CN108899750A - A kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel and preparation method thereof - Google Patents

A kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel and preparation method thereof Download PDF

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CN108899750A
CN108899750A CN201810695455.8A CN201810695455A CN108899750A CN 108899750 A CN108899750 A CN 108899750A CN 201810695455 A CN201810695455 A CN 201810695455A CN 108899750 A CN108899750 A CN 108899750A
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knot
hollow micro
whispering
gallery
resonant cavity
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CN108899750B (en
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董国平
欧阳天昶
康世亮
蔡振禄
邱建荣
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South China University of Technology SCUT
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01SDEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
    • H01S3/00Lasers, i.e. devices using stimulated emission of electromagnetic radiation in the infrared, visible or ultraviolet wave range
    • H01S3/05Construction or shape of optical resonators; Accommodation of active medium therein; Shape of active medium
    • H01S3/06Construction or shape of active medium
    • H01S3/063Waveguide lasers, i.e. whereby the dimensions of the waveguide are of the order of the light wavelength
    • H01S3/067Fibre lasers
    • H01S3/06708Constructional details of the fibre, e.g. compositions, cross-section, shape or tapering
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01SDEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
    • H01S3/00Lasers, i.e. devices using stimulated emission of electromagnetic radiation in the infrared, visible or ultraviolet wave range
    • H01S3/05Construction or shape of optical resonators; Accommodation of active medium therein; Shape of active medium
    • H01S3/08Construction or shape of optical resonators or components thereof
    • H01S3/08013Resonator comprising a fibre, e.g. for modifying dispersion or repetition rate

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  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Optics & Photonics (AREA)
  • Lasers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention belongs to optical device field, a kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel and preparation method thereof is disclosed.The intermediate position of cellular glass capillary is drawn into the hollow micro-nano fiber that outer diameter is 0.5~10 μm with melt-drawing method, hollow micro- knot chamber is then formed by knots tied by microoperation;Liquid gain media is injected by way of capillary force sucking or external force injection in the fiber duct of hollow micro- knot chamber, is then coupled with conical fiber, encapsulate, obtain the hollow micro- knot Whispering-gallery-mode resonant cavity of the multi-pore channel.Preparation process of the present invention is simple, the hollow micro- knot chamber being prepared can inject various liquid gain medias by capillary force sucking or external force, the hollow micro- knot Whispering-gallery-mode resonant cavity of gained multi-pore channel has multiple gain channels, it can be achieved that Low threshold, high slope efficiency, the output of high power Echo Wall laser.

