CN108908923A - A kind of polyfluortetraethylene pipe technique - Google Patents

A kind of polyfluortetraethylene pipe technique Download PDF

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Publication number
CN108908923A
CN108908923A CN201810739359.9A CN201810739359A CN108908923A CN 108908923 A CN108908923 A CN 108908923A CN 201810739359 A CN201810739359 A CN 201810739359A CN 108908923 A CN108908923 A CN 108908923A
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China
Prior art keywords
sintering
temperature
polyfluortetraethylene pipe
mixing
controlled
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CN201810739359.9A
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Inventor
周志国
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Dongguan Yu Chen Insulation Material Co Ltd
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Dongguan Yu Chen Insulation Material Co Ltd
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Priority to CN201810739359.9A priority Critical patent/CN108908923A/en
Publication of CN108908923A publication Critical patent/CN108908923A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C61/00Shaping by liberation of internal stresses; Making preforms having internal stresses; Apparatus therefor
    • B29C61/06Making preforms having internal stresses, e.g. plastic memory
    • B29C61/08Making preforms having internal stresses, e.g. plastic memory by stretching tubes

Abstract

The invention discloses a kind of polyfluortetraethylene pipe techniques, include the following steps:Mixing:PTFE and extrusion aid are mixed by mixing machine, incorporation time 10min-20min, mixing temperature is no more than 19 DEG C;Storage:It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;It is preforming:By preforming mechanism embryo, compression speed 50mm/min, pressure is controlled in 0-3MPa;It pushes:It is pushed by upright push machine, material chamber temperature when pushing is controlled at 30 DEG C -50 DEG C.Polyfluortetraethylene pipe produced by the invention has the characteristic of heat shrinkable, therefore the appearance of other workpiece can be closely coated on, the workpiece is set to have corrosion-resistant, electrical isolation and antistick characteristic, it can be widely used for the industry such as electrical, chemical industry, machinery, printing, FIFE heat-shrinkable tube maximum contraction rate is greater than 75%, the problem of polyfluortetraethylene pipe heat shrinkable for solving prior art production is poor, can not effectively improve the corrosion-resistant of workpiece, electrical insulating property and antistick characteristic.

Description

A kind of polyfluortetraethylene pipe technique
Technical field
The present invention relates to technical field of plastic, specially a kind of polyfluortetraethylene pipe technique.
Background technique
Polytetrafluoroethylene (PTFE) is referred to as " kings of plastics ", with colourless, nontoxic, temperature resistant range is wide, chemical inertness and friction are A variety of excellent properties such as small are counted, are become now centered on the industry such as automobile, national defence, machinery, chemical industry, electronics, building The all indispensable important materials of all branchs of industry.
Polyfluortetraethylene pipe is to make steel pipe and plastics using special processing process using the plunger work extruding pipe of high quality Pipe is combined closely, and positive pressure 1.6Mpa, negative pressure can be born:77Kpa;Can in -60 DEG C~+260 DEG C normal use, have reliable Excellent corrosion resistance.The strong corrosive air-liquid body under high temperature is conveyed, this is that other pipeline institutes are irreplaceable.
A kind of polytetrafluoroethylhose hose manufacturing process of the disclosure of the invention of Patent No. CN102416701A, it is characterised in that Include the following steps:1)Ingredient;1.1)With the polyflon material after screening, by weight 1000g:200g polytetrafluoroethyl-ne The ratio of olefine resin and 200 ﹟ gasoline carries out mixing, and parks 24 hours;1.2)Also ingredient can be rocked by hand and makes the tree of immersion oil Rouge particle is uniformly mixed;1.3)Mixed ingredient is put on blender, revolving speed be 0~100r/min, rotate 20 minutes, such as There is viscosity phenomenon, can have a power failure within 10 minutes under gently vibration, be further continued for mixing to the stipulated time;1.4)It is small that 48 are placed at 25 ± 5 DEG C of room temperature When, in case slug press.The polyfluortetraethylene pipe heat shrinkable of prior art production is poor, can not effectively improve the corrosion resistant of workpiece Erosion, electrical insulating property and antistick characteristic, for this purpose, it is proposed that a kind of polyfluortetraethylene pipe technique.
