CN108864962A - A kind of shuttlecock processing is stained with adhesive process with high-quality green tea - Google Patents
A kind of shuttlecock processing is stained with adhesive process with high-quality green tea Download PDFInfo
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- CN108864962A CN108864962A CN201810669954.XA CN201810669954A CN108864962A CN 108864962 A CN108864962 A CN 108864962A CN 201810669954 A CN201810669954 A CN 201810669954A CN 108864962 A CN108864962 A CN 108864962A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J5/00—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers
- C09J5/06—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers involving heating of the applied adhesive
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B67/00—Sporting games or accessories therefor, not provided for in groups A63B1/00 - A63B65/00
- A63B67/18—Badminton or similar games with feathered missiles
- A63B67/183—Feathered missiles
- A63B67/187—Shuttlecocks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09J161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
- C09J161/14—Modified phenol-aldehyde condensates
-
- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B2102/00—Application of clubs, bats, rackets or the like to the sporting activity ; particular sports involving the use of balls and clubs, bats, rackets, or the like
- A63B2102/04—Badminton
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Physical Education & Sports Medicine (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of shuttlecock processing to be stained with adhesive process with high-quality green tea, is related to shuttlecock manufacture field；(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, next procedure is entered for the qualified product of equidistant distribution；(2) viscose glue is put into round dispenser calandria and is heated；(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing syringe apart from high-quality green tea height 0.5-0.8mm；(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, and viscose glue is stained on high-quality green tea in the continuous rotary course of shuttlecock, and glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.6-0.8mm；(5) it the shuttlecock after glue will be stained with is put into 0.8-1Mpa nitrogen and stand 20min；High-quality green tea is stained with glue, high-quality green tea is firmly combined to each other, to will not be scattered after being hit, extends shuttlecock service life.
Description
Technical field：
The present invention relates to shuttlecock manufacture fields, and in particular to a kind of shuttlecock processing is stained with adhesive process with high-quality green tea.
Background technique：
Good shuttlecock hair must use goose knife hair, if using duck knife hair and its quality of other workprints
It is difficult to guarantee.The classification of ball hair is very complicated, due to the classification number standard that unification of the motherland is formulated not yet, each production
The label of the shuttlecock of producer's production is all made by oneself, and different manufacturers can not indicate theirs if there is the product of same label
Quality is the same.It is classified as large, medium and small hair according to wool type, is divided into one, two, three, four, Pyatyi according still further to the quality of hair, then
Again according to each point of five standards of prying of hair, the thickness obstructed further according to hair, the thickness of workprint sort out similar workprint.Same
16 feathers used on shuttlecock must be same class and similar as far as possible, 16 hairs that high-grade product uses
Piece more unanimously will just can guarantee the flight quality of product.
The feather of high quality shuttlecock must all use high-quality goose feather.The intensity, toughness of goose feather is all particularly suitable for shuttlecock
Requirement, but the supply limited amount of its higher cost and raw material, so in some shuttlecock producers of less demanding
It is only to be difficult to distinguish drake feather and goose feather, and the flying quality of the drake feather shuttlecock of sophisticated technologies from appearance using drake feather
Also very good, since the hair stalk structure of two kinds of workprints is different, many poorer than the shuttlecock of goose feather of durable resistance, just
It is just easy to fracture in normal batting, since the price of drake feather is more much lower than goose feather, cost can be effectively reduced using drake feather.
The either goose feather of high quality or general drake feather, under the strong impaction of racket, plumage over time
Mao mao tip position will be scattered, influence using.
Summary of the invention：
Technical problem to be solved by the present invention lies in providing a kind of shuttlecock processing to be stained with adhesive process with high-quality green tea, so that high-quality green tea
It is firmly combined, will not be impacted and be scattered, to extend shuttlecock service life.
The following technical solution is employed for the technical problems to be solved by the invention to realize：
A kind of shuttlecock processing is stained with adhesive process with high-quality green tea, includes the following steps：
(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, for the qualified product of equidistant distribution
Into next procedure；
(2) viscose glue is put into round dispenser calandria and is heated；
(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing
Syringe is 0.5-0.8mm apart from high-quality green tea height；
(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, will be glued in the continuous rotary course of shuttlecock
Glue is stained on high-quality green tea, and glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.6-0.8mm；
(5) it the shuttlecock after glue will be stained with is put into 0.8-1Mpa nitrogen and stand 20min.
