CN108842297A - A kind of celery fiber mask substrate and preparation method thereof - Google Patents
A kind of celery fiber mask substrate and preparation method thereof Download PDFInfo
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- CN108842297A CN108842297A CN201810803148.7A CN201810803148A CN108842297A CN 108842297 A CN108842297 A CN 108842297A CN 201810803148 A CN201810803148 A CN 201810803148A CN 108842297 A CN108842297 A CN 108842297A
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- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 title claims abstract description 156
- 235000010591 Appio Nutrition 0.000 title claims abstract description 156
- 239000000835 fiber Substances 0.000 title claims abstract description 116
- 239000000758 substrate Substances 0.000 title claims abstract description 105
- 238000002360 preparation method Methods 0.000 title claims abstract description 84
- 244000101724 Apium graveolens Dulce Group Species 0.000 title 1
- 240000007087 Apium graveolens Species 0.000 claims abstract description 155
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 39
- 238000009987 spinning Methods 0.000 claims abstract description 29
- 229920002678 cellulose Polymers 0.000 claims abstract description 22
- 239000001913 cellulose Substances 0.000 claims abstract description 22
- 230000007071 enzymatic hydrolysis Effects 0.000 claims abstract description 17
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims abstract description 17
- 238000010041 electrostatic spinning Methods 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 102000004190 Enzymes Human genes 0.000 claims abstract description 10
- 108090000790 Enzymes Proteins 0.000 claims abstract description 10
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 230000009849 deactivation Effects 0.000 claims abstract description 9
- 238000007873 sieving Methods 0.000 claims abstract 2
- 238000005406 washing Methods 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 14
- 239000004744 fabric Substances 0.000 claims description 10
- 230000001815 facial effect Effects 0.000 claims description 9
- 238000001291 vacuum drying Methods 0.000 claims description 7
- LFTLOKWAGJYHHR-UHFFFAOYSA-N N-methylmorpholine N-oxide Chemical compound CN1(=O)CCOCC1 LFTLOKWAGJYHHR-UHFFFAOYSA-N 0.000 claims description 5
- 238000007605 air drying Methods 0.000 claims description 5
- 241000238631 Hexapoda Species 0.000 claims description 4
- 241000607479 Yersinia pestis Species 0.000 claims description 4
- 238000000643 oven drying Methods 0.000 claims description 4
- 238000009423 ventilation Methods 0.000 claims description 4
- 238000002791 soaking Methods 0.000 claims description 3
- 206010008190 Cerebrovascular accident Diseases 0.000 claims 1
- 208000006011 Stroke Diseases 0.000 claims 1
- 238000009837 dry grinding Methods 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 abstract description 10
- 229910001385 heavy metal Inorganic materials 0.000 abstract description 6
- 230000035699 permeability Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 230000003712 anti-aging effect Effects 0.000 abstract description 4
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 4
- 238000010298 pulverizing process Methods 0.000 abstract description 4
- 238000003756 stirring Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 7
- 230000006870 function Effects 0.000 description 6
- 229920001410 Microfiber Polymers 0.000 description 4
- 239000003658 microfiber Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 241000222122 Candida albicans Species 0.000 description 3
- 241000588724 Escherichia coli Species 0.000 description 3
- 241000191967 Staphylococcus aureus Species 0.000 description 3
- 229940095731 candida albicans Drugs 0.000 description 3
- 239000002537 cosmetic Substances 0.000 description 3
- 230000005714 functional activity Effects 0.000 description 3
- 229910021645 metal ion Inorganic materials 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 240000008067 Cucumis sativus Species 0.000 description 2
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000000287 crude extract Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 230000000144 pharmacologic effect Effects 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 241000208306 Apium Species 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 206010020649 Hyperkeratosis Diseases 0.000 description 1
- 208000001126 Keratosis Diseases 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000018927 edible plant Nutrition 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- -1 flavonoids Compound Chemical class 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 230000002757 inflammatory effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000004215 skin function Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4266—Natural fibres not provided for in group D04H1/425
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
- D01D1/02—Preparation of spinning solutions
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D13/00—Complete machines for producing artificial threads
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/492—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres by fluid jet
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
- D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
- D04H1/728—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by electro-spinning
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Respiratory Apparatuses And Protective Means (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Nonwoven Fabrics (AREA)
Abstract
A kind of celery fiber mask substrate and preparation method thereof, it belongs to mask substrate preparation field.Celery of the present invention crushes, sieving, celery dry powder is made to be impregnated with NaOH solution, enzymatic hydrolysis, enzyme deactivation after enzymatic hydrolysis, filtering, residue washing dries pulverizing is made celery cellulose and adds water, fiber pulp is made, N-methylmorpholine-N- the oxide solution of addition, after being slowly stirred at 70~80 DEG C, then at 90~105 DEG C, vacuum degree is that 2~5h of stirring is completely dissolved cellulose under 0.095~0.098MPa, cellulose solution is made, it is made after filtering deaeration in spinning solution addition Multi needle electrostatic spinning case and carries out electrostatic spinning, it is dried in vacuo after spinning, celery fibrofelt is made to be reinforced with spun lacing, celery fiber mask substrate is made.The effect of mask substrate prepared by the present invention not only has the docile property good permeability of plant fiber, is the good carrier of Essence, has anti-inflammatory, anti-aging, removes skin heavy metal ion.