Summary of the invention
The purpose of the present invention is to provide a kind of polyfluortetraethylene pipe techniques, to solve mentioned above in the background art ask Topic.
To achieve the above object, the present invention provides the following technical solutions:A kind of polyfluortetraethylene pipe technique, including walk as follows Suddenly:
(1)Mixing:PTFE and extrusion aid are mixed by mixing machine, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C;
(2)Storage:It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;
(3)It is preforming:By preforming mechanism embryo, compression speed 50mm/min, pressure is controlled in 0-3MPa;
(4)It pushes:It is pushed by upright push machine, material chamber temperature control when pushing is at 30 DEG C -50 DEG C, die temperature control System is at 50 DEG C -60 DEG C;
(5)It is dry:The material after pushing is dried at 210 DEG C or less by dry and sintering furnace, drying time control exists 2h-3h;
(6)Sintering:After the completion of drying, dry and sintering furnace carries out indirect sintering, 60 DEG C/h of heating rate, 375 DEG C of ± 5 DEG C of heat preservations 4h, then continuous sintering are cooled down after the completion of sintering;
(7)Heat treatment:The process being quenched after the good pipe of drying and sintering is further sufficiently sintered at high temperature again, temperature 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid;
(8)Inflation:At 310 DEG C or so, 0.98MPa or less compressed gas, blow-up ratio 200%- are filled with by inflation machine 400%;
(9)It is cooling:Finished product is obtained through supercooling after the completion of inflation, cooling zone temperature is controlled at 300 DEG C or less.
Preferably, the step(1)The group of the formula number of middle teflon rod is divided into:Dispersion PTFE resin 100 parts, 20-22 parts of extrusion aid.
Preferably, the step(4)Middle pushing rate becomes smaller with the increase of caliber, accelerates with becoming smaller for wall thickness.
Preferably, the step(5)At 100 DEG C -250 DEG C, preheating zone temperature is controlled 250 for middle dry section temperature control DEG C -330 DEG C, sintering zone temperature is controlled at 380 DEG C -420 DEG C.
Preferably, the dielectric strength of the polyfluortetraethylene pipe is 37-50Kv/mm, and shrinkage temperature is greater than 330 DEG C, specific gravity It is 2.15 × 103kg/m3
Preferably, the polyfluortetraethylene pipe tensile strength of the production is 19.6MPa, and specific elongation rate is 250%.
Preferably, the partial size of the dispersion PTFE resin is 500 μm, and apparent density 0.45g/ml-0.55g/ml is helped crowded No. 200 or No. 260 solvent naphthas are selected in agent.
Compared with prior art, the beneficial effects of the invention are as follows:The present invention is processed into using dispersion P1 resin, principle It is that FIFE work in-process is allowed to freeze by forced high-elastic deformation, this deformation is generated after stress with invertibity, low temperature, if weight Newly heating the forced high-elastic deformation freezed will fade away and be returned to original state, and the polyfluortetraethylene pipe of production has heated The characteristic of contraction, therefore can closely be coated on the appearance of other workpiece makes the workpiece have corrosion-resistant, electrical isolation and anti-sticking Property, it can be widely used for the industry such as electrical, chemical industry, machinery, printing, FIFE heat-shrinkable tube maximum contraction rate is greater than 75%, solves The polyfluortetraethylene pipe heat shrinkable of prior art production is poor, can not effectively improve the corrosion-resistant of workpiece, electrical insulating property and prevent The problem of viscosity.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
The present invention provides a kind of technical solution:A kind of polyfluortetraethylene pipe technique, includes the following steps:
(1)Mixing:PTFE and extrusion aid are mixed by mixing machine, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C;
(2)Storage:It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;
(3)It is preforming:By preforming mechanism embryo, compression speed 50mm/min, pressure is controlled in 0-3MPa;
(4)It pushes:It is pushed by upright push machine, material chamber temperature control when pushing is at 30 DEG C -50 DEG C, die temperature control System is at 50 DEG C -60 DEG C;
(5)It is dry:The material after pushing is dried at 210 DEG C or less by dry and sintering furnace, drying time control exists 2h-3h;
(6)Sintering:After the completion of drying, dry and sintering furnace carries out indirect sintering, 60 DEG C/h of heating rate, 375 DEG C of ± 5 DEG C of heat preservations 4h, then continuous sintering are cooled down after the completion of sintering;
(7)Heat treatment:The process being quenched after the good pipe of drying and sintering is further sufficiently sintered at high temperature again, temperature 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid;
(8)Inflation:At 310 DEG C or so, 0.98MPa or less compressed gas, blow-up ratio 200%- are filled with by inflation machine 400%;
(9)It is cooling:Finished product is obtained through supercooling after the completion of inflation, cooling zone temperature is controlled at 300 DEG C or less.