The viscose glue is made of the raw material of following parts by weight：80-100 parts of methyl acrylate phenol-formaldehyde resin modified, guar gum
60-80 parts, 20-40 parts of isocyanates, 15-25 parts of polyvinyl formal, 12-15 parts of saleratus, 8-10 parts of resorcinol,
15-25 parts of polyoxyethylene sorbitol acid anhydride, 18-24 parts of diacetyl tartarate monoglyceride, 26-32 parts of sodium alginate, Peppermint essential oil
20-30 parts, 5-8 parts of terpene resin, 12-16 parts of aluminum stearate, phenylalanine grafting carboxymethyl cellulose 15-20 parts, water 400-
500 parts.
The preparation method of the methyl acrylate phenol-formaldehyde resin modified is：
(1) methyl acrylate and phenolic resin are uniformly mixed, are put into high-speed mixer in 600-800r/min revolving speed
30-40min is stirred, 120-150 DEG C of heat preservation 20-30min is warming up to after stirring, naturally cools to room temperature；
(2) treated mixture is sent into extruder to the sheet being extruded into a thickness of 2-3mm, to flaky material table
It is 15-25% that magnesium chloride solution to flaky material water content is sprayed in face；
(3) flaky material after sprinkling is put into nitrogen atmosphere stove in 300-350 DEG C of sintering 2-3h, is cooled to room temperature；
(4) sintered mixture is put into 40-50 DEG C of water and impregnates 10min, be centrifuged, sediment is put into vacuum drying oven
It is dry, methyl acrylate phenol-formaldehyde resin modified is made.
The mass ratio of the methyl acrylate and phenolic resin is 3：17, the concentration of magnesium chloride solution is 2.2-2.6%.
The preparation method of phenylalanine grafting carboxymethyl cellulose is：
(1) phenylalanine and diphenylhydroxyethanone are uniformly mixed, 1.6 times of mixture weight of water is added, is adjusted with hydrochloric acid
PH value is 5.5-6；
(2) carboxymethyl cellulose is added into said mixture, 15-20min is stirred under 200-260r/min revolving speed, it is quiet
Set 5-6h；
(3) mixture after standing is stirred, while with ultraviolet light irradiation mixture under 80-100r/min revolving speed, is shone
Mixture is centrifuged after penetrating, sediment is dissolved in ethyl alcohol, ultrasound 20min, is centrifuged again under the conditions of 30KHz, 180W, will sink
Starch is dry, and phenylalanine is made and is grafted carboxymethyl cellulose.
The mass ratio of the phenylalanine and carboxymethyl cellulose is 1：4, the mass ratio of phenylalanine and diphenylhydroxyethanone
It is 49：1.
The intensity of the ultraviolet light irradiation is 30-40W/m2, irradiation time 20-30min.
The present invention provides a kind of shuttlecock processing to be stained with adhesive process with high-quality green tea, and its advantages are：
(1) shuttlecock high-quality green tea is easy to be scattered and prevent shuttlecock from being used, and solves not yet about this problem at present
Scheme, and present invention applicant recognizes this problem in time and therefrom finds solution, and high-quality green tea is stained with glue, makes high-quality green tea each other
Between be firmly combined, to will not be scattered after being hit, extend shuttlecock service life.
(2) viscose glue uses special formula composition, and not only bonding force is strong, can realize and bond particular for feather, and environmental protection
It is pollution-free, it is generated without volatile noxious material, and be bonded securely, is not easy degumming, even if under by great external force,
Still will not be from matrix stripping, ageing resistance is good.
(3) preparation of methyl acrylate phenol-formaldehyde resin modified can increase the viscosity of phenolic resin, while increase phenolic aldehyde tree
The hydrophily of rouge, to be easy to prepare the strong viscose glue of bonding force.
(4) phenylalanine grafting carboxymethyl cellulose can increase the mobility of viscose glue, keep viscose glue equal in shuttlecock distribution
It is even, avoid viscose glue that localized clusters occur and influence the uniformity of viscose glue thickness since viscosity is too strong.
