CN108855430A - A kind of multiple tank controllable temperature planetary type ball-milling instrument - Google Patents
A kind of multiple tank controllable temperature planetary type ball-milling instrument Download PDFInfo
- Publication number
- CN108855430A CN108855430A CN201710332112.0A CN201710332112A CN108855430A CN 108855430 A CN108855430 A CN 108855430A CN 201710332112 A CN201710332112 A CN 201710332112A CN 108855430 A CN108855430 A CN 108855430A
- Authority
- CN
- China
- Prior art keywords
- fixed
- tank
- master
- support plate
- collector
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000498 ball milling Methods 0.000 title claims abstract description 15
- 230000008676 import Effects 0.000 claims description 11
- 230000000694 effects Effects 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 abstract description 9
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 230000003068 static effect Effects 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000003507 refrigerant Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000005551 mechanical alloying Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 210000003739 neck Anatomy 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 239000012450 pharmaceutical intermediate Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000001238 wet grinding Methods 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
- B02C17/18—Details
- B02C17/1815—Cooling or heating devices
Abstract
The present invention discloses a kind of multiple tank controllable temperature planetary type ball-milling instrument, and the side of the master is equipped with motor wheel, and the top of the motor wheel, which is drivingly connected, motor;The side of the master is drivingly connected by belt and motor wheel;The lower section of the master is equipped with lower fixed disk;The top of the master is equipped with support plate;The top end surface of the master is uniformly fixed with multiple planetary gears;The top end surface center of the support plate is fixed with lower collector;The top of the support plate is equipped with upper fixed disk;The top outer surface of the planetary gear is fixed with fangs;Multiple connecting columns are fixed between fixed disk and the support plate.The beneficial effect that the present invention can reach safety, accurately control reaction temperature.
Description
Technical field
The invention belongs to ball grinding technique field, in particular to a kind of multiple tank controllable temperature planetary type ball-milling instrument.
Background technique
In necks such as chemical synthesis, pharmaceutical intermediate preparation, catalyst load study, mechanical alloying, nano material preparations
Domain, shock of traditional planetary ball mill instrument due to abrading-ball to jar, can generate a large amount of heat, into reaction system, can not go
It removes.Will lead to system temperature raising, so as to cause the change of object phase and physical property, cannot really the demand of experiment at a temperature of it is anti-
Mirror the variation of reaction process;Moreover, when wet grinding sometimes, grinding aids such as alcohols, nitrile, alkanes, aromatic hydrocarbons and molten
Agent, fusing point boiling point is all very low, and increasing for heat will lead to the volatilization of these substances, boiling, loses its original effect, volatilizees past
Toward the abruptly increase for being accompanied by air pressure, increase the danger of explosion.Vast researcher there is an urgent need to it is a kind of it is safe, can precisely control
The appearance of the planetary type ball-milling instrument of reaction temperature processed.But for apparatus manufacturer, in high-speed rotating sun gear and planetary gear
Between, it is passed through the cold and hot medium of static flowing safely, is an extremely difficult topic.
Summary of the invention
The present invention for the technical problems in the prior art, provides a kind of multiple tank controllable temperature planetary type ball-milling instrument, can
The beneficial effect for reaching safety, accurately controlling reaction temperature.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:A kind of multiple tank controllable temperature planetary type ball-milling instrument,
Including motor, motor wheel, master, planetary gear, upper collector, collector be association of activity and inertia device, upper valve, handle, tank drain pipe,
Liner tank, fangs, lower collector, lower valve, row wheel sound device, row wheel drain pipe, upper fixed disk, inlet tube, import sound
Device, lower inlet tube, lower fixed disk, support plate and connecting column,
The side of the master is equipped with motor wheel, and the top of the motor wheel, which is drivingly connected, motor;The one of the master
Side is drivingly connected by belt and motor wheel;The lower section of the master is equipped with lower fixed disk;The top of the master is equipped with support
Disk;The top end surface of the master is uniformly fixed with multiple planetary gears;The top end surface center of the support plate is fixed with
Lower collector;The top of the support plate is equipped with upper fixed disk;The top outer surface of the planetary gear is fixed with fangs;It is described
Multiple connecting columns are fixed between upper fixed disk and the support plate.