Description
Technical field
The invention belongs to mask substrate preparation fields；More particularly to a kind of celery fiber mask substrate and preparation method thereof.
Background technique
Facial mask has been indispensable a kind of cosmetology product in people's life at present, it can temporarily by face with
Outside air pollution isolation, promotes skin pore expansion, improves skin oxygen content, makes moisture and other beneficiating ingredients in facial mask
Keratoderma is penetrated into, so that skin water be made to moisten high resilience.And carrier of the mask substrate as this process, itself is to skin
The functionality of skin is paid more and more attention.But current mask substrate is mostly as just Essence carrier, and have ignored its function
It can property.Plant fiber is the research hotspot of recent cosmetic field as mask substrate, and the docile property gas permeability of plant fiber is high, and
And there is good toughness and water absorbing capacity, natural environmental-protective, and it can be played as carrier with suitable plant fiber
To the function of skin-protection and health-care.
Celery (Apium gravelous L) is widely applied in uighur medicine as medicinal and edible plant and is big
Crowd is known well, and is had very high nutritive value and pharmacological action.Functional activity substance rich in celery, wherein flavonoids
Compound, volatile oil etc. can remove skin free radical, inhibit multiple pathogenic microorganisms well, have anti-aging, antioxygen
Change and the multiple pharmacological effects such as antibacterial bacteriostatic.Vitamin rich in celery, can play whitening and skin-protecting function.And celery
Insoluble fibre rich content in dish can be very good to agree with skin, have absorption to remove the pollutions such as heavy metal in skin
Function.Therefore, celery has very important significance in the research and development tool of cosmetic field.
Summary of the invention
It is an object of the present invention to provide a kind of celery fiber mask substrates and preparation method thereof.
The invention is realized by the following technical scheme：
A kind of preparation method of celery fiber mask substrate, includes the following steps：
Baking oven drying after step 1, celery remove the insect pest cauline leaf that rots, clean, shred, air-drying at ventilation opening, is put into crushing
It crushes, be sieved in machine, celery dry powder is made；
Step 2 impregnates celery dry powder made from step 1 with NaOH solution, enzymatic hydrolysis, and enzyme deactivation, filtering, filter residue are washed after enzymatic hydrolysis
It washs dries pulverizing and celery cellulose is made；
Celery cellulose made from step 2 is added 5~10wt% of water by step 3, and fiber pulp is made, and 10~20wt% is added
N-methylmorpholine-N- oxide solution, after being slowly stirred at 70~80 DEG C, then at 90~105 DEG C, vacuum degree is
2~5h is stirred under 0.095~0.098MPa is completely dissolved cellulose, and cellulose solution is made, and spinning is made after filtering deaeration
Stoste；
Step 4 will carry out electrostatic spinning in the addition Multi needle electrostatic spinning case of spinning solution made from step 3, after spinning
Celery fibrofelt is made in vacuum drying；
Step 5 reinforces celery fibrofelt made from step 4 with spun lacing, and celery fiber mask substrate is made.
A kind of preparation method of celery fiber mask substrate of the present invention, air-dry time 2 days in step 1, drying temperature
Degree is 50 DEG C, 2~5h of drying time, smashes it through 40~60 meshes in step 1.
A kind of preparation method of celery fiber mask substrate of the present invention, NaOH solution concentration is quality in step 2
The solid-liquid ratio 1 of score 10%, celery dry powder and NaOH solution：20~1：25g/mL, pH value of solution 8.0, soaking time 70~
90min。
A kind of preparation method of celery fiber mask substrate of the present invention, enzymatic hydrolysis is molten for after steeping in step 2
1wt% trypsase is added in liquid, 2h, 95 DEG C of enzyme deactivation 10min after enzymatic hydrolysis, filter residue drying temperature are incubated in 45 DEG C of insulating boxs
Degree is 50 DEG C, 4~6h of drying time.