Specific embodiment：
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1：
A kind of shuttlecock processing is stained with adhesive process with high-quality green tea, includes the following steps：
(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, for the qualified product of equidistant distribution
Into next procedure；
(2) viscose glue is put into round dispenser calandria and is heated；
(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing
Syringe is 0.5mm apart from high-quality green tea height；
(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, will be glued in the continuous rotary course of shuttlecock
Glue is stained on high-quality green tea, and glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.6mm；
(5) it the shuttlecock after glue will be stained with is put into 0.8Mpa nitrogen and stand 20min.
Embodiment 2：
A kind of shuttlecock processing is stained with adhesive process with high-quality green tea, includes the following steps：
(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, for the qualified product of equidistant distribution
Into next procedure；
(2) viscose glue is put into round dispenser calandria and is heated；
(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing
Syringe is 0.6mm apart from high-quality green tea height；
(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, will be glued in the continuous rotary course of shuttlecock
Glue is stained on high-quality green tea, and glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.7mm；
(5) it the shuttlecock after glue will be stained with is put into 0.9Mpa nitrogen and stand 20min.
The viscose glue is made of the raw material of following parts by weight：80 parts of methyl acrylate phenol-formaldehyde resin modified, 60 parts of guar gum,
20 parts of isocyanates, 15 parts of polyvinyl formal, 12 parts of saleratus, 8 parts of resorcinol, polyoxyethylene sorbitol acid anhydride 15
Part, 18 parts of diacetyl tartarate monoglyceride, 26 parts of sodium alginate, 20 parts of Peppermint essential oil, 5 parts of terpene resin, aluminum stearate 12
Part, phenylalanine are grafted 15 parts of carboxymethyl cellulose, 400 parts of water.
The preparation method of the methyl acrylate phenol-formaldehyde resin modified is：
(1) methyl acrylate and phenolic resin are uniformly mixed, are put into high-speed mixer and are stirred in 600r/min revolving speed
30min is warming up to 120 DEG C of heat preservation 20min, naturally cools to room temperature after stirring；
(2) treated mixture is sent into extruder to the sheet being extruded into a thickness of 2mm, to flaky material surface
Spraying magnesium chloride solution to flaky material water content is 15%；
(3) flaky material after sprinkling is put into nitrogen atmosphere stove in 300 DEG C of sintering 2h, is cooled to room temperature；
(4) sintered mixture is put into 40 DEG C of water and impregnates 10min, be centrifuged, sediment is put into vacuum drying oven and is done
It is dry, methyl acrylate phenol-formaldehyde resin modified is made.
The mass ratio of the methyl acrylate and phenolic resin is 3：17, the concentration of magnesium chloride solution is 2.2%.
Embodiment 3：
A kind of shuttlecock processing is stained with adhesive process with high-quality green tea, includes the following steps：
(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, for the qualified product of equidistant distribution
Into next procedure；
(2) viscose glue is put into round dispenser calandria and is heated；
(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing
Syringe is 0.7mm apart from high-quality green tea height；
(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, will be glued in the continuous rotary course of shuttlecock
Glue is stained on high-quality green tea, and glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.8mm；
(5) it the shuttlecock after glue will be stained with is put into 1Mpa nitrogen and stand 20min.
The preparation method of phenylalanine grafting carboxymethyl cellulose is：
(1) phenylalanine and diphenylhydroxyethanone are uniformly mixed, 1.6 times of mixture weight of water is added, is adjusted with hydrochloric acid
PH value is 5.5；
(2) carboxymethyl cellulose is added into said mixture, 15min is stirred under 200r/min revolving speed, stands 5h；
(3) mixture after standing is stirred under 80r/min revolving speed, while with ultraviolet light irradiation mixture, after irradiation
Mixture is centrifuged, sediment is dissolved in ethyl alcohol, ultrasound 20min, is centrifuged again under the conditions of 30KHz, 180W, by sediment
It is dry, phenylalanine is made and is grafted carboxymethyl cellulose.
The mass ratio of the phenylalanine and carboxymethyl cellulose is 1：4, the mass ratio of phenylalanine and diphenylhydroxyethanone
It is 49：1.
The intensity of the ultraviolet light irradiation is 30W/m2, irradiation time 20min.
Embodiment 4：
A kind of shuttlecock processing is stained with adhesive process with high-quality green tea, includes the following steps：
(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, for the qualified product of equidistant distribution
Into next procedure；
(2) viscose glue is put into round dispenser calandria and is heated；
(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing
Syringe is 0.8mm apart from high-quality green tea height；
(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, will be glued in the continuous rotary course of shuttlecock
Glue is stained on high-quality green tea, and glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.8mm；
(5) it the shuttlecock after glue will be stained with is put into 0.9Mpa nitrogen and stand 20min.