Embodiment one:
PTFE and extrusion aid are mixed by mixing machine first, incorporation time 10min-20min, mixing temperature is no more than 19℃;It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;By preforming mechanism embryo, compression speed is 50mm/min, pressure are controlled in 0-3MPa;Then it is pushed by upright push machine, material chamber temperature when pushing is controlled 30 DEG C -50 DEG C, die temperature is controlled at 50 DEG C -60 DEG C;Pass through dry and sintering furnace after pushing at 210 DEG C or less to the object after pushing Material is dried, and drying time controls in 2h-3h;After the completion of drying, dry and sintering furnace carries out indirect sintering, heating rate 60 DEG C/h, 375 DEG C of ± 5 DEG C of heat preservation 4h, then continuous sintering, sintering after the completion of cooled down;By pipe that drying and sintering is good after sintering The process that son is quenched after being further sufficiently sintered at high temperature again, 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid of temperature;After heat treatment 310 DEG C or so, 0.98MPa or less compressed gas, blow-up ratio 200%-400% are filled with by inflation machine;Inflation passes through after completing Supercooling obtains finished product, and cooling zone temperature is controlled at 300 DEG C or less.
Embodiment two:
In example 1, following processes are added:
Step(1)The group of the formula number of middle teflon rod is divided into:100 parts of dispersion PTFE resin, extrusion aid 20- 22 parts.
PTFE and extrusion aid are mixed by mixing machine first, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C, wherein the group of the formula number of teflon rod is divided into:100 parts of dispersion PTFE resin, extrusion aid 20- 22 parts;It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;By preforming mechanism embryo, compression speed is 50mm/min, pressure are controlled in 0-3MPa;Then it is pushed by upright push machine, material chamber temperature when pushing is controlled 30 DEG C -50 DEG C, die temperature is controlled at 50 DEG C -60 DEG C;Pass through dry and sintering furnace after pushing at 210 DEG C or less to the object after pushing Material is dried, and drying time controls in 2h-3h;After the completion of drying, dry and sintering furnace carries out indirect sintering, heating rate 60 DEG C/h, 375 DEG C of ± 5 DEG C of heat preservation 4h, then continuous sintering, sintering after the completion of cooled down;By pipe that drying and sintering is good after sintering The process that son is quenched after being further sufficiently sintered at high temperature again, 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid of temperature;After heat treatment 310 DEG C or so, 0.98MPa or less compressed gas, blow-up ratio 200%-400% are filled with by inflation machine;Inflation passes through after completing Supercooling obtains finished product, and cooling zone temperature is controlled at 300 DEG C or less.
Embodiment three:
In example 2, following processes are added:
Step(4)Middle pushing rate becomes smaller with the increase of caliber, accelerates with becoming smaller for wall thickness.
PTFE and extrusion aid are mixed by mixing machine first, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C, wherein the group of the formula number of teflon rod is divided into:100 parts of dispersion PTFE resin, extrusion aid 20- 22 parts;It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;By preforming mechanism embryo, compression speed is 50mm/min, pressure are controlled in 0-3MPa;Then it is pushed by upright push machine, material chamber temperature when pushing is controlled 30 DEG C -50 DEG C, die temperature is controlled at 50 DEG C -60 DEG C, is pushed rate and is become smaller with the increase of caliber, with becoming smaller for wall thickness plus Fastly;The material after pushing is dried at 210 DEG C or less by dry and sintering furnace after pushing, drying time controls in 2h- 3h;After the completion of drying, dry and sintering furnace carries out indirect sintering, heating rate 60 DEG C/h, then 375 DEG C of ± 5 DEG C of heat preservation 4h connect Continuous sintering, is cooled down after the completion of sintering;The further sufficiently sintering at high temperature again by the good pipe of drying and sintering after sintering The process being quenched afterwards, 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid of temperature;At 310 DEG C or so after heat treatment, it is filled with by inflation machine 0.98MPa or less compressed gas, blow-up ratio 200%-400%;Finished product, cooling zone temperature are obtained through supercooling after the completion of inflation Control is at 300 DEG C or less.