A kind of preparation method of celery fiber mask substrate of the present invention, the N-methylmorpholine-N- oxidation in step 3
Object solution concentration is mass fraction 70~80%.
A kind of preparation method of celery fiber mask substrate of the present invention is slowly stirred in step 3 at 70~80 DEG C
30~60min of time, the concentration of cellulose solution obtained are mass fraction 10~20%.
A kind of preparation method of celery fiber mask substrate of the present invention, it is 6 that spinning parameter, which is filament mouth, in step 4
Number syringe needle, spinning voltage are 15~25 kilovolts, and spinning solution flow velocity is 0.20~0.40mL/min, spinning pole span is 10~
15cm, 60 DEG C of vacuum drying after electrostatic spinning, is made celery fibrofelt.
A kind of preparation method of celery fiber mask substrate of the present invention, it is spun lacing pressure that spun lacing, which is reinforced, in step 5
20~25bar, water needle hole exits diameter are 0.10~0.14mm.
A kind of preparation method of celery fiber mask substrate of the present invention, the celery fiber mask substrate thickness
0.35~0.55mm, base fabric surface density 25-45g/m2。
A kind of preparation method of celery fiber mask substrate of the present invention, the celery fiber mask substrate are held
Liquid rate is 1425%~1561%.
The preparation method of a kind of celery fiber mask substrate of the present invention, using celery as primary raw material, by celery
Ultra-microfibers preparation, the techniques such as fiber tabletting are completed, and it is docile that the mask substrate of the method for the present invention preparation not only has plant fiber
Property good permeability, be the good carrier of Essence, and anti-inflammatory, the anti-aging of celery, remove the skin cares such as skin heavy metal ion
Function is played well.
A kind of celery fiber mask substrate of the preparation method preparation of celery fiber mask substrate of the present invention is to gold
The bacteriostasis rate of staphylococcus aureus is 99.4%, to the bacteriostasis rate of Escherichia coli is 95.2%, is to Candida albicans bacteriostasis rate
98.7%, bacteriostasis rate is all larger than 95%, has good fungistatic effect.
A kind of preparation method of celery fiber mask substrate of the present invention, using in celery fiber crude extract containing compared with
More functional activity substances remains the skin-protecting function of celery, and natural plant fibre is high to skin compatible degree, convenient for taking
Band is easy to degrade, safety and environmental protection.
A kind of preparation method of celery fiber mask substrate of the present invention, celery used are Bao Qin, celery fiber
Mask substrate also provides wide prospect as value-added product for the development in pluralism of Bao Qin.
Specific embodiment
Specific embodiment one：
A kind of preparation method of celery fiber mask substrate, includes the following steps：
Baking oven drying after step 1, celery remove the insect pest cauline leaf that rots, clean, shred, air-drying at ventilation opening, is put into crushing
It crushes, be sieved in machine, celery dry powder is made；
Step 2 impregnates celery dry powder made from step 1 with NaOH solution, enzymatic hydrolysis, and enzyme deactivation, filtering, filter residue are washed after enzymatic hydrolysis
It washs dries pulverizing and celery cellulose is made；
Celery cellulose made from step 2 is added water 5wt% by step 3, and fiber pulp is made, and the N- methyl of 20wt% is added
Methylmorpholine-N-oxide solution, after being slowly stirred at 75 DEG C, then at 105 DEG C, vacuum degree is that stirring 3h makes fibre under 0.095MPa
Dimension element is completely dissolved, and cellulose solution is made, and spinning solution is made after filtering deaeration；
Step 4 will carry out electrostatic spinning in the addition Multi needle electrostatic spinning case of spinning solution made from step 3, after spinning
Celery fibrofelt is made in vacuum drying；
Step 5 reinforces celery fibrofelt made from step 4 with spun lacing, and celery fiber mask substrate is made.
A kind of preparation method of celery fiber mask substrate described in present embodiment air-dry time 2 days in step 1, is dried
Dry temperature is 50 DEG C, drying time 3h, smashes it through 60 meshes in step 1.