Description

A kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel and preparation method thereof
Technical field
The invention belongs to optical device fields, and in particular to a kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel and its Preparation method.
Background technique
Light due to that can be limited in intracavitary with high quality factor and minimum mode volume by Echo Wall optical microcavity The interaction for enhancing light and substance, there is important application prospect in fields such as integrated optical circuit, information processing, sensings.Micro- knot Echo Wall microcavity be micro-nano fiber is made by way of knotting on micromanipulation platform its constitute diameter tens arrive it is several hundred The ring resonator of micron.Compared with the miniature optical resonant cavity of traditional semiconductor etching, micro- knot Echo Wall microcavity has knot Structure is simple and convenient to operate, advantage at low cost, can meet different field application demand.And micro- knot Echo Wall microcavity can flexibly be set It counts ring structure (such as bicyclic, polycyclic, asymmetric ring), to realize the tunable output of zlasing mode.
Currently, micro- knot Echo Wall microcavity is prepared with solid active micro-nano fiber, this micro- knot Echo Wall microcavity is suitable Gain media is limited, can only realize the laser output of active micro-nano fiber.Although and can be obtained in Whispering-gallery-mode microcavity The output of Low threshold laser is obtained, but the slope efficiency of laser and output power are generally lower.
Summary of the invention
In place of the above shortcoming and defect of the existing technology, the primary purpose of the present invention is that providing a kind of porous The preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity in road.Preparation method simple process of the invention, applicable a variety of gains Medium, and inside has a plurality of gain channel, increases light path under the premise of keeping low-loss, the slope efficiency for exporting laser It is improved with power.
Another object of the present invention is to provide a kind of hollow micro- knot echoes of multi-pore channel being prepared by the above method Wall mode resonances chamber.
The object of the invention is achieved through the following technical solutions:
A kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel, including following preparation step:
(1) the intermediate position of cellular glass capillary is drawn into outer diameter with melt-drawing method is 0.5~10 μm hollow Micro-nano fiber;
(2) micro-nano fiber in step (1) is formed by knots tied by hollow micro- knot chamber by microoperation;
(3) that liquid gain media is injected into step (2) by way of capillary force sucking or external force injection is hollow In the fiber duct of micro- knot chamber;
(4) Commercial fibers are drawn into conical fiber on drawing cone platform, then by hollow micro- knot chamber of itself and step (3) It is coupled, encapsulates, obtain the hollow micro- knot Whispering-gallery-mode resonant cavity of the multi-pore channel.
Further, cellular glass capillary described in step (1) is at least quartz in two holes or other glass materials Matter capillary.Capillary outer diameter is 100 μm~5mm, and aperture is 20 μm~1mm.
As further instruction, the capillary end surface structural schematic diagram with two holes and four holes is as shown in Figure 1.
Further, melt-drawing method described in step (1) refer to oxyhydrogen flame or carbon dioxide laser or other Heating source melts capillary midsection, and clamps capillary both ends with clip, equal to two sides using stepper motor or other equipment Even stretching, obtaining outer diameter is 0.5~10 μm, and the hollow micro-nano fiber of former internal-and external diameter scale smaller is pressed in aperture.
Further, being formed by knots tied the cavity diameter of hollow micro- knot chamber by microoperation in step (2) is 20~500 μm, And having two root long degree at knotting is that 5 μm~5mm can truncated free end.The presence of free end can facilitate liquid gain media Sucking or injection.As further instruction, the structural schematic diagram of hollow micro- knot chamber is as shown in Figure 2.
Further, liquid gain media described in step (3) be laser dye or it is evenly dispersed in organic solvent Nanocrystal solution or other can be used for realizing laser output liquid gain media.
Further, the tail diameter of conical fiber described in step (4) is 0.5~10 μm, and length is 5~50 μm.It should Structure can effectively be injected into pump light in hollow micro- knot chamber by the optical fiber that traditional core packet interface is transmitted.
A kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel, is prepared by the above method.
The hollow micro- knot Echo Wall resonant cavity of multi-pore channel of the invention is to melt cellular glass capillary to be pulled to micron or nanometer Then dimension scale uses microoperation, it is made to constitute the annular resonance that diameter tens arrives several hundred microns by way of knotting Chamber.Microcavity can be sucked by capillary force, liquid gain media can also be injected by external force, in swashing for conical fiber evanscent field It gives and realizes laser output, can be used for the application such as sensing.Compared with conventional solid annular resonant cavity, hollow micro- knot Echo Wall is micro- The applicable a variety of liquid gain medias of chamber almost include all laser dyes and are dispersed in the nanocrystalline molten of organic solvent Liquid, laser output cover ultraviolet, visible, near-infrared and middle infrared band.