Example IV:
In the third embodiment, following processes are added:
Step(5)The control of middle dry section temperature is at 100 DEG C -250 DEG C, and temperature control in preheating zone is at 250 DEG C -330 DEG C, sintering zone temperature Degree control is at 380 DEG C -420 DEG C.
PTFE and extrusion aid are mixed by mixing machine first, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C, wherein the group of the formula number of teflon rod is divided into:100 parts of dispersion PTFE resin, extrusion aid 20- 22 parts;It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;By preforming mechanism embryo, compression speed is 50mm/min, pressure are controlled in 0-3MPa;Then it is pushed by upright push machine, material chamber temperature when pushing is controlled 30 DEG C -50 DEG C, die temperature is controlled at 50 DEG C -60 DEG C, is pushed rate and is become smaller with the increase of caliber, with becoming smaller for wall thickness plus Fastly;The material after pushing is dried at 210 DEG C or less by dry and sintering furnace after pushing, drying time controls in 2h- 3h, the control of dry section temperature is at 100 DEG C -250 DEG C, and at 250 DEG C -330 DEG C, temperature control in sintering zone exists the control of preheating zone temperature 380℃-420℃;After the completion of drying, dry and sintering furnace carries out indirect sintering, 60 DEG C/h of heating rate, 375 DEG C of ± 5 DEG C of heat preservations 4h, then continuous sintering are cooled down after the completion of sintering;It is after sintering that the good pipe of drying and sintering is further at high temperature again The process being sufficiently quenched after sintering, 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid of temperature;At 310 DEG C or so after heat treatment, pass through inflation machine It is filled with 0.98MPa or less compressed gas, blow-up ratio 200%-400%;Finished product, cooling zone are obtained through supercooling after the completion of inflation Temperature is controlled at 300 DEG C or less.
Embodiment five:
In example IV, following processes are added:
The dielectric strength of polyfluortetraethylene pipe is 37-50Kv/mm, and shrinkage temperature is greater than 330 DEG C, and specific gravity is 2.15 × 103kg/ m3;The polyfluortetraethylene pipe tensile strength of production is 19.6MPa, and specific elongation rate is 250%.
PTFE and extrusion aid are mixed by mixing machine first, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C, wherein the group of the formula number of teflon rod is divided into:100 parts of dispersion PTFE resin, extrusion aid 20- 22 parts;It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;By preforming mechanism embryo, compression speed is 50mm/min, pressure are controlled in 0-3MPa;Then it is pushed by upright push machine, material chamber temperature when pushing is controlled 30 DEG C -50 DEG C, die temperature is controlled at 50 DEG C -60 DEG C, is pushed rate and is become smaller with the increase of caliber, with becoming smaller for wall thickness plus Fastly;The material after pushing is dried at 210 DEG C or less by dry and sintering furnace after pushing, drying time controls in 2h- 3h, the control of dry section temperature is at 100 DEG C -250 DEG C, and at 250 DEG C -330 DEG C, temperature control in sintering zone exists the control of preheating zone temperature 380℃-420℃;After the completion of drying, dry and sintering furnace carries out indirect sintering, 60 DEG C/h of heating rate, 375 DEG C of ± 5 DEG C of heat preservations 4h, then continuous sintering are cooled down after the completion of sintering;It is after sintering that the good pipe of drying and sintering is further at high temperature again The process being sufficiently quenched after sintering, 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid of temperature;At 310 DEG C or so after heat treatment, pass through inflation machine It is filled with 0.98MPa or less compressed gas, blow-up ratio 200%-400%;Finished product, cooling zone are obtained through supercooling after the completion of inflation Temperature is controlled at 300 DEG C or less;The dielectric strength of polyfluortetraethylene pipe is 37-50Kv/mm, and shrinkage temperature is greater than 330 DEG C, specific gravity It is 2.15 × 103kg/m3;The polyfluortetraethylene pipe tensile strength of production is 19.6MPa, and specific elongation rate is 250%.