A kind of preparation method of celery fiber mask substrate described in present embodiment, NaOH solution concentration is in step 2
The solid-liquid ratio 1 of mass fraction 10%, celery dry powder and NaOH solution：25g/ml, pH value of solution 8.0, soaking time 90min.
A kind of preparation method of celery fiber mask substrate described in present embodiment, enzymatic hydrolysis is after steeping in step 2
Solution in 1wt% trypsase is added, be incubated for 2h in 45 DEG C of insulating boxs, 95 DEG C of enzyme deactivation 10min after enzymatic hydrolysis, filter residue dries
Dry temperature is 50 DEG C, drying time 5h.
A kind of preparation method of celery fiber mask substrate described in present embodiment, the N-methylmorpholine-N- in step 3
Oxide solution concentration is mass fraction 70~80%.
A kind of preparation method of celery fiber mask substrate described in present embodiment, in step 3 at 70~80 DEG C slowly
Mixing time 60min, the concentration of cellulose solution obtained are mass fraction 15%.
A kind of preparation method of celery fiber mask substrate described in present embodiment, spinning parameter is wire vent in step 4
Mouth is No. 6 syringe needles, and spinning voltage is 15 kilovolts, and spinning solution flow velocity is 0.30mL/min, and spinning pole span is 15cm, electrostatic spinning
After 60 DEG C vacuum drying, be made celery fibrofelt.
A kind of preparation method of celery fiber mask substrate described in present embodiment, it is spun lacing that spun lacing, which is reinforced, in step 5
Pressure 20bar, water needle hole exits diameter are 0.10mm.
Specific embodiment two：
A kind of celery fiber of the preparation method preparation of celery fiber mask substrate according to specific embodiment one
Mask substrate, celery fiber mask substrate thickness 0.4mm, the base fabric surface density 35g/m2。
A kind of celery fiber mask substrate of the preparation method preparation of celery fiber mask substrate described in present embodiment,
The liquid holdup of the celery fiber mask substrate is 1425%~1561%.
A kind of celery fiber mask substrate of the preparation method preparation of celery fiber mask substrate described in present embodiment,
It carries out holding liquid ability and anti-microbial property test：
Liquid holdup detection：Test method is by mask substrate (weight m1) be immersed in the dedicated Essence of facial mask, sufficiently
10s is impregnated, then takes out hanging placement 1min, weigh m2, liquid holdup=(m2-m1)/m1X100%.Three times, control group selects for test
Commercially available common facial mask is taken, test result is as shown in table 1：
1 liquid holdup contrast table of table
From table 1 it can be seen that the celery fiber mask substrate liquid holdup of present embodiment be respectively 1425%, 1501%,
1456%, and common non-woven fabric mask substrate liquid holdup is 383% or so, a kind of celery fiber facial mask described in present embodiment
The celery fiber mask substrate of the preparation method preparation of base fabric, liquid holdup is 3~4 times of common base fabric.
A kind of celery fiber mask substrate of the preparation method preparation of celery fiber mask substrate described in present embodiment
Bacteriostasis rate to staphylococcus aureus is 99.4%, is 95.2% to the bacteriostasis rate of Escherichia coli, antibacterial to Candida albicans
Rate is 98.7%, and bacteriostasis rate is all larger than 95%, has good fungistatic effect.
A kind of celery fiber mask substrate of the preparation method preparation of celery fiber mask substrate described in present embodiment
Metal adsorption amount is tested, control group chooses commercially available common facial mask, and test result is as shown in table 2：
2 heavy metal adsorption amount contrast table (mg/cm of table2)
, it can be seen that a kind of celery of the preparation preparation of celery fiber mask substrate described in present embodiment from table 2
Fiber mask substrate is prepared using celery as primary raw material by celery ultra-microfibers, and the techniques such as fiber tabletting are completed, preparation
Mask substrate not only has the docile property good permeability of plant fiber, is the good carrier of Essence, and has and remove skin weight
The effect of metal ion, the celery fiber mask substrate of present embodiment is to the adsorbance of heavy metal ion compared to common facial mask
Base fabric improves 10 times or more, has good suction-operated to the remaining metal ion of cosmetics is smeared on human skin.