Compared with prior art, the invention has the advantages that and beneficial effect:
(1) preparation process of the present invention is simple, and the hollow micro- knot chamber being prepared can be by capillary force sucking or external force Various liquid gain medias are injected, a variety of gain medias are applicable in, such as various laser dyes and are dispersed in organic solvent The optical maser wavelength of nanocrystal solution, output can cover the infrared band from ultraviolet to middle.
(2) the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel of the method for the present invention preparation has multiple gain channels, can Realize Low threshold, high slope efficiency, the output of high power Echo Wall laser.
Detailed description of the invention
Fig. 1 is the capillary end surface structural schematic diagram that the present invention has two holes and four holes.
Fig. 2 is the structural schematic diagram of the hollow micro- knot chamber of the present invention.
Fig. 3 is the light path device structure formed by the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel in the embodiment of the present invention Schematic diagram.
Fig. 4 is the hollow micro- knot Whispering-gallery-mode resonant cavity (NaYF of Nd doping in two ducts of gained in the embodiment of the present invention 14 It is nanocrystalline) laser light spectrogram.
Fig. 5 is the hollow micro- knot Whispering-gallery-mode resonant cavity (NaYF of Nd doping in four ducts of gained in the embodiment of the present invention 24 It is nanocrystalline) laser light spectrogram.
Fig. 6 is that (Er and Yb are co-doped with the hollow micro- knot Whispering-gallery-mode resonant cavity in two ducts of gained in the embodiment of the present invention 3 YOF is nanocrystalline) laser light spectrogram.
Specific embodiment
Present invention will now be described in further detail with reference to the embodiments and the accompanying drawings, but embodiments of the present invention are unlimited In this.
Embodiment 1
(1) two hole quartz capillaries (outer diameter 3mm, two diameter of bores are about 0.5mm) is chosen, length is cut into about 5cm. Middle section is melted with heating sources such as carbon dioxide laser or oxyhydrogen flames, and clamps capillary both ends with clip, while with walking It is uniformly stretched into motor to both ends, obtains the hollow micro-nano fiber that diameter is 0.5 μm~10 μm, length is about 1mm~10mm.
(2) micro-nano fiber of acquisition is then knotted into cavity diameter using microoperation is about 250 μm of hollow micro- knot chambers.
(3) NaYF for then being adulterated Nd by way of capillary force sucking or external force injection4Nanocrystalline liquid increases Beneficial medium (nanocrystalline diameter is about 5nm~50nm, is scattered in cyclohexane solution, and solution concentration is 0.2 μM~5 μM) is injected into In the fiber duct of hollow micro- knot chamber in step (2).
(4) Commercial fibers are drawn into conical fiber on drawing cone platform, then by hollow micro- knot chamber of itself and step (3) It is coupled, is encapsulated, obtain the hollow micro- knot Whispering-gallery-mode resonant cavity (NaYF of Nd doping in two ducts4It is nanocrystalline).
Two duct of gained it is hollow it is micro- knot Whispering-gallery-mode resonant cavity formed light path device structural schematic diagram as shown in figure 3, By hollow micro- knot chamber, substrate (the magnesium fluoride substrate that refractive index is 1.38, having a size of 1 × 2cm), light wavelength division multiplexing (WDM), half Conductor pump laser and output port are constituted.The pumping wavelength of semiconductor pump laser is 808nm in the present embodiment, defeated Power adjustable is humorous out, and output tail optical fiber is single mode optical fiber.By Commercial fibers pull into cone optical fiber (optical taper tail diameter be 0.5 μm~ 10 μm, length is 5 μm~50 μm), tapered end is connected with hollow micro- knot chamber, the other end and semiconductor pump laser tail optical fiber phase Even.The common end of light wavelength division multiplexing is drawn and is connected after boring with hollow micro- knot chamber.Under the excitation of semiconductor pump laser, return Sound wall laser is exported by light wavelength division multiplexing output port.
The hollow micro- knot Whispering-gallery-mode resonant cavity (NaYF of Nd doping in two ducts obtained by the present embodiment4It is nanocrystalline) laser Spectrogram is as shown in Figure 4.From fig. 4, it can be seen that it is the laser output near 1059nm that this example, which realizes central wavelength, power is up to 75 μ W are (due to being limited by laboratory pumping source power, if the laser that raising pumping source power can obtain higher power is defeated Out).
Embodiment 2