Preferably, the inside of the fangs is equipped with liner tank;The bottom outer surface of the liner tank is fixed with capable wheel
Sound device;The row wheel sound device passes through the bottom end of fangs and the top of planetary gear and is embedded in and connects;The top of the liner tank
End outer surface is fixed with handle;The handle runs through the top of fangs.
Preferably, the planetary gear is fixedly connected through support plate;Between the lower collector and the planetary gear
The top end surface of the support plate, is fixed with lower valve;The bottom end of the lower valve is equipped with lower inlet tube and row schedule
Liquid pipe.
Preferably, the lower valve is connect by lower inlet tube with the bottom end of lower collector;The lower valve passes through row
Wheel drain pipe is connect with the bottom end of row wheel sound device;The row wheel drain pipe runs through master and support plate.
Preferably, the bottom center of the lower fixed disk is fixed with import sound device, the import sound device
It is connect between lower collector by inlet tube;The lower fixed disk does not rotate;The inlet tube runs through master and support plate.
It is association of activity and inertia device preferably, the top center of fixed disk is fixed with collector, it is fixed
The bottom center of disk is fixed with collector;The upper collector passes through tank drain pipe and connect across fangs with liner tank;
The tank drain pipe is equipped with valve.
Preferably, the fangs, which is set as two, four, six or eight, is set as two, four, six or eight etc.,
The medium flow of the liner tank can individually be controlled by upper valve and lower valve, for different sample comminutions.
Compared with prior art, beneficial effect possessed by the present invention is:The present invention can safely, accurately control reaction temperature
Degree.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
1- motor in figure, 2- motor wheel, 3- master, 4- planetary gear, the upper collector of 5-, 6- collector are association of activity and inertia device,
The upper valve of 7-, 8- handle, 9- tank drain pipe, 10- liner tank, 11- fangs, collector under 12-, 13- lower valve, 14- row move in turn
Quiet device, 15- row wheel drain pipe, the upper fixed disk of 16-, 17- inlet tube, 18- import sound device, inlet tube under 19-, under 20-
Fixed disk, 21- support plate, 22- connecting column.
Specific embodiment
Technical solution in order to enable those skilled in the art to better understand the present invention, in the following with reference to the drawings and specific embodiments
It elaborates to the present invention.
Embodiment of the invention discloses a kind of multiple tank controllable temperature planetary type ball-milling instrument, as shown in the figure comprising motor 1,
Motor wheel 2, master 3, planetary gear 4, upper collector 5, collector be association of activity and inertia device 6, upper valve 7, handle 8, tank drain pipe 9,
Liner tank 10, fangs 11, lower collector 12, lower valve 13, row wheel sound device 14, row wheel drain pipe 15, upper fixed disk 16, into
Liquid pipe 17, import sound device 18, lower inlet tube 19, lower fixed disk 20, support plate 21 and connecting column 22,
The side of master 3 is equipped with motor wheel 2, and the top of motor wheel 2, which is drivingly connected, motor 1;The side of master 3 passes through skin
Band is drivingly connected with motor wheel 2;The lower section of master 3 is equipped with lower fixed disk 20;The top of master 3 is equipped with support plate 21;Master 3
Top end surface is uniformly fixed with multiple planetary gears 4;The top end surface center of support plate 21 is fixed with lower collector 12;Support
The top of disk 21 is equipped with upper fixed disk 16;The top outer surface of planetary gear 4 is fixed with fangs 11;Upper fixed disk 16 and support plate
Multiple connecting columns 22 are fixed between 21.
In the present embodiment, the inside of fangs 11 is equipped with liner tank 10;The bottom outer surface of liner tank 10 is fixed with capable wheel
Sound device 14;Row wheel sound device 14 passes through the bottom end of fangs 11 and the top of planetary gear 4 and is embedded in and connects;The top of liner tank 10
End outer surface is fixed with handle 8;Handle 8 runs through the top of fangs 11.
In the present embodiment, planetary gear 4 is fixedly connected through support plate 21;Support between lower collector 12 and planetary gear 4
The top end surface of disk 21 is fixed with lower valve 13;The bottom end of lower valve 13 is equipped with lower inlet tube 19 and row wheel drain pipe
15。
In the present embodiment, lower valve 13 is connect by lower inlet tube 19 with the bottom end of lower collector 12;Lower valve 13 passes through
Row wheel drain pipe 15 is connect with the bottom end of row wheel sound device 14;Row wheel drain pipe 15 runs through master 3 and support plate 21.