Specific embodiment three：
A kind of preparation method of celery fiber mask substrate, includes the following steps：
Baking oven drying after step 1, celery remove the insect pest cauline leaf that rots, clean, shred, air-drying at ventilation opening, is put into crushing
It crushes, be sieved in machine, celery dry powder is made；
Step 2 impregnates celery dry powder made from step 1 with NaOH solution, enzymatic hydrolysis, and enzyme deactivation, filtering, filter residue are washed after enzymatic hydrolysis
It washs dries pulverizing and celery cellulose is made；
Celery cellulose made from step 2 is added 5~10wt% of water by step 3, and fiber pulp is made, and 10~20wt% is added
N-methylmorpholine-N- oxide solution, after being slowly stirred at 70~80 DEG C, then at 90~105 DEG C, vacuum degree is
2~5h is stirred under 0.095~0.098MPa is completely dissolved cellulose, and cellulose solution is made, and spinning is made after filtering deaeration
Stoste；
Step 4 will carry out electrostatic spinning in the addition Multi needle electrostatic spinning case of spinning solution made from step 3, after spinning
Celery fibrofelt is made in vacuum drying；
Step 5 reinforces celery fibrofelt made from step 4 with spun lacing, and celery fiber mask substrate is made.
Specific embodiment four：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, when air-drying in step 1
Between 2 days, drying temperature is 50 DEG C, 2~5h of drying time, smashes it through 40~60 meshes in step 1.
Specific embodiment five：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, NaOH is molten in step 2
Liquid concentration is mass fraction 10%, the solid-liquid ratio 1 of celery dry powder and NaOH solution：20~1：25g/ml, pH value of solution 8.0, leaching
Steep 70~90min of time.
Specific embodiment six：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, enzymatic hydrolysis is in step 2
1wt% trypsase is added in solution after steeping, 2h, 95 DEG C of enzyme deactivations after enzymatic hydrolysis are incubated in 45 DEG C of insulating boxs
10min, filter residue drying temperature are 50 DEG C, 4~6h of drying time.
Specific embodiment seven：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, the N- first in step 3
Base methylmorpholine-N-oxide solution concentration is mass fraction 70~80%.
Specific embodiment eight：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, 70~80 in step 3
30~60min of time is slowly stirred at DEG C, the concentration of cellulose solution obtained is mass fraction 10~20%.
Specific embodiment nine：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, spinning ginseng in step 4
Number is that filament mouth is No. 6 syringe needles, and spinning voltage is 15~25 kilovolts, and spinning solution flow velocity is 0.20~0.40mL/min, spinning
Pole span is 10~15cm, and celery fibrofelt is made in 60 DEG C of vacuum drying after electrostatic spinning.
Specific embodiment ten：
A kind of preparation method of celery fiber mask substrate according to specific embodiment three, spun lacing adds in step 5
Admittedly being 20~25bar of spun lacing pressure, water needle hole exits diameter is 0.10~0.14mm.
Specific embodiment 11：
A kind of celery fiber facial mask of the preparation preparation of celery fiber mask substrate according to specific embodiment three
Base fabric, 0.35~0.55mm of celery fiber mask substrate thickness, the base fabric surface density 25-45g/m2。
A kind of celery fiber mask substrate of the preparation preparation of celery fiber mask substrate, described described in present embodiment
Celery fiber mask substrate liquid holdup be 1425%~1561%.
A kind of celery fiber mask substrate of the preparation preparation of celery fiber mask substrate described in present embodiment, to gold
The bacteriostasis rate of staphylococcus aureus is 99.4%, to the bacteriostasis rate of Escherichia coli is 95.2%, is to Candida albicans bacteriostasis rate
98.7%.
A kind of celery fiber mask substrate of the preparation preparation of celery fiber mask substrate described in present embodiment, with celery
Dish is primary raw material, is prepared by celery ultra-microfibers, and the techniques such as fiber tabletting are completed, and the mask substrate of preparation not only has plant
The docile property good permeability of fibres, is the good carrier of Essence, and anti-inflammatory, the anti-aging of celery, removes skin heavy metal
The skin-protecting functions such as ion are played well.
A kind of celery fiber mask substrate of the preparation preparation of celery fiber mask substrate, utilizes described in present embodiment
Contain more functional activity substance in celery fiber crude extract, remains the skin-protecting function of celery, and natural plant fibre
It is high to skin compatible degree, it is easy to carry, it is easy to degrade, safety and environmental protection.
A kind of celery fiber mask substrate of the preparation preparation of celery fiber mask substrate, used described in present embodiment
Celery be Bao Qin, celery fiber mask substrate as value-added product also for the development in pluralism of Bao Qin provide it is wide before
Scape.