(1) four hole quartz capillaries (outer diameter 3.5mm, four diameter of bores are about 0.5mm) is chosen, length is cut into about 5cm.Middle section is melted with heating sources such as carbon dioxide laser or oxyhydrogen flames, and clamps capillary both ends with clip, simultaneously Uniformly stretched to both ends with stepper motor, obtaining diameter is 0.5 μm~10 μm of hollow micro-nano fiber, length be about 1mm~ 10mm。
(2) micro-nano fiber of acquisition is then knotted into cavity diameter using microoperation is about 250 μm of hollow micro- knot chambers.
(3) NaYF for then being adulterated Nd by way of capillary force sucking or external force injection4Nanocrystalline liquid increases Beneficial medium (nanocrystalline diameter is about 5nm~50nm, is scattered in cyclohexane solution, and solution concentration is 0.2 μM~5 μM) is injected into In the fiber duct of hollow micro- knot chamber in step (2).
(4) Commercial fibers are drawn into conical fiber on drawing cone platform, then by hollow micro- knot chamber of itself and step (3) It is coupled, is encapsulated, obtain the hollow micro- knot Whispering-gallery-mode resonant cavity (NaYF of Nd doping in four ducts4It is nanocrystalline).
Four duct of gained it is hollow it is micro- knot Whispering-gallery-mode resonant cavity formed light path device structural schematic diagram as shown in figure 3, By hollow micro- knot chamber, substrate (the magnesium fluoride substrate that refractive index is 1.38, having a size of 1 × 2cm), light wavelength division multiplexing (WDM), half Conductor pump laser and output port are constituted.The pumping wavelength of semiconductor pump laser is 808nm in the present embodiment, defeated Power adjustable is humorous out, and output tail optical fiber is single mode optical fiber.By Commercial fibers pull into cone optical fiber (optical taper tail diameter be 0.5 μm~ 10 μm, length is 5 μm~50 μm), tapered end is connected with hollow micro- knot chamber, the other end and semiconductor pump laser tail optical fiber phase Even.The common end of light wavelength division multiplexing is drawn and is connected after boring with hollow micro- knot chamber.Under the excitation of semiconductor pump laser, return Sound wall laser is exported by light wavelength division multiplexing output port.
The hollow micro- knot Whispering-gallery-mode resonant cavity (NaYF of Nd doping in four ducts obtained by the present embodiment4It is nanocrystalline) laser Spectrogram is as shown in Figure 5.As seen from Figure 5, it is the laser output near 1061nm that this example, which realizes central wavelength, and power is up to 215 μ W are (due to being limited by laboratory pumping source power, if the laser that raising pumping source power can obtain higher power is defeated Out).
Embodiment 3
(1) two hole quartz capillaries (outer diameter 3mm, two diameter of bores are about 0.5mm) is chosen, length is cut into about 5cm. Middle section is melted with heating sources such as carbon dioxide laser or oxyhydrogen flames, and clamps capillary both ends with clip, while with walking It is uniformly stretched into motor to both ends, obtains the hollow micro-nano fiber that diameter is 0.5 μm~10 μm, length is about 1mm~10mm.
(2) micro-nano fiber of acquisition is then knotted into cavity diameter using microoperation is about 250 μm of hollow micro- knot chambers.
(3) the nanocrystalline liquid of YOF for being then co-doped with Er and Yb by way of capillary force sucking or external force injection Gain media (nanocrystalline diameter is about 5nm~50nm, is scattered in cyclohexane solution, and solution concentration is 0.2 μM~5 μM) injection In hollow micro- knot chamber in step (2).
(4) Commercial fibers are drawn into conical fiber on drawing cone platform, then by hollow micro- knot chamber of itself and step (3) It is coupled, encapsulates, obtain the hollow micro- knot Whispering-gallery-mode resonant cavity in two ducts (YOF that Er and Yb are co-doped with is nanocrystalline).
Two duct of gained it is hollow it is micro- knot Whispering-gallery-mode resonant cavity formed light path device structural schematic diagram as shown in figure 3, By hollow micro- knot chamber, substrate (the magnesium fluoride substrate that refractive index is 1.38, having a size of 1 × 2cm), light wavelength division multiplexing (WDM), half Conductor pump laser and output port are constituted.The pumping wavelength of semiconductor pump laser is 808nm in the present embodiment, defeated Power adjustable is humorous out, and output tail optical fiber is single mode optical fiber.By Commercial fibers pull into cone optical fiber (optical taper tail diameter be 0.5 μm~ 10 μm, length is 5 μm~50 μm), tapered end is connected with hollow micro- knot chamber, the other end and semiconductor pump laser tail optical fiber phase Even.The common end of light wavelength division multiplexing is drawn and is connected after boring with hollow micro- knot chamber.Under the excitation of semiconductor pump laser, return Sound wall laser is exported by light wavelength division multiplexing output port.
Hollow micro- knot Whispering-gallery-mode resonant cavity (YOF that Er and Yb are co-doped with is nanocrystalline) in two ducts obtained by the present embodiment is swashed Light spectrogram is as shown in Figure 6.As seen from Figure 6, it is about the laser output near 1550nm that this example, which realizes central wavelength,.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention, It should be equivalent substitute mode, be included within the scope of the present invention.