The viscose glue is made of the raw material of following parts by weight：100 parts of methyl acrylate phenol-formaldehyde resin modified, guar gum 80
Part, 40 parts of isocyanates, 25 parts of polyvinyl formal, 15 parts of saleratus, 10 parts of resorcinol, polyoxyethylene sorbitol acid anhydride
25 parts, 24 parts of diacetyl tartarate monoglyceride, 32 parts of sodium alginate, 30 parts of Peppermint essential oil, 8 parts of terpene resin, aluminum stearate
16 parts, phenylalanine grafting 20 parts of carboxymethyl cellulose, 500 parts of water.
The preparation method of the methyl acrylate phenol-formaldehyde resin modified is：
(1) methyl acrylate and phenolic resin are uniformly mixed, are put into high-speed mixer and are stirred in 800r/min revolving speed
40min is warming up to 150 DEG C of heat preservation 30min, naturally cools to room temperature after stirring；
(2) treated mixture is sent into extruder to the sheet being extruded into a thickness of 3mm, to flaky material surface
Spraying magnesium chloride solution to flaky material water content is 25%；
(3) flaky material after sprinkling is put into nitrogen atmosphere stove in 350 DEG C of sintering 3h, is cooled to room temperature；
(4) sintered mixture is put into 50 DEG C of water and impregnates 10min, be centrifuged, sediment is put into vacuum drying oven and is done
It is dry, methyl acrylate phenol-formaldehyde resin modified is made.
The mass ratio of the methyl acrylate and phenolic resin is 3：17, the concentration of magnesium chloride solution is 2.6%.
The preparation method of phenylalanine grafting carboxymethyl cellulose is：
(1) phenylalanine and diphenylhydroxyethanone are uniformly mixed, 1.6 times of mixture weight of water is added, is adjusted with hydrochloric acid
PH value is 6；
(2) carboxymethyl cellulose is added into said mixture, 20min is stirred under 260r/min revolving speed, stands 6h；
(3) mixture after standing is stirred under 100r/min revolving speed, while with ultraviolet light irradiation mixture, after irradiation
Mixture is centrifuged, sediment is dissolved in ethyl alcohol, ultrasound 20min, is centrifuged again under the conditions of 30KHz, 180W, by sediment
It is dry, phenylalanine is made and is grafted carboxymethyl cellulose.
The mass ratio of the phenylalanine and carboxymethyl cellulose is 1：4, the mass ratio of phenylalanine and diphenylhydroxyethanone
It is 49：1.
The intensity of the ultraviolet light irradiation is 40W/m2, irradiation time 30min.
Shuttlecock and ordinary badminton after various embodiments of the present invention are processed carry out impact resistance detection, are scattered with feather
When the power born be examination parameter, it is as a result as follows：
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (7)
1. a kind of shuttlecock processing is stained with adhesive process with high-quality green tea, which is characterized in that include the following steps：
(1) after shuttlecock completes, the whether equidistant distribution of feather high-quality green tea is examined, the qualified product of equidistant distribution is entered
Next procedure；
(2) viscose glue is put into round dispenser calandria and is heated；
(3) shuttlecock is put on round dispenser jig, the height of setting program adjust automatically dispensing syringe makes dispensing syringe
It is 0.5-0.8mm apart from high-quality green tea height；
(4) shuttlecock revolving speed is set as 30r/min, and dispensing speed is 2mm/s, is stained with viscose glue in the continuous rotary course of shuttlecock
Onto high-quality green tea, glue is stained in the stopping that often rotating a circle to be made to be stained with glue drying, stops being stained with glue when viscose glue thickness reaches 0.6-0.8mm；
(5) it the shuttlecock after glue will be stained with is put into 0.8-1Mpa nitrogen and stand 20min.
