of temperature.
Embodiment 5
S1:Take 25 parts of glycerol, 15 parts of allyl glycidyl ethers, 5 parts of ammonium citrates, 7 parts of radix scutellariaes, 6 portions of Cortex Phellodendris, 5 portions of folium artemisiae argyis and
45 parts of distilled water increase temperature to 110 DEG C, stir 3h, then filter to obtain supernatant antimicrobial fluid;Silk is immersed in antimicrobial fluid, two
Person's solid-to-liquid ratio is 1:20;In 55 DEG C of immersion 2h of temperature;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 6:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 7, refining agent are bathed in desizing:3g/L, sodium bicarbonate:4g/L, bath raio:1:11, temperature:85 DEG C, the time:
10min;
S4:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 2.3:1,3.5h is reacted at 155 DEG C, is made
It is standby to obtain finishing agent;After embryo cloth is added, control bath raio is 1:15, in 25 DEG C of processing 35min;In 115 DEG C of processing 40s of temperature.
The foregoing is merely better embodiment of the invention, protection scope of the present invention is not with above embodiment
Limit, as long as those of ordinary skill in the art's equivalent modification or variation made by disclosure according to the present invention, should all be included in power
In the protection scope recorded in sharp claim.
Claims (8)
1. natural silk antiseptic underwear, which is characterized in that include the following steps:
S1:Silk is immersed in antimicrobial fluid, the two solid-to-liquid ratio is 1:15-25;In 50-70 DEG C of immersion 1-3h of temperature;
S2:Using silk and fleece-flower root vinc fiber, the two ratio is 5-8:1, blended silk thread progress is blended to be made into fabric;
S3:Embryo cloth is subjected to starching and oiling treatment;Desizing refining processing is carried out using low bath raio high-pressure injection overflow machine, specifically
Condition is as follows:PH value 6.5-7.5, refining agent are bathed in desizing:2-4g/L, sodium bicarbonate:3-5g/L, bath raio:1:10-12, temperature:
80-90 DEG C, the time:8-12min;
S4:It then arranged, be formed, drying and processing, the antiseptic underwear can be obtained.
2. natural silk antiseptic underwear according to claim 1, which is characterized in that antimicrobial fluid matches in step S1
It is as follows to set process:Take 20-30 parts of glycerol, 10-20 parts of allyl glycidyl ethers, 3-7 parts of ammonium citrates, 5-10 parts of radix scutellariaes, 3-8
Part Cortex Phellodendri, 4-8 portion folium artemisiae argyis and 30-60 part distilled water, increase temperature to 100-120 DEG C, stirring 2-4h, then filter supernatant resists
Bacterium solution;Both silk and antimicrobial fluid solid-to-liquid ratio are 1:20;In 55 DEG C of immersion 2h of temperature.
3. natural silk antiseptic underwear according to claim 2, which is characterized in that the configuration process of antimicrobial fluid is such as
Under:Take 25 parts of glycerol, 15 parts of allyl glycidyl ethers, 5 parts of ammonium citrates, 7 parts of radix scutellariaes, 6 portions of Cortex Phellodendris, 5 portions of folium artemisiae argyis and 45 parts
Distilled water increases temperature to 110 DEG C, stirs 3h, then filter to obtain supernatant antimicrobial fluid.
4. natural silk antiseptic underwear according to claim 1, which is characterized in that silk and what head in step S2
Both black vinc fibers ratio is 6:1.
5. natural silk antiseptic underwear according to claim 1, which is characterized in that the bath of desizing described in step S3
PH value 7, refining agent:3g/L, sodium bicarbonate:4g/L, bath raio:1:11, temperature:85 DEG C, the time:10min.
6. natural silk antiseptic underwear according to claim 1, which is characterized in that arranged described in step S4
Journey is as follows:By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 2-3:1,3- is reacted at 150-160 DEG C
Finishing agent is prepared in 5h;After embryo cloth is added, control bath raio is 1:14-16, in 20-30 DEG C of processing 30-40min.
7. natural silk antiseptic underwear according to claim 6, which is characterized in that the arrangement process is as follows:
By polyethylene glycol and 5- norbornene -2,3- dicarboxylic anhydride with mass ratio 2.3:1,3.5h is reacted at 155 DEG C, is prepared whole
Manage agent;After embryo cloth is added, control bath raio is 1:15, in 25 DEG C of processing 35min.
8. natural silk antiseptic underwear according to claim 1, which is characterized in that sizing described in step S4,
Drying course is as follows:In 115 DEG C of processing 40s of temperature.
Priority Applications (1)
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CN201810528970.7A CN108914585A (en) | 2018-05-29 | 2018-05-29 | Natural silk antiseptic underwear |
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CN201810528970.7A CN108914585A (en) | 2018-05-29 | 2018-05-29 | Natural silk antiseptic underwear |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112832028A (en) * | 2021-02-05 | 2021-05-25 | 浙江红督服饰有限公司 | Preparation method of natural silk antibacterial cloth |
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2018
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112832028A (en) * | 2021-02-05 | 2021-05-25 | 浙江红督服饰有限公司 | Preparation method of natural silk antibacterial cloth |
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