CN108890224A - A method of improving Q345E ring low-temperature impact toughness - Google Patents

A method of improving Q345E ring low-temperature impact toughness Download PDF

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Publication number
CN108890224A
CN108890224A CN201810694336.0A CN201810694336A CN108890224A CN 108890224 A CN108890224 A CN 108890224A CN 201810694336 A CN201810694336 A CN 201810694336A CN 108890224 A CN108890224 A CN 108890224A
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CN
China
Prior art keywords
ring
upset
impact toughness
low
temperature impact
Prior art date
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Pending
Application number
CN201810694336.0A
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Chinese (zh)
Inventor
孙传金
徐仁伟
王超
安凤军
徐高太
赵鹏程
王俊平
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DANDONG FENGNENG INDUSTRIAL ABILITY Co Ltd
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DANDONG FENGNENG INDUSTRIAL ABILITY Co Ltd
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Priority to CN201810694336.0A priority Critical patent/CN108890224A/en
Publication of CN108890224A publication Critical patent/CN108890224A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23PMETAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
    • B23P15/00Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/002Hybrid process, e.g. forging following casting
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/40Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for rings; for bearing races

Abstract

The invention discloses a kind of methods for improving Q345E ring low-temperature impact toughness, belong to technical field of metal material.This method is successively to carry out upset, punching for Q345E continuous cast round billets, roll over ring and heat treatment, to improve the low-temperature impact toughness of gained Q345E ring;Wherein, strict control Q345E carbon equivalent ce V, and increase using reaming after the upset plate of taper is upset and punching the forging ratio of manufacturing process;It is cooled down after being warming up to 910 DEG C ± 10 DEG C and heat preservation and heat preservation by power after being warming up to 650 DEG C ± 10 DEG C using room temperature shove charge, by power and keeping the temperature 1 hour and makes cooling velocity >=0.5 DEG C/s;After being processed using the method for the present invention, banded structure inside ring, refinement crystal grain are eliminated, the low-temperature impact toughness of ring is greatly improved, part by one-step qualification rate is greater than 95%.