In the present embodiment, the bottom center of lower fixed disk 20 is fixed with import sound device 18, import sound device 18
It is connect between lower collector 12 by inlet tube 17;Lower fixed disk 20 does not rotate;Inlet tube 17 runs through master 3 and support plate
21。
In the present embodiment, the top center of upper fixed disk 16 is fixed with collector and is association of activity and inertia device 6, upper fixed disk 16
Bottom center be fixed with collector 5;Upper collector 5 passes through fangs 11 by tank drain pipe 9 and connect with liner tank 10;
Tank drain pipe 9 is equipped with valve 7.
In the present embodiment, fangs 11 is set as two, four, six or eight and is set as two, four, six or eight etc.,
The medium flow of liner tank 10 can individually be controlled by upper valve 7 and lower valve 13, for different sample comminutions.
In the present embodiment, heating agent (such as oil bath) can be led to, can also leading to refrigerant, (such as water circulation vavuum pump, low temperature are permanent
Warm slot, certainly pressurization liquid nitrogen container), refrigerant, heating agent abbreviation medium;Medium is continuously passed through interior by mating medium feedway
Serve as a contrast the chuck layer of tank;The internal layer of liner tank can be with inlaid polytetrafluoroethylsliders, agate, zirconium oxide liner;Liquid nitrogen pair in chuck layer
Liner tank, mill ball and sample carry out temperature control.
In the present embodiment, when operating, by the friction between the impact force and mill ball and liner tank skin of mill ball high energy
Power, impact force crush sample;Liner tank, sample and mill ball carry out rotation in the support plate that a reverse phase rotates.?
When grinding starts, the active force that the rotation of liner tank generates mainly passes through mill ball caused by the liner top tank structure frictional impact
Power crushes sample;When running to sometime, the powerful centrifugal force that support plate generates makes the sample of liner top tank structure and grinds
Abrading-ball is separated from each other.Mill ball is along liner top tank structure, and ceaselessly high-speed impact sample, reduces the ruler of sample by impact force
It is very little;By the medium of chuck layer, take away abrading-ball and hit the energy generated, be pooled to collected overhead device, flow back to recyclable device or
Emptying.
In the present embodiment, motor 1 drives master 3 to rotate, medium is by being fixed on lower fixed disk 20 by motor wheel 2
(this is the rotation of the lower wall first order, static conversion equipment to import sound device 18, and medium and the master for mainly solving absolute rest are exhausted
Problem is passed through to the medium of rotation), into inlet tube 17, it is pooled to lower collector 12, the different medium of multiply is divided into, flows through
Lower inlet tube 19, and row take turns drain pipe 15, control the chuck layer of liner tank 10, row wheel drain pipe between two pipes by lower valve 13
Having the row of a sealing to take turns sound device 14 between 15 and liner tank 10, (this is the rotation of the lower wall second level, static conversion equipment, mainly
The medium for solving the problems, such as that opposing stationary medium and row wheel relatively rotate is passed through), liner tank 10 is close by handle 8 and fangs 11
In conjunction with preventing rotation process from loosening.Medium is by after the material and abrading-ball temperature control in liner tank 10, by tank drain pipe 9, upper valve
7 control flows, are pooled to collector 5, are then association of activity and inertia 6 (this of device by the collector that is fixed in fixed disk 16
For the rotation of the upper disk third level, static conversion equipment, the medium static state relatively rotated reflux is mainly solved the problems, such as) enter recycling dress
It sets or empties.
It is described the invention in detail above by embodiment, but the content is only exemplary implementation of the invention
Example, should not be considered as limiting the scope of the invention.Protection scope of the present invention is defined by the claims.All utilizations
Technical solutions according to the invention or those skilled in the art are under the inspiration of technical solution of the present invention, in reality of the invention
In matter and protection scope, designs similar technical solution and reach above-mentioned technical effect, or to made by application range
All the changes and improvements etc. should still belong to patent of the invention and cover within protection scope.