A kind of celery fiber mask substrate of the preparation method preparation of celery fiber mask substrate described in present embodiment
Using effect is tested, 120 22-52 years old faces is selected to have the women trial edition of the inflammatory problems such as red capillary or erythema
Invention, the present invention are impregnated by common cucumber water (such as thousand fine careless cucumber waters), and trying out the time is 3 months, test result such as 3 institute of table
Show (common mask substrate is as control), every group is tried out common mask substrate and each 10 people of the present invention：
3 trial effect contrast table of table
, it can be seen that a kind of celery of the preparation preparation of celery fiber mask substrate described in present embodiment from table 3
Fiber mask substrate is prepared using celery as primary raw material by celery ultra-microfibers, and the techniques such as fiber tabletting are completed, preparation
Mask substrate not only has the docile property good permeability of plant fiber, is the good carrier of Essence, and has and remove skin weight
The effect of metal ion and anti-inflammatory.
Claims (10)
1. a kind of preparation method of celery fiber mask substrate, it is characterised in that：Include the following steps：
Baking oven drying after step 1, celery remove the insect pest cauline leaf that rots, clean, shred, air-drying at ventilation opening, is put into pulverizer
It crushes, sieving, celery dry powder is made；
Step 2 impregnates celery dry powder made from step 1 with NaOH solution, enzymatic hydrolysis, and enzyme deactivation, filtering, residue washing dry after enzymatic hydrolysis
Celery cellulose is made in dry grinding；
Celery cellulose made from step 2 is added 5~10wt% of water by step 3, and fiber pulp is made, and the N- of 10~20wt% is added
Methyhnorpholine-N-oxide solution, after being slowly stirred at 70~80 DEG C, then at 90~105 DEG C, vacuum degree is 0.095~
2~5h is stirred under 0.098MPa is completely dissolved cellulose, and cellulose solution is made, and spinning solution is made after filtering deaeration；
Step 4 will carry out electrostatic spinning, vacuum after spinning in the addition Multi needle electrostatic spinning case of spinning solution made from step 3
It is dry, celery fibrofelt is made；
Step 5 reinforces celery fibrofelt made from step 4 with spun lacing, and celery fiber mask substrate is made.
2. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：Step 1 apoplexy
Dry 2 days time, drying temperature are 50 DEG C, 2~5h of drying time, smash it through 40~60 meshes in step 1.
3. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：In step 2
NaOH solution concentration is mass fraction 10%, the solid-liquid ratio 1 of celery dry powder and NaOH solution：20~1：25g/mL, pH value of solution are
8.0,70~90min of soaking time.
4. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：Enzyme in step 2
Solution is incubated for 2h, 95 DEG C of enzyme deactivations after enzymatic hydrolysis for 1wt% trypsase is added in solution after steeping in 45 DEG C of insulating boxs
10min, filter residue drying temperature are 50 DEG C, 4~6h of drying time.
5. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：In step 3
N-methylmorpholine-N- oxide solution concentration is mass fraction 70~80%.
6. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：70 in step 3
30~60min of time is slowly stirred at~80 DEG C, the concentration of cellulose solution obtained is mass fraction 10~20%.
7. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：It is spun in step 4
Silk parameter is that filament mouth is No. 6 syringe needles, and spinning voltage is 15~25 kilovolts, and spinning solution flow velocity is 0.20~0.40mL/min,
Spinning pole span is 10~15cm, and celery fibrofelt is made in 60 DEG C of vacuum drying after electrostatic spinning.
8. a kind of preparation method of celery fiber mask substrate according to claim 1, it is characterised in that：Water in step 5
It is 20~25bar of spun lacing pressure that thorn, which is reinforced, and water needle hole exits diameter is 0.10~0.14mm.
9. a kind of celery fibrous face of the preparation method preparation of celery fiber mask substrate described in a kind of one of claim 1-8
Film base fabric, it is characterised in that：0.35~0.55mm of celery fiber mask substrate thickness, the base fabric surface density 25-45g/m2。
10. celery fiber facial mask base prepared by a kind of preparation method of celery fiber mask substrate according to claim 9
Cloth, it is characterised in that：The liquid holdup of the celery fiber mask substrate is 1425%~1561%.
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| CN111793227A (en) * | 2019-04-09 | 2020-10-20 | 中国科学院大连化学物理研究所 | Method for forming film by nano-cellulose |
| CN111793898A (en) * | 2019-04-09 | 2020-10-20 | 中国科学院大连化学物理研究所 | Nano cellulose membrane and preparation method thereof |
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| CN108842297B (en) | 2020-02-21 |
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