Description

A method of improving Q345E ring low-temperature impact toughness
Technical field
The present invention relates to technical field of metal material, and in particular to a kind of side for improving Q345E ring low-temperature impact toughness Method.
Background technique
Q345E has good intensity, toughness and low temperature impact properties, is widely used as low-alloy structural steel Stringent field is required solderability and low-temperature impact toughness in wind-powered electricity generation, ship, aerospace etc., according to most stringent of standard, It is required that low-temperature impact toughness (- 50 DEG C):Impact of collision function >=50J, side knock function >=34J.Therefore, it is necessary to by Q345E Ring process optimizes, to improve its low-temperature impact toughness, to meet the requirement under limiting condition.
Summary of the invention
The purpose of the present invention is to provide a kind of methods for improving Q345E ring low-temperature impact toughness, pass through strict control Carbon equivalent ce V, increase forging ratio, heating heat treatment process appropriate and accelerate cooling velocity after being heat-treated and rushed to improve low temperature Hit toughness.
To achieve the above object, the technical solution adopted in the present invention is as follows:
A method of improve Q345E ring low-temperature impact toughness, this method be for Q345E continuous cast round billets, successively into Row is upset, punching, rolles over ring and heat treatment, to improve the low-temperature impact toughness of gained Q345E ring;This method specifically include as Lower step:
(1) upset processing:Continuous cast round billets are carried out using taper upset plate upset;The upset ratio of the continuous cast round billets is greater than 1.7;It is described it is upset than refer to the upset preceding cutting length of continuous cast round billets and it is upset after height ratio;
(2) punching is handled:Upset treated that ring blank is punched out, and obtains ring blank through reaming again after punching Interim size;Piercing process middle section ratio is greater than 1.0;The section than refer to after punching with the ring section after reaming The ratio between product;
(3) ring processing is rolled over:Ring blank after expanding treatment carries out rolling ring, the blank ring of specification needed for obtaining;Roll over ring Rolling than being greater than 2.3 in processing, it is described roll than refer to after reaming with roll over the ratio between ring sectional area after ring;
(4) it is heat-treated:After blank ring shove charge after rolling over ring, first it is warming up to 640-660 DEG C and keeps the temperature 1 hour, then heat up To 900-920 DEG C and held for some time, ring is taken out after heat preservation, and 600 DEG C or less are cooled to outside furnace.The Q345E continuous casting Carbon equivalent ce V≤0.45 of round billet.
In above-mentioned steps (1), the upset plate of taper includes the Upper cylindrical being connected and lower part rotary table, cylinder and rotary table Upper bottom surface be connected (upper bottom surface diameter be greater than bottom surface diameter);The diameter of section of cylinder is greater than the upper bottom surface diameter of rotary table; The angle of rotary table bus and axis is 20-30 °.
In above-mentioned steps (2), the requirement of the punching hole diameter d in punching is:50%≤d of blank diameter≤blank diameter 55%, to prevent blank from deflection deformation occur;It is too big that subsequent reaming process deflection is avoided result in simultaneously, and influences deformation matter Amount and production efficiency;Reach the inner hole size of interim size by expanding treatment.
In above-mentioned steps (4), forging is room temperature when ring shove charge and furnace temperature is not higher than 300 DEG C;Multiple rings exist when shove charge It is placed in furnace according to way of stacking, the way of stacking refers to, each ring stacks placement in the vertical direction and forms a line, total N Column;The distance between each column≤3 meters, N >=3 are separated between two neighboring ring using multiple equal-height padding irons in each column, and parallels is high Degree is greater than 50mm, and the spacing between each parallels placed in each plane is less than 1500mm.
In above-mentioned steps (4), when ring is in 900-920 DEG C of heat preservation, soaking time is calculated by ring effective thickness, Its effective thickness is the minimum value for taking wall thickness and height, soaking time=effective thickness × 1.2min/mm.
In above-mentioned steps (4), when ring is cooling, cooling velocity >=0.5 DEG C/s;The watering of cooled region ground, water surface elevation For 2~3mm.Preferably cooling condition is:When room temperature≤15 DEG C, effective thickness≤150mm, ring cooling need to be in outdoor dispersion Cooling, cooling velocity is 0.5 DEG C/s;When room temperature≤15 DEG C, effective thickness >=150mm, ring cooling needs air blast cooling, makes Cooling velocity >=0.5 DEG C/s;When 15 DEG C of room temperature >, ring cooling needs air blast cooling, makes cooling velocity >=0.5 DEG C/s.
The Q345E ring is after processing, in -50 DEG C of low-temperature impact toughness:Impact of collision function >=50J, laterally punching Hit function >=34J;Time processing part qualification rate is greater than 95%.
Advantages of the present invention and benefit are:
1, it after Q345E ring is using the method for the present invention processing, eliminates internal banded structure, refinement crystal grain, improve ingredient Segregation improves internal content of pearlite in alloy and eliminates internal stress, make low-temperature impact toughness reach -50 DEG C, impact of collision function >= 50J, side knock function >=34J.