2. shuttlecock processing according to claim 1 is stained with adhesive process with high-quality green tea, which is characterized in that the viscose glue is by following heavy
Measure the raw material composition of part：80-100 parts of methyl acrylate phenol-formaldehyde resin modified, 60-80 parts of guar gum, 20-40 parts of isocyanates,
15-25 parts of polyvinyl formal, 12-15 parts of saleratus, 8-10 parts of resorcinol, 15-25 parts of polyoxyethylene sorbitol acid anhydride,
It is 18-24 parts of diacetyl tartarate monoglyceride, 26-32 parts of sodium alginate, 20-30 parts of Peppermint essential oil, 5-8 parts of terpene resin, hard
12-16 parts of resin acid aluminium, phenylalanine are grafted carboxymethyl cellulose 15-20 parts, 400-500 parts of water.
3. shuttlecock processing according to claim 2 is stained with adhesive process with high-quality green tea, which is characterized in that the methyl acrylate changes
The preparation method of property phenolic resin is：
(1) methyl acrylate and phenolic resin are uniformly mixed, are put into high-speed mixer and are stirred in 600-800r/min revolving speed
30-40min is warming up to 120-150 DEG C of heat preservation 20-30min, naturally cools to room temperature after stirring；
(2) treated mixture is sent into extruder to the sheet being extruded into a thickness of 2-3mm, is sprayed to flaky material surface
Spilling magnesium chloride solution to flaky material water content is 15-25%；
(3) flaky material after sprinkling is put into nitrogen atmosphere stove in 300-350 DEG C of sintering 2-3h, is cooled to room temperature；
(4) sintered mixture is put into 40-50 DEG C of water and impregnates 10min, be centrifuged, sediment is put into vacuum drying oven and is done
It is dry, methyl acrylate phenol-formaldehyde resin modified is made.
4. shuttlecock processing according to claim 3 is stained with adhesive process with high-quality green tea, which is characterized in that the methyl acrylate and
The mass ratio of phenolic resin is 3：17, the concentration of magnesium chloride solution is 2.2-2.6%.
5. shuttlecock processing according to claim 2 is stained with adhesive process with high-quality green tea, which is characterized in that the phenylalanine grafting
The preparation method of carboxymethyl cellulose is：
(1) phenylalanine and diphenylhydroxyethanone are uniformly mixed, 1.6 times of mixture weight of water is added, adjust pH value with hydrochloric acid
For 5.5-6；
(2) carboxymethyl cellulose is added into said mixture, 15-20min is stirred under 200-260r/min revolving speed, stands 5-
6h；
(3) mixture after standing is stirred under 80-100r/min revolving speed, while with ultraviolet light irradiation mixture, after irradiation
Mixture is centrifuged, sediment is dissolved in ethyl alcohol, ultrasound 20min, is centrifuged again under the conditions of 30KHz, 180W, by sediment
It is dry, phenylalanine is made and is grafted carboxymethyl cellulose.
6. shuttlecock processing according to claim 5 is stained with adhesive process with high-quality green tea, which is characterized in that the phenylalanine and carboxylic
The mass ratio of methylcellulose is 1：4, the mass ratio of phenylalanine and diphenylhydroxyethanone is 49：1.
7. shuttlecock processing according to claim 5 is stained with adhesive process with high-quality green tea, which is characterized in that the ultraviolet light irradiation
Intensity is 30-40W/m2, irradiation time 20-30min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810669954.XA CN108864962A (en) | 2018-06-26 | 2018-06-26 | A kind of shuttlecock processing is stained with adhesive process with high-quality green tea |
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| CN205914346U (en) * | 2016-08-01 | 2017-02-01 | 宁波双智智能控制设备有限公司 | Circular point gum machine |
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|---|---|---|---|---|
| CN201643607U (en) * | 2010-03-25 | 2010-11-24 | 南京胜利体育用品实业有限公司 | Badminton |
| CN103937197A (en) * | 2014-02-14 | 2014-07-23 | 东莞市想联实业投资有限公司 | Polyurethane synthetic resin for preparing traceless glue sticker and traceless glue sticker prepared by applying polyurethane synthetic resin |
| CN104119808A (en) * | 2014-06-26 | 2014-10-29 | 安徽图强文具股份有限公司 | Beeswax-containing special high softening point hot-melt adhesive for gluing notebooks |
| CN104371583A (en) * | 2014-10-30 | 2015-02-25 | 田琳琳 | High-temperature double-sided adhesive tape |
| CN205914346U (en) * | 2016-08-01 | 2017-02-01 | 宁波双智智能控制设备有限公司 | Circular point gum machine |
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Application publication date: 20181123 |