Embodiment six:
In embodiment five, following processes are added:
The partial size of dispersion PTFE resin be 500 μm, apparent density 0.45g/ml-0.55g/ml, extrusion aid select No. 200 or No. 260 solvent naphthas.
PTFE and extrusion aid are mixed by mixing machine first, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C, wherein the group of the formula number of teflon rod is divided into:100 parts of dispersion PTFE resin, extrusion aid 20- 22 parts, the partial size of dispersion PTFE resin is 500 μm, apparent density 0.45g/ml-0.55g/ml, extrusion aid select No. 200 or No. 260 solvent naphthas;It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;Pass through preforming mechanism embryo, compression Rate is 50mm/min, and pressure is controlled in 0-3MPa;Then it is pushed by upright push machine, material chamber temperature control when pushing At 30 DEG C -50 DEG C, die temperature is controlled at 50 DEG C -60 DEG C system, is pushed rate and is become smaller with the increase of caliber, with becoming smaller for wall thickness And accelerate;The material after pushing is dried at 210 DEG C or less by dry and sintering furnace after pushing, drying time control exists 2h-3h, the control of dry section temperature is at 100 DEG C -250 DEG C, and at 250 DEG C -330 DEG C, sintering zone temperature controls the control of preheating zone temperature At 380 DEG C -420 DEG C;After the completion of drying, dry and sintering furnace carries out indirect sintering, 60 DEG C/h of heating rate, 375 DEG C of ± 5 DEG C of guarantors Warm 4h, then continuous sintering are cooled down after the completion of sintering;By the good pipe of drying and sintering again at high temperature into one after sintering The process being quenched after step sufficiently sintering, 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid of temperature;At 310 DEG C or so after heat treatment, pass through inflation Machine is filled with 0.98MPa or less compressed gas, blow-up ratio 200%-400%;Finished product is obtained through supercooling after the completion of inflation, it is cooling Area's temperature is controlled at 300 DEG C or less;The dielectric strength of polyfluortetraethylene pipe is 37-50Kv/mm, and shrinkage temperature is greater than 330 DEG C, than Weight is 2.15 × 103kg/m3;The polyfluortetraethylene pipe tensile strength of production is 19.6MPa, and specific elongation rate is 250%.
The present invention is processed into using dispersion P1 resin, and principle is that FIFE work in-process is forced high by generating after stress Deformation is played, this deformation has invertibity, and low temperature is allowed to freeze, if reheating the forced high-elastic deformation freezed will gradually disappear Original state is lost and is returned to, the polyfluortetraethylene pipe of production has the characteristic of heat shrinkable, therefore can closely be coated on other The appearance of workpiece makes the workpiece have corrosion-resistant, electrical isolation and antistick characteristic, can be widely used for electrical, chemical industry, machinery, printing etc. Industry, FIFE heat-shrinkable tube maximum contraction rate are greater than 75%, solve the polyfluortetraethylene pipe heat shrinkable of prior art production The problem of property is poor, can not effectively improve the corrosion-resistant of workpiece, electrical insulating property and antistick characteristic.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (7)

1. a kind of polyfluortetraethylene pipe technique, it is characterised in that:Include the following steps:
(1)Mixing:PTFE and extrusion aid are mixed by mixing machine, incorporation time 10min-20min, mixing temperature is not More than 19 DEG C;
(2)Storage:It is stored 24 hours or more under conditions of 25 DEG C -30 DEG C after mixing;
(3)It is preforming:By preforming mechanism embryo, compression speed 50mm/min, pressure is controlled in 0-3MPa;
(4)It pushes:It is pushed by upright push machine, material chamber temperature control when pushing is at 30 DEG C -50 DEG C, die temperature control System is at 50 DEG C -60 DEG C;
(5)It is dry:The material after pushing is dried at 210 DEG C or less by dry and sintering furnace, drying time control exists 2h-3h;
(6)Sintering:After the completion of drying, dry and sintering furnace carries out indirect sintering, 60 DEG C/h of heating rate, 375 DEG C of ± 5 DEG C of heat preservations 4h, then continuous sintering are cooled down after the completion of sintering;
(7)Heat treatment:The process being quenched after the good pipe of drying and sintering is further sufficiently sintered at high temperature again, temperature 390 DEG C ± 2 DEG C, -5 DEG C of coolant liquid;
(8)Inflation:At 310 DEG C or so, 0.98MPa or less compressed gas, blow-up ratio 200%- are filled with by inflation machine 400%;
(9)It is cooling:Finished product is obtained through supercooling after the completion of inflation, cooling zone temperature is controlled at 300 DEG C or less.