Claims (7)
1. a kind of multiple tank controllable temperature planetary type ball-milling instrument, including motor, motor wheel, master, planetary gear, upper collector, collector
Be association of activity and inertia device, upper valve, handle, tank drain pipe, liner tank, fangs, lower collector, lower valve, row wheel sound device, row
Take turns drain pipe, upper fixed disk, inlet tube, import sound device, lower inlet tube, lower fixed disk, support plate and connecting column, feature
It is,
The side of the master is equipped with motor wheel, and the top of the motor wheel, which is drivingly connected, motor;The side of the master is logical
It crosses belt and motor wheel is drivingly connected;The lower section of the master is equipped with lower fixed disk;The top of the master is equipped with support plate;Institute
The top end surface for stating master is uniformly fixed with multiple planetary gears;The top end surface center of the support plate is fixed with lower collection
Device;The top of the support plate is equipped with upper fixed disk;The top outer surface of the planetary gear is fixed with fangs;It is fixed
Multiple connecting columns are fixed between disk and the support plate.
2. a kind of multiple tank controllable temperature planetary type ball-milling instrument according to claim 1, which is characterized in that the inside of the fangs
Equipped with liner tank;The bottom outer surface of the liner tank is fixed with row wheel sound device;The row wheel sound device passes through tank
The bottom end of seat and the top of planetary gear are embedded in and connect;The top outer surface of the liner tank is fixed with handle;The handle passes through
Wear the top of fangs.
3. a kind of multiple tank controllable temperature planetary type ball-milling instrument according to claim 1, which is characterized in that the planetary gear runs through
Support plate is fixedly connected;The top end surface of the support plate between the lower collector and the planetary gear, is fixed with
Lower valve;The bottom end of the lower valve is equipped with lower inlet tube and row wheel drain pipe.
4. a kind of multiple tank controllable temperature planetary type ball-milling instrument according to claim 1, which is characterized in that the lower valve passes through
Lower inlet tube is connect with the bottom end of lower collector;The lower valve is connected by the bottom end of row wheel drain pipe and row wheel sound device
It connects;The row wheel drain pipe runs through master and support plate.
5. a kind of multiple tank controllable temperature planetary type ball-milling instrument according to claim 1, which is characterized in that the lower fixed disk
Bottom center is fixed with import sound device, is connected between the import sound device and lower collector by inlet tube;Institute
Lower fixed disk is stated not rotate;The inlet tube runs through master and support plate.
6. a kind of multiple tank controllable temperature planetary type ball-milling instrument according to claim 1, which is characterized in that fixed disk
Top center is fixed with collector and is association of activity and inertia device, and the bottom center of fixed disk is fixed with collector;Institute
It states collector and passes through tank drain pipe and connect with liner tank across fangs;The tank drain pipe is equipped with valve.
7. a kind of multiple tank controllable temperature planetary type ball-milling instrument according to claim 1, which is characterized in that the fangs is set as two
A, four, six or eight.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710332112.0A CN108855430A (en) | 2017-05-12 | 2017-05-12 | A kind of multiple tank controllable temperature planetary type ball-milling instrument |
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CN201710332112.0A CN108855430A (en) | 2017-05-12 | 2017-05-12 | A kind of multiple tank controllable temperature planetary type ball-milling instrument |
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Publication Number | Publication Date |
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Family
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CN201710332112.0A Pending CN108855430A (en) | 2017-05-12 | 2017-05-12 | A kind of multiple tank controllable temperature planetary type ball-milling instrument |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110237901A (en) * | 2019-06-18 | 2019-09-17 | 长沙米淇仪器设备有限公司 | A kind of integration self-emptying is changed the shuttle planetary type ball-milling machine people |
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2017
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JPH0647304A (en) * | 1992-06-30 | 1994-02-22 | Kurimoto Ltd | Batch type planet ball mill with temperature control mechanism |
KR19980014312U (en) * | 1998-03-05 | 1998-06-05 | 최병석 | Ball Mill Stirring Device |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110237901A (en) * | 2019-06-18 | 2019-09-17 | 长沙米淇仪器设备有限公司 | A kind of integration self-emptying is changed the shuttle planetary type ball-milling machine people |
CN110237901B (en) * | 2019-06-18 | 2020-07-03 | 长沙米淇仪器设备有限公司 | Planetary ball-milling robot of integration automatic discharging ball of trading |
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