Claims (7)

1. a kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel, it is characterised in that including preparing step as follows Suddenly:
(1) the intermediate position of cellular glass capillary is drawn into the hollow micro-nano that outer diameter is 0.5~10 μm with melt-drawing method Fiber;
(2) micro-nano fiber in step (1) is formed by knots tied by hollow micro- knot chamber by microoperation;
(3) liquid gain media is injected into the hollow micro- knot of step (2) by way of capillary force sucking or external force injection In the fiber duct of chamber;
(4) Commercial fibers are drawn into conical fiber on drawing cone platform, then carry out hollow micro- knot chamber of itself and step (3) Coupling, encapsulation, obtains the hollow micro- knot Whispering-gallery-mode resonant cavity of the multi-pore channel.
2. a kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel according to claim 1, feature It is:Cellular glass capillary described in step (1) is at least quartz in two holes or other glass material capillaries;Capillary Pipe outside diameter is 100 μm~5mm, and aperture is 20 μm~1mm.
3. a kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel according to claim 1, feature It is:Melt-drawing method described in step (1), which refers to, melts capillary midsection with oxyhydrogen flame or carbon dioxide laser, is used in combination Clip clamps capillary both ends, and using stepper motor to two sides Uniform Tension, obtaining outer diameter is 0.5~10 μm, and aperture is by original The hollow micro-nano fiber of outer diameter scale smaller.
4. a kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel according to claim 1, feature It is:Being formed by knots tied the cavity diameter of hollow micro- knot chamber by microoperation in step (2) is 20~500 μm, and is had at knotting Having two root long degree is that 5 μm~5mm can truncated free end.
5. a kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel according to claim 1, feature It is:Liquid gain media described in step (3) is laser dye or evenly dispersed nanocrystal solution in organic solvent.
6. a kind of preparation method of the hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel according to claim 1, feature It is:The tail diameter of conical fiber described in step (4) is 0.5~10 μm, and length is 5~50 μm.
7. a kind of hollow micro- knot Whispering-gallery-mode resonant cavity of multi-pore channel, it is characterised in that:Pass through any one of claim 1~6 institute The method stated is prepared.
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CN109884013A (en) * 2019-03-05 2019-06-14 中北大学 The method for improving diamond NV colour center phosphor collection efficiency
CN111579847A (en) * 2020-04-30 2020-08-25 杭州电子科技大学 Double-enhancement current sensing system based on micro fiber junctions and magnetic fluid
CN112285838A (en) * 2020-11-18 2021-01-29 海南大学 Optical fiber echo wall resonator

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CN109809685A (en) * 2019-03-18 2019-05-28 华南理工大学 Devitrified glass Whispering-gallery-mode resonant cavity of exportable single mode High-performance lasers and preparation method thereof
CN111579847A (en) * 2020-04-30 2020-08-25 杭州电子科技大学 Double-enhancement current sensing system based on micro fiber junctions and magnetic fluid
CN112285838A (en) * 2020-11-18 2021-01-29 海南大学 Optical fiber echo wall resonator

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