2. a kind of polyfluortetraethylene pipe technique according to claim 1, it is characterised in that:The step(1)Middle polytetrafluoro The group of the formula number of ethylene stick is divided into:100 parts of dispersion PTFE resin, 20-22 parts of extrusion aid.
3. a kind of polyfluortetraethylene pipe technique according to claim 1, it is characterised in that:The step(4)Middle pushing speed Rate becomes smaller with the increase of caliber, accelerates with becoming smaller for wall thickness.
4. a kind of polyfluortetraethylene pipe technique according to claim 1, it is characterised in that:The step(5)Middle dry section Temperature control is at 100 DEG C -250 DEG C, and at 250 DEG C -330 DEG C, sintering zone temperature is controlled at 380 DEG C -420 the control of preheating zone temperature ℃。
5. a kind of polyfluortetraethylene pipe technique according to claim 1, it is characterised in that:The polyfluortetraethylene pipe it is exhausted Edge intensity is 37-50Kv/mm, and shrinkage temperature is greater than 330 DEG C, and specific gravity is 2.15 × 103kg/m3
6. a kind of polyfluortetraethylene pipe technique according to claim 1, it is characterised in that:The polytetrafluoroethylene (PTFE) of the production Pipe tensile strength is 19.6MPa, and specific elongation rate is 250%.
7. a kind of polyfluortetraethylene pipe technique according to claim 2, it is characterised in that:The grain of the dispersion PTFE resin Diameter is 500 μm, apparent density 0.45g/ml-0.55g/ml, and extrusion aid selects No. 200 or No. 260 solvent naphthas.
CN201810739359.9A 2018-07-06 2018-07-06 A kind of polyfluortetraethylene pipe technique Pending CN108908923A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113480817A (en) * 2021-06-11 2021-10-08 湖北宇辰新材料有限公司 Preparation method of polytetrafluoroethylene rod

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1267251A (en) * 1997-08-21 2000-09-20 大金工业株式会社 Polytetrafluoroethylene tubing and extruder for production therefor
CA2436308A1 (en) * 2000-12-26 2002-07-04 Boston Scientific Limited Method of reducing the wall thickness of a ptfe tube and product formed thereby
CN1154798C (en) * 1998-12-24 2004-06-23 吉列恩·惠特沃斯 PTFE tube
CN102276950A (en) * 2011-05-18 2011-12-14 湖州松华橡塑有限公司 Polytetrafluoroethylene (PTFE) composite material sealing ring with high temperature resistance and low creep, and preparation method thereof
CN107263884A (en) * 2017-05-05 2017-10-20 江阴市江南氟塑有限公司 A kind of super large caliber PTFE tube part paste extrusion preparation method and its extrusion equipment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1267251A (en) * 1997-08-21 2000-09-20 大金工业株式会社 Polytetrafluoroethylene tubing and extruder for production therefor
CN1154798C (en) * 1998-12-24 2004-06-23 吉列恩·惠特沃斯 PTFE tube
CA2436308A1 (en) * 2000-12-26 2002-07-04 Boston Scientific Limited Method of reducing the wall thickness of a ptfe tube and product formed thereby
CN102276950A (en) * 2011-05-18 2011-12-14 湖州松华橡塑有限公司 Polytetrafluoroethylene (PTFE) composite material sealing ring with high temperature resistance and low creep, and preparation method thereof
CN107263884A (en) * 2017-05-05 2017-10-20 江阴市江南氟塑有限公司 A kind of super large caliber PTFE tube part paste extrusion preparation method and its extrusion equipment

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
徐下忠,吾良福,王文理,方晓琴: "聚四氟乙烯主要成型制品及生产工艺", 《塑料科技》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113480817A (en) * 2021-06-11 2021-10-08 湖北宇辰新材料有限公司 Preparation method of polytetrafluoroethylene rod

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Application publication date: 20181130