2, using the method for the present invention, percent defective will be caused to be reduced in product by 30% since low-temperature impact toughness is relatively low To 5%, hence it is evident that improve the qualification rate of product.Not only meet the product quality of customer requirement, but also saves manufacture product cost 15% or so, improve Enterprise Integrated competitiveness.
Detailed description of the invention
Fig. 1 is tapered upset hardened structure used in the method for the present invention.
Fig. 2 is heat treatment cycle curve of the present invention.
Fig. 3 is normative heat treatment process curve.
Fig. 4 is the metallographic structure figure obtained using process of the invention and ballistic work numerical value.
Fig. 5 is the metallographic structure figure obtained using conventional process and ballistic work numerical value.
Specific embodiment
The present invention is described in detail with reference to the accompanying drawings and examples.
Using Q345E continuous cast round billets as original blank in following embodiment, carbon equivalent ce V≤0.45;The taper pier used Structure snd size such as Fig. 1 of thick plate.The upset plate of taper includes the Upper cylindrical being connected and lower part rotary table, cylinder and rotary table it is upper Bottom surface is connected (upper bottom surface diameter is greater than bottom surface diameter);The diameter of section of cylinder is greater than the upper bottom surface diameter of rotary table;Rotary table The angle of bus and axis is 20-30 °.
Embodiment 1:
The method that the present embodiment improves Q345E ring low-temperature impact toughness is specific as follows:
(1) upset processing:Continuous cast round billets are carried out using taper upset plate upset;The upset ratio of the continuous cast round billets is greater than 1.7;It is described it is upset than refer to the upset preceding cutting length of continuous cast round billets and it is upset after height ratio;
(2) punching is handled:Upset treated that ring blank is punched out, and obtains ring blank through reaming again after punching Interim size;The section ratio is greater than 1.0;The section than refer to after punching with the ratio between the ring sectional area after reaming;Its In:The requirement of punching hole diameter d is:50%≤d of blank diameter≤round billet diameter 55%, to prevent blank from bending deformation occur Shape;It is too big to avoid result in subsequent reaming process deflection simultaneously, and influences texturing quality and production efficiency;Pass through expanding treatment Reach the inner hole size of interim size.
(3) ring processing is rolled over:Ring blank after expanding treatment carries out rolling ring, the blank ring of specification needed for obtaining;It is described Roll than being greater than 2.3, it is described roll than refer to after reaming with roll over the ratio between ring sectional area after ring;With the upset plate of taper it is upset and Reaming increases the forging ratio of manufacturing process after punching, makes forging ratio >=5;The forging ratio refers to above-mentioned (1), (2), (3) The upset ratio of process, section ratio and roll than the sum of.
(4) it is heat-treated:After ring shove charge after reaming, first it is warming up to 650 DEG C and keeps the temperature 1 hour, then be warming up to 910 DEG C simultaneously Held for some time, ring is taken out after heat preservation, and 600 DEG C are cooled to outside furnace hereinafter, process curve is as shown in Figure 2.
Forging is room temperature when ring shove charge and furnace temperature is not higher than 300 DEG C;Multiple rings are in furnace according to stacking side when shove charge Formula is placed, and the way of stacking refers to, each ring stacks placement in the vertical direction and forms a line, totally 3 column;Between each column away from From≤3 meters, separated between two neighboring ring using 8 equal-height padding irons in each column, parallels height 60mm, is placed in each plane Each parallels between spacing be less than 1000mm.
When ring is in 900-920 DEG C of heat preservation, soaking time is calculated by ring effective thickness, and effective thickness is to take The minimum value of wall thickness and height, soaking time=effective thickness × 1.2min/mm.
When ring is cooling, the watering of cooled region ground, water surface elevation 3mm.Room temperature≤15 DEG C when cooling, effective thickness≤ 150mm, ring is cooling in outdoor dispersion, and cooling velocity is 0.5 DEG C/s.
Fig. 4 is the ring product metallographic structure figure obtained using the present embodiment, it can be seen that Q345E ring uses this hair After bright method processing, internal banded structure, refinement crystal grain are eliminated.
After processing, in -50 DEG C of low-temperature impact toughness such as table 1, time processing part qualification rate is big for the Q345E ring In 95%.
1 embodiment of table, 1 ring low-temperature impact toughness
Comparative example 1:
With embodiment the difference is that:Using heat treatment cycle curve as shown in Figure 3.
Fig. 5 is the ring product metallographic structure figure obtained using the comparative example, it can be seen that is had inside Q345E ring Banded structure, coarse grains.
After processing, in -50 DEG C of low-temperature impact toughness such as table 2, time processing part qualification rate is about for the Q345E ring It is 70%.
2 comparative example of table, 1 ring low-temperature impact toughness
Certainly, above description is not limitation of the present invention, and the present invention is also not limited to above-mentioned narration, the art The variations, modifications, additions or substitutions that those of ordinary skill is made within the essential scope of the present invention also belong to guarantor of the invention Protect range.

Claims (9)

1. a kind of method for improving Q345E ring low-temperature impact toughness, it is characterised in that:This method is for Q345E continuous casting circle Base successively carries out upset, punching, rolles over ring and heat treatment, to improve the low-temperature impact toughness of gained Q345E ring;This method Specifically comprise the following steps:
(1) upset processing:Continuous cast round billets are carried out using taper upset plate upset;The upset ratio of the continuous cast round billets is greater than 1.7; It is described it is upset than refer to the upset preceding cutting length of continuous cast round billets and it is upset after height ratio;
(2) punching is handled:Upset treated that ring blank is punched out, and obtains the mistake of ring blank through reaming again after punching Cross size;Piercing process middle section ratio is greater than 1.0;The section than refer to after punching with the ring sectional area after reaming it Than;
(3) ring processing is rolled over:Ring blank after expanding treatment carries out rolling ring-rolling, the blank ring of specification needed for obtaining;Roll over ring Rolling than being greater than 2.3 in processing;It is described roll than refer to after reaming with roll over the ratio between ring sectional area after ring;
(4) it is heat-treated:After blank ring shove charge after rolling over ring, first it is warming up to 640-660 DEG C and keeps the temperature 1 hour, then be warming up to 900-920 DEG C and held for some time, ring is taken out after heat preservation, and 600 DEG C or less are cooled to outside furnace.
2. the method according to claim 1 for improving Q345E ring low-temperature impact toughness, it is characterised in that:The Q345E Carbon equivalent ce V≤0.45 of continuous cast round billets.
3. the method according to claim 1 for improving Q345E ring low-temperature impact toughness, it is characterised in that:Step (1) In, the upset plate of taper includes the Upper cylindrical being connected and lower part rotary table, and cylinder is connected with the upper bottom surface of rotary table;Cylinder Diameter of section be greater than rotary table upper bottom surface diameter;The angle of rotary table bus and axis is 20-30 °.
4. the method according to claim 1 for improving Q345E ring low-temperature impact toughness, it is characterised in that:Step (2) In, the requirement of the punching hole diameter d in punching is:50%≤d of round billet diameter≤round billet blank diameter 55%, to prevent blank There is deflection deformation;It is too big to avoid result in subsequent reaming process deflection simultaneously, and influences texturing quality and production efficiency;It is logical Cross the inner hole size that expanding treatment reaches interim size.
5. the method according to claim 1 for improving Q345E ring low-temperature impact toughness, it is characterised in that:Step (4) In, forging is room temperature when ring shove charge and furnace temperature is not higher than 300 DEG C;Multiple rings are put in furnace according to way of stacking when shove charge It sets, the way of stacking refers to, each ring stacks placement in the vertical direction and forms a line, total N column;The distance between each column≤ 3 meters, N >=3 are separated between two neighboring ring using multiple equal-height padding irons in each column, and parallels height is greater than 50mm, each plane Spacing between each parallels of upper placement is less than 1500mm.
6. the method according to claim 1 for improving Q345E ring low-temperature impact toughness, it is characterised in that:Step (4) In, when ring is in 900-920 DEG C of heat preservation, soaking time is calculated by ring effective thickness, and effective thickness is to take wall thickness With the minimum value of height, soaking time=effective thickness × 1.2min/mm.
7. the method according to claim 1 for improving Q345E ring low-temperature impact toughness, it is characterised in that:Step (4) In, when ring is cooling, cooling velocity >=0.5 DEG C/s;The watering of cooled region ground, water surface elevation are 2~3mm.
8. the method according to claim 7 for improving Q345E ring low-temperature impact toughness, it is characterised in that:Step (4) In, when ring is cooling, when room temperature≤15 DEG C, effective thickness≤150mm, ring cooling need to be cooling in outdoor dispersion, cooling Speed is 0.5 DEG C/s;When room temperature≤15 DEG C, effective thickness >=150mm, ring cooling need air blast cooling, make cooling velocity >= 0.5℃/s;When 15 DEG C of room temperature >, ring cooling needs air blast cooling, makes cooling velocity >=0.5 DEG C/s.
9. the method for -8 any raising Q345E ring low-temperature impact toughness according to claim 1, it is characterised in that:Institute It states Q345E ring after processing, is in -50 DEG C of low-temperature impact toughness:Impact of collision function >=50J, side knock function >=34J; Time processing part qualification rate is greater than 95%.
CN201810694336.0A 2018-06-29 2018-06-29 A method of improving Q345E ring low-temperature impact toughness Pending CN108890224A (en)

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Publication number Priority date Publication date Assignee Title
CN110993040A (en) * 2019-11-28 2020-04-10 太原科技大学 Method for determining critical value of 30Cr2Ni4MoV steel converted from casting state to forging state

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110993040A (en) * 2019-11-28 2020-04-10 太原科技大学 Method for determining critical value of 30Cr2Ni4MoV steel converted from casting state to forging state
CN110993040B (en) * 2019-11-28 2023-03-14 太原科技大学 Method for determining critical value of 30Cr2Ni4MoV steel converted from cast state to forged state

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Application publication date